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    Spinworks 3: Spms - Std1H (Org) Cdcl3 (D:/Spms/Cbc/Teachinglab/Sem2-13) Cm3061-4 41

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    Lieren Chen
    The document contains data from three 1H NMR spectra, including frequency information, number of data points, and peak assignments in ppm. The spectra show peaks between 0-8 ppm, which are typical of proton NMR spectra of organic compounds in deuterated chloroform.

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    Spinworks 3: Spms - Std1H (Org) Cdcl3 (D:/Spms/Cbc/Teachinglab/Sem2-13) Cm3061-4 41

    Uploaded by

    Lieren Chen
    20 views10 pages
    The document contains data from three 1H NMR spectra, including frequency information, number of data points, and peak assignments in ppm. The spectra show peaks between 0-8 ppm, which are typical of proton NMR spectra of organic compounds in deuterated chloroform.

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    Original Title

    3n7

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    The document contains data from three 1H NMR spectra, including frequency information, number of data points, and peak assignments in ppm. The spectra show peaks between 0-8 ppm, which are typical of proton NMR spectra of organic compounds in deuterated chloroform.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    20 views10 pages

    Spinworks 3: Spms - Std1H (Org) Cdcl3 (D:/Spms/Cbc/Teachinglab/Sem2-13) Cm3061-4 41

    Uploaded by

    Lieren Chen
    The document contains data from three 1H NMR spectra, including frequency information, number of data points, and peak assignments in ppm. The spectra show peaks between 0-8 ppm, which are typical of proton NMR spectra of organic compounds in deuterated chloroform.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    of 10

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-4 41

    2.4

    freq. of 0 ppm: 500.130013 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 162.647 ppm/cm: 0.32521

    number of scans: 8

    2.0

    1.6

    1.2

    0.0000
    0.0063

    2.8

    3.123

    3.2

    1.1470
    1.1613
    1.1755

    3.6

    1.282

    4.0

    1.5902

    4.4

    2.055

    4.8

    3.131

    expt: <zg30>

    5.2

    2.1708

    file: ...r\Desktop\expt 3b\Lab 2\2-10\1\fid

    5.6

    2.3514

    6.0

    1.996

    6.4

    4.0502
    4.0569
    4.0644
    4.0712
    4.0786
    4.0854
    4.0928
    4.0997

    6.8

    0.999

    1.740
    3.529

    0.922

    7.2609
    7.3135
    7.3224

    0.915

    7.2

    5.4010
    5.4062
    5.5723

    7.7094

    PPM

    0.8

    0.4

    0.0

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-4 56


    0.0000

    1.0066
    1.0197
    1.2443
    1.2586
    1.2729

    6.8

    6.4

    6.0

    file: ...ktop\expt 3b\Lab 2\2-group19\1\fid

    5.6

    expt: <zg30>

    5.2

    4.8

    4.4

    4.0

    3.6

    3.2

    2.8

    2.4

    freq. of 0 ppm: 500.130014 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 164.586 ppm/cm: 0.32908

    number of scans: 8

    1.5767

    2.0440

    1.994

    7.932

    7.2

    4.1141
    4.1283

    4.9307

    7.0114
    7.0141
    7.0215
    7.2590
    7.2785
    7.2837
    7.2858
    7.2939
    7.3358
    7.3395
    7.3457
    7.3500
    7.5047
    7.5084
    7.5241

    PPM

    2.0

    1.6

    1.2

    0.8

    0.4

    0.0

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-2 54

    4.4

    4.0

    3.6

    3.2

    2.8

    2.4

    freq. of 0 ppm: 500.130012 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 161.872 ppm/cm: 0.32366

    number of scans: 8

    0.0000

    4.8

    2.997

    expt: <zg30>

    5.2

    1.1505
    1.1648
    1.1790

    file: ...op\Studies\CM3061\Lab 2\2-10\1\fid

    5.6

    1.5763
    1.6116

    6.0

    2.944

    6.4

    1.912

    6.8

    2.3575

    4.0539
    4.0607
    4.0681
    4.0750
    4.0823
    4.0893
    4.0966
    4.1035

    0.976

    3.676
    3.549

    7.2

    4.7784

    5.4080

    7.2628
    7.3168
    7.3254

    PPM

    2.0

    1.6

    1.2

    0.8

    0.4

    0.0

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-4 41

    2.10

    file: ...r\Desktop\expt 3b\Lab 2\2-10\1\fid

    2.00
    expt: <zg30>

    1.90

    1.80

    1.70

    1.60

    3.123

    2.20

    1.282

    2.055

    3.131

    2.30

    1.1470
    1.1613
    1.1755

    1.5902

    2.1708

    2.3514

    PPM

    1.50

    1.40

    freq. of 0 ppm: 500.130013 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 27.807 ppm/cm: 0.05560

    number of scans: 8

    1.30

    1.20

    1.10

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-2 54


    1.1505
    1.1648
    1.1790

    1.5763

    1.6116

    2.3575

    2.997

    2.944

    PPM

    2.30

    2.20

    2.10

    file: ...op\Studies\CM3061\Lab 2\2-10\1\fid

    2.00
    expt: <zg30>

    1.90

    1.80

    1.70

    1.60

    1.50

    freq. of 0 ppm: 500.130012 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 27.544 ppm/cm: 0.05507

    number of scans: 8

    1.40

    1.30

    1.20

    1.10

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-4 41


    4.0502
    4.0569
    4.0644
    4.0712
    4.0786
    4.0854
    4.0928
    4.0997

    5.4010
    5.4062

    5.5723

    5.50

    5.40

    1.996

    0.999

    0.922

    PPM

    5.30

    file: ...r\Desktop\expt 3b\Lab 2\2-10\1\fid

    5.20

    5.10

    expt: <zg30>

    5.00

    4.90

    4.80

    4.70

    4.60

    4.50

    freq. of 0 ppm: 500.130013 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 33.538 ppm/cm: 0.06706

    number of scans: 8

    4.40

    4.30

    4.20

    4.10

    4.00

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-2 54


    4.0539
    4.0607
    4.0681
    4.0750
    4.0823
    4.0893
    4.0966
    4.1035

    4.7784

    5.4080

    5.40

    1.912

    0.976

    PPM

    5.30

    5.20

    file: ...op\Studies\CM3061\Lab 2\2-10\1\fid

    5.10

    5.00

    expt: <zg30>

    4.90

    4.80

    4.70

    4.60

    4.50

    4.40

    freq. of 0 ppm: 500.130012 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 30.436 ppm/cm: 0.06086

    number of scans: 8

    4.30

    4.20

    4.10

    4.00

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-4 56


    4.9307

    7.0114
    7.0141
    7.0215

    7.2590
    7.2785
    7.2837
    7.2858
    7.2939
    7.3358
    7.3395
    7.3457
    7.3500

    7.5047
    7.5084
    7.5241

    7.4

    1.994

    7.932

    PPM

    7.2

    7.0

    file: ...ktop\expt 3b\Lab 2\2-group19\1\fid

    6.8
    expt: <zg30>

    6.6

    6.4

    6.2

    6.0

    5.8

    freq. of 0 ppm: 500.130014 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 55.637 ppm/cm: 0.11125

    number of scans: 8

    5.6

    5.4

    5.2

    5.0

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-4 41

    expt: <zg30>

    7.60

    7.50

    7.40

    1.740

    file: ...r\Desktop\expt 3b\Lab 2\2-10\1\fid

    7.70

    7.2609

    7.80

    3.529

    0.915

    7.90

    7.3135
    7.3224

    7.7094

    PPM

    7.30

    freq. of 0 ppm: 500.130013 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 20.355 ppm/cm: 0.04070

    number of scans: 8

    7.20

    7.10

    7.00

    SpinWorks 3: spms_std1H(org) CDCl3 {D:\spms\cbc\TeachingLab\Sem2-13} CM3061-2 54


    7.2628

    7.3168

    7.3254

    3.676

    3.549

    PPM

    7.46 7.44 7.42 7.40 7.38 7.36 7.34 7.32 7.30 7.28 7.26 7.24 7.22 7.20 7.18 7.16 7.14 7.12 7.10 7.08 7.06 7.04

    file: ...op\Studies\CM3061\Lab 2\2-10\1\fid

    expt: <zg30>

    freq. of 0 ppm: 500.130012 MHz

    transmitter freq.: 500.132751 MHz

    processed size: 32768 complex points

    time domain size: 18748 points


    width: 6009.62 Hz = 12.0160 ppm = 0.320547 Hz/pt

    LB: 0.000 GF: 0.0000


    Hz/cm: 9.605 ppm/cm: 0.01921

    number of scans: 8

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