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  • Polysorbate 80

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    This document contains results from an analysis of ethylene glycol standards at different concentrations. It reports the peak areas, corrected areas, sample weights, measured concentrations in parts per million, theoretical concentrations, and percent recoveries for unspiked samples and samples spiked at 80%, 100%, and 120% of the theoretical concentration. The results show good accuracy with average percent recoveries ranging from 118% to 92%.

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    This document contains results from an analysis of ethylene glycol standards at different concentrations. It reports the peak areas, corrected areas, sample weights, measured concentrations in parts per million, theoretical concentrations, and percent recoveries for unspiked samples and samples spiked at 80%, 100%, and 120% of the theoretical concentration. The results show good accuracy with average percent recoveries ranging from 118% to 92%.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as XLS, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as xls, pdf, or txt
    15 views3 pages

    Polysorbate 80

    Uploaded by

    truckgal80
    This document contains results from an analysis of ethylene glycol standards at different concentrations. It reports the peak areas, corrected areas, sample weights, measured concentrations in parts per million, theoretical concentrations, and percent recoveries for unspiked samples and samples spiked at 80%, 100%, and 120% of the theoretical concentration. The results show good accuracy with average percent recoveries ranging from 118% to 92%.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as XLS, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as xls, pdf, or txt
    of 3

    Peak Areas

    STD Set 1
    Vial

    Ethylene Glycol

    1911472.68684

    1982054.79179

    Solution Weight

    Ethylene Glycol

    Set 1
    Set 2
    Set 3

    311.27000
    311.27000
    311.27000

    Accuracy
    Area
    271066.6423
    291075.9634
    287201.6148
    283114.7402

    Corrected Area

    Unspike 1
    Unspike 2
    Unspike 3
    Average
    80% Spiked 1
    80% Spiked 2
    80% Spiked 3

    2149756.033
    2135240.09566
    2143875.052

    1866641.29262
    1852125.356
    1860760.31167

    100% Spiked 1
    100% Spiked 2
    100% Spiked 3

    2609196.24139
    2648553.08675
    2616413.08123

    2326081.50124
    2365438.34660
    2333298.34108

    120% Spiked 1
    120% Spiked 2
    120% Spiked 3

    2989586.296
    2965306.175
    3025818.761

    2706471.556
    2682191.435
    2742704.021

    1971600.26958

    2006773.89596

    1968982.03524

    Sample Wt(mg)

    ppm Recovery

    Theoretical ppm

    5009.380
    5009.380
    5009.380

    590.97233
    586.37664
    589.11044

    498.03200
    498.03200
    498.03200
    Mean
    Std Dev
    %RSD

    5011.500
    5011.500
    5011.500

    734.73965
    747.17131
    737.01924

    622.54000
    622.54000
    622.54000
    Mean
    Std Dev
    %RSD

    5007.170
    5007.170
    5007.170

    855.63279
    847.95679
    867.08744

    933.81000
    933.81000
    933.81000
    Mean
    Std Dev
    %RSD

    Average

    1957220.57922

    1966350.70977

    % Recovery

    119
    118
    118
    118
    0.5
    0.4
    118
    120
    118
    119
    1.1
    0.9
    92
    91
    93
    92
    1.0
    1.1

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