Statoil PTL MON Crude Oil and Products (CP)

CRUDE OIL ASSAY

Statoil Cheecham Blend

STATOIL
PRODUCT TECHNOLOGY
AND
LABORATORIES (PTL)
Crude Oil and Products (CP)
DATE:

204-130

22/12/11

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CONTENTS
*******************

1. SAMPLE DATA

2. DISTILLATION CONDITIONS

3. ANALYTICAL RESULTS

4. ANALYTICAL METHODS

204-130

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1. S A M P L E D A T A
****************************

204-130

SAMPLE:

Dilbit

DESCRIPTION:

Statoil Cheecham Blend

Diluent used: OSN

DATE OF SAMPLING:

28 April 2011

SAMPLE VOLUME:

60 litres

SAMPLE PACKAGE:

Jerrycans

LABORATORY:

This assay was prepared by Statoil PTL MON

Crude Oil and Products (CP)

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2. D I S T I L L A T I O N C O N D I T I O N S
***********************************************************
The following conditions according to ASTM are used:
TRUE BOILING POINT DISTILLATION
EQUIPMENT:
The distillation up to 343C is performed according
to D-2892, and from 343C according to
internal HiVac method (modified D-5236).

CONDITIONS:
The cutpoints are as follows:

Atmospheric distillation:

C5 - 177C AET

100 Torr:

177 - 232C AET

10 Torr:

232 - 288C AET

5 Torr:

288 - 343C AET

From 1 to 0.1 Torr:

343 - 524C AET

The atmospheric cutting points are corrected to

760 mmHg.

VOLUME:
Volume expansion or contraction are normalized among fractions
boiling below 177C in proportion to their yields.
(Usually the "Loss" is negative due to volume expansion)

HOLD UP:
Hold up at 343C AET is distributed as follows:
50% on the first fraction of the HiVac method (343C420C) and 50% in accordance with the mass-ratios
of the fractions from 420C AET.
LOSS:
Loss up to 343C AET is distributed with 2/3 in
the gas-fraction and 1/3 in the first liquidfraction.

204-130

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Statoil PTL MON Crude Oil and Products (CP)

3. ANALYTICAL RESULTS
*******************************
PROJECT:
REF.NO:

CRUDE OIL ASSAY

204-130

*****************************************************************************************************************************************
Table 1a
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
Analysis of the whole crude:

Light ends - see tables 8a-8e

Density at 15C
Specific gravity at 60/60F
API gravity at 60/60F
Dry oil density at 15C

kg/l

Sulphur
Mercaptan sulphur
Total Acid Number (TAN)

mass %
mg/kg
mg KOH/g

Reid Vapor Pressure (RVP)

Pour point

kPa
C

Kin. viscosity at 5C (D7042)

Kin. viscosity at 10C (D7042)
Kin. viscosity at 20C (D7042)

mm/s (cSt)
mm/s (cSt)
mm/s (cSt)

420
280
160

Kin. viscosity at 13C (D445)

Kin. viscosity at 30C (D445)

mm/s (cSt)
mm/s (cSt)

342
122

Nitrogen

mg/kg

Hydrogen sulphide

mass %

Mercury(Hg)

g/kg

Salt as NaCl

mg/l

14

Flash point
Water content

C
mass %

<10
0.17

Asphaltenes
n-Pentane insolubles
Organic chlorides

mass %
mass %
g/g

8.6
12.9
<1

API
kg/l

0.9241
0.9246
21.5
0.9239
3.633
54
2.0
43.0
<-45
(1)
(1)
(1)

3400
ND

(3)

(4)

ND: not detectable

Comments attached

204-130

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Table 1b
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
Metals Analysis
Aluminum
Barium
Beryllium
Cadmuim
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdeum
Nickel
Phosphorus
Silicon
Sodium
Strontium
Titanium
Vanadium
Zinc

204-130

mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg

0.4
<0,1
<0,1
<0,1
<0,1
0.1
0.2
<0,1
3.0
<0,3
<0,1
<0,1
7.9
60
2.1
<0,3
1.0
<0,1
2.0
180
0.2

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Table 2
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************

Fraction
Fraction

C
F

Yield on crude
Yield on crude
Position in crude
Position in crude
Mid mass
Mid vol

mass %
vol %
mass %
vol %
mass %
vol %

Density at 15C
Specific gravity at 60/60F
API gravity at 60/60F

kg/l

204-130

API

C5-74
C5-165

74-110
165-230

110-177
230-350

8.00
11.18
0,75-8,75
1,17-12,36
4.75
6.76

3.88
4.84
8,75-12,63
12,36-17,20
10.69
14.78

6.12
7.25
12,63-18,75
17,20-24,44
15.69
20.82

0.6474
0.6474
87.1

0.7256
0.7258
63.5

0.7638
0.7640
53.7

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Table 3a
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
Fraction
Fraction

C
F

C5-177
C5-350

177-232
350-450

232-288
450-550

288-343
550-649

Yield on crude
Yield on crude
Position in crude
Position in crude
Mid mass
Mid vol

mass %
vol %
mass %
vol %
mass %
vol %

18.00
23.27
0,75-18,75
1,17-24,44
9.75
12.81

4.02
4.54
18,75-22,77
24,44-28,99
20.76
26.72

5.26
5.61
22,77-28,03
28,99-34,60
25.40
31.80

6.66
6.82
28,03-34,69
34,60-41,42
31.36
38.01

Density at 15C
Specific gravity at 60/60F
API gravity at 60/60F

kg/l

0.7017
0.7018
70.1

0.8171
0.8174
41.6

0.8666
0.8670
31.7

0.9021
0.9026
25.3

Sulphur
Mercaptan sulphur
Copper corrosion
Total Acid Number (TAN)
Bromine number

mass %
mg/kg

0.006
37

0.801

1.698

0.01
0.4

0.143
18
1a
0.03
1.5

mg KOH/g
g Br/100 g

1a
0.23
3.6

1.40

n-Paraffins
i-Paraffins
Olefins
Naphtenes
Aromatics
Oxygenates

mass %
mass %
mass %
mass %
mass %
mass %

32.1
36.4
<0,2
24.9
6.7
<0,2

3.2
59.0
<0,2
20.2
17.6
<0,2

Paraffins
i-Paraffins
Olefins
Naphtenes
Aromatics
Oxygenates

vol %
vol %
vol %
vol %
vol %
vol %

34.1
38.2
<0,2
22.4
5.3
<0,2

3.5
61.5
<0,2
19.0
16.0
<0,2

Aromatics (HPLC)
Total
Mono-Aromatics
Di-Aromatics
Polycyclic Aromatics

mass %
mass %
mass %
mass %

25.1
19.1
6.0
<0,1

40.8
27.3
12.7
0.8

204-130

API

16.5
15.6
0.9
<0,1

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Table 3b
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
Fraction
Fraction

C
F

Naphtalenes
Aniline point
Smoke point
Flash point
Vapor pressure (DVPE)

vol %
C
mm
C

Freezing point
Cloud point
Cold Filter Plugging Point (CFPP)
Pour point

C
C
C
C

Research Octane Number (RON)

Motor Octane Number (MON)

C5-177
C5-350

177-232
350-450

232-288
450-550

288-343
550-649

58.0

0.31
56.6
21.0

2.10
58.8
17.0

7,47
57.9

<-60
<-51
<-51

-38
(6)
<-38
<-38
-42

-27
-7
-30

38.1
36.6
37.3
41.9

39.3
39.9
39.3
42.2

41.4
39.9
41.7
38.5

(5)

<10
62.5
<-60

61.0
58.7

Cetane number
Cetane index (D-976)
CCI (D-4737)
CGSB Cetane index
Kin. viscosity at 5C (D7042)
Kin. viscosity at 10C (D7042)
Kin. viscosity at 20C (D7042)
Kin. viscosity at 40C (D7042)
Kin. viscosity at 60C (D7042)

mm/s (cSt)
mm/s (cSt)
mm/s (cSt)
mm/s (cSt)
mm/s (cSt)

0.39
0.38
0.36
0.28

2.27
2.06
1.73
1.27
0.99

7.69
6.50
4.84
3.00
2.06

38.9
29.1
17.7
8.20
4.65

Kin. viscosity at 20C (D445)

Kin. viscosity at 30C (D445)
Kin. viscosity at 50C (D445)

mm/s (cSt)
mm/s (cSt)
mm/s (cSt)

0.57
0.53

1.78
1.51

4.76
3.67
2.40

11.5
5.93

Nitrogen
Basic nitrogen

mg/kg
mass %

1.8

9.3

25

130
0.011

Distillation D-86 (50%)

83.9

197.2

257.8

311.1

Comments attached

204-130

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Table 4
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
Fraction
Fraction

C
F

Yield on crude
Yield on crude
Position in crude, mass%
Position in crude, volume%
Mid mass%
Mid vol%

mass %
vol %

Density at 15C
Specific gravity at 60/60F
API gravity at 60/60F

kg/l

Sulphur
Total Acid Number (TAN)

mass %
mg KOH/g

Aniline point
Watson K-factor

52.3
11.3

Pour point
Conradson Carbon Residue (CCR)

C
mass %

0
0.19

Kin. viscosity at 40C (D7042)

Kin. viscosity at 60C (D7042)

mm/s (cSt)
mm/s (cSt)

302
77.0

Kin. viscosity at 50C (D445)

Kin. viscosity at 100C (D445)

mm/s (cSt)
mm/s (cSt)

144
13.4

Vanadium (V)
Nickel (Ni)

mg/kg
mg/kg

<0,1
<0,1

Nitrogen
Basic nitrogen

mg/kg
mass %

Refractive index at 67C

Refractive index at 20C

204-130

API

343-524
649-975
24.06
22.89
34,69-58,75
41,42-64,31
46.72
52.87
0.9716
0.9722
14.0
3.551
3.90

1700
0.055
1.521
1.538

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Table 5
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
Fraction
Fraction

C
F

343+
649+

524+
975+

Yield on crude
Yield on crude
Position in crude, mass%
Position in crude, volume%
Mid mass%
Mid vol%

mass %
vol %

65.31
58.58
34,69-100
41,42-100
67.35
70.71

41.25
35.69
58,75-100
64,31-100
79.38
82.16

Density at 15C
Specific gravity at 60/60F
API gravity at 60/60F

kg/l

1.0306
1.0313
5.7

1.0679
1.0687
0.9

(7)

Sulphur
Total Acid Number (TAN)

mass %
mg KOH/g

5.16
2.90

6.23

(8)

Aniline point

>130

CNBD

Pour point
Conradson Carbon Residue (CCR)

C
mass %

33
15.3

CNBD
24.6

Asphaltenes
n-Pentane insolubles
Ash

mass %
mass %
mass %

13.1
18.6
0.085

22.6
31.7
0.110

Kin. viscosity at 135C (D445)

Kin. viscosity at 150C (D445)

mm/s (cSt)
mm/s (cSt)

152
85.3

CNBD
2200

Vanadium (V)
Nickel (Ni)

mg/kg
mg/kg

270
100

420
170

Nitrogen
Basic nitrogen

mg/kg
mass %

5200
0.141

7500
0.196

Penetration at 25C
Refractive index at 67C

0.1mm

175
CNBD

API

(9)

CNBD: Could Not Be Done due to the nature of the sample

Comments attached

204-130

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Table 6
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************

DISTILLATION
YIELD MASS-%
********************

Date:
Intake:
Density at 15C:

FRACTION

Loss

11-Oct-11
25009.8 g
0.9241 kg/l

Mass
g

Yield
mass %

Cumul. yield
mass %

Temperature
C

0.0

0.00

0.00

Gases

187.8

0.75

0.75

15

C5-74

2000.8

8.00

8.75

74

74-110

971.2

3.88

12.63

110

110-177

1529.7

6.12

18.75

177

177-232

1004.7

4.02

22.77

232

232-288

1316.6

5.26

28.03

288

288-343

1664.9

6.66

34.69

343

343-420

2442.5

9.77

44.46

420

420-524

3575.3

14.30

58.75

524

10316.3

41.25

100.00

524+

524+

204-130

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Table 7
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
DISTILLATION
YIELD VOL-% AND DENSITY
*************************************

Date:
Intake:
Density at 15C:
FRACTION

11-Oct-11
25009.8 g
0.9241 kg/l
Density at
15C (kg/l)

Loss

Yield
vol %

Cumul. yield
vol %
0.00

0.00

Temperature
C

Gases

0.5782

1.17

1.17

15

C5-74

0.6474

11.18

12.36

74

74-110

0.7256

4.84

17.20

110

110-177

0.7638

7.25

24.44

177

177-232

0.8171

4.54

28.99

232

232-288

0.8666

5.61

34.60

288

288-343

0.9021

6.82

41.42

343

343-524

0.9716

22.89

64.31

524

524+

1.0679

35.69

100.00

524+

204-130

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Table 8a
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************

COMPOSITIONAL ANALYSIS OF CRUDE OIL (ASTM D-5134)

(MASS-PERCENT)

**************** NORMAL PARAFFINS ****************

METHANE
ETHANE
PROPANE
BUTANE
PENTANE
HEXANE
HEPTANE
OCTANE
NONANE
--------------------------------------------------------SUM N-PARAFFINS

<0.01
<0.01
0.01
0.55
2.39
1.26
0.87
0.66
0.49
6.24

************** C4 HYDROCARBONS ***************

ISO-BUTANE

0.10

*************** C5 HYDROCARBONS ***************

ISO-PARAFFINS:
-------------------------2,2-DIMETHYLPROPANE
ISO-PENTANE
--------------------------------------------------------SUM C5 ISO-PARAFFINS

0.01
2.12
2.13

NAPHTENES:
---------------------CYCLOPENTANE

204-130

0.22

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Table 8b
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************

*************** C6 HYDROCARBONS ***************

ISO-PARAFFINS:
-------------------------2,2-DIMETHYLBUTANE
2,3-DIMETHYLBUTANE
2-METHYLPENTANE
3-METHYLPENTANE
--------------------------------------------------------SUM C6 ISO-PARAFFINS

0.04
0.11
0.88
0.47
1.51

NAPHTENES:
---------------------METHYLCYCLOPENTANE
CYCLOHEXANE
--------------------------------------------------------SUM C6 NAPHTENES

0.61
0.33
0.94

AROMATICS:
---------------------BENZENE

204-130

0.13

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Table 8c
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************

*************** C7 HYDROCARBONS ***************

ISO-PARAFFINS:
-------------------------2,2,3-TRIMETHYLBUTANE
3,3-DIMETHYLPENTANE
2,4-DIMETHYLPENTANE
2-METHYLHEXANE
2,3-DIMETHYLPENTANE
3-METHYLHEXANE
2,2-DIMETHYLPENTANE
--------------------------------------------------------SUM C7 ISO-PARAFFINS

<0.01
0.01
0.04
0.29
0.11
0.38
0.02
0.85

NAPHTENES:
---------------------CIS-1,3-DIMETHYLCYCLOPENTANE
TRANS-1,3-DIMETHYLCYCLOPENTANE
TRANS-1,2-DIMETHYLCYCLOPENTANE
METHYLCYCLOHEXANE
ETHYLCYCLOPENTANE
1,1-DIMETHYLCYCLOPENTANE
--------------------------------------------------------SUM C7 NAPHTENES

0.14
0.11
0.21
0.67
0.12
0.04
1.28

AROMATICS:
---------------------TOLUENE

204-130

0.34

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Table 8d
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
*************** C8 HYDROCARBONS ***************
ISO-COMPOUNDS:
------------------------------2,5-DIMETHYLHEXANE
2,4-DIMETHYLHEXANE
3,3-DIMETHYLHEXANE
2,3-DIMETHYLHEXANE
2-METHYL 3-ETHYLPENTANE
2-METHYLHEPTANE
4-METHYLHEPTANE
2,3,4-TRIMETHYLPENTANE
--------------------------------------------------------SUM C8 ISO-PARAFFINS

0.03
0.03
<0.01
0.03
0.01
0.35
0.12
<0.01
0.57

NAPHTENES:
---------------------1,1,3-TRIMETHYLCYCLOPENTANE
(INCL. 2,2-DIMETHYLHEXANE)
TRANS,CIS-1,2,4-TRIMETHYLCYCLOPENTANE
TRANS,CIS-1,2,3-TRIMETHYLCYCLOPENTANE
1,1-DIMETHYLCYCLOHEXANE
TRANS-1-METHYL-3-ETHYLCYCLOPENTANE
CIC-1-METHYL-3-ETHYLCYCLOPENTANE
TRANS-1-METHYL-2-ETHYLCYCLOPENTANE
TRANS-1,2-DIMETHYLCYCLOHEXANE
ISOPROPYLCYCLOPENTANE
CIS-1,2-DIMETHYLCYCLOHEXANE
ETHYLCYCLOHEXANE (INCL. N-PROPYLCYCLOPENTANE)
1-METHYL-1-ETHYLCYCLOPENTANE
1,1,2-TRIMETHYLCYCLOPENTANE
UNIDENTIFIED C8 NAPHTENES
--------------------------------------------------------SUM C8 NAPHTENES

204-130

0.04
0.06
0.05
0.03
0.06
0.04
0.06
0.06
<0.01
0.03
0.16
<0.01
0.02
0.42
1.02

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Table 8e
SAMPLE:
204-130
Statoil Cheecham Blend
*****************************************************************************************************************************************
AROMATICS:
---------------------ETHYLBENZENE
META-DIMETHYLBENZENE (XYLENE)
PARA-DIMETHYLBENZENE (XYLENE)
ORTHO-DIMETHYLBENZENE (XYLENE)
--------------------------------------------------------SUM C8 AROMATICS

0.07
0.23
0.07
0.14
0.51

*************** C9 HYDROCARBONS ***************

ISO-PARAFFINS:
-------------------------3,5-DIMETHYLHEPTANE
4-METHYLOCTANE
2-METHYLOCTANE
3-METHYLOCTANE
2,3-DIMETHYLHEPTANE
3,4-DIMETHYLHEPTANE
4-ETHYLHEPTANE
2,3,4-TRIMETHYLHEXANE
--------------------------------------------------------SUM C9 ISO-PARAFFINS

0.12
0.08
0.11
0.17
0.05
0.02
0.02
0.01
0.57

NAPHTENES:
---------------------1,1,3-TRIMETHYLCYCLOHEXANE
1,1,4-TRIMETHYLCYCLOHEXANE
UNIDENTIFIED C9 NAPHTENES
--------------------------------------------------------SUM C9 NAPHTENES

0.11
0.04
0.19
0.34

TOTAL IDENTIFIED
TOTAL UNIDENTIFIED

16.7566
0.1481

TOTAL C10+

83.0953

********************************************** ******************************************

204-130

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Statoil PTL MON Crude Oil and Products (CP)

4. ANALYTICAL METHODS
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Table 10a
204-130
Statoil Cheecham Blend
********************************************************************************************

TEST

UNITS

METHOD

Density at 15C
Specific gravity at 60/60 F
Dry Oil Density at 15C

kg/l
kg/l

D-4052/D-5002
IP479

Total Sulphur
Total Sulphur
Hydrogen sulphide
Mercaptan sulphur

mass %
mass %
Pos. / Neg.
mg/kg

D-4294
D-5453 for sulphur content less than 0,01%
Lead Acetate Paper
D-3227

n-Paraffins
i-Paraffins
Naphthenes
Aromatics
Olefines
Oxygenates
Aromatics - HPLC

mass %
mass %
mass %
mass %
mass %
mass %
mass %

EN ISO 22854/D-6839
EN ISO 22854/D-6839
EN ISO 22854/D-6839
EN ISO 22854/D-6839
EN ISO 22854/D-6839
EN ISO 22854/D-6839
D-6591

Naphthalene
Watson K
Vapor Pressure (DVPE)
Reid Vapor Pressure (RVP)
Flash point (Pensky Martens)
Freezing point
Cloud point
Pour point
Could Filter Plugging Point
Kin. Viscosity
Kin. Viscosity

vol %

D-1840
UOP 375
D-5191
D-323
D-6450
D-2386
D-5772
D-5853/D-5950
IP 309
D-445
D-7042

204-130

kPa
kPa
C
C
C
C
C
mm/s (cSt)
mm/s (cSt)

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Statoil PTL MON Crude Oil and Products (CP)

::
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Table 10b
204-130
Statoil Cheecham Blend
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TEST

UNITS

METHOD

Aniline Point
Research Octane Number (RON)
Motor Octane Number (MON)
Cetane index
Calculated Cetane Index (CCI)
Cetane number
CGSB Cetane index
Smoke point

D-611
D-2699
D-2700
D-976
D-4737
D-613
CAN/CGSB-3.0
D-1322

mm

Distillation of the whole crude up to 375C

Distillation of the indivudal fractions
Distillation of 375+ C
Simulated distillation
High Temperature simulated distillation

D-2892
D-86
D-5236
D-2887
IP/PM-CF98

Total Acid Number (TAN)

Bromine number
Copper corrosion
Nitrogen
Nitrogen

mgKOH/g
g Br/100 g
<100 mg/kg
>40 mg/kg

D-664
D-1159
D-130
D-4629
D-5762

Basic nitrogen

mass %

UOP 269

Vanadium (V)
Nickel (Ni)
Sodium (Na)
Mercury (Hg)
Other metals
Salt as NaCl

mg/kg
mg/kg
mg/kg
g/kg
mg/kg
mg/l

ICP
ICP
ICP
FIMS (inhouse method)
ICP
IP 265

Carbon Residue (Micro Method)

Asphaltenes
Organic chlorides
n-C5 Insolubles
Ash

mass %
mass %
g/g
mass %
mass %

D-4530
IP 143
D-4929-07
D-4055
D-482

Penetration at 25C

0.1mm

D-1321

Refractive index at 67C

Wax content
Water content

mass %
mass %

Abbe refractometer
UOP 46 (mod. acetone precip.)
D-4928

Compsitional analysis of crude oil

mass %

D-5134

204-130

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