RIAIDT

UNIDADE DE ESPECTROMETRIA DE MASAS E PROTEMICA

Edificio CACTUS * Campus Vida
15782 Santiago de Compostela (Spain)
Tel. 981 563 100. Ext. 16242 * Fax 981 528098
E-mail: sxemasas@usc.es
Web: http://www.ti.usc.es/riaidt/masas/masas.htm

ESPECTRO ESI-FIA-TOF
Analysis Info
Sample Name
Method

Intens.
x105

EG-1_508_1-C,1_01_7825.d
fia_pos_medio_350-1500_egf.m

Acquisition Date 12/27/2012 4:02:30 PM

Instrument
micrOTOF

593.3932 1+

316.3210 1+

+MS, 2.3-2.3min #(152-156), Background Subtracted

0.0

300

400

500

Bruker Compass DataAnalysis 4.0

600

700

printed:

800

12/28/2012

1185.7806 1+
1207.7618

880.6757

908.7057

807.6725

647.3142

551.4379

492.3016
508.2770

460.3646

437.1930 1+

371.3266 1+

0.5

397.3073

332.3163 1+

1.0

615.3753 1+

416.3369 1+

288.2900 1+

1.5

900

1000

11:51:01 AM

1100

1200 m/z

Page 1 of 6

#
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66

m/z
272.2944
284.2952
288.2900
289.2932
290.2959
295.1945
296.1971
298.3106
301.2118
302.2669
304.2848
305.2879
306.2874
310.2710
311.1677
312.1723
314.3102
316.1747
316.3210
316.6784
317.3248
318.3268
319.3303
325.2197
326.3415
327.2535
327.3450
330.3011
332.3163
333.3193
338.2995
340.3573
341.3610
342.1889
344.3468
348.3200
349.3221
354.3053
359.1358
360.3506
361.3527
362.3365
365.2151
371.3266
372.3214
373.3234
376.3440
385.3417
388.3114
394.2931
395.2967
397.3073
398.0948
398.3118
400.3424
404.3421
409.2745
410.2749
414.0657
415.3177
416.3369
417.3400
418.3423
419.1549
422.3269
422.7158

I
825
745
118124
22730
2942
7048
1207
1482
1143
1132
32523
5855
684
2923
5610
1499
1000
2643
177186
1651
50022
6110
743
1827
20670
799
4436
1682
45125
10188
2171
9816
2425
1189
2110
7699
1736
1890
2554
5986
1379
1687
1640
25806
9450
1815
1440
2921
1504
5519
1332
15328
1811
3650
3206
1261
6361
1496
1348
8327
94612
20215
3908
1103
2099
1435

Res.
16338
17193
14594
13005
13906
14953
14551
12583
16898
14887
15848
13053
12344
14304
12754
15243
20641
11407
12649
16654
14781
14880
18316
14235
16342
14242
13205
16997
14911
15434
18032
14462
16932
15447
18693
14136
11784
25789
15457
17612
16125
16366
17106
13495
9637
10590
18960
13601
17353
19455
17010
16207
15135
12811
13691
14384
19351
13638
20148
14487
17648
14079
15272
19508
15787
17293

Bruker Compass DataAnalysis 4.0

FWHM
0.0167
0.0165
0.0198
0.0222
0.0209
0.0197
0.0204
0.0237
0.0178
0.0203
0.0192
0.0234
0.0248
0.0217
0.0244
0.0205
0.0152
0.0277
0.0250
0.0190
0.0215
0.0214
0.0174
0.0228
0.0200
0.0230
0.0248
0.0194
0.0223
0.0216
0.0188
0.0235
0.0202
0.0222
0.0184
0.0246
0.0296
0.0137
0.0232
0.0205
0.0224
0.0221
0.0214
0.0275
0.0386
0.0353
0.0198
0.0283
0.0224
0.0203
0.0232
0.0245
0.0263
0.0311
0.0292
0.0281
0.0212
0.0301
0.0206
0.0287
0.0236
0.0296
0.0274
0.0215
0.0268
0.0244

Mol. Mass

1+
1+
1+

288.2900
288.2900
288.2900

1+
1+
1+

304.2847
304.2847
304.2847

1+

316.3211

1+
1+
1+

316.3211
316.3211
316.3211

1+

326.3415

1+

326.3415

1+
1+

332.3162
332.3162

1+
1+
1+

371.3240
371.3240
371.3240

1+
1+
1+

416.3368
416.3368
416.3368

printed:

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11:51:01 AM

Page 2 of 6

#
67
68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
102
103
104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132

m/z
425.2755
432.3328
433.3383
437.1930
438.1955
441.2547
444.3685
445.3718
446.3735
457.2225
460.3646
461.3695
476.3719
481.3202
481.8187
488.3948
492.3016
495.3279
499.3184
508.2770
509.2797
515.2915
524.2491
525.2500
526.2498
531.2565
534.4050
535.4571
536.4616
544.3824
545.3853
548.4670
551.4379
552.4434
567.4102
568.4172
569.4301
572.4153
573.4175
580.4559
581.4600
591.3827
593.3932
594.3966
595.4006
596.4102
598.4291
604.3822
607.3772
608.3933
609.4926
610.4955
611.4981
612.3715
612.8697
613.3759
615.3753
616.3780
617.3813
618.3886
625.4703
626.4754
631.3451
632.3492
637.3612
637.5222

I
2071
8149
2185
43043
9216
3247
42466
10326
1824
3093
5638
1770
1972
2508
1740
1178
3185
1496
1234
7920
1679
1944
7100
1650
1826
1413
2066
3633
2011
12136
3951
2239
13239
4601
11613
2950
1749
5120
1900
1283
1058
1232
148507
54870
11389
2071
1267
1040
3109
1236
3043
1565
959
5954
5132
1880
76013
27095
7119
1251
5985
2220
6116
2914
1787
1394

Res.
15625
17274
20446
21013
15084
21978
19668
15346
15006
21715
14905
21339
12764
22743
23584
19104
16753
20541
30621
15657
17369
17666
16688
18334
22199
25385
17962
19895
18900
16823
19157
17716
18271
25000
18012
14099
15721
17841
17877
14739
20537
16416
19625
16140
15764
14785
16436
14654
18338
16056
16880
15375
15262
19465
21369
18188
18115
15712
18431
17191
16142
17085
15666
18275
16232
17900

Bruker Compass DataAnalysis 4.0

FWHM
0.0272
0.0250
0.0212
0.0208
0.0291
0.0201
0.0226
0.0290
0.0297
0.0211
0.0309
0.0216
0.0373
0.0212
0.0204
0.0256
0.0294
0.0241
0.0163
0.0325
0.0293
0.0292
0.0314
0.0286
0.0237
0.0209
0.0298
0.0269
0.0284
0.0324
0.0285
0.0310
0.0302
0.0221
0.0315
0.0403
0.0362
0.0321
0.0321
0.0394
0.0283
0.0360
0.0302
0.0368
0.0378
0.0403
0.0364
0.0412
0.0331
0.0379
0.0361
0.0397
0.0401
0.0315
0.0287
0.0337
0.0340
0.0392
0.0335
0.0360
0.0387
0.0367
0.0403
0.0346
0.0393
0.0356

Mol. Mass

1+
1+

437.1928
437.1928

1+
1+
1+

444.3684
444.3684
444.3684

1+
1+
1+
1+

593.3933
593.3933
593.3933
593.3933

1+
1+
1+
1+

615.3751
615.3751
615.3751
615.3751

printed:

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11:51:01 AM

Page 3 of 6

#
133
134
135
136
137
138
139
140
141
142
143
144
145
146
147
148
149
150
151
152
153
154
155
156
157
158
159
160
161
162
163
164
165
166
167
168
169
170
171
172
173
174
175
176
177
178
179
180
181
182
183
184
185
186
187
188
189
190
191
192
193
194
195
196
197
198

m/z
638.5239
640.4373
641.4430
641.5773
642.4454
643.4514
647.3142
648.3167
649.3213
653.4997
654.5065
662.4485
669.4733
709.3987
721.3547
723.3657
725.3747
737.3317
739.5478
740.5465
748.5466
750.5320
764.5203
765.5237
767.5795
768.5781
777.4001
780.4897
781.4911
782.4877
791.6969
792.7012
793.6926
807.6725
808.6766
809.6802
822.6181
823.6451
824.6463
825.6534
826.6549
836.6513
837.6561
838.5559
839.5609
840.5653
850.6138
851.3903
854.5369
864.6773
865.7182
866.5979
866.7217
867.6014
867.7266
871.6086
872.6071
873.6003
880.6757
881.6950
882.7026
883.7084
887.5836
888.5860
889.5889
893.7661

I
761
774
5352
936
2376
1266
7700
3627
1593
2327
923
1554
1710
802
708
368
524
604
640
308
792
316
2038
893
691
310
508
2062
624
560
1148
840
552
4546
2282
773
351
3407
1784
867
289
1274
578
1262
874
283
314
297
664
667
876
402
594
426
467
1093
828
649
4867
4265
1945
565
3049
1728
494
450

Res.
25139
16817
15998
17357
18401
12763
15963
16350
20648
15422
23174
19906
18873
18866
21919
29091
19375
17633
23921
32451
23003
30246
18448
23260
17509
12233
19845
19136
19264
22746
17645
16806
13779
19332
17962
18202
5614
19931
19349
18895
18975
21111
17058
17956
31595
23361
24634
37171
19185
17905
11090
13443
13645
22172
18850
18881
17064
20815
18147
13267
12688
18480
20168
21776
19743
19830

Bruker Compass DataAnalysis 4.0

FWHM
0.0254
0.0381
0.0401
0.0370
0.0349
0.0504
0.0406
0.0397
0.0314
0.0424
0.0282
0.0333
0.0355
0.0376
0.0329
0.0249
0.0374
0.0418
0.0309
0.0228
0.0325
0.0248
0.0414
0.0329
0.0438
0.0628
0.0392
0.0408
0.0406
0.0344
0.0449
0.0472
0.0576
0.0418
0.0450
0.0445
0.1465
0.0413
0.0426
0.0437
0.0436
0.0396
0.0491
0.0467
0.0266
0.0360
0.0345
0.0229
0.0445
0.0483
0.0781
0.0645
0.0635
0.0391
0.0460
0.0462
0.0511
0.0420
0.0485
0.0665
0.0696
0.0478
0.0440
0.0408
0.0451
0.0451

Mol. Mass

printed:

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11:51:01 AM

Page 4 of 6

#
199
200
201
202
203
204
205
206
207
208
209
210
211
212
213
214
215
216
217
218
219
220
221
222
223
224
225
226
227
228
229
230
231
232
233
234
235
236
237
238
239
240
241
242
243
244
245
246
247
248
249
250
251
252
253
254
255
256
257
258
259
260
261
262
263
264

m/z
895.7332
896.6722
897.6796
898.6294
899.6325
900.6389
902.5539
903.5543
904.5582
905.5602
906.5563
908.5730
908.7057
909.0638
909.5749
909.7205
910.0648
910.7286
911.7331
918.7248
919.7278
924.7037
925.7101
926.6637
927.6727
929.5362
930.7256
932.7390
933.7439
945.6383
946.6461
947.6420
950.7337
951.5359
951.7382
955.7499
956.7471
961.6204
962.6291
963.6986
964.7101
965.7041
973.6820
977.5937
978.6040
979.6007
986.6781
987.6854
989.6414
990.6511
992.7160
1001.6571
1002.6627
1004.7821
1005.6325
1006.6292
1007.6081
1008.6116
1020.7538
1021.7544
1029.5779
1030.5875
1036.7220
1047.9362
1048.9431
1063.9190

I
259
1666
1853
1763
1121
403
584
1312
607
377
270
1633
3543
2028
1457
3173
480
1450
472
1152
669
1194
1076
842
276
290
557
687
376
292
554
333
605
254
556
506
290
983
799
644
871
467
323
1167
647
428
692
425
525
395
322
409
295
326
476
393
413
325
812
539
621
390
252
320
341
672

Res.
13159
17606
18003
9796
21724
17220
23019
17984
16077
20980
21913
20663
18125
23687
21701
13670
16140
16935
15611
18071
17266
20442
15725
9642
15187
27989
21321
20099
16967
15620
22028
26317
17917
18001
28657
14214
19757
18974
20657
17182
16029
18120
25929
17908
18731
14884
21328
20474
17036
17110
14283
26333
17715
24062
16711
15717
14673
19991
22220
30161
19213
18536
23476
16703
20704
21616

Bruker Compass DataAnalysis 4.0

FWHM
0.0681
0.0509
0.0499
0.0917
0.0414
0.0523
0.0392
0.0502
0.0563
0.0432
0.0414
0.0440
0.0501
0.0384
0.0419
0.0665
0.0564
0.0538
0.0584
0.0508
0.0533
0.0452
0.0589
0.0961
0.0611
0.0332
0.0437
0.0464
0.0550
0.0605
0.0430
0.0360
0.0531
0.0529
0.0332
0.0672
0.0484
0.0507
0.0466
0.0561
0.0602
0.0533
0.0376
0.0546
0.0522
0.0658
0.0463
0.0482
0.0581
0.0579
0.0695
0.0380
0.0566
0.0418
0.0602
0.0640
0.0687
0.0505
0.0459
0.0339
0.0536
0.0556
0.0442
0.0627
0.0507
0.0492

Mol. Mass

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#
265
266
267
268
269
270
271
272
273
274
275
276
277
278
279
280
281
282
283
284
285
286
287
288
289
290
291
292
293
294
295
296
297
298
299
300
301
302
303
304
305
306
307
308
309
310
311
312
313
314
315

m/z
1064.9212
1127.8454
1157.7527
1158.7679
1185.7806
1186.7837
1187.7869
1188.7919
1189.7920
1190.7964
1199.7746
1200.7905
1201.7809
1202.7960
1203.7548
1204.7479
1205.2620
1205.7625
1207.7618
1208.7649
1209.7680
1210.7698
1211.7780
1223.7338
1224.7350
1225.7336
1226.7229
1229.7452
1230.7533
1239.7029
1240.7072
1241.7109
1242.7038
1245.7149
1255.8401
1256.8335
1352.6208
1353.6234
1354.6306
1380.6590
1381.6569
1778.1576
1779.1656
1780.1721
1781.1654
1800.1386
1801.1434
1802.1419
1816.1112
1817.1124
1818.1122

I
592
442
300
250
28341
21512
10139
3185
564
222
371
204
407
328
278
388
354
442
10484
9101
3718
1139
343
1268
1184
563
294
339
261
1170
821
432
220
202
396
294
620
479
259
247
232
565
866
575
209
394
557
332
207
383
198

Res.
30463
29476
25556
14117
19204
18587
18829
20201
15869
24557
15724
13153
18779
10983
11157
17771
20640
19614
17669
18655
16831
15636
20552
16418
17054
16928
14944
19105
19980
16836
15728
15092
17467
32548
19628
16623
19990
18680
16750
19996
23683
17719
20331
21581
20107
17106
19179
17700
14992
21288
15350

Bruker Compass DataAnalysis 4.0

FWHM
0.0350
0.0383
0.0453
0.0821
0.0617
0.0639
0.0631
0.0588
0.0750
0.0485
0.0763
0.0913
0.0640
0.1095
0.1079
0.0678
0.0584
0.0615
0.0684
0.0648
0.0719
0.0774
0.0590
0.0745
0.0718
0.0724
0.0821
0.0644
0.0616
0.0736
0.0789
0.0823
0.0711
0.0383
0.0640
0.0756
0.0677
0.0725
0.0809
0.0690
0.0583
0.1004
0.0875
0.0825
0.0886
0.1052
0.0939
0.1018
0.1211
0.0854
0.1184

Mol. Mass

1+
1+
1+
1+
1+
1+

1185.7805
1185.7805
1185.7805
1185.7805
1185.7805
1185.7805

printed:

12/28/2012

11:51:01 AM

Page 6 of 6