X

Y estimated Z estimated
451
1
452.6 0.995458
454.2 0.990714
455.8 0.985763
457.4 0.980596
459 0.975208
460.6 0.969591
462.2 0.96374
463.8 0.957648
465.4 0.951309
467 0.944715
468.6 0.937862
470.2 0.930743
471.8 0.923351
473.4 0.915683
475 0.907731
476.6 0.899492
478.2 0.89096
479.8 0.882132
481.4 0.873003
483 0.86357
484.6 0.85383
486.2 0.843782
487.8 0.833422
489.4 0.822751
491 0.811768
492.6 0.800473
494.2 0.788867
495.8 0.776954
497.4 0.764735
499 0.752216
500.6
0.7394
502.2 0.726293
503.8 0.712904
505.4 0.699239
507 0.685309
508.6 0.671123
510.2 0.656694
511.8 0.642033
513.4 0.627155
515 0.612075
516.6 0.596809
518.2 0.581373
519.8 0.565788
521.4 0.550071

523
524.6
526.2
527.8
529.4
531
532.6
534.2
535.8
537.4
539
540.6
542.2
543.8
545.4
547
548.6
550.2
551.8
553.4
555
556.6
558.2
559.8
561.4
563
564.6
566.2
567.8
569.4
571
572.6
574.2
575.8
577.4
579
580.6
582.2
583.8
585.4
587
588.6
590.2
591.8
593.4
595
596.6

0.534243
0.518326
0.502342
0.486314
0.470264
0.454219
0.438202
0.422238
0.406352
0.390571
0.374918
0.359421
0.344102
0.328987
0.314099
0.299462
0.285097
0.271026
0.257268
0.243842
0.230765
0.218053
0.205721
0.19378
0.182242
0.171115
0.160407
0.150124
0.140268
0.130842
0.121846
0.113279
0.105137
0.097415
0.090108
0.083208
0.076706
0.070593
0.064856
0.059486
0.054468
0.049789
0.045436
0.041395
0.037651
0.034189
0.030995

598.2 0.028054
599.8 0.025352
601.4 0.022873
603 0.020605
604.6 0.018533
606.2 0.016643
607.8 0.014924
609.4 0.013363
611 0.011947
-------------------------------------

Y estimated Z estimated
364
1
364.87 0.994906
365.74 0.989582
366.61 0.98402
367.48 0.978211
368.35 0.972148
369.22 0.965822
370.09 0.959224
370.96 0.952346
371.83 0.945179
372.7 0.937716
373.57 0.929947
374.44 0.921864
375.31 0.913461
376.18 0.904728
377.05 0.895657
377.92 0.886243
378.79 0.876477
379.66 0.866354
380.53 0.855867
381.4 0.84501
382.27 0.83378
383.14 0.822171
384.01 0.81018
384.88 0.797805
385.75 0.785044
386.62 0.771897
387.49 0.758363
388.36 0.744445
389.23 0.730145
390.1 0.715469
390.97 0.700421
391.84 0.685009
392.71 0.669243
393.58 0.653132
394.45 0.63669
395.32 0.61993
396.19 0.60287
397.06 0.585527
397.93 0.567923
398.8 0.550079
399.67 0.532019
400.54 0.513772
401.41 0.495364
402.28 0.476827

403.15
404.02
404.89
405.76
406.63
407.5
408.37
409.24
410.11
410.98
411.85
412.72
413.59
414.46
415.33
416.2
417.07
417.94
418.81
419.68
420.55
421.42
422.29
423.16
424.03
424.9
425.77
426.64
427.51
428.38
429.25
430.12
430.99
431.86
432.73
433.6
434.47
435.34
436.21
437.08
437.95
438.82
439.69
440.56
441.43
442.3
443.17

0.458194
0.439498
0.420776
0.402066
0.383407
0.364839
0.346404
0.328143
0.3101
0.292318
0.274838
0.257703
0.240955
0.224633
0.208776
0.19342
0.178599
0.164344
0.150683
0.13764
0.125237
0.113489
0.10241
0.092006
0.082282
0.073236
0.064862
0.05715
0.050085
0.043649
0.037821
0.032573
0.027877
0.023703
0.020018
0.016786
0.013974
0.011543
0.00946
0.00769
0.006197
0.004949
0.003916
0.003069
0.002381
0.001828
0.001389

444.04 0.001043
444.91 0.000774
445.78 0.000568
446.65 0.000411
447.52 0.000294
448.39 0.000207
449.26 0.000144
450.13 9.85E-05
451 6.64E-05
-------------------------------------

1.1
1.0
Friedman model

0.9

TGA Experiment
0.8

(1-a ) [-]

0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0

100

200

300

400

500

temperaure (OC)

600

700

800

900

1000

Y estimated Z estimated i
29
1
0 9.14281
32.35
1
0
35.7
1
0
39.05
1
0
42.4
1
0
45.75
1
0
49.1
1
0
52.45
1
1E-10
55.8
1
1E-10
59.15
1
2E-10
62.5
1
3E-10
65.85
1
5E-10
69.2
1
7E-10
72.55
1
1.2E-09
75.9
1
1.9E-09
79.25
1
2.9E-09
82.6
1
4.6E-09
85.95
1
7.1E-09
89.3
1 1.08E-08
92.65
1 1.65E-08
96
1 2.48E-08
99.35
1 3.72E-08
102.7
1 5.54E-08
106.05
1 8.18E-08
109.4
1
1.2E-07
112.75
1 1.75E-07
116.1
1 2.53E-07
119.45
1 3.65E-07
122.8 0.999999 5.22E-07
126.15 0.999999 7.42E-07
129.5 0.999999 1.05E-06
132.85 0.999999 1.48E-06
136.2 0.999998 2.06E-06
139.55 0.999997 2.87E-06
142.9 0.999996 3.98E-06
146.25 0.999995 5.48E-06
149.6 0.999992
7.5E-06
152.95 0.99999 1.02E-05
156.3 0.999986 1.39E-05
159.65 0.999981 1.88E-05
163 0.999975 2.52E-05
166.35 0.999966 3.38E-05
169.7 0.999955 4.51E-05
173.05 0.99994 5.98E-05
176.4 0.999921 7.91E-05

0
9.1428

1-alfa
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825

0
0
0
0
0
0
0
9.83E-12
9.83E-12
1.97E-11
2.95E-11
4.91E-11
6.88E-11
1.18E-10
1.87E-10
2.85E-10
4.52E-10
6.98E-10
1.06E-09
1.62E-09
2.44E-09
3.65E-09
5.44E-09
8.04E-09
1.18E-08
1.72E-08
2.49E-08
3.58E-08
5.12E-08
7.29E-08
1.03E-07
1.45E-07
2.03E-07
2.82E-07
3.91E-07
5.38E-07
7.37E-07
1.01E-06
1.36E-06
1.84E-06
2.48E-06
3.32E-06
4.43E-06
5.88E-06
7.77E-06

29
32.35
35.7
39.05
42.4
45.75
49.1
52.45
55.8
59.15
62.5
65.85
69.2
72.55
75.9
79.25
82.6
85.95
89.3
92.65
96
99.35
102.7
106.05
109.4
112.75
116.1
119.45
122.8
126.15
129.5
132.85
136.2
139.55
142.9
146.25
149.6
152.95
156.3
159.65
163
166.35
169.7
173.05
176.4

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.999999
0.999999
0.999999
0.999999
0.999998
0.999998
0.999997
0.999996
0.999994
0.999992

179.75
183.1
186.45
189.8
193.15
196.5
199.85
203.2
206.55
209.9
213.25
216.6
219.95
223.3
226.65
230
233.35
236.7
240.05
243.4
246.75
250.1
253.45
256.8
260.15
263.5
266.85
270.2
273.55
276.9
280.25
283.6
286.95
290.3
293.65
297
300.35
303.7
307.05
310.4
313.75
317.1
320.45
323.8
327.15
330.5
333.85

0.999896
0.999863
0.999821
0.999768
0.999699
0.99961
0.999498
0.999356
0.999177
0.998951
0.998667
0.998312
0.99787
0.997319
0.996637
0.995794
0.994755
0.99348
0.991918
0.99001
0.987689
0.984871
0.981463
0.977354
0.972415
0.9665
0.959441
0.951049
0.941112
0.929396
0.915647
0.899592
0.880948
0.859426
0.834745
0.806649
0.774924
0.739422
0.70009
0.657
0.610378
0.560627
0.508348
0.454342
0.399591
0.345224
0.292448

0.000104
0.000137
0.000179
0.000232
0.000301
0.00039
0.000502
0.000644
0.000823
0.001049
0.001333
0.001688
0.00213
0.002681
0.003363
0.004206
0.005245
0.00652
0.008082
0.00999
0.012311
0.015129
0.018537
0.022646
0.027585
0.0335
0.040559
0.048951
0.058888
0.070604
0.084353
0.100408
0.119052
0.140574
0.165255
0.193351
0.225076
0.260578
0.29991
0.343
0.389622
0.439373
0.491652
0.545658
0.600409
0.654776
0.707552

0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825

1.02E-05
1.34E-05
1.75E-05
2.28E-05
2.96E-05
3.83E-05
4.93E-05
6.32E-05
8.09E-05
0.000103
0.000131
0.000166
0.000209
0.000263
0.00033
0.000413
0.000515
0.000641
0.000794
0.000981
0.00121
0.001486
0.001821
0.002225
0.00271
0.003291
0.003985
0.004809
0.005786
0.006937
0.008288
0.009865
0.011697
0.013811
0.016236
0.018997
0.022114
0.025602
0.029466
0.0337
0.03828
0.043168
0.048305
0.053611
0.05899
0.064332
0.069517

179.75
183.1
186.45
189.8
193.15
196.5
199.85
203.2
206.55
209.9
213.25
216.6
219.95
223.3
226.65
230
233.35
236.7
240.05
243.4
246.75
250.1
253.45
256.8
260.15
263.5
266.85
270.2
273.55
276.9
280.25
283.6
286.95
290.3
293.65
297
300.35
303.7
307.05
310.4
313.75
317.1
320.45
323.8
327.15
330.5
333.85

0.99999
0.999987
0.999982
0.999977
0.99997
0.999962
0.999951
0.999937
0.999919
0.999897
0.999869
0.999834
0.999791
0.999737
0.99967
0.999587
0.999485
0.999359
0.999206
0.999019
0.99879
0.998514
0.998179
0.997775
0.99729
0.996709
0.996015
0.995191
0.994214
0.993063
0.991712
0.990135
0.988303
0.986189
0.983764
0.981003
0.977886
0.974398
0.970534
0.9663
0.96172
0.956832
0.951695
0.946389
0.94101
0.935668
0.930483

337.2
340.55
343.9
347.25
350.6
353.95
357.3
360.65
364
364.87
365.74
366.61
367.48
368.35
369.22
370.09
370.96
371.83
372.7
373.57
374.44
375.31
376.18
377.05
377.92
378.79
379.66
380.53
381.4
382.27
383.14
384.01
384.88
385.75
386.62
387.49
388.36
389.23
390.1
390.97
391.84
392.71
393.58
394.45
395.32
396.19
397.06

0.242467
0.196384
0.155101
0.11924
0.089089
0.064594
0.045396
0.030894
0.020348
0.994906
0.989582
0.98402
0.978211
0.972148
0.965822
0.959224
0.952346
0.945179
0.937716
0.929947
0.921864
0.913461
0.904728
0.895657
0.886243
0.876477
0.866354
0.855867
0.84501
0.83378
0.822171
0.81018
0.797805
0.785044
0.771897
0.758363
0.744445
0.730145
0.715469
0.700421
0.685009
0.669243
0.653132
0.63669
0.61993
0.60287
0.585527

0.757533
0.803616
0.844899
0.88076
0.910911
0.935406
0.954604
0.969106
0.979652
0.005094
0.010418
0.01598
0.021789
0.027852
0.034178
0.040776
0.047654
0.054821
0.062284
0.070053
0.078136
0.086539
0.095272
0.104343
0.113757
0.123523
0.133646
0.144133
0.15499
0.16622
0.177829
0.18982
0.202195
0.214956
0.228103
0.241637
0.255555
0.269855
0.284531
0.299579
0.314991
0.330757
0.346868
0.36331
0.38007
0.39713
0.414473

8.24453
8.24453

0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0.09825
0 0.09825
9.4128 0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374
0.108374

0.074428
0.078955
0.083011
0.086535
0.089497
0.091904
0.09379
0.095215
0.096251
0.000552
0.001129
0.001732
0.002361
0.003018
0.003704
0.004419
0.005164
0.005941
0.00675
0.007592
0.008468
0.009379
0.010325
0.011308
0.012328
0.013387
0.014484
0.01562
0.016797
0.018014
0.019272
0.020572
0.021913
0.023296
0.02472
0.026187
0.027696
0.029245
0.030836
0.032467
0.034137
0.035846
0.037591
0.039373
0.04119
0.043039
0.044918

337.2
340.55
343.9
347.25
350.6
353.95
357.3
360.65
364
364.87
365.74
366.61
367.48
368.35
369.22
370.09
370.96
371.83
372.7
373.57
374.44
375.31
376.18
377.05
377.92
378.79
379.66
380.53
381.4
382.27
383.14
384.01
384.88
385.75
386.62
387.49
388.36
389.23
390.1
390.97
391.84
392.71
393.58
394.45
395.32
396.19
397.06

0.925572
0.921045
0.916989
0.913465
0.910503
0.908096
0.90621
0.904785
0.903749
0.903197
0.90262
0.902017
0.901388
0.900731
0.900045
0.89933
0.898585
0.897808
0.896999
0.896157
0.895281
0.894371
0.893424
0.892441
0.891421
0.890363
0.889265
0.888129
0.886952
0.885735
0.884477
0.883178
0.881837
0.880454
0.879029
0.877562
0.876054
0.874504
0.872913
0.871283
0.869612
0.867904
0.866158
0.864376
0.862559
0.860711
0.858831

397.93
398.8
399.67
400.54
401.41
402.28
403.15
404.02
404.89
405.76
406.63
407.5
408.37
409.24
410.11
410.98
411.85
412.72
413.59
414.46
415.33
416.2
417.07
417.94
418.81
419.68
420.55
421.42
422.29
423.16
424.03
424.9
425.77
426.64
427.51
428.38
429.25
430.12
430.99
431.86
432.73
433.6
434.47
435.34
436.21
437.08
437.95

0.567923
0.550079
0.532019
0.513772
0.495364
0.476827
0.458194
0.439498
0.420776
0.402066
0.383407
0.364839
0.346404
0.328143
0.3101
0.292318
0.274838
0.257703
0.240955
0.224633
0.208776
0.19342
0.178599
0.164344
0.150683
0.13764
0.125237
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397.93
398.8
399.67
400.54
401.41
402.28
403.15
404.02
404.89
405.76
406.63
407.5
408.37
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414.46
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417.07
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419.68
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423.16
424.03
424.9
425.77
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433.6
434.47
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436.21
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437.95

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0.796209
0.796047

438.82
439.69
440.56
441.43
442.3
443.17
444.04
444.91
445.78
446.65
447.52
448.39
449.26
450.13
451
452.6
454.2
455.8
457.4
459
460.6
462.2
463.8
465.4
467
468.6
470.2
471.8
473.4
475
476.6
478.2
479.8
481.4
483
484.6
486.2
487.8
489.4
491
492.6
494.2
495.8
497.4
499
500.6
502.2

0.004949
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438.82
439.69
440.56
441.43
442.3
443.17
444.04
444.91
445.78
446.65
447.52
448.39
449.26
450.13
451
452.6
454.2
455.8
457.4
459
460.6
462.2
463.8
465.4
467
468.6
470.2
471.8
473.4
475
476.6
478.2
479.8
481.4
483
484.6
486.2
487.8
489.4
491
492.6
494.2
495.8
497.4
499
500.6
502.2

0.795912
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0.756836
0.754898

503.8
505.4
507
508.6
510.2
511.8
513.4
515
516.6
518.2
519.8
521.4
523
524.6
526.2
527.8
529.4
531
532.6
534.2
535.8
537.4
539
540.6
542.2
543.8
545.4
547
548.6
550.2
551.8
553.4
555
556.6
558.2
559.8
561.4
563
564.6
566.2
567.8
569.4
571
572.6
574.2
575.8
577.4

0.712904
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503.8
505.4
507
508.6
510.2
511.8
513.4
515
516.6
518.2
519.8
521.4
523
524.6
526.2
527.8
529.4
531
532.6
534.2
535.8
537.4
539
540.6
542.2
543.8
545.4
547
548.6
550.2
551.8
553.4
555
556.6
558.2
559.8
561.4
563
564.6
566.2
567.8
569.4
571
572.6
574.2
575.8
577.4

0.752917
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0.661878
0.660798

579
580.6
582.2
583.8
585.4
587
588.6
590.2
591.8
593.4
595
596.6
598.2
599.8
601.4
603
604.6
606.2
607.8
609.4
611
613.59
616.18
618.77
621.36
623.95
626.54
629.13
631.72
634.31
636.9
639.49
642.08
644.67
647.26
649.85
652.44
655.03
657.62
660.21
662.8
665.39
667.98
670.57
673.16
675.75
678.34

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0.044136
0.046873

579
580.6
582.2
583.8
585.4
587
588.6
590.2
591.8
593.4
595
596.6
598.2
599.8
601.4
603
604.6
606.2
607.8
609.4
611
613.59
616.18
618.77
621.36
623.95
626.54
629.13
631.72
634.31
636.9
639.49
642.08
644.67
647.26
649.85
652.44
655.03
657.62
660.21
662.8
665.39
667.98
670.57
673.16
675.75
678.34

0.659777
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0.6051
0.602363

680.93
683.52
686.11
688.7
691.29
693.88
696.47
699.06
701.65
704.24
706.83
709.42
712.01
714.6
717.19
719.78
722.37
724.96
727.55
730.14
732.73
735.32
737.91
740.5
743.09
745.68
748.27
750.86
753.45
756.04
758.63
761.22
763.81
766.4
768.99
771.58
774.17
776.76
779.35
781.94
784.53
787.12
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792.3
794.89
797.48
800.07

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0.002481
0.00255
0.00262
0.00269
0.002762
0.002835
0.002908
0.002983
0.003058
0.003134
0.003211
0.003289
0.003367
0.003445
0.003524
0.003603
0.003682
0.003762
0.00384
0.003919
0.003997

-0.00407
-0.00415
-0.00422
-0.0043
-0.00437
-0.00444
-0.0045
-0.00456
-0.00462
-0.00468
-0.00472
-0.00477
-0.0048
-0.00483
-0.00484
-0.00485
-0.00484
-0.00481
-0.00477
-0.0047
-0.0046
-0.00447
-0.00428
-0.00402
-0.00364
-0.00303
#VALUE!

0.004074
0.00415
0.004224
0.004297
0.004368
0.004436
0.004502
0.004564
0.004622
0.004675
0.004723
0.004765
0.0048
0.004826
0.004842
0.004847
0.004838
0.004813
0.004768
0.0047
0.004601
0.004465
0.004278
0.004018
0.003645
0.00303
#VALUE!

Series1

500