Pace Lab RPT - FR

Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
(336)623-8921
(828)254-7176
(704)875-9092
LIMS USE: FR - STEVE BARRICK

LIMS OBJECT ID: 92119797
June 11, 2012
Mr. Steve Barrick

Arcadis
801 Corporate Center Drv
Suite 300
Raleigh, NC 27607
RE: Project: SQUARE D- ASHEVILLE , NC

Pace Project No.: 92119797
Dear Mr. Barrick:
Enclosed are the analytical results for sample(s) received by the laboratory on June 01, 2012. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
bonnie.mckee@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
CERTIFICATIONS
Project:
SQUARE D- ASHEVILLE , NC
Pace Project No.:
92119797
Charlotte Certification IDs

9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104

Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460144

Page 2 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
SAMPLE ANALYTE COUNT

Project:
Pace Project No.:
92119797
Lab ID
Sample ID
92119797001
Analytes
Reported
Method
Analysts
MW-12
EPA 8260
MCK
63
PASI-C
92119797002
WW-1
EPA 8260
KJM
63
PASI-C
92119797003
MW-14
EPA 8260
MCK
63
PASI-C
92119797004
MW-15
EPA 8260
MCK
63
PASI-C
Laboratory
92119797005
TW-1
EPA 8260
MCK
63
PASI-C
92119797006
WW-2
EPA 8260
MCK
63
PASI-C
92119797007
MW-16
EPA 8260
MCK
63
PASI-C
92119797008
TW-2
EPA 8260
MCK
63
PASI-C
92119797009
MW-6
EPA 8260
MCK
63
PASI-C
92119797010
MW-18D
EPA 8260
MCK
63
PASI-C
92119797011
MW-17DD
EPA 8260
MCK
63
PASI-C
92119797012
BR-1
EPA 8260
MCK
63
PASI-C
92119797013
MW-5
EPA 8260
MCK
63
PASI-C
92119797014
MW-4
EPA 8260
MCK
63
PASI-C
92119797015
MW-7
EPA 8260
MCK
63
PASI-C
92119797016
MW-10D
EPA 8260
MCK
63
PASI-C
92119797017
MW-15Dd
EPA 8260
MCK
63
PASI-C
92119797018
MW-15DS
EPA 8260
MCK
63
PASI-C
92119797019
MW-3
EPA 8260
MCK
63
PASI-C
92119797020
MW-13D
EPA 8260
MCK
63
PASI-C
92119797021
MW-1
EPA 8260
MCK
63
PASI-C
92119797022
TB-1
EPA 8260
MCK
63
PASI-C

Page 3 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-12
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797001

Results
Collected: 05/30/12 17:30
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 4 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-12
Parameters
8260 MSV Low Level
Toluene
1,2,3-Trichlorobenzene
1,1,1-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797001

Results
Collected: 05/30/12 17:30
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
97
102
103
98
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
06/04/12 18:32
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 5 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: WW-1
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797002

Results
Collected: 05/30/12 14:15
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
149
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 6 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: WW-1
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797002

Results
Collected: 05/30/12 14:15
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
1.0
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
99
109
119
98
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
06/06/12 23:46
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 7 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-14
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797003

Results
Collected: 05/30/12 11:20
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 8 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-14
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797003

Results
Collected: 05/30/12 11:20
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
102
109
116
102
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
06/04/12 18:48
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 9 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-15
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797004

Results
Collected: 05/30/12 12:20
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.5
ND
2.2
11.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
123
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 10 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-15
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797004

Results
Collected: 05/30/12 12:20
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
287
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
101
106
107
98
%
%
%
%
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
5
1
1
1
1
1
1
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/05/12 22:40
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
06/04/12 19:03
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 11 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: TW-1
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797005

Results
Collected: 05/30/12 13:30
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
43.9
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 12 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: TW-1
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797005

Results
Collected: 05/30/12 13:30
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
25.0
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
102
102
97
98
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
06/05/12 08:37
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 13 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: WW-2
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797006

Results
Collected: 05/30/12 18:00
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
117
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 14 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: WW-2
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797006

Results
Collected: 05/30/12 18:00
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
6.2
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
98
105
113
105
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
06/05/12 08:52
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 15 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-16
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797007

Results
Collected: 05/30/12 15:20
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.2
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 16 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-16
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797007

Results
Collected: 05/30/12 15:20
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
1.2
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
101
107
108
101
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
06/04/12 19:19
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 17 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: TW-2
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797008

Results
Collected: 05/30/12 16:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
60.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 18 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: TW-2
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797008

Results
Collected: 05/30/12 16:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
21.7
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
99
104
107
100
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
06/04/12 19:34
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 19 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-6
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797009

Results
Collected: 05/30/12 16:55
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.2
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 20 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-6
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797009

Results
Collected: 05/30/12 16:55
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
2.0
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
100
106
113
100
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
06/04/12 21:08
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 21 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-18D
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797010

Results
Collected: 05/31/12 13:30
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
14.5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
32.1
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 22 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-18D
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797010

Results
Collected: 05/31/12 13:30
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
49.9
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
101
100
104
98
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
06/05/12 09:08
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 23 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-17DD
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797011

Results
Collected: 05/31/12 13:45
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
242
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
50.0
2.0
2.0
2.0
2.0
2.0
4.0
10.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
10.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
10.0
2.0
4.0
10.0
2.0
2.0
2.0
2.0
2.0
2.0
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2

06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 24 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-17DD
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797011

Results
Collected: 05/31/12 13:45
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
49.9
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
104
101
103
97
%
%
%
%
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
4.0
2.0
4.0
2.0
2
2
2
2
2
2
2
2
2
2
2
2
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
2
2
2
2
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
06/05/12 09:24
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 25 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: BR-1
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797012

Results
Collected: 05/31/12 10:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
35.1
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 26 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: BR-1
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797012

Results
Collected: 05/31/12 10:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
44.2
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
102
101
98
97
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
06/05/12 09:39
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 27 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-5
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797013

Results
Collected: 05/31/12 11:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
13.3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.1
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 28 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-5
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797013

Results
Collected: 05/31/12 11:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
36.8
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
101
111
105
101
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
06/05/12 09:55
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 29 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-4
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797014

Results
Collected: 05/31/12 12:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12.8
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 30 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-4
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797014

Results
Collected: 05/31/12 12:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
33.9
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
102
113
107
101
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
06/04/12 21:24
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 31 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-7
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797015

Results
Collected: 05/31/12 13:15
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
60.1
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 32 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-7
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797015

Results
Collected: 05/31/12 13:15
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
43.9
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
102
100
106
97
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
06/04/12 21:40
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 33 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-10D
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797016

Results
Collected: 05/31/12 19:30
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
87.0
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 34 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-10D
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797016

Results
Collected: 05/31/12 19:30
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
8.4
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
102
101
105
98
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
06/05/12 10:11
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 35 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-15Dd
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797017

Results
Collected: 05/31/12 15:20
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
72.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 36 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-15Dd
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797017

Results
Collected: 05/31/12 15:20
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
73.1
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
99
108
114
97
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
06/04/12 21:55
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 37 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-15DS
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797018

Results
Collected: 05/31/12 16:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
6.6
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 38 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-15DS
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797018

Results
Collected: 05/31/12 16:10
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
9.0
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
98
102
107
102
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
06/04/12 22:11
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 39 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-3
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797019

Results
Collected: 05/31/12 17:05
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11.8
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 40 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-3
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797019

Results
Collected: 05/31/12 17:05
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
23.1
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
102
101
105
97
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
06/05/12 10:27
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 41 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-13D
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797020

Results
Collected: 05/31/12 20:00
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
28.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 42 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-13D
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797020

Results
Collected: 05/31/12 20:00
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

2.8
ND
ND
ND
ND
17.1
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
101
107
112
99
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
06/05/12 18:30
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 43 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-1
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797021

Results
Collected: 05/31/12 19:00
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.9
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
13.5
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 44 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: MW-1
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797021

Results
Collected: 05/31/12 19:00
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
37.3
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
97
101
101
99
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
06/05/12 18:46
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 45 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: TB-1
Parameters
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
Naphthalene
Styrene
Tetrachloroethene
Date: 06/11/2012 12:44 PM
Lab ID: 92119797022

Results
Collected: 05/31/12 00:00
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25.0
1.0
1.0
1.0
1.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
2.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
591-78-6
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
100-42-5
630-20-6
79-34-5
127-18-4
Page 46 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project:
Pace Project No.:
92119797
Sample: TB-1
Parameters
8260 MSV Low Level
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Lab ID: 92119797022

Results
Collected: 05/31/12 00:00
Units
Report Limit
Received: 06/01/12 12:50
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
103
101
100
99
%
%
%
%
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1
1
1
1
1
1
1
1
1
1
1
1
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
108-05-4
75-01-4
179601-23-1
95-47-6
70-130
70-130
70-130
70-130
1
1
1
1
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
06/05/12 06:00
460-00-4
1868-53-7
17060-07-0
2037-26-5

Page 47 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
QUALITY CONTROL DATA

Project:
Pace Project No.:
92119797
QC Batch:
MSV/19322
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
Analysis Description:
8260 MSV Low Level
Associated Lab Samples:

METHOD BLANK:
92119797001, 92119797003, 92119797004, 92119797007, 92119797008
772640

Parameter
Matrix: Water
92119797001, 92119797003, 92119797004, 92119797007, 92119797008
Blank
Reporting
Units
Result
Limit
Analyzed
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
Date: 06/11/2012 12:44 PM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
5.0
1.0
5.0
25.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Qualifiers
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24

Page 48 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
METHOD BLANK:
772640

Parameter
Matrix: Water
92119797001, 92119797003, 92119797004, 92119797007, 92119797008
Blank
Reporting
Units
Result
Limit
Analyzed
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
LABORATORY CONTROL SAMPLE:
772641
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
Date: 06/11/2012 12:44 PM
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
106
100
99
100
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
1.0
2.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
70-130
70-130
70-130
70-130
LCS
Result
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
06/04/12 15:24
% Rec
Limits
LCS
% Rec
50.8
47.1
49.9
52.5
43.5
48.5
48.2
49.1
53.0
49.5
51.6
50.0
47.0
47.9
49.4
47.3
49.5
47.9
44.1
108
46.6
Qualifiers
102
94
100
105
87
97
96
98
106
99
103
100
94
96
99
95
99
96
88
108
93

Qualifiers
70-130
70-130
70-130
70-130
70-130
70-132
70-130
70-135
70-130
70-134
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
58-145
70-145
70-130
Page 49 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
772641
Parameter
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
Spike
Conc.
100
50
100
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
100
50
LCS
Result
% Rec
Limits
LCS
% Rec
111
48.7
107
124
49.4
47.2
49.3
48.1
52.3
38.2
52.7
49.1
52.5
46.9
43.8
48.1
50.6
52.0
50.2
35.4
50.3
48.9
53.8
94.9
50.4
54.7
49.2
46.0
51.7
50.0
49.0
47.4
47.6
51.7
50.5
49.4
94.4
46.7
111
97
107
124
99
94
99
96
105
76
105
98
105
94
88
96
101
104
100
71
101
98
108
95
101
109
98
92
103
100
98
95
95
103
101
99
94
93
97
104
100
99

Qualifiers
70-144
70-130
70-140
50-175
70-130
70-130
70-130
70-130
70-130
54-130
70-132
70-130
64-134
70-130
64-130
70-131
70-130
70-130
70-131
56-130
70-130
70-130
70-130
70-130
70-130
63-130
70-138
70-130
70-130
70-130
70-130
70-130
70-130
70-132
70-130
62-133
66-157
69-130
70-130
70-130
70-130
70-130
Page 50 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
1,1-Dichloroethene
Benzene
Chlorobenzene
Toluene
Trichloroethene
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
772642
92119860001
Units
Result
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
ND
ND
ND
772643
MS
Spike
Conc.
50
50
50
MSD
Spike
Conc.
50
50
50
MS
Result
60.2
47.7
57.7
56.1
61.4
MSD
Result
MS
% Rec
56.4
46.9
57.5
56.2
61.8

MSD
% Rec
% Rec
Limits
95
115
112
94
115
112
70-148
70-146
70-155
112
104
105
100
105
102
100
99
70-130
70-130
70-130
70-130
RPD
Qual
6
2
0
0
1
Page 51 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
QC Batch:
MSV/19323
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
8260 MSV Low Level

METHOD BLANK:
92119797009, 92119797014, 92119797015, 92119797017, 92119797018
772644

Parameter
Matrix: Water
92119797009, 92119797014, 92119797015, 92119797017, 92119797018
Blank
Reporting
Units
Result
Limit
Analyzed
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
Date: 06/11/2012 12:44 PM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
5.0
1.0
5.0
25.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Qualifiers
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40

Page 52 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
METHOD BLANK:
772644

Parameter
Matrix: Water
92119797009, 92119797014, 92119797015, 92119797017, 92119797018
Blank
Reporting
Units
Result
Limit
Analyzed
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
772645
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
Date: 06/11/2012 12:44 PM
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
109
102
107
100
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
1.0
2.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
70-130
70-130
70-130
70-130
LCS
Result
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
06/04/12 15:40
% Rec
Limits
LCS
% Rec
49.9
48.5
48.7
51.9
42.6
45.6
47.9
48.4
51.7
48.2
51.1
49.7
46.7
46.5
48.2
46.3
48.2
45.7
39.6
102
45.2
Qualifiers
100
97
97
104
85
91
96
97
103
96
102
99
93
93
96
93
96
91
79
102
90

Qualifiers
70-130
70-130
70-130
70-130
70-130
70-132
70-130
70-135
70-130
70-134
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
58-145
70-145
70-130
Page 53 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
772645
Parameter
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
Spike
Conc.
100
50
100
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
100
50
LCS
Result
% Rec
Limits
LCS
% Rec
105
46.0
101
120
48.6
45.7
47.7
49.0
51.2
30.4
50.1
48.0
63.8
48.3
47.5
46.7
47.9
49.1
49.3
32.5
47.1
48.6
48.4
96.4
49.6
51.7
49.2
46.0
48.7
49.5
47.1
47.1
45.1
49.6
50.1
46.5
87.9
44.6
105
92
101
120
97
91
95
98
102
61
100
96
128
97
95
93
96
98
99
65
94
97
97
96
99
103
98
92
97
99
94
94
90
99
100
93
88
89
94
103
96
99

Qualifiers
70-144
70-130
70-140
50-175
70-130
70-130
70-130
70-130
70-130
54-130
70-132
70-130
64-134
70-130
64-130
70-131
70-130
70-130
70-131
56-130
70-130
70-130
70-130
70-130
70-130
63-130
70-138
70-130
70-130
70-130
70-130
70-130
70-130
70-132
70-130
62-133
66-157
69-130
70-130
70-130
70-130
70-130
Page 54 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
Parameter
1,1-Dichloroethene
Benzene
Chlorobenzene
Toluene
Trichloroethene
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
772646
92119860022
Units
Result
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
ND
ND
ND
772647
MS
Spike
Conc.
50
50
50
MSD
Spike
Conc.
50
50
50
MS
Result
57.2
43.8
53.5
51.8
57.0
MSD
Result
MS
% Rec
55.4
48.6
54.7
54.2
57.9

MSD
% Rec
% Rec
Limits
88
107
104
97
109
108
70-148
70-146
70-155
106
100
107
98
101
102
102
99
70-130
70-130
70-130
70-130
RPD
Qual
3
10
2
5
2
Page 55 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
QC Batch:
MSV/19325
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
8260 MSV Low Level

METHOD BLANK:
92119797022
772766
Matrix: Water
92119797022
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Blank
Result
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
5.0
1.0
5.0
25.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Analyzed
Qualifiers
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08

Page 56 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
METHOD BLANK:
772766
Matrix: Water
92119797022
Parameter
Units
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
772767
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
Date: 06/11/2012 12:44 PM
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
102
103
105
99
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Blank
Result
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
1.0
2.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
70-130
70-130
70-130
70-130
LCS
Result
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
06/05/12 03:08
% Rec
Limits
LCS
% Rec
50.2
43.7
49.4
52.9
40.6
45.0
45.5
48.1
53.2
47.6
50.4
51.1
46.1
46.9
48.8
45.9
49.2
46.1
37.4
98.9
45.9
Qualifiers
Analyzed
100
87
99
106
81
90
91
96
106
95
101
102
92
94
98
92
98
92
75
99
92

Qualifiers
70-130
70-130
70-130
70-130
70-130
70-132
70-130
70-135
70-130
70-134
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
58-145
70-145
70-130
Page 57 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
772767
Parameter
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
Spike
Conc.
100
50
100
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
100
50
LCS
Result
% Rec
Limits
LCS
% Rec
104
47.0
103
116
48.8
45.8
44.9
47.6
52.2
41.3
49.8
47.2
64.7
44.2
46.7
45.7
47.2
49.8
50.0
31.0
45.1
47.9
49.4
93.8
49.5
50.0
48.7
45.5
49.3
48.5
46.5
46.6
44.8
49.5
49.4
46.1
85.0
43.6
104
94
103
116
98
92
90
95
104
83
100
94
129
88
93
91
94
100
100
62
90
96
99
94
99
100
97
91
99
97
93
93
90
99
99
92
85
87
89
103
95
99

Qualifiers
70-144
70-130
70-140
50-175
70-130
70-130
70-130
70-130
70-130
54-130
70-132
70-130
64-134
70-130
64-130
70-131
70-130
70-130
70-131
56-130
70-130
70-130
70-130
70-130
70-130
63-130
70-138
70-130
70-130
70-130
70-130
70-130
70-130
70-132
70-130
62-133
66-157
69-130
70-130
70-130
70-130
70-130
Page 58 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
Parameter
1,2-Dichloroethane
Benzene
Chlorobenzene
Ethylbenzene
m&p-Xylene
Naphthalene
o-Xylene
Toluene
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
772769
92119671002
Units
Result
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
ND
ND
ND
ND
ND
1.1
ND
ND
ND
772770
MS
Spike
Conc.
50
50
50
50
100
50
50
50
50
MSD
Spike
Conc.
50
50
50
50
100
50
50
50
50
MS
Result
52.9
53.9
53.3
53.7
106
52.2
50.8
50.2
51.8
MSD
Result
MS
% Rec
53.5
57.1
55.6
56.9
110
52.4
53.9
53.1
53.8

106
108
107
107
106
102
102
100
103
100
99
101
100
MSD
% Rec
107
114
111
114
110
103
108
106
107
95
98
96
100
% Rec
Limits
70-130
70-148
70-146
70-130
70-130
70-130
70-130
70-130
70-155
70-130
70-130
70-130
70-130
Qual
RPD
1
6 pH
4
6
4
0
6
6
4
Page 59 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
QC Batch:
MSV/19326
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
8260 MSV Low Level

METHOD BLANK:
92119797005, 92119797006, 92119797010, 92119797011, 92119797012, 92119797013, 92119797016,

92119797019
772775
Parameter
Matrix: Water
92119797005, 92119797006, 92119797010, 92119797011, 92119797012, 92119797013, 92119797016,
92119797019
Blank
Reporting
Units
Result
Limit
Analyzed
Qualifiers
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Date: 06/11/2012 12:44 PM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
5.0
1.0
5.0
25.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52

Page 60 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
METHOD BLANK:
772775
Parameter
Matrix: Water
92119797005, 92119797006, 92119797010, 92119797011, 92119797012, 92119797013, 92119797016,
92119797019
Blank
Reporting
Units
Result
Limit
Qualifiers
Analyzed
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
772776
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
Date: 06/11/2012 12:44 PM
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
94
103
98
101
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
70-130
70-130
70-130
70-130
LCS
Result
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
06/05/12 02:52
% Rec
Limits
LCS
% Rec
49.7
43.1
49.5
54.8
41.4
44.7
45.2
50.7
53.2
50.1
51.2
50.6
47.7
43.2
51.4
46.8
48.6
47.5
99
86
99
110
83
89
90
101
106
100
102
101
95
86
103
94
97
95

Qualifiers
70-130
70-130
70-130
70-130
70-130
70-132
70-130
70-135
70-130
70-134
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
Page 61 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
772776
Parameter
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
Spike
Conc.
50
100
50
100
50
100
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
100
50
LCS
Result
% Rec
Limits
LCS
% Rec
36.6
99.1
45.4
107
46.5
109
114
49.5
47.0
48.4
51.1
52.4
44.9
52.9
47.6
51.9
45.2
46.4
45.4
50.7
51.0
53.5
30.7
45.3
48.0
51.6
96.0
48.9
49.7
50.8
46.2
50.3
48.3
48.3
50.0
44.2
50.3
53.4
51.3
83.7
43.8
73
99
91
107
93
109
114
99
94
97
102
105
90
106
95
104
90
93
91
101
102
107
61
91
96
103
96
98
99
102
92
101
97
97
100
88
101
107
103
84
88
85
103
94
105

Qualifiers
58-145
70-145
70-130
70-144
70-130
70-140
50-175
70-130
70-130
70-130
70-130
70-130
54-130
70-132
70-130
64-134
70-130
64-130
70-131
70-130
70-130
70-131
56-130
70-130
70-130
70-130
70-130
70-130
63-130
70-138
70-130
70-130
70-130
70-130
70-130
70-130
70-132
70-130
62-133
66-157
69-130
70-130
70-130
70-130
70-130
Page 62 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
Parameter
1,1-Dichloroethene
Benzene
Chlorobenzene
Toluene
Trichloroethene
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
773214
92119797019
Units
Result
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
ND
ND
ND
ND
23.1
773215
MS
Spike
Conc.
50
50
50
50
50
MSD
Spike
Conc.
50
50
50
50
50
MS
Result
65.0
52.8
63.2
61.5
119
MSD
Result
MS
% Rec
70.6
53.4
65.9
62.9
118

130
106
126
123
193
94
102
101
99
MSD
% Rec
141
107
132
126
190
102
102
104
98
% Rec
Limits
70-166
70-148
70-146
70-155
69-151
70-130
70-130
70-130
70-130
Qual
RPD
8
1
4
2
1 M0
Page 63 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
QC Batch:
MSV/19335
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
8260 MSV Low Level

METHOD BLANK:
92119797002
773046
Matrix: Water
92119797002
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Blank
Result
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
5.0
1.0
5.0
25.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Analyzed
Qualifiers
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57

Page 64 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
METHOD BLANK:
773046
Matrix: Water
92119797002
Parameter
Units
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
773047
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
Date: 06/11/2012 12:44 PM
Reporting
Limit
3.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
116
98
109
97
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Blank
Result
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
1.0
2.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
70-130
70-130
70-130
70-130
LCS
Result
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
06/06/12 21:57
% Rec
Limits
LCS
% Rec
54.4
47.8
46.5
51.9
41.0
49.9
48.2
56.9
53.4
56.5
55.4
51.0
51.8
48.8
47.0
51.4
48.9
50.3
45.5
87.8
52.3
Qualifiers
Analyzed
109
96
93
104
82
100
96
114
107
113
111
102
104
98
94
103
98
101
91
88
105

Qualifiers
70-130
70-130
70-130
70-130
70-130
70-132
70-130
70-135
70-130
70-134
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
58-145
70-145
70-130
Page 65 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
773047
Parameter
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
Spike
Conc.
100
50
100
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
100
50
LCS
Result
% Rec
Limits
LCS
% Rec
97.6
54.4
97.2
102
49.7
48.7
49.3
52.3
54.0
49.5
57.6
51.0
56.0
47.5
51.4
48.6
53.3
54.9
54.2
55.8
44.8
53.0
57.0
110
51.7
52.9
50.8
46.8
54.0
47.0
53.2
50.9
47.4
56.4
52.4
61.8
90.9
49.0
98
109
97
102
99
97
99
105
108
99
115
102
112
95
103
97
107
110
108
112
90
106
114
110
103
106
102
94
108
94
106
102
95
113
105
124
91
98
95
107
95
99

Qualifiers
70-144
70-130
70-140
50-175
70-130
70-130
70-130
70-130
70-130
54-130
70-132
70-130
64-134
70-130
64-130
70-131
70-130
70-130
70-131
56-130 SS
70-130
70-130
70-130
70-130
70-130
63-130
70-138
70-130
70-130
70-130
70-130
70-130
70-130
70-132
70-130
62-133
66-157
69-130
70-130
70-130
70-130
70-130
Page 66 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
Parameter
1,1-Dichloroethene
Benzene
Chlorobenzene
Toluene
Trichloroethene
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
773048
92119749001
Units
Result
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
ND
ND
ND
ND
ND
773049
MS
Spike
Conc.
50
50
50
50
50
MSD
Spike
Conc.
50
50
50
50
50
MS
Result
56.1
45.0
57.2
53.7
57.1
MSD
Result
MS
% Rec
55.3
43.9
56.5
52.6
56.5

112
90
114
107
114
104
101
98
94
MSD
% Rec
111
88
113
105
113
110
101
101
92
% Rec
Limits
70-166
70-148
70-146
70-155
69-151
70-130
70-130
70-130
70-130
RPD
Qual
1
2
1
2
1
Page 67 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
QC Batch:
MSV/19343
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
8260 MSV Low Level

METHOD BLANK:
92119797020, 92119797021
773203
Matrix: Water
92119797020, 92119797021
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Blank
Result
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
5.0
1.0
5.0
25.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Analyzed
Qualifiers
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25

Page 68 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
METHOD BLANK:
773203
Matrix: Water
92119797020, 92119797021
Parameter
Units
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
773204
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
Date: 06/11/2012 12:44 PM
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
113
99
107
99
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Blank
Result
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
1.0
2.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
70-130
70-130
70-130
70-130
LCS
Result
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
06/05/12 16:25
% Rec
Limits
LCS
% Rec
55.1
51.1
52.0
57.8
48.3
52.9
52.6
51.7
54.9
51.8
51.2
55.0
49.9
53.0
54.2
49.8
53.4
50.2
49.7
106
48.5
Qualifiers
Analyzed
110
102
104
116
97
106
105
103
110
104
102
110
100
106
108
100
107
100
99
106
97

Qualifiers
70-130
70-130
70-130
70-130
70-130
70-132
70-130
70-135
70-130
70-134
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
58-145
70-145
70-130
Page 69 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
773204
Parameter
2-Hexanone
4-Chlorotoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methylene Chloride
Naphthalene
o-Xylene
p-Isopropyltoluene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl acetate
Vinyl chloride
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
Spike
Conc.
100
50
100
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
100
50
LCS
Result
% Rec
Limits
LCS
% Rec
107
50.4
111
122
51.1
49.0
51.5
54.5
55.9
53.5
57.9
52.0
104
56.8
61.0
52.6
56.2
55.9
54.9
47.0
59.2
52.7
55.8
103
55.2
61.4
50.4
50.7
53.5
53.1
52.2
52.5
52.9
57.4
53.8
58.4
103
56.4
107
101
111
122
102
98
103
109
112
107
116
104
207
114
122
105
112
112
110
94
118
105
112
103
110
123
101
101
107
106
104
105
106
115
108
117
103
113
94
104
101
101

Qualifiers
70-144
70-130
70-140
50-175
70-130
70-130
70-130
70-130
70-130
54-130
70-132
70-130
64-134 L0
70-130
64-130
70-131
70-130
70-130
70-131
56-130
70-130
70-130
70-130
70-130
70-130
63-130
70-138
70-130
70-130
70-130
70-130
70-130
70-130
70-132
70-130
62-133
66-157
69-130
70-130
70-130
70-130
70-130
Page 70 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092

Project:
Pace Project No.:
92119797
Parameter
1,1-Dichloroethene
Benzene
Chlorobenzene
Toluene
Trichloroethene
Toluene-d8 (S)
Date: 06/11/2012 12:44 PM
773205
92119860029
Units
Result
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
ND
ND
ND
773206
MS
Spike
Conc.
50
50
50
MSD
Spike
Conc.
50
50
50
MS
Result
49.3
44.9
53.3
50.9
54.9
MSD
Result
MS
% Rec
51.1
46.9
57.8
54.5
58.4

MSD
% Rec
% Rec
Limits
90
107
102
94
116
109
70-148
70-146
70-155
104
101
101
97
96
104
97
99
70-130
70-130
70-130
70-130
RPD
Qual
3
4
8
7
6
Page 71 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
QUALIFIERS
Project:
Pace Project No.:
92119797
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C
Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B
Analyte was detected in the associated method blank.
L0
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
M0
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
This analyte did not meet the secondary source verification criteria for the initial calibration. The reported result should be
considered an estimated value.
Post-analysis pH measurement indicates insufficient VOA sample preservation.
SS
pH
Date: 06/11/2012 12:44 PM

Page 72 of 73
2225 Riverside Dr.
Eden, NC 27288
Asheville, NC 28804
(336)623-8921
(828)254-7176
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE

Project:
Pace Project No.:
92119797
Lab ID
Sample ID
QC Batch Method
QC Batch
92119797001
MW-12
EPA 8260
MSV/19322
92119797002
WW-1
EPA 8260
MSV/19335
92119797003
92119797004
MW-14
MW-15
EPA 8260
EPA 8260
MSV/19322
MSV/19322
92119797005
92119797006
TW-1
WW-2
EPA 8260
EPA 8260
MSV/19326
MSV/19326
92119797007
92119797008
MW-16
TW-2
EPA 8260
EPA 8260
MSV/19322
MSV/19322
92119797009
MW-6
EPA 8260
MSV/19323
92119797010
92119797011
92119797012
92119797013
MW-18D
MW-17DD
BR-1
MW-5
EPA 8260
EPA 8260
EPA 8260
EPA 8260
MSV/19326
MSV/19326
MSV/19326
MSV/19326
92119797014
92119797015
MW-4
MW-7
EPA 8260
EPA 8260
MSV/19323
MSV/19323
92119797016
MW-10D
EPA 8260
MSV/19326
92119797017
92119797018
MW-15Dd
MW-15DS
EPA 8260
EPA 8260
MSV/19323
MSV/19323
92119797019
MW-3
EPA 8260
MSV/19326
92119797020
92119797021
MW-13D
MW-1
EPA 8260
EPA 8260
MSV/19343
MSV/19343
92119797022
TB-1
EPA 8260
MSV/19325
Date: 06/11/2012 12:44 PM

Analytical Method
Analytical
Batch
Page 73 of 73

Pace Lab RPT - FR

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Pace Lab RPT - FR

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Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

205 East Meadow Road - Suite A

2225 Riverside Dr.

9800 Kincey Ave. Suite 100

LIMS USE: FR - STEVE BARRICK

June 11, 2012

Mr. Steve Barrick

RE: Project: SQUARE D- ASHEVILLE , NC

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

205 East Meadow Road - Suite A

2225 Riverside Dr.

9800 Kincey Ave. Suite 100

Pace Project No.:

Charlotte Certification IDs

Connecticut Certification #: PH-0104

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

205 East Meadow Road - Suite A

2225 Riverside Dr.

9800 Kincey Ave. Suite 100

SAMPLE ANALYTE COUNT

Pace Project No.:

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

205 East Meadow Road - Suite A

2225 Riverside Dr.

9800 Kincey Ave. Suite 100

Pace Project No.:

Lab ID: 92119797001

Collected: 05/30/12 17:30

Received: 06/01/12 12:50

Analytical Method: EPA 8260

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

205 East Meadow Road - Suite A

2225 Riverside Dr.

9800 Kincey Ave. Suite 100

Pace Project No.:

Date: 06/11/2012 12:44 PM

Lab ID: 92119797001

Collected: 05/30/12 17:30

Received: 06/01/12 12:50

Analytical Method: EPA 8260

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

Pace Analytical Services, Inc.

205 East Meadow Road - Suite A

2225 Riverside Dr.

9800 Kincey Ave. Suite 100

Pace Project No.: