ALI ASGHAR SHABBIR ( H0401007 )

OBJECT:-
Water analysis by chemical treatment.
PROCEDURE:-
Chemical introduce in water:
i). Lime ii). Bleach iii). Soda Ash
iv).FeCl3
First of all filter the re!uired sam"le.
After filteration ta#e $% ml sam"le in Sam"lin& bottle '.
(emainnin& sam"le "asses from column ) %' Activated Carbon Column *Before
utili+e the column re&enerate with ta" water as well as distilled water ,.$ litre).
After full collection from column )%' a&ain ta#e $% ml sam"le in sam"lin& bottle
) %,.
(emainin& sam"le "asses from column )%, *(esins column).*-o the same wor#
li#e the column )%').
After full collection from the "resent column ta#e $% ml sam"le in sam"lin&
bottle ) %3.
OBSERVATIONS:-
SAMPLE LIME:-
pH TDS
Before "assin& throu&h
Activated Carbon
'%.,. %.3%
$% ml sam"le *After "assin&
thou&h Activated Carbon)
/.0$ %.3%
$% ml sam"le
*After "assin& throu&h (esin)
/.00 %.3'
HARDNESS:-
PROCEDURE:-
1a#e ,$ ml sam"le at '%( ,ml Buffer solution *'0.. &m 234Cl '43 ml 2335,$% ml) sha#in& u"
to ' min add few crystal B.6.1*6richrome Blac# indicator) a&ain sha#in& u" to ' min. 1itrate
with %.%' 2 6-1A till u" to "ermanent blue color is "roduced.
3ardness7
WATER ANALYSIS BY CHEMICAL TREATMENT ( EXPERIMENT # 2 )
ALI ASGHAR SHABBIR ( H0401007 )
Befoe !"##$%& '(o)&( A*'$+"'e, C"-o%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % '3.0 '3.0
9olume of %.%' 2 6-1A 7 '3.0 ml
Af'e !"##$%& '(o)&( A*'$+"'e, C"-o%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % $.0 $.0
Vo.)/e of 0001 N EDTA 1 203 /.
Af'e !"##$%& '(o)&( Re#$%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % ,.$ ,.$
Vo.)/e of 0001 N EDTA 1 402 /.
SAMPLE BLEACH:-
pH TDS
Before "assin& throu&h
Activated Carbon
''.3. %./'
$% ml sam"le *After
Activated Carbon)
/./% %.4:
$% ml sam"le
*After (esin)
..%, %.44
HARDNESS:-
Befoe !"##$%& '(o)&( A*'$+"'e, C"-o%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % '%., '%.,
9olume of %.%' 2 6-1A 7 '%., ml
Af'e !"##$%& '(o)&( A*'$+"'e, C"-o%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % :.% :.%
9olume of %.%' 2 6-1A 7 :.% ml
Af'e !"##$%& '(o)&( Re#$%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % ,.$ ,.$
9olume of %.%' 2 6-1A 7 ,.$ ml
WATER ANALYSIS BY CHEMICAL TREATMENT ( EXPERIMENT # 2 )
ALI ASGHAR SHABBIR ( H0401007 )
SAMPLE SOIDIUM CARBONATE (N"
4
CO
5
):-
pH TDS
Before "assin& throu&h
Activated Carbon
''.'% '.3,
$% ml sam"le *After "assin&
thou&h Activated Carbon)
..3, %.$$
$% ml sam"le
*After "assin& throu&h (esin)
..34 %.$$
HARDNESS:-
PROCEDURE:-
1a#e ,$ ml sam"le at '%( ,ml Buffer solution *'0.. &m 234Cl '43 ml 2335,$% ml) sha#in& u"
to ' min add few crystal B.6.1 *6richrome Blac# indicator) a&ain sha#in& u" to ' min. 1itrate
with %.%' 2 6-1A till u" to "ermanent blue color is "roduced.
3ardness7
Befoe !"##$%& '(o)&( A*'$+"'e, C"-o%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % 4.. 4..
9olume of %.%' 2 6-1A 7 4.. ml
Af'e !"##$%& '(o)&( A*'$+"'e, C"-o%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % $.4 $.4
9olume of %.%' 2 6-1A 7 $.4 ml
Af'e !"##$%& '(o)&( Re#$%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % ,.' ,.'
9olume of %.%' 2 6-1A 7 ,.' ml
SAMPLE 6ERRIC CHLORIDE (6eC.
5
):-
pH TDS
Before "assin& throu&h
Activated Carbon
/.:. %.03
$% ml sam"le *After
Activated Carbon)
..%0 %.44
$% ml sam"le
*After (esin)
..'' %.44
WATER ANALYSIS BY CHEMICAL TREATMENT ( EXPERIMENT # 2 )
ALI ASGHAR SHABBIR ( H0401007 )
HARDNESS:-
Befoe !"##$%& '(o)&( "*'$+"'e, C"-o%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % '% '%
9olume of %.%' 2 6-1A 7 '% ml
Af'e !"##$%& '(o)&( A*'$+"'e, C"-o%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % :.0 :.0
9olume of %.%' 2 6-1A 7 :.% ml
Af'e !"##$%& '(o)&( Re#$%
S.2o 8nitial (eadin& *ml) Final (eadin& *ml) -ifference *ml)
'. % ..% ..%
9olume of %.%' 2 6-1A 7 ..% ml
CALCULATION:-
HARDNESS:-
3ardness7
6OR SAMPLE LIME
6OR SAMPLE (Befoe !"##$%& '(o)&( A*'$+"'e, C"-o%):-
Concordant readin& of %.%' 2 6-1A 7 '3.0 ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 5440 N
6OR SAMPLE (Af'e !"##$%& '(o)&( A*'$+"'e, C"-o%):-
Concordant readin& of %.%' 2 6-1A 7 $.0 ml
WATER ANALYSIS BY CHEMICAL TREATMENT ( EXPERIMENT # 2 )
ALI ASGHAR SHABBIR ( H0401007 )
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 2240 N
6OR SAMPLE (Af'e !"##$%& '(o)&( Re#$%):-
Concordant readin& of %.%' 2 6-1A 7 ,.$ ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 1000 N
6OR SAMPLE BLEACH
6OR SAMPLE (Befoe !"##$%& '(o)&( A*'$+"'e, C"-o%):-
Concordant readin& of %.%' 2 6-1A 7 '%., ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 4080 N
6OR SAMPLE (Af'e !"##$%& '(o)&( A*'$+"'e, C"-o%):-
Concordant readin& of %.%' 2 6-1A 7 :.% ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 2800 N
6OR SAMPLE (Af'e !"##$%& '(o)&( Re#$%):-
Concordant readin& of %.%' 2 6-1A 7 ,.$ ml
WATER ANALYSIS BY CHEMICAL TREATMENT ( EXPERIMENT # 2 )
ALI ASGHAR SHABBIR ( H0401007 )
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 1000 N
6OR SOIDIUM CARBONATE (N"
4
CO
5
):-
6OR SAMPLE (Befoe !"##$%& '(o)&( A*'$+"'e, C"-o%):-
Concordant readin& of %.%' 2 6-1A 7 4.. ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 1960 N
6OR SAMPLE (Af'e !"##$%& '(o)&( A*'$+"'e, C"-o%):-
Concordant readin& of %.%' 2 6-1A 7 $.4 ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 2160 N

6OR SAMPLE (Af'e !"##$%& '(o)&( Re#$%):-
Concordant readin& of %.%' 2 6-1A 7 ,.' ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 840 N
WATER ANALYSIS BY CHEMICAL TREATMENT ( EXPERIMENT # 2 )
ALI ASGHAR SHABBIR ( H0401007 )
6OR SAMPLE 6ERRIC CHLORIDE (6eC.
5
):-
6OR SAMPLE (Befoe !"##$%& '(o)&( A*'$+"'e, C"-o%):-
Concordant readin& of %.%' 2 6-1A 7 '% ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 4000 N
6OR SAMPLE (Af'e !"##$%& '(o)&( A*'$+"'e, C"-o%):-
Concordant readin& of %.%' 2 6-1A 7 :.0 ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 3040 N
6OR SAMPLE (Af'e !"##$%& '(o)&( Re#$%):-
Concordant readin& of %.%' 2 6-1A 7 ..% ml
9olume of sam"le 7 ,$ ml
3ardness7
Hardness of sample A= 3600 N
RESULT:-
6OR SAMPLE LIME:-
pH TDS Hardness (N)
Before Activated
Carbon
'%.,. %.3% $44% 2
After "assin& throu&h
Activated Carbon
/.0$ %.3% ,,4% 2
After "assin& throu&h /.00 %.3' '%%% 2
WATER ANALYSIS BY CHEMICAL TREATMENT ( EXPERIMENT # 2 )
ALI ASGHAR SHABBIR ( H0401007 )
(esins
6OR SAMPLE BLEACH:-
pH TDS Hardness (N)
Before Activated
Carbon
''.3. %./' 4%/% 2
After "assin& throu&h
Activated Carbon
/./% %.4: ,/%% 2
After "assin& throu&h
(esins
..%, %.44 '%%% 2
6OR SAMPLE SOIDIUM CARBONATE (N"
4
CO
5
):-
pH TDS Hardness (N)
Before Activated
Carbon
''.'% '.3, '.0% 2
After "assin& throu&h
Activated Carbon
..3, %.$$ ,'0% 2
After "assin& throu&h
(esins
..3, %.$$ /4% 2
SAMPLE 6ERRIC CHLORIDE (6eC.
5
):-
pH TDS Hardness (N)
Before Activated
Carbon
/.:. %.03 4%%% 2
After "assin& throu&h
Activated Carbon
..%0 %.44 3%4% 2
After "assin& throu&h
(esins
..'' %.44 30%% 2
WATER ANALYSIS BY CHEMICAL TREATMENT ( EXPERIMENT # 2 )