Without Spillage

P
F

1157.4074
1326.2374

Component
MEK
2 Butanol

xF
0.8727
0.0998
Total

Mass (kg)
1157.4074
132.3585
1289.7659

% mass
89.74
10.26
100.00

Moles
16.08
1.79
17.8637

% mol
89.99
10.01
100.00

Component
MEK
2-Butanol

xF
0.8718
0.0001
Total

Mass
1156.2500
0.1324
1156.3823

% mass
99.90
0.10
99.90

Moles
16.06
0.00
16.06

% mol
99.99
0.01
100.00

For Recycle @ Reactor

Component
2-Butanol
MEK

xF
0.0997
0.0009
Total

Mass
132.2261
1.1574
133.3835

% mass
99.90
0.10
99.90

Moles
1.7868
0.0161
1.8029

% mol
99.11
0.89
100.00

Component
MEK
2-Butanol
TCE

xF
0.1372
0.00784
0.5412
Total

Mass (kg)
181.9598
10.3977
717.7597
910.1172

%
19.99
1.14
78.86
100.00

Moles
2.53
0.14
5.46
8.1305

%mol
31.08
1.73
67.19
100.00

Component
MEK
2-Butanol

xF
0.1372
0.00784
Total

Mass
181.9598
10.3977
192.3575

%
94.59
5.41
100.00

2.53
0.14
2.6677

94.73
5.27
100.00

Component
TCE

xF
0.5412
Total

Mass
717.7597
717.7597

%
100.00
100.00

5.46
5.4628

100.00
100.00

Component

xF

Mass

% Mass

Moles

% Mol

Distillation Column
F

Solvent Recovery
Column
F

Extraction
F

MEK
2-Butanol
EtOH

0.1437
0.00784
1.2859
Total

190.5803
10.3977
1705.4087
1906.3867

10.00
0.55
89.46
100.00

2.65
0.14
37.02
39.8052

6.65
0.35
93.00
100.00

Component
MEK
EtOH

xF
0.006462
1.2859
Total

Mass
8.5701
1705.4087
1713.9788

% Mass
0.50
99.50
100.00

Moles
0.12
37.02
37.1368

% Mol
0.32
99.68
100.00

Component
MEK
2-Butanol
TCE

xF
0.1372
0.00784
0.5412
Total

Mass
181.9598
10.3977
717.7597
910.1172

% Mass
19.99
1.14
78.86
100.00

Moles
2.53
0.14
5.46
8.1305

% Mol
31.08
1.73
67.19
100.00

Component
TCE

xF
0.5412
Total

Mass
717.7597
717.7597

% Mass
100.00
100.00

Moles
5.46
5.4628

% Mol
100.00
100.00

Component
MEK
2-Butanol
H2

xF
0.1401
0.008
0.0243
Total

Mass
185.8059
10.6099
32.2276
228.6433

% Mass
81.26
4.64
14.10
100.00

Moles
2.58
0.14
16.11
18.8378

% Mol
13.70
0.76
85.54
100.00

Component
MEK
EtOH

xF
0.006462
1.2859
Total

Mass
8.5701
1705.4087
1713.9788

% Mass
0.50
99.50
100.00

Moles
0.12
37.02
37.1368

% Mol
0.32
99.68
100.00

Component
MEK
2-Butanol
H2

xF
0.002802
0.00016
0.0243
Total

Mass
3.7161
0.2122
32.2276
36.1559

% Mass
10.28
0.59
89.14
100.00

Moles
0.05
0.00
16.11
16.1683

% Mol
0.32
0.02
99.66
100.00

Component
MEK
2-Butanol
EtOH

xF
0.1437
0.00784
1.2859

Mass
190.5803
10.3977
1705.4087

% Mass
10.00
0.55
89.46

Moles
2.65
0.14
37.02

% Mol
6.65
0.35
93.00

Absorption
Non Condensate
F

COOLER CONDENSER
F

Condensate
V

Non Condensate
L

Total

1906.3867

100.00

39.8052

100.00

Component
MEK
2-Butanol
H2

xF
0.8757
0.1
0.0243
Total

Mass
1161.3861
132.6237
32.2276
1326.2374

% Mass
87.57
10.00
2.43
100.00

Moles
16.13
1.79
16.11
34.0364

% Mol
47.39
5.27
47.34
100.00

Component
MEK
2-Butanol
H2

xF
0.7356
0.092
Total

Mass
975.5802
122.0138
0.0000
1097.5941

% Mass
88.88
11.12
0.00
100.00

Moles
13.55
1.65
0.00
15.1986

% Mol
89.15
10.85
0.00
100.00

xF
0.1401
0.008
0.0243
Total

Mass
185.8059
10.6099
32.2276
228.6433

% Mass
81.26
4.64
14.10
100.00

Moles
2.58
0.14
16.11
18.8378

% Mol
13.70
0.76
85.54
100.00

Moles
16.13
1.79
16.11
34.0364

%
Moles
47.39
5.27
47.34
100.00

Component
MEK
2-Butanol
H2

Reactor
Out

Component
MEK
2-Butanol
H2

xF
0.8757
0.1
0.0243
Total

With .05% Spillage

P
1157.4074
F
1332.8686

Mass
1161.3861
132.6237
32.2276
1326.2374

% Mass
87.57
10.00
2.43
100.00

For Recycle @
Reactor

Distillation Column
Component
xF
MEK
0.8727
2 Butanol
0.0998
Total

Mass (kg)
1163.1944
133.0203
1296.2147

% mass
89.74
10.26
100.00

Moles
16.16
1.80
17.9530

% mol
89.99
10.01
100.00

Component
MEK
2-Butanol

xF
0.8718
0.0001
Total

Mass
1162.0312
0.1330
1162.1642

% mass
99.90
0.10
100.00

Moles
16.14
0.00
16.14

% mol
99.99
0.01
100.00

Component
2-Butanol
MEK

xF
0.0997
0.0009
Total

Mass
132.8873
1.1632
134.0505

% mass
99.90
0.10
100.00

Moles
1.7958
0.0162
1.8119

% mol
99.11
0.89
100.00

Mass
182.8696
10.4497
721.3485
914.6677

% Mass
19.99
1.14
78.86
100.00

Moles
2.54
0.14
5.49
8.1712

% Moles
31.08
1.73
67.19
100.00

Solvent Recovery Column

Component
xF
MEK
0.1372
2-Butanol
0.00784
TCE
0.5412
Total

Component
MEK
2-Butanol

xF
0.1372
0.00784
Total

Mass
182.8696
10.4497
193.3193

% Mass
94.59
5.41
100.00

Moles
2.54
0.14
2.6811

% Moles
94.73
5.27
100.00

Component
TCE

xF
0.5412
Total

Mass
721.3485
721.3485

% Mass
100.00
100.00

Moles
5.49
5.4901

% Moles
100.00
100.00

Extraction
Component
xF
MEK
0.1437
2-Butanol
0.00784
EtOH
1.2859
Total

Mass
191.5332
10.4497
1713.9357
1915.9186

% Mass
10.00
0.55
89.46
100.00

Moles
2.66
0.14
37.20
40.0043

% Moles
6.65
0.35
93.00
100.00

Component
MEK
EtOH

xF
0.006462
1.2859
Total

Mass
8.6130
1713.9357
1722.5487

% Mass
0.50
99.50
100.00

Moles
0.12
37.20
37.3225

% Moles
0.32
99.68
100.00

Component
MEK
2-Butanol
TCE

xF
0.1372
0.00784
0.5412
Total

Mass
182.8696
10.4497
721.3485
914.6677

% Mass
19.99
1.14
78.86
100.00

Moles
2.54
0.14
5.49
8.1712

% Moles
31.08
1.73
67.19
100.00

Component
TCE

xF
0.5412
Total

Mass
721.3485
721.3485

% Mass
100.00
100.00

Moles
5.49
5.4901

% Moles
100.00
100.00

Absorption
Component
xF
MEK
0.1401
2-Butanol
0.008
H2
0.0243
Total

Mass
186.7349
10.6629
32.3887
229.7865

% Mass
81.26
4.64
14.10
100.00

Moles
2.59
0.14
16.19
18.9320

% Moles
13.70
0.76
85.54
100.00

Non Condensate
F

Component
MEK
EtOH

xF
0.006462
1.2859
Total

Mass
8.6130
1713.9357
1722.5487

% Mass
0.50
99.50
100.00

Moles
0.12
37.20
37.3225

% Moles
0.32
99.68
100.00

Component
MEK
2-Butanol
H2

xF
0.002802
0.00016
0.0243
Total

Mass
3.7347
0.2133
32.3887
36.3367

% Mass
10.28
0.59
89.14
100.00

Moles
0.05
0.00
16.19
16.2491

% Moles
0.32
0.02
99.66
100.00

Component
MEK
2-Butanol
EtOH

xF
0.1437
0.00784
1.2859
Total

Mass
191.5332
10.4497
1713.9357
1915.9186

% Mass
10.00
0.55
89.46
100.00

Moles
2.66
0.14
37.20
40.0043

% Moles
6.65
0.35
93.00
100.00

COOLER CONDENSER

Component
MEK
2-Butanol
H2

xF
0.8756
0.1
0.0243
Total

Mass
1167.0597
133.2869
32.3887
1332.7353

% Mass
87.57
10.00
2.43
100.00

Moles
16.21
1.80
16.19
34.2047

% Mol
47.39
5.27
47.35
100.00

Condensate
V

Component
MEK
2-Butanol
H2

xF
0.7355
0.092
Total

Mass
980.3248
122.6239
0.0000
1102.9488

% Mass
88.88
11.12
0.00
100.00

Moles
13.62
1.66
0.00
15.2727

% Mol
89.15
10.85
0.00
100.00

xF
0.1401
0.008
0.0243
Total

Mass
186.7349
10.6629
32.3887
229.7865

% Mass
81.26
4.64
14.10
100.00

Moles
2.59
0.14
16.19
18.9320

% Mol
13.70
0.76
85.54
100.00

Reactor
Component
xF
MEK
0.8757
2-Butanol
0.1
H2
0.0243
Total

Mass
1167.1930
133.2869
32.3887
1332.8686

% Mass
87.57
10.00
2.43
100.00

Moles
16.21
1.80
16.19
34.2065

% Mol
47.39
5.27
47.34
100.00

Non Condensate
L

Out

Component
MEK
2-Butanol
H2