water layer wt%

acetic acid
0
0.0069
0.0141
0.0289
0.0642
0.133
0.255
0.367
0.443
0.464
0.362
0.311
0.216
0.114
0.0482
0.0193
0.0079
0.0037
0.0018
0

0
0.69
1.41
2.89
6.42
13.3
25.5
36.7
44.3
46.4
36.2
31.1
21.6
11.4
4.82
1.93
0.79
0.37
0.18
0

water
0.988
0.981
0.971
0.955
0.917
0.844
0.711
0.589
0.451
0.371
0.151
0.108
0.069
0.039
0.019
0.01
0.008
0.007
0.005
0.006

98.8
98.1
97.1
95.5
91.7
84.4
71.1
58.9
45.1
37.1
15.1
10.8
6.9
3.9
1.9
1
0.8
0.7
0.5
0.6

ether
0.012
0.012
0.015
0.016
0.019
0.023
0.034
0.044
0.106
0.165
0.487
0.581
0.715
0.847
0.933
0.971
0.984
0.989
0.993
0.994

1.2
1.2
1.5
1.6
1.9
2.3
3.4
4.4
10.6
16.5
48.7
58.1
71.5
84.7
93.3
97.1
98.4
98.9
99.3
99.4

isopropl layer
acetic acid
water
ether
0
0.6
99.4
0.18
0.5
99.3
0.37
0.7
98.9
0.79
0.8
98.4
1.93
1
97.1
4.82
1.9
93.3
11.4
3.9
84.7
21.6
6.9
71.5
31.1
10.8
58.1
36.2
15.1
48.7

y
0
0.0069
0.0141
0.0289
0.0642
0.133
0.255
0.367
0.443
0.464
0.464

0
0.0018
0.0037
0.0079
0.0193
0.0482
0.114
0.216
0.311
0.362
0.464

y
1
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0

1
0.9

0.8
mass fraction C (Xc,Yc)

x
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

0.7
0.6
0.5
0.4

0.3
0.2

0
0.1
0.2
0.3
0.4
0.5

0.1
0
0

0.1

0.2

0.3

B (water)

0.4

0.5

0.6

0.7

0.8

mass fraction A (xA, yA)

0.5
Ether layer (extract) , Ya

0
0.1
0.2
0.3
0.4
0.5

0.4
0.3
0.2
0.1

0
0

0.1

0.2

0.3

0.4

0.5

0.6

water layer (rafinate) , Xa

0.7

0.8

Series1
Series2

A (acetic acid)
0.9

Series1
Series2

0.9

water layer wt%

acetic acid
0
0.0069
0.0141
0.0289
0.0642
0.133
0.255
0.367
0.443
0.464
0.362
0.311
0.216
0.114
0.0482
0.0193
0.0079
0.0037
0.0018
0

0
0.69
1.41
2.89
6.42
13.3
25.5
36.7
44.3
46.4
36.2
31.1
21.6
11.4
4.82
1.93
0.79
0.37
0.18
0

water
0.988
0.981
0.971
0.955
0.917
0.844
0.711
0.589
0.451
0.371
0.151
0.108
0.069
0.039
0.019
0.01
0.008
0.007
0.005
0.006

98.8
98.1
97.1
95.5
91.7
84.4
71.1
58.9
45.1
37.1
15.1
10.8
6.9
3.9
1.9
1
0.8
0.7
0.5
0.6

ether
0.012
0.012
0.015
0.016
0.019
0.023
0.034
0.044
0.106
0.165
0.487
0.581
0.715
0.847
0.933
0.971
0.984
0.989
0.993
0.994

1.2
1.2
1.5
1.6
1.9
2.3
3.4
4.4
10.6
16.5
48.7
58.1
71.5
84.7
93.3
97.1
98.4
98.9
99.3
99.4

isopropl layer
acetic acid
water
ether
0
0.6
99.4
0.18
0.5
99.3
0.37
0.7
98.9
0.79
0.8
98.4
1.93
1
97.1
4.82
1.9
93.3
11.4
3.9
84.7
21.6
6.9
71.5
31.1
10.8
58.1
36.2
15.1
48.7

y
0
0.0069
0.0141
0.0289
0.0642
0.133
0.255
0.367
0.443
0.464
0.464

0
0.0018
0.0037
0.0079
0.0193
0.0482
0.114
0.216
0.311
0.362
0.464

0
0.1
0.2
0.3
0.4
0.5

1.5
1.4
1.3
1.2
1.1
1
mass fraction C (Xc,Yc)

0
0.1
0.2
0.3
0.4
0.5

y
1
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0

0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0

-0.5

-0.4 -0.3
(water)

-0.2

-0.1

0.1

0.2

0.3

0.4

0.5

0.6

0.5

0.6

mass fraction A (xA, yA)

0.5
Ether layer (extract) , Ya

x
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

0.4
0.3
0.2
0.1
0

-0.5

-0.4

-0.3

-0.2

-0.1

0.1

0.2

0.3

0.4

water layer (rafinate) , Xa

45
0.075
0.75

Series1
Series2

A (acetic acid)
0.6

0.7

0.8

0.9

Series1
Series2

0.6

0.7

0.8

0.9

water layer wt%

acetic acid
0
0.0069
0.0141
0.0289
0.0642
0.133
0.255
0.367
0.443
0.464
0.362
0.311
0.216
0.114
0.0482
0.0193
0.0079
0.0037
0.0018
0

0
0.69
1.41
2.89
6.42
13.3
25.5
36.7
44.3
46.4
36.2
31.1
21.6
11.4
4.82
1.93
0.79
0.37
0.18
0

water
0.988
0.981
0.971
0.955
0.917
0.844
0.711
0.589
0.451
0.371
0.151
0.108
0.069
0.039
0.019
0.01
0.008
0.007
0.005
0.006

98.8
98.1
97.1
95.5
91.7
84.4
71.1
58.9
45.1
37.1
15.1
10.8
6.9
3.9
1.9
1
0.8
0.7
0.5
0.6

ether
0.012
0.012
0.015
0.016
0.019
0.023
0.034
0.044
0.106
0.165
0.487
0.581
0.715
0.847
0.933
0.971
0.984
0.989
0.993
0.994

1.2
1.2
1.5
1.6
1.9
2.3
3.4
4.4
10.6
16.5
48.7
58.1
71.5
84.7
93.3
97.1
98.4
98.9
99.3
99.4

isopropl layer
acetic acid
water
ether
0
0.6
99.4
0.18
0.5
99.3
0.37
0.7
98.9
0.79
0.8
98.4
1.93
1
97.1
4.82
1.9
93.3
11.4
3.9
84.7
21.6
6.9
71.5
31.1
10.8
58.1
36.2
15.1
48.7

y
0
0.0069
0.0141
0.0289
0.0642
0.133
0.255
0.367
0.443
0.464
0.464

0
0.0018
0.0037
0.0079
0.0193
0.0482
0.114
0.216
0.311
0.362
0.464

0
0.1
0.2
0.3
0.4
0.5

1.5
1.4
1.3
1.2
1.1
1
mass fraction C (Xc,Yc)

0
0.1
0.2
0.3
0.4
0.5

y
1
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0

0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0

-0.5

-0.4 -0.3
(water)

-0.2

-0.1

0.1

0.2

0.3

0.4

0.5

0.6

0.5

0.6

mass fraction A (xA, yA)

0.5
Ether layer (extract) , Ya

x
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

0.4
0.3
0.2
0.1
0

-0.5

-0.4

-0.3

-0.2

-0.1

0.1

0.2

0.3

0.4

water layer (rafinate) , Xa

45
0.075
0.75

Series1
Series2

A (acetic acid)
0.6

0.7

0.8

0.9

Series1
Series2

0.6

0.7

0.8

0.9