Assay Report

Country
Authorization status Item Code: Material Description (JDE): Item Description: Shelf life:

Confidential Page no: Page 1 of 1

Issue no;

Pakistan

Authorized, issued on November, 2008

22901 Saccharin Sodium

Sodium Saccharine (BP 2008) 5.0 Years.

01

General Information
PO No. Invoice/DC No. Supplier Name: Quantity Received. Q.C. Log. Ref: Supplier B.No/Lot. No: Manufacturer Name: Sampled by/ On

Specifications
Tests Specifications Limits Results Sign

1. *Appearance 2. *Solubility 3. *Identification 4. Appearance of solution 5. *Acidity or 6. Alkalinity *Melting point of

isolated saccharine

A white crystalline powder or colourless crystals. Free from foreign particles. Freely soluble in water.Sparingly soluble in alcohol.Insoluble in Ether. Positive Clear solution 4.5 5.5ml of 0.01 M NaOH is required 226 C 230 C Complies B.P. 20 ppm. max. 15% max. 99.0 101.0%. (Titramatric method)
o o

7. o-and pToluenesul phonamide 8. Heavy Metals 9. *Water

10. *Assay (on anhydrous basis)

An (*) indicates required QC tests for each batch. Test # 4, 7 & 9 will be done on new source sample.

QC Disposition Meets / Does not meet specification

Approved / Rejected by

QC Analyst:

QC Manager:

1- Prepared by: M. Zaki Khan- RB Pakistan 2- Reviewed by: M. Irfan Khan- RB Pakistan 3- Approved by: M. Asif Ali- RB Pakistan 4- Approved by: Irfan Ali Zaib- RB Pakistan

Sr. Executive Quality Control Assistant Manager Quality Control Quality Control Manager Quality Assurance Manager