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Nd:YAG KW (SEM) X (XRD) : Gordani@mut-Es - Ac.ir Shoja - R@mut-Es - Ac.ir
Nd:YAG KW (SEM) X (XRD) : Gordani@mut-Es - Ac.ir Shoja - R@mut-Es - Ac.ir
.
Nd:YAG 1kw .
.
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XRD
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-1 - - gordani@mut-es.ac.ir -
-2 - - shoja_r@mut-es.ac.ir -
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60202mm .
500
. 1 .
: 1
SiO2
Al2O3
CaO
Fe2O3
TiO2
MgO
Na2O3
92/87
3/7
<0/04
<0/04
<0/02
<0/1
<0/1
Nd:YAG 1
. 250 1000
15 . 2
. ZnSe 1
0/001
. %50
. 1 .
: 2
)(mm
)(mm/min
)(mj
15
250
15
500
15
750
15
1000
: 1
5lit/min .
(XRD)X .
UV/VIS .
2 .
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: 3
(A (B
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SiO2 .
SiO2.
: 4 XRD SiO2 A
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5 XRD 500
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. XRD
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Cos
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=t
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: 5 XRD SiO2 B
:6 XRD SiO2 C
750mj
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: 7 XRD SiO2 D
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UV/VIS
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1. M.C. Goncalves and G.S. Attard, "Nanostructured Mesoporous Silica films", Rev.
Adv. Mater. Sci. 4, 2003, 147-164.
2. J.T. Hosson and D.H.J. Teeuw, "Nano ceramic coatings produced by laser treatment",
Surface Engineering vol. 15, No. 3, 1999.
...
gordani@mut-es.ac.ir
Abstract
Nd:YAG 1KW pulsed laser was used to sintering and crystallization of silica sol-gel
coatings on glass substrate. These coatings has prepared by laser process then compared
to conventional sol-gel coating in structural item. Results show that laser sintering
process produced a very dense film with a low density of porosity and crack. XRD analysis
pattern and mathematical equation, indicated that laser sintered coats had nanocrystalline
structure. That shown very short range in grain size.
Keywords: silica sol-gel coating, Nanocrystalline, laser sintering
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