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  • Jo202566h Si 001

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    Karthik Saran
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    This document provides supporting information for a study on the copper-catalyzed oxidative trifluoromethylation of terminal alkynes and aryl boronic acids using (trifluoromethyl)trimethylsilane. It includes copies of 1H NMR and 19F NMR spectra of compounds synthesized in the study from pages S2 to S14 and copies of 1H NMR and 13C NMR spectra of additional compounds from pages S15 to S21. The document supports the research presented in exploring a new method for introducing trifluoromethyl groups.

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    This document provides supporting information for a study on the copper-catalyzed oxidative trifluoromethylation of terminal alkynes and aryl boronic acids using (trifluoromethyl)trimethylsilane. It includes copies of 1H NMR and 19F NMR spectra of compounds synthesized in the study from pages S2 to S14 and copies of 1H NMR and 13C NMR spectra of additional compounds from pages S15 to S21. The document supports the research presented in exploring a new method for introducing trifluoromethyl groups.

    Copyright:

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    Download as PDF, TXT or read online from Scribd
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    18 views21 pages

    Jo202566h Si 001

    Uploaded by

    Karthik Saran
    This document provides supporting information for a study on the copper-catalyzed oxidative trifluoromethylation of terminal alkynes and aryl boronic acids using (trifluoromethyl)trimethylsilane. It includes copies of 1H NMR and 19F NMR spectra of compounds synthesized in the study from pages S2 to S14 and copies of 1H NMR and 13C NMR spectra of additional compounds from pages S15 to S21. The document supports the research presented in exploring a new method for introducing trifluoromethyl groups.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
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    of 21

    Supporting Information

    Copper-Catalyzed Oxidative Trifluoromethylation of Terminal Alkynes and Aryl Boronic Acids Using (Trifluoromethyl)trimethylsilane
    Xueliang Jiang, Lingling Chu, and Feng-Ling Qing*,,

    Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 345 Lingling Lu, Shanghai 200032, China

    College of Chemistry, Chemical Engineering and Biotechnology, Donghua University, 2999 North Renmin Lu, Shanghai 201620, China

    Table of Contents

    Copies of 1H NMR and 19F NMR spectra of compounds 2b-2g, 4a-4g Copies of 1H NMR and 13C NMR spectra of compounds 6-8, 10-13

    S2-S14 S15-S21

    S1

    2b

    2b

    S2

    2c

    2c

    S3

    2d

    2d

    S4

    2e

    2e

    S5

    2f

    2f

    S6

    2g

    2g

    S7

    4a

    4a

    S8

    4b

    4b

    S9

    4c

    4c

    S10

    4d

    4d

    S11

    4e

    4e

    S12

    4f

    4f

    S13

    4g

    4g

    S14

    S15

    S16

    S17

    10

    10

    S18

    11

    11

    S19

    12

    12

    S20

    13

    13

    S21

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