Scribd Logo
Upload

Welcome to Scribd!

  • 1.calibration of Glasware

    Uploaded by

    barb201
    19 views4 pages
    This document summarizes the calibration of a buret, beaker, Erlenmeyer flask, and volumetric flask. It provides the initial and final masses and calculated volumes of deionized water delivered to each vessel over multiple trials. The average volumes, standard deviations, and percent relative standard deviations were calculated. The results show that the volumetric flask delivered volumes with the lowest percent error at 0.6%, while the beaker had the highest error at 5.4%.

    Original Description:

    Sample table with results, calculations, and graph sample

    Original Title

    1.Calibration of Glasware

    Copyright

    © Attribution Non-Commercial (BY-NC)

    Available Formats

    XLSX, PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Report this Document
    This document summarizes the calibration of a buret, beaker, Erlenmeyer flask, and volumetric flask. It provides the initial and final masses and calculated volumes of deionized water delivered to each vessel over multiple trials. The average volumes, standard deviations, and percent relative standard deviations were calculated. The results show that the volumetric flask delivered volumes with the lowest percent error at 0.6%, while the beaker had the highest error at 5.4%.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as XLSX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as xlsx, pdf, or txt
    19 views4 pages

    1.calibration of Glasware

    Uploaded by

    barb201
    This document summarizes the calibration of a buret, beaker, Erlenmeyer flask, and volumetric flask. It provides the initial and final masses and calculated volumes of deionized water delivered to each vessel over multiple trials. The average volumes, standard deviations, and percent relative standard deviations were calculated. The results show that the volumetric flask delivered volumes with the lowest percent error at 0.6%, while the beaker had the highest error at 5.4%.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as XLSX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as xlsx, pdf, or txt
    of 4

    Table 1: Calibration of buret (50 mL) (DI H2O temp 21C)

    Trials
    1A
    2A
    3A
    4A
    5A
    1B
    2B
    3B
    4B
    5B

    Vi (mL)
    0.05
    0.03
    9.97
    19.99
    29.97
    39.96
    0.00
    10.00
    19.91
    29.90
    40.00

    Vf (mL)
    0.05
    9.97
    19.99
    29.97
    39.96
    49.95
    10.00
    19.91
    29.90
    40.00
    49.91

    Vt (mL)
    0.07
    9.94
    10.02
    9.98
    9.99
    9.99
    10.00
    9.91
    9.99
    10.10
    9.91

    Mi (g)
    0.0002
    64.7513
    74.5929
    84.5533
    94.4675
    104.3925
    64.7511
    74.6248
    84.5508
    94.3946
    104.4550

    Mf (g)
    0.0002
    74.5928
    84.5533
    94.4675
    104.3925
    114.3352
    74.6248
    84.5508
    94.3946
    104.4550
    114.3476

    MH2O (g)
    0.0003
    9.8415
    9.9606
    9.9142
    9.9250
    9.9427
    9.8737
    9.9260
    9.8438
    10.0604
    9.8926

    0.05

    0.9979955 g/mL
    0.00
    Correction (mL)

    dH2O (21C)=

    10

    20

    30

    40

    -0.05

    -0.10

    -0.15

    Volume Delivered (mL0

    Figure 1: Graph of Calibration of Buret

    50

    VH2O (mL) Correction


    0.0003
    (mL)
    9.8613
    -0.08
    9.9806
    -0.04
    9.9341
    -0.05
    9.9449
    -0.05
    9.9627
    -0.03
    9.8935
    -0.11
    9.9459
    0.04
    9.8636
    -0.13
    10.0806
    -0.02
    9.9125
    0.00

    50

    60
    Trial A
    Trial B

    Table 2: Calibration of Beaker (30 mL), Erlenmeyer (25 mL) and Volumetric Flask (25 mL)
    Mi (g)
    Mf (g)
    0.0002
    0.0002
    30 mL Beaker (DI H2O temp 21C)
    1
    20.7442
    44.1861
    2
    20.7442
    44.3238
    3
    20.7442
    44.5099
    Trial

    MH2O (g)
    0.0003

    25 mL Erlenmeyer (DI H2O temp 21C)


    1
    25.0680
    50.0462
    2
    25.0680
    50.0949
    3
    25.0680
    50.0577

    25 mL Volumetric Flask (DI H2O temp 21C)


    1
    20.2702
    45.0661
    2
    20.2702
    45.0717
    3
    20.2702
    45.0694

    dH2O (21C)=
    TINV(0.05,2)=
    true volume=

    0.9979955 g/mL
    4.303
    25 mL

    VH2O (mL)
    0.0003

    23.4419
    23.5796
    23.7657
    Average
    Stddev
    % RSD
    95% CI
    % error

    23.4890
    23.6270
    23.8134
    23.6431
    0.1628
    0.6887
    0.4045
    5.4

    24.9782
    25.0269
    24.9897
    Average
    Stddev
    % RSD
    95% CI
    % error

    25.0284
    25.0772
    25.0399
    25.0485
    0.0255
    0.1018
    0.0634
    0.2

    24.7959
    24.8015
    24.7992
    Average
    Stddev
    % RSD
    95% CI
    % error

    24.8457
    24.8513
    24.8490
    24.8487
    0.0028
    0.0114
    0.0070
    0.6

    %RSD = percent relative standa

    RSD = percent relative standard deviation

    You might also like