MUI N TCVN 3973 - 84 --- TCVN 3974 - 84 - C quan bin son: Cc Cng nghip mui B Cng nghip thc

phm - C quan ngh ban hnh: B Cng nghip thc phm - C quan trnh duyt: Tng cc tiu chun - o lng - Cht lng - C quan xt duyt v ban hnh: y ban Khoa hc v K thut Nh nc - Quyt nh ban hnh s 107/Q ngy 20/11/1984. MUI N (Natri Clorua) Phng php th
Solar salt Method of test

TCVN 3973 - 84
C hiu lc t ngy 01/01/1986

Tiu chun ny quy nh cch ly mu v phng php xc nh cc ch tiu cm quan v ha l ca mui n (Natri clorua - NaCl). 1. Ly mu. 1.1. Cht lng ca mt l hng mui c xc nh da trn c s kt qu phn tch mu trung bnh ca l hng. L hng mui l lng mui cng hng, sn xut theo cng dy chuyn cng ngh, c giao nhn cng mt ln. Mu trung bnh c ly t cc mu ban u ca l hng. Trc khi ly mu ban u, cn quan st dng bn ngoi, cc tp cht l, tnh trng bao b. 1.2. Ly mu ban u. 1.2.1. Gp tt c cc mu ban u ca l hng thnh mu chung. Khi lng mi mu ban u phi ly sao cho khi lng ca mu chung khng t hn 20kg. 1.2.2. i vi mui ri nh ng, mui ri cha kho, mui ri trn toa tu. Mu ban u c ly trn ba ng rnh tr ln o su 0,5m rng 0,5m, dng xng thc su t trn xung vo trong lp mui (khng co ngang) ti 9 im phn b u dc theo ng rnh. Ti cc l hng ln khong 1.000 tn tr ln th khong 20 tn ly mt 1

mu phn b u theo chiu cao, v theo mt ct ngang ca l hng, ly kt hp trong qu trnh bc d mui. 1.2.3. i vi mui ri trong thuyn, trong s lan. Mu ban u c ly 3 t khi d hng: lc bt u d, sau khi d c 1/4 v sau khi d c 3/4 l hng - ly 10 mu cc v tr khc nhau ca thuyn hay s lan. Ring thuyn 3 - 5 tn, mi thuyn ly ba mu. 1.2.4. i vi mui bao gi ln hay ng nh. Mu ban u c ly trong 3% s bao hay ng nhng khng t hn 3 bao hay ng. Ly theo kiu chn la phn on tun t. V d l hng c 100 bao, ly mu ca cc bao th 20, 50, 80, v..v... 1.3. Ly mu trung bnh. Trn u mu trung, ri u trn mt phng sch thnh hnh vung, chia hnh vung theo ng cho thnh 4 phn tam gic, b 2 phn i din, trn u hai phn cn li, lp li qu trnh chia mu nh trn n khi lng mu cn li khong 1,5kg. l mu trung bnh. Chia mu trung bnh thnh 3 phn bng nhau cho vo l c nt kn hay ti polyetylen hai lp, hn kn ming, mt mu chuyn n phng th nghim phn tch, mt mu lu phn tch trng ti, mt mu lu ngi giao hay nhn hng. Trn mu trung bnh c dn nhn ghi: tn c s sn xut, tn sn phm, hng cht lng, khi lng l hng, ngy v ni ly mu, h tn ngi ly mu. C quan phn tch trng ti v ni bo qun mu trng ti theo s tha thun gia bn giao v bn nhn. Ch thch: 1. Mu chung thng c chia ti khi lng 1,5kg (mu trung bnh) chia phn u nhau ngay ti ni ly mu, trc khi a v phng th nghim. 2. ni no c bc d mui bng bng ti, mng trt th mu ban u c ly khi mui ri khi u bng ti hay ming mng trt. Dng khay c kch thc 0,60,6m su 0,05m hng ct ngang qua cng lc dng mui ang chy u. Khi lng mu cng ly nh trn. 1.4. Dng c ly mu. Tt c cc dng c ly mu u m bo kh, sch. Dng c ly mu v ng mu gm c: dao con, khay men hoc khay nha cng 505020cm v 808020cm nu l khay g phi c lt nylon, xng g (ging nh xng xc ct) xng xc mui trong sn xut mui phi ct, cc l c nt kn, cc ti 2

Polyetylen hai lp c kch thc 2025cm, dng c khu bao v hn ming ti, bao ay bao ci hai lp (lp trong l nylon) ng mu mui ban u. 2. Phng php th. Trong tt c cc php th, dng thuc th loi tinh khit phn tch. 2.1. Xc nh mu sc: Ri u mu th ln mt phng, sch mu trng sao cho lp mui dy 1cm; quan st mu sc. 2.2. Xc nh mi v: Cn 5g mui ha tan trong 100ml nc ct nhit phng, nm xc nh v. 2.3. Xc nh mi: Cn 20g mui, nghin trong ci s nhit phng ri ngi xc nh mi. 2.4. Xc nh hm lng m. 2.4.1. Dng c chn s c np. My sy c th sy nhit 1400C. 2.4.2. Tin hnh th: Sy chn s c np nhit 1400C lm ngui trong bnh ht m, cn chn, tip tc sy chn ti khi lng khng i. Cn khong 10g mui chnh xc ti 0,01g cho vo chn sy. Sy mui nhit 140 100C trong 3 gi. Ly chn ra y np lm ngui trong bnh ht m ri cn. Sy tip 30 pht, cn cho ti khi chnh lch gia hai ln cn lin tip khng qu 0,01g. 2.4.3. Tnh kt qu: Hm lng m ca mui tnh bng phn trm (X1) tnh theo cng thc:
X1 = m1 m2 100 m

Trong : m1 m2 m : Khi lng chn v mui trc khi sy, tnh bng gam. : Khi lng chn v mui sau khi sy, tnh bng gam. : Lng cn mui tnh bng gam.

2.5. Xc nh hm lng tp cht khng tan trong nc. 2.5.1. Dng c. - Cn phn tch, chnh xc 0,001g. - Bnh ht m. - Giy lc. 2.5.2. Tin hnh th. Cn 25g mui sy kh (ly mui sy kh ti khi lng khng i) cho vo cc c dung tch 400ml, dng 100ml nc ct ha tan mui. 3

Dun si dung dch trong 10 pht, y np bnh v dung tip trong 30 pht, ngui ti nhit phng. Tin hnh lc trn phu c giy lc (giy lc sy kh v bit khi lng). Nc trng v ra c chuyn ln phu lc. Sau , tin hnh ra cht khng tan ngay trn giy lc nhiu ln bng nc ct ti khi th nc ra bng dung dch bc nitrat 0,1N, khng thy kt ta trng ca bc Clorua l c. Cho dung dch lc v ra vo bnh nh mc c dung tch 500ml, ngui v thm nc ct ti vch mc, lc u v dung dch ny phn tch cc ion. Giy lc v cht khng tan c chuyn vo knh ng h, sy nhit 105 20C trong 3 gi, sau lm ngui trong bnh ht m, ri cn, lp li qu trnh trn cho ti khi chnh lch gia hai ln cn lin tip khng qu 0,001g. 2.5.3. Tnh kt qu. Hm lng tp cht khng tan trong nc tnh bng phn trm cht kh (X2) theo cng thc:
X2 = m1 m2 100 m

Trong : m1 : Khi lng giy lc v cht khng tan sy, tnh bng gam. m2 : Khi lng giy lc, tnh bng gam. m : Lng cn mui tnh bng gam. Kt qu l trung bnh cng ca 2 ln xc nh song song. 2.6. Xc nh hm lng ion Clo (Cl-). 2.6.1. Nguyn tc: Chun ion Clo bng dung dch bc Nitrat (AgNO3) vi ch th Kali Cromat (K2CrO4). 2.6.2. Thuc th v dng c. - Bc Nitrat, dung dch 0,1N. - Kali Cromat, dung dch 10%. - Bnh nh mc 250ml. 2.6.3. Tin hnh th: Ly 25ml dung dch mui t bnh nh mc 500ml (im 2.5), cho vo bnh nh mc 250ml, pha long bng nc ct ti vch mc, lc u. Ly 25ml dung dch mui trong bnh 250ml cho vo bnh tam gic c dung tch 150ml, thm 25ml nc ct, thm 5 - 10 git Kali Cromat dung dch 10% dung dch c mu vng nht. Chun bng dung dch bc Nitrat 0,1N, n khi dung dch chuyn sang mu bn. 2.6.4. Tnh kt qu. Hm lng ion Clo tnh bng phn trm cht kh (X3) theo cng thc: 4

X3 =

0,00355 V 200 100 m

Trong : 0,00355 V 200 : Lng ion Clo ng vi 1ml dung dch AgNO3.0,1N tnh bng gam. : Th tch AgNO3.0.1N tiu tn khi chun tnh bng ml.
25 25 1 = : H s pha long 500 250 200

Ly kt qu trung bnh cng hai ln xc nh song song. Chnh lch kt qu gia hai ln xc nh song song nh hn 0,1%. 2.7. Xc nh hm lng ion Sunfat (SO4- -) (Phng php trng ti). 2.7.1. Nguyn tc: Phng php ny da trn c s kt ta SO4- - di dng Bari Sunfat bng Bari Clorua, trong mi trng axit, nung v cu kt ta, t tnh ra hm lng SO4- -. 2.7.2. Dng c v thuc th. - Axit Clohydric, dung dch 10% (pH = 5 - 6). - Bari Clorua, dung dch 0,1N. - L nung, c nhit nung 650 50C. 2.7.3. Tin hnh th. Ly 100ml nc mui trong bnh nh mc 500ml (im 2.5) cho vo cc dung tch 200ml, thm 3ml dung dch HCl 10%, un si ng thi cng un 10ml dung dch BaCl2 n gn si, ri cho dung dch BaCl2 nng vo dung dch mui, dng a thy tinh khuy dung dch trong 3 pht, ngui n nhit phng (cho vo phn trong ca dung dch my git BaCl2, thy khng kt ta l c). Tin hnh lc kt ta bng giy lc dy, trc ht lc phn trong pha trn kt ta, ri thm 25ml nc ct un si vo cc gn lc, lm nh vy 5 ln, sau chuyn ht kt ta ln giy lc, trng cc v ra kt ta 5 ln bng nc ct nng cho ti khi nc lc ra khng c phn ng Clo (th bng AgNO3 0,1N) l c. Ly giy lc c kt ta BaSO4 ra khi phu v t ln knh ng h, tin hnh sy nhit 1050C trong vng 1 gi, sau chuyn kt ta vo chn nung (chn kh bit khi lng) c np. Nung chn c kt ta nhit 650 50C trong 1 gi, lm ngui trong bnh ht m, ri cn kt ta, lp li qu trnh nung cn cho ti khi khi lng chnh nhau di 0,001g l c. 2.7.4. Tnh kt qu. Hm lng Sufat tnh bng phn trm cht kh (X4) theo cng thc: 5

X4 =

0,445 (m1 m2 ) V mv

Trong : 0,445 : H s chuyn t BaSO4 ra SO- -. m1 m2 m V v : Khi lng chn nung c kt ta, tnh bng gam. : Khi lng chn nung khng c kt ta, tnh bng gam. : Lng cn mu mui tnh bng gam. : Dung tch bnh nh mc, tnh bng ml. : Th tch dung dch ht t bnh nh mc, tnh bng ml.

Kt qu l trung bnh cng ca 2 ln xc nh song song, chnh lch gia 2 ln xc nh song song khng ln hn 0,1%. 2.8. Xc nh hm lng ion Sunfat (SO4- -) 2.8.1. Nguyn tc. Dng lng Bari Clorua d kt ta ion Sunfat SO4- - ca mui mi trng axit yu (kt ta BaSO4). Dng Trilon B chun cc ion Ba+ + d, Mg+ + v Ca+ + trong mi trng c NH4OH - NH4Cl (pH = 10), cht ch th l Eriocrom T en v Metyla . ng thi cng dng Trilon B chun lng dung dch BaCl2 dng, chun ion Ca+ +, Mg+ + ca nc mui, c mi trng v cht ch th nh trn. T 3 ln chun s tnh c hm lng ion SO4- -. 2.8.2. Dng c v thuc th. - Dung dch Trilon B 0,025M. - Bari Clorua, dung dch 0,05M. - Dung dch m NH4OH - NH4Cl, pH = 10. - Dung dch ch th ET00 0,5% - Metyla , dung dch 0,2%. - Axit Clohydric m c. - Buret. 2.8.3. Tin hnh th. Ly 20ml dung dch nc mui trong bnh nh mc 500ml (iu 2,5) cho vo bnh tam gic 250ml, thm 30ml nc ct, 1 git dung dch HCl m c, va lc dung dch va thm 5ml dung dch BaCl2 khi co kt ta trng th yn dung dch 1 - 2 pht na ri thm 2ml dung dch m NH4OH - NH4Cl v 10 git ET100, 10 git Metyla . Dng dung dch Trilon B chun n khi 6

dung dch chuyn t mu sang mu tro, ri sang xanh l cy th dng li, ghi lng Trilon B dng (V1). Ly 20ml dung dch nc mui trong bnh nh mc 500ml (iu 2,5) cho vo bnh tam gic 250ml, ln lt thm 30ml nc ct, 2ml dung dch Trolon B cho ti khi dung dch chuyn mu nh ln trc. Ghi ly lng Trilon B dng (V2). 2.8.4. Tnh kt qu. thc: Hm lng ion SO4- - tnh bng phn trm cht kh (X4) theo cng
X4 =
96 25 (V1 + V2 V1 ) M 100 100 m

Trong : 96 : Phn t lng ion SO- -.

20 25 : H s pha long 500

V1 : Th tch Trilon B chun ln th nht (chun lng Mg+ + , Ca+ + v Ba+ +), tnh bng ml. V2 : Th tch Trilon B dng ln th 2 (chun lng 5ml dung dch BaCl2) tnh bng ml. M m : Nng phn t Trilon B. : Lng cn mu mui, tnh bng g.

Kt qu cui cng l trung bnh cng gia hai ln xc nh song song, chnh lch kt qu gia hai ln xc nh song song nh hn 0,5%. 2.9. Xc nh hm lng ion Canxi (Ca+ +). 2.9.1. Nguyn tc. Trong dung dch nc mui c pH = 12 cht ch th Canxein kt hp vi ion Canxi xut hin mu . Khi c Trilon B trong dung dch, n s to thnh phc cht vi Canxi v y Canxein ra dng t do, dung dch chuyn sang mu vng nh xanh. Cn c vo lng Trilon B tiu hao, s xc nh c hm lng Canxi trong dung dch. 2.9.2. Dng c v thuc th. - Trilon B, dung dch 0,01N. - Dung dch cht ch th Canxein 0,5%. - Natri hydroxyt, dung dch 1N. - Buret.

2.9.3. Tin hnh th. Ly 20ml dung dch mui trong bnh nh mc 500ml (im 2.5), thm 30ml nc ct, 5ml NaOH 1N, 1 git Canxein 0,5%. Tin hnh chun th mt mu bit Trilon B cn dng. Chun b li mu th nghim nh trn ri cho vo dung dch khong 90% lng Trilon B ghi c mu th trn. Sau thm 5ml dung dch NaOH 1N v 4 git Canxein 0,5%. Dng Buret vi lng tip tc chun bng Trilon B cho n khi dung dch chuyn t mu sang mu vng nh xanh, ghi ly tng lng dung dch Trilon B dng 2 ln. 2.9.4. Tnh kt qu. Hm lng Canxi tnh bng phn trm cht kh (X5) theo cng thc:
X5 = 0,0004 V1 500 100 V2 m

Trong : 0,0004 : Lng Canxi tng tng vi 4ml Trilon B, tnh bng gam. V1 V2 500 m : Th tch dung dch Trilon B 0,01N tiu tn khi chun, tnh bng ml. : Th tch dung dch mui c ly t bnh nh mc, tnh bng ml. : Dung tch bnh nh mc, tnh bng ml. : Lng cn mu mui, tnh bng gam.

Kt qu cui cng l trung bnh cng ca kt qu 2 ln xc nh song song, chnh lch gia 2 ln xc nh song song nh hn 0,05%. 2.10. Xc nh hm lng ion Magi (Mg+ +). 2.10.1. Nguyn tc. Phng php ny da trn c s chun tng lng Ca+ +, Mg+ + bng dung dch Trilon B, cht ch th l Criocrom T en trong mi trng pH = 10, kt hp vi phng php xc nh Canxi (im 2.9) s xc nh c hm lng Magi. 2.10.2. Dng c v thuc th. - Trilon B, dung dch 0,01N. - Tinh th Criocrom T en. - Dung dch m NH4OH - NH4Cl; pH = 10. - Buret. 2.10.3. Tin hnh th. Ly 20ml dung dch dch nc mui trong bnh nh mc 500ml (im 8

2.5) cho vo bnh tam gic 250ml, thm 30ml nc ct, 10ml dung dch m pH = 10, vi tinh th ETOO. Dng Trilon B 0,01N chun cho n khi dung dch chuyn t mu tm sang xanh hon ton, ghi li lng Trilon B dng. 2.10.4. Tnh kt qu. thc: Hm lng ion Magi tnh bng phn trm cht kh (X6) theo cng
X6 = 0,00024 (V2 V1 ) 500 100 V m

Trong : 0,00024 : Lng Magi tng ng vi 1ml Trilon B 0,01N, tnh bng gam. V1 V2 V m : Lng Trilon B dung dch 0,01N dng chun Mg+ +, tnh bng ml. : Lng Trilon B dung dch 0,01N chun Ca+ +, tnh bng ml (im 2.9 cng lng mu nh xc nh Mg+ +). : Th tch dung dch mui ly t bnh nh mc, tnh bng ml. : Lng cn mu mui, tnh bng g.

Kt qu cui cng l trung bnh cng ca kt qu 2 ln xc nh song song, chnh lch kt qu gia 2 ln xc nh song song khng ln hn 0,5%. 2.11. Xc nh hm lng ion Kali (K+). 2.11.1. Nguyn tc. Trong mi trng axt yu, Tetrapheyl Borat Natri c phn ng vi ion K cho kt ta trng tan rt t trong nc. Sy v kt ta xc nh hm lng Kali.
+

2.11.2. Dng c v thuc th. - Tetraphenyl Borat Natri. Cn 3g Tetraphenyl Borat Natri NaB(C6H5)4 v 0,5g Nitrat nhm Al(NO3)3 ha tan trong nc ct thnh dung dch c dung tch 10ml qua 1 m (ch pha trc khi dng); - Axit Axetic, dung dch 1N. Dung dch ra: dng 100ml nc ct pha thm 2ml dung dch tetraphenyl Borat Natri 3% v 2ml dung dch axit Axetic 1N. - Phu lc xp s 4. 2.11.3. Tin hnh th. Ly 20ml dung dch nc mui trong bnh nh mc 500ml (im 2.5) 9

cho vo bnh nh mc 250ml, thm nc ti vch. Ly 50ml dung dch trong bnh nh mc 250ml trn, cho vo cc dung tch 150ml axit ha bng 5ml dung dch axit Axetic 1N, em un nng 40 500C cho t t 10ml dung dch Tetraphenyl Borat Natri 3%. Khuy mnh ri lm ngui bng nc ti nhit phng. Dng phu xp s 4 ( sy ti khi lng khng i nhit 120 5 C. Lc ly kt ta. Ra kt ta ngay trn phu 4 ln, mi ln 3ml dung dch ra v 3 ln nc ct, mi ln 3ml, ht kh kt ta, sy kt ta (c phu) nhit 120 50C trong 1 gi, lm ngui trong bnh ht m ri cn.
0

Lp li qu trnh sy, lm ngui v cn ti khi lng khng i. 2.11.4. Tnh kt qu. Hm lng ion Kali tnh bng phn trm cht kh (X7) theo cng thc:
X7 = 0,1091 125 M 100 m

Trong : 0,1091 125 M m : H s tnh chuyn Kali t NaB(C6H5)4.

20 50 1 = : H s pha long 500 250 125

: Khi lng kt ta, tnh bng gam. : Lng cn mu mui, tnh bng gam.

Kt qu cui cng l trung bnh cng ca kt qu 2 ln xc nh song song, chnh lch kt qu gia 2 ln xc nh song song nh hn 0,5%. 2.12. Xc nh hm lng ion Natri (Na+). 2.12.1. Nguyn tc. Dng Antimonat Kali K2H2Sb2O7 kt ta Natri trong mi trng trung tnh hay axt yu, ha tan kt ta trong hn hp axt Clohydric v Iodua Kali ri dng Thiosunfat Natri nh phn It t do, t tnh ra hm lng Na+. Trc ht phi loi cc ion Mg+ +, Ca+ + khi dung dch bng cch cho dung dch tc dng vi 8 xy Quinolin kt ta Mg(C9H6NO2)2.4H2O. gim ha tan ca Na2H2Sb2O7.4H2O trong nc, qu trnh kt ta c tin hnh trong dung dch Etanola. 2.12.2. Dng c v thuc th. - Dung dch 8 oxy Aninolin 2% trong Etanola. - Dung dch to kt ta: ly 20g Antimonat Kali ha tan trong 1 lt nc ct si, lm ngui v thm vo 1g KOH, qua mt m, nu c vn 10

c phi lc. - Natri Thiosufat, dung dch 0,05N. - Etanola khan. - Axit Clohydric m c. - Kali Iodua tinh th. - H tinh bt, dung dch 0,5% Amoni Hydroxyt dung dch 10%. - Ni cch thy. 2.12.3. Tin hnh th. Ly 20ml dung dch nc mui trong bnh nh mc 500ml (im 2.5) cho vo cc dung tch 150ml, un si nh (khi si tm) thm 10ml dung dch 8 Oxy Aninolin 2% v nh thm khong 0,3ml dung dch NH4OH 10% un cch thy cho dung dch si trong 1 - 2 pht; ngui, lc kt ta trn phu s 4, dng 100ml nc ct chia lm nhiu ln ra kt ta (nh vy loi c 2 ion Mg+ + v Ca+ + ra khi dung dch). em dung dch lc ra trn c c ti th tch 25ml, ri nh vo 25ml cn Etanola khan. un hn hp trn ni cch thy v cho t t 25ml dung dch K2H2Sb2O7 va cho vo va khuy. Khi thy c kt ta to thnh th cho nhanh hn. yn nhit phng trong 1 gi ri lc kt ta trn phu s 4, dng 40ml dung dch Etanola ra 7 ln. Chuyn ton b kt ta trn phu vo cc c dung tch 150ml v ha tan kt ta bng 8ml HCl c, ly nc ct ra phu lc thnh cc v thm nc ct dung dch xp x 50ml. Cho vo dung dch 1g tinh th KI yn trong 5 pht ri chun bng dung dch Thiosufat Natri cho n khi dung dch c mu vng nht. Thm 5ml cht ch th h tinh bt 0,5% lc v tip tc chun cho ti khi dung dch ht mu. 2.12.4. Tnh kt qu. thc: Hm lng ion Natri tnh bng phm trm cht kh (X9) theo cng
V N

X9 =

23 500 100 2 vm

Trong : V N v m : Th tch Na2S2O3 tiu tn khi chun, tnh bng ml. : Nng ng lng ca Na2S2O3. : Lng nc mui ly, tnh bng ml. : Lng cn mu mui, tnh bng gam. 11

23 2

: H s tnh chuyn ra Natri. : Dung tch bnh nh mc, tnh bng ml.

500

Kt qu cui cng l trung bnh cng ca kt qu 2 ln xc nh song song, chnh lch gia 2 ln xc nh song song khng ln hn 0,1%. 2.13. Cch biu th thnh phn mui n. Khi c kt qu phn tch hm lng cc ion c trong mui n nh trn, cn biu th ra cc hp cht nh sau: - Cho Ca+ + kt hp vi SO4- - biu th thnh CaSO4. - Ly tng lng SO4- - tr i lng SO4- - kt hp vi Ca+ +, phn cn li kt hp vi MgSO4. - Ly tng lng Mg+ + tr i Mg+ + kt hp vi SO4- -, phn cn li kt hp vi Clo thnh MgCl. Tm tt cch biu th thnh phn mui n. Cation Anion SO4- ClCa+ + CaSO4 Mg+ + MgSO4 MgCl2 KCl NaCl K+ Na+

Ch thch: Hm lng Natri xc nh theo phng php trn (im 2.12) c th cho kt hp vi Clo biu th thnh phn NaCl. Nu thy khp vi kt qu trn l c. Nu khng khp th dng s liu tham kho.

MUI N (Natri Clorua) Yu cu k thut

Solar salt Technical requirements

TCVN 3974 - 84
C hiu lc t ngy 01/01/1986

Tiu chun ny p dng cho mui n (Natri Clorua - NaCl) tinh th loi th, cha qua tinh ch, c sn xut t nc bin theo phng php phi nc hoc phng php phi ct. 1. Phn hng. 1.1. Ty theo phng php sn xut v cht lng sn phm m mui c xp thnh nhng hng sau y: 12

1.1.1. Mui phi nc. - Thng hng. - Hng 1. - Hng 2. 1.1.2. Mui phi ct. - Thng hng. - Hng 1. - Hng 2. 2. Yu cu k thut. 2.1. Cc ch tiu cn quan tm v ha l ca mui phi ph hp vi cc yu cu ghi trong cc bng sau: Bng 1: Cho mui phi nc.
Hng Tn ch tiu Ch tiu cm quan Thng hng Hng 1 Hng 2 Trng xm, trng nu

1. Mu sc

Trng trong, Trng, nh trng xm, nh vng, nh hng - Khng mi

2. Mi v

- Dung dch mui 5% c v mn thun khit, khng c v l. - Kh ro, sch - C ht 1 - 15mm 97,00 95,00 93,00

3. Dng bn ngoi v c ht 4. Hm lng NaCl tnh theo % khi lng kh, khng nh hn: 5. Hm lng cht khng tan trong nc, tnh theo % khi lng kh, khng ln hn: 6. Hm lng m tnh theo % khng ln hn: 7. Hm lng cc ion tnh theo % khi lng kh, khng ln hn: Ca+ + Mg+ + SO4- -

Ch tiu ha l

0,25

0,40

0,80

9,50 0,30 0,40 1,40

10,00 0,45 0,70 1,80

10,50 0,55 1,00 2,35

13

Bng 2: Cho mui phi ct.

Hng Tn ch tiu Ch tiu cm quan Thng hng Trng trong, trng Hng 1 Trng Hng 2 Trng , nh xm, nh vng, nh hng

1. Mu sc

- Khng mi 2. Mi v - Dung dch mui 5% c v mn thun khit, khng c v l. - Kh ro, sch - C ht 1 - 5mm 97,00 92,00 90,00

3. Dng bn ngoi v c ht 4. Hm lng NaCl tnh theo % khi lng kh, khng nh hn: 5. Hm lng cht khng tan trong nc, tnh theo % khi lng kh, khng ln hn: 6. Hm lng m tnh theo % khng ln hn: 7. Hm lng cc ion tnh theo % khi lng kh, khng ln hn: Ca+ + Mg+ + SO4- -

Ch tiu ha l

0,25

0,30

0,40

9,50 0,30 0,40 1,40

13,00 0,65 1,30 2,70

13,50 0,80 1,60 3,50

2.2. Mui phi c sn xut theo ng yu cu ca tiu chun ny v mi l hng xut phi km theo giy chng nhn cht lng. 3. Bao gi, ghi nhn, vn chuyn v bo qun. 3.1. Mui dng n v ch bin thc phm phi c ng bao. i vi cc mc ch s dng khc, mui c th ri hoc ng bao ty theo yu cu, nhng vn phi m bo yu cu ca cc iu 4.4; 4.5 v bo qun v vn chuyn. 3.2. Bao b c th l bao ci, bao ay, bao si tng hp bn chc. Bao mui c ng gi kn, m bo khng b ri vi (phi sch, bn, khng c mi l, khng gy mu cho mui). 3.3. Khuyn khch ghi nhn cc bao gi vi ni dung sau: - Tn c s sn xut. 14

- Tn c quan qun l c s sn xut. - Tn sn phm (mui n phi nc, mui n phi ct). - Hng cht lng. - Khi lng tnh. - Ngy, thng sn xut. - K hiu v s hiu tiu chun ny. 3.4. Khi vn chuyn phi che y, gi gn sch s, khng gim cht lng mui. 3.5. Ni cha v bo qun mui cn m bo nhng yu cu sau: sch, kh ro, thot nc, khng c hng ha hay sn phm khc c nh hng xu n cht lng mui.

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