Scribd Logo
Upload

Welcome to Scribd!

  • Polysorbate 80

    Uploaded by

    truckgal80
    31 views6 pages
    The document contains peak area data from gas chromatography analyses of samples with different concentrations of ethylene glycol and dimethlyformamide. There are three tables showing peak area results for standard solutions and spiked samples with varying concentrations of the compounds. The tables include information on solution weights, peak areas, calculated concentrations, theoretical concentrations, and recovery percentages.

    Original Description:

    polysorbate 80

    Copyright

    © Attribution Non-Commercial (BY-NC)

    Available Formats

    XLS, PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Report this Document
    The document contains peak area data from gas chromatography analyses of samples with different concentrations of ethylene glycol and dimethlyformamide. There are three tables showing peak area results for standard solutions and spiked samples with varying concentrations of the compounds. The tables include information on solution weights, peak areas, calculated concentrations, theoretical concentrations, and recovery percentages.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as XLS, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as xls, pdf, or txt
    31 views6 pages

    Polysorbate 80

    Uploaded by

    truckgal80
    The document contains peak area data from gas chromatography analyses of samples with different concentrations of ethylene glycol and dimethlyformamide. There are three tables showing peak area results for standard solutions and spiked samples with varying concentrations of the compounds. The tables include information on solution weights, peak areas, calculated concentrations, theoretical concentrations, and recovery percentages.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as XLS, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as xls, pdf, or txt
    of 6

    Peak Areas

    STD Set 1
    Vial

    Ethylene Glycol

    2279484.28200

    2311935.05100

    Solution Weight

    Dimethlyformamide

    Set 1
    Set 2
    Set 3

    315.16000
    315.16000
    315.16000

    Accuracy
    Area
    77784.433
    54340.58
    62742.614
    64955.87567

    Corrected Area

    Unspike 1
    Unspike 2
    Unspike 3
    Average
    80% Spiked 1
    80% Spiked 2
    80% Spiked 3

    1933093.4
    1915285.12600
    1894313.759

    1785906.311
    1850329.25
    1829357.88333

    100% Spiked 1
    100% Spiked 2
    100% Spiked 3

    2338221.89000
    2305936.96700
    2343505.60100

    2273266.01433
    2240981.09133
    2278549.72533

    120% Spiked 1
    120% Spiked 2
    120% Spiked 3

    Peak Areas

    2797780.377
    2803931.825
    2811348.877

    2732824.501
    2738975.949
    2746393.001

    Note: areas from system suit for MP1_16FEB12_SS

    STD Set 1
    Vial

    Dimethlyformamide

    307639.28478

    318546.08100

    Solution Weight

    Dimethlyformamide

    Set 2

    0.43491

    Peak Areas

    Note: areas from system suit for MP1_28FEB12_SS

    STD Set 1
    Vial

    Dimethlyformamide

    297506.88990

    298182.85651

    Solution Weight

    Dimethlyformamide

    Set 1
    Set 2
    Set 3

    0.44086
    0.44596
    0.44819

    2256486.12800

    2297433.00800

    4337445.78000

    Sample Wt(mg)

    ppm Recovery

    Theoretical ppm

    5003.540
    5003.540
    5003.540

    341.72745
    353.80408
    349.79411

    504.25600
    504.25600
    504.25600
    Mean
    Std Dev
    %RSD

    5006.730
    5011.500
    5011.500

    542.99683
    534.77570
    543.74088

    630.32000
    630.32000
    630.32000
    Mean
    Std Dev
    %RSD

    5007.170
    5007.170
    5007.170

    783.25263
    785.01569
    787.14148

    756.38400
    756.38400
    756.38400
    Mean
    Std Dev
    %RSD

    309639.30738

    309720.19756

    310244.04836

    SS

    SS
    5

    293329.69531

    296496.13336

    297941.34889

    Average

    2329009.26500

    2635298.91900

    % Recovery

    68
    70
    69
    69
    1.2
    1.8
    86
    85
    86
    86
    0.8
    0.9
    104
    104
    104
    104
    0.3
    0.2

    11

    Average

    307704.82509

    311264.98346

    310679.81823

    11

    Average

    296558.72519

    298371.24838

    296912.41393

    You might also like