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FORM 13 (See Rule 46) THE DRUGS AND COSMETICS RULES, 1945 CERTIFICATE OF TEST OR ANALYSIS BY GOVERNMENT ANALYST

UNDER SECTION 25(1) OF DRUGS ACT, 1940. 1. Name of the Inspector from whom Received 2. Serial Number and the date of Inspectors Memorandum. 3. Number of Sample. 4. Date of Receipt 5. Name of the Drugs purported to be Contained in the sample. 6. Condition of seals on the package 7. Result of test or analysis with Protocols of test applied Composition: Acetaminophen U.S.P. Description: White powder present inside the sealed cover. Q/R: 1 X 50 gr Exp. Dt:Nov 2012 Acetaminophen U.S.P. 80618

Test for Identification: 1)Positive for Acetaminophen.

Assay for Acetaminophen: Ref I.P.1996 Weight of sample taken: Sample dilution : 0.07019 gr 100 ____ 10 0.501 X 100 X ______ 10 100 ______ = 99.8 % / 100 % 100 X 100 ____ 10

100 X ______ 0.07019

A Value : 715 Sample absorbance at 257 nm : Calculation: 0.501 X _____ 715 100 X _______ 0.07019

100 _____ 10

( Limit : 98 % to 101 % ) Residue on Ignition: Ref U.S.P. P.No.1927 Weight of Platinum crucible : 23.3254 gr Weight of sample taken : 1.0024 gr Weight of Platinum crucible + Sample taken :24.3278 gr Weight of Platinum crucible after ignition : 23.3262 gr Calculation: 100 X 0.0008 _______________ = 0.07 % 1.0024 ( Limit : Not more than 0.1 % )

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