Nephelin A09-1819final

Report: A09-1819 Final Report
Report Date: 15/05/2009 Activation Laboratories
Analyte Symbol B Mass Cl Mass CO2 F H20+ H20- SiO2 Al2O3 Fe2O3(T) MnO MgO CaO Na2O K2O TiO2 P2O5
Unit Symbol ppm g % g % % % % % % % % % % % % % %
Detection Limit 2 0.01 0.01 0.01 0.1 0.1 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01
Analysis Method PGNAA PGNAA INAA INAA COUL FUS-ISE GRAV GRAV FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP
#1 WANNIGRAT/VS (CH) <2 1.02 < 0.01 1.02 < 0.01 2.7 < 0.1 62.14 14.2 2.64 0.025 1.96 0.1 1.87 0.12 0.043 0.18
#2 SEILAND (N) 0.1 1.03 0.05 < 0.01 1 < 0.1 43.36 33.05 0.37 0.004 0.03 0.8 14.62 5.06 0.008 < 0.01
#3 TANZANIA 0.02 1.05 < 0.01 < 0.1 < 0.1 36.64 61.42 1.37 0.197 0.04 0.1 0.03 0.02 0.182 0.11
Page 1 of 14
Analyte Symbol LOI Total Sc Be V Cr Co Ni Cu Zn Ga Ge As Rb Sr Y Zr
Unit Symbol % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm
Detection Limit 0.01 1 1 5 20 1 20 10 30 1 1 5 2 2 2 4
Analysis Method FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-ICP FUS-ICP
#1 WANNIGRAT/VS (CH) 83.28 7 45230 68 40 <1 < 20 260 180 9 <1 <5 29 8 <2 20
#2 SEILAND (N) 1.47 98.79 <1 19 <5 60 4 < 20 20 < 30 25 <1 11 70 183 <2 23
#3 TANZANIA 0.4 100.5 <1 26 <5 70 <1 < 20 < 10 < 30 15 2 15 <2 16 14 438
Page 2 of 14
Analyte Symbol Nb Mo Ag In Sn Sb Cs Ba La Bi Ce Pr Nd Sm Eu Gd Tb
Unit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm
Detection Limit 1 2 0.5 0.2 1 0.5 0.5 3 0.1 0.4 0.1 0.05 0.1 0.1 0.05 0.1 0.1
Analysis Method FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS
#1 WANNIGRAT/VS (CH) 2 2 < 0.5 < 0.2 <1 < 0.5 75.4 42 2.3 < 0.4 3.3 0.41 1.4 0.2 0.05 0.2 < 0.1
#2 SEILAND (N) <1 <2 < 0.5 < 0.2 <1 1.8 < 0.5 25 0.8 < 0.4 0.5 0.06 0.2 < 0.1 < 0.05 < 0.1 < 0.1
#3 TANZANIA 6 <2 < 0.5 < 0.2 <1 0.7 < 0.5 35 34.3 0.5 33.1 7.26 22.5 3.8 0.79 3.4 0.5
Page 3 of 14
Analyte Symbol Dy Ho Er Tm Yb Lu Hf Ta W Tl Pb Th U Li
Unit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm
Detection Limit 0.1 0.1 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1 1
Analysis Method FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS TD-ICP
#1 WANNIGRAT/VS (CH) 0.2 < 0.1 < 0.1 < 0.05 0.1 < 0.04 0.7 0.1 3 0.3 <5 1 0.4 282
#2 SEILAND (N) < 0.1 < 0.1 < 0.1 < 0.05 < 0.1 < 0.04 0.4 < 0.1 <1 0.4 5 0.1 0.2
#3 TANZANIA 2.2 0.4 1.4 0.2 1.2 0.2 11.2 1.2 <1 < 0.1 <5 5.9 0.6
Page 4 of 14
Activation Laboratories
Analyte Symbol B Cl CO2 F H20+ H20- SiO2 Al2O3 Fe2O3(T) MnO MgO CaO Na2O K2O TiO2 P2O5 Sc Be
Unit Symbol ppm % % % % % % % % % % % % % % % ppm ppm
Detection Limit 2 0.01 0.01 0.01 0.1 0.1 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 1 1
Analysis Method PGNAA INAA COUL FUS-ISE GRAV GRAV FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP
GXR-1 Meas
GXR-1 Cert
GXR-1 Meas
GXR-1 Cert
WMG-1 Meas
WMG-1 Cert
NIST 694 Meas 3.17 11.25 1.9 0.73 0.011 0.33 43.44 0.87 0.54 0.112 30.2
NIST 694 Cert 3.2 11.2 1.8 0.79 0.0116 0.33 43.6 0.86 0.51 0.11 30.2
DNC-1 Meas < 0.01 47.34 18.56 9.92 0.144 10.21 11.44 1.92 0.22 0.488 0.08 31 <1
DNC-1 Cert 0.0066 47 18.3 9.93 0.149 10.1 11.3 1.87 0.234 0.48 0.09 31 1
DNC-1 Meas < 0.01
DNC-1 Cert 0.0066
GBW 07113 Meas 0.13 72.7 12.84 3.07 0.142 0.15 0.59 2.45 5.44 0.286 0.05 5 4
GBW 07113 Cert 0.13 72.8 13 3.21 0.14 0.16 0.59 2.57 5.43 0.3 0.05 5 4
GBW 07113 Meas 0.13
GBW 07113 Cert 0.13
GXR-4 Meas
GXR-4 Cert
GXR-4 Meas
GXR-4 Cert
GXR-2 Meas
GXR-2 Cert
GXR-2 Meas
GXR-2 Cert
SDC-1 Meas
SDC-1 Cert
SDC-1 Meas
SDC-1 Cert
SCO-1 Meas
SCO-1 Cert
SCO-1 Meas
SCO-1 Cert
GXR-6 Meas
GXR-6 Cert
GXR-6 Meas
GXR-6 Cert
LKSD-3 Meas
LKSD-3 Cert
MAG-1 (Depleted) Meas
MAG-1 (Depleted) Cert
NIST 1633b Meas 50.17 29.03 11.86 0.019 0.79 2.16 0.29 2.48 1.327 0.59 41
NIST 1633b Cert 49.2 28.4 11.1 0.02 0.8 2.11 0.27 2.35 1.32 0.53 41
NIST 1633b Meas 48.49 28.01 11.02 0.026 0.77 2.14 0.27 2.28 1.276 0.53 39
NIST 1633b Cert 49.2 28.4 11.1 0.02 0.8 2.11 0.27 2.35 1.32 0.53 41
SY-2 Meas 90
SY-2 Cert 88
Page 5 of 14
Detection Limit 2 0.01 0.01 0.01 0.1 0.1 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 1 1
GXR-1 Meas
SY-3 Meas 105
SY-3 Cert 107
DR-N Meas 0.06
DR-N Cert 0.05
DR-N Meas 0.06
DR-N Cert 0.05
DR-N Meas 0.06
DR-N Cert 0.05
UB-N Meas 0.01
UB-N Cert 0.0095
NIST 1632c Meas 0.11
NIST 1632c Cert 0.11
W-2a Meas 0.02 52.33 15.35 10.68 0.163 6.23 10.75 2.21 0.63 1.083 0.14 35 1
W-2a Cert 0.0205 52.4 15.4 10.7 0.163 6.37 10.9 2.14 0.626 1.06 0.13 36 1.3
W-2a Meas 0.02
W-2a Cert 0.0205
NIST 696 Meas 3.79 53.66 8.51 0.004 0.02 0.02 < 0.01 2.603 0.05
NIST 696 Cert 3.79 54.5 8.7 0.004 0.012 0.018 0.009 2.64 0.05
SY-4 Meas 49.13 20.3 6.17 0.103 0.51 7.9 7 1.7 0.283 0.14 1 3
SY-4 Cert 49.9 20.69 6.21 0.108 0.54 8.05 7.1 1.66 0.287 0.131 1.1 2.6
CTA-AC-1 Meas
CTA-AC-1 Cert
BIR-1a Meas 48.78 15.95 11.5 0.174 9.74 13.47 1.84 < 0.01 0.99 0.03 44 <1
BIR-1a Cert 47.8 15.4 11.3 0.171 9.68 13.2 1.75 0.03 0.96 0.05 44 0.58
Calcium Carbonate Meas 44.3
Calcium Carbonate Cert 44.05
JLk-1 Meas 9.3 4
JLk-1 Cert 6.372 3.701
JSd-1 Meas 3.1 0.8
JSd-1 Cert 2.301 0.836
JSl-2 Meas 4.5 0.3
JSl-2 Cert 4.158 0.362
SGR-1b Meas 0.2
SGR-1b Cert 0
SGR-1b Meas 0.2
SGR-1b Cert 0
#1 WANNIGRAT/VS (CH) Orig < 0.01 62.05 14.2 2.64 0.026 1.96 0.11 1.87 0.11 0.043 0.18 7 45200
#1 WANNIGRAT/VS (CH) Dup < 0.01 62.23 14.19 2.64 0.024 1.96 0.08 1.87 0.13 0.043 0.17 7 45260
Method Blank Method Blank
Method Blank Method Blank < 0.01
Page 6 of 14
Detection Limit 2 0.01 0.01 0.01 0.1 0.1 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 1 1
GXR-1 Meas
Page 7 of 14
Analyte Symbol V Cr Co Ni Cu Zn Ga Ge As Rb Sr Y Zr Nb Mo Ag In
Detection Limit 5 20 1 20 10 30 1 1 5 2 2 2 4 1 2 0.5 0.2
Analysis Method FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS
GXR-1 Meas < 20 5 40 1110 760 16 428 3 1 18 35.7 0.8
GXR-1 Cert 12 8.2 41 1110 760 13.8 427 14 0.8 18 31 0.77
GXR-1 Meas
GXR-1 Cert
WMG-1 Meas 780 201 2500 5820 120 10 8 4 <2 1.9
WMG-1 Cert 770 200 2700 5900 110 10.3 7 6 1.4 2.7
NIST 694 Meas 1679
NIST 694 Cert 1740
DNC-1 Meas 155 280 57 250 100 80 14 1 <5 4 145 16 37 1 <2 < 0.5
DNC-1 Cert 148 285 54.7 247 96 66 15 1.3 0.2 4.5 145 18 41 3 0.7 0.027
DNC-1 Meas
DNC-1 Cert
GBW 07113 Meas 7 41 47 429
GBW 07113 Cert 5 43 43 403
GBW 07113 Meas
GBW 07113 Cert
GXR-4 Meas
GXR-4 Cert
GXR-4 Meas
GXR-4 Cert
GXR-2 Meas 30 6 < 20 70 390 36 18 81 10 <2 8.6 < 0.2
GXR-2 Cert 36 8.6 21 76 530 37 25 78 11 2.1 17 0.252
GXR-2 Meas
GXR-2 Cert
SDC-1 Meas
SDC-1 Cert
SDC-1 Meas
SDC-1 Cert
SCO-1 Meas
SCO-1 Cert
SCO-1 Meas
SCO-1 Cert
GXR-6 Meas
GXR-6 Cert
GXR-6 Meas
GXR-6 Cert
LKSD-3 Meas 80 29 50 30 140 22 75 8 <2 1.5
LKSD-3 Cert 87 30 47 35 152 27 78 8 2 2.7
MAG-1 (Depleted) Meas 100 20 50 30 130 22 <5 149 13 <2 < 0.5 < 0.2
MAG-1 (Depleted) Cert 97 20.4 53 30 130 20.4 9.2 149 12 1.6 0.08 0.18
NIST 1633b Meas 308 1070
NIST 1633b Cert 296 1040
NIST 1633b Meas 300 1031
NIST 1633b Cert 296 1040
SY-2 Meas
SY-2 Cert
Page 8 of 14
Analyte Symbol V Cr Co Ni Cu Zn Ga Ge As Rb Sr Y Zr Nb Mo Ag In
Detection Limit 5 20 1 20 10 30 1 1 5 2 2 2 4 1 2 0.5 0.2
Analysis Method FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS
GXR-1 Meas < 20 5 40 1110 760 16 428 3 1 18 35.7 0.8
SY-3 Meas
SY-3 Cert
DR-N Meas
DR-N Cert
DR-N Meas
DR-N Cert
DR-N Meas
DR-N Cert
UB-N Meas
UB-N Cert
NIST 1632c Meas
NIST 1632c Cert
W-2a Meas 276 90 43 70 110 90 17 2 <5 20 199 20 87 6 <2 < 0.5
W-2a Cert 262 92 43 70 110 80 17 1 1.2 21 190 24 94 7.9 0.6 0.046
W-2a Meas
W-2a Cert
NIST 696 Meas 400 1018
NIST 696 Cert 403 1040
SY-4 Meas 8 1195 119 522
SY-4 Cert 8 1191 119 517
CTA-AC-1 Meas <1 50 40
CTA-AC-1 Cert 2.72 54 38
BIR-1a Meas 344 390 51 160 120 90 15 1 <5 <2 112 14 16 <1 <2 < 0.5
BIR-1a Cert 313 382 51.4 166 126 71 16 1.5 0.44 0.25 108 16 16 0.6 0.5 0.036
Calcium Carbonate Meas
Calcium Carbonate Cert
JLk-1 Meas
JLk-1 Cert
JSd-1 Meas
JSd-1 Cert
JSl-2 Meas
JSl-2 Cert
SGR-1b Meas
SGR-1b Cert
SGR-1b Meas
SGR-1b Cert
#1 WANNIGRAT/VS (CH) Orig 68 50 <1 < 20 260 180 9 <1 <5 28 8 <2 24 2 2 < 0.5 < 0.2
#1 WANNIGRAT/VS (CH) Dup 68 40 <1 < 20 250 180 9 <1 <5 30 8 <2 16 1 2 < 0.5 < 0.2
Page 9 of 14
Analyte Symbol Sn Sb Cs Ba La Bi Ce Pr Nd Sm Eu Gd Tb Dy Ho Er Tm Yb
Unit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm
Detection Limit 1 0.5 0.5 3 0.1 0.4 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05 0.1
Analysis Method FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS
GXR-1 Meas 26 122 2.9 8 1380 15.7 8.4 2.9 0.65 3.9 0.8 4.8 0.41 2.3
GXR-1 Cert 54 122 3 7.5 1380 17 18 2.7 0.69 4.2 0.83 4.3 0.43 1.9
GXR-1 Meas
GXR-1 Cert
WMG-1 Meas <1 6.5 < 0.5 8.4 17.5 9.3 2.3 0.76 0.4 2.4 0.5 0.21 1.3
WMG-1 Cert 2.2 1.8 0.48 8.2 16 9 2.3 0.82 0.3 2.8 0.5 0.2 1.3
NIST 694 Meas
NIST 694 Cert
DNC-1 Meas 2.8 < 0.5 106 3.8 < 0.4 8.5 1.2 4.8 1.4 0.61 2 0.4 2.8 0.6 2 0.55 2
DNC-1 Cert 0.96 0.34 114 3.8 0.02 10.6 1.3 4.9 1.38 0.59 2 0.41 2.7 0.62 2 0.38 2.01
DNC-1 Meas
DNC-1 Cert
GBW 07113 Meas 502
GBW 07113 Cert 506
GBW 07113 Meas
GBW 07113 Cert
GXR-4 Meas
GXR-4 Cert
GXR-4 Meas
GXR-4 Cert
GXR-2 Meas <1 17.2 5.3 26.2 < 0.4 53.4 19.8 3.7 0.77 3.1 0.5 2.9 0.29 1.8
GXR-2 Cert 1.7 49 5.2 25.6 0.69 51.4 19 3.5 0.81 3.3 0.48 3.3 0.3 2.04
GXR-2 Meas
GXR-2 Cert
SDC-1 Meas
SDC-1 Cert
SDC-1 Meas
SDC-1 Cert
SCO-1 Meas
SCO-1 Cert
SCO-1 Meas
SCO-1 Cert
GXR-6 Meas
GXR-6 Cert
GXR-6 Meas
GXR-6 Cert
LKSD-3 Meas <1 3.3 2.3 48.1 90.4 42.1 7.8 1.47 0.9 4.8 2.8
LKSD-3 Cert 3 1.3 2.3 52 90 44 8 1.5 1 4.9 2.7
MAG-1 (Depleted) Meas 5 1.3 8.6 43.3 < 0.4 88 11.1 36.7 7.2 1.5 5.9 1 5.1 1 3 0.44 2.7
MAG-1 (Depleted) Cert 3.6 0.96 8.6 43 0.34 88 9.3 38 7.5 1.6 5.8 0.96 5.2 1.02 3 0.43 2.6
NIST 1633b Meas 754
NIST 1633b Cert 709
NIST 1633b Meas 712
NIST 1633b Cert 709
SY-2 Meas
SY-2 Cert
Page 10 of 14
Analyte Symbol Sn Sb Cs Ba La Bi Ce Pr Nd Sm Eu Gd Tb Dy Ho Er Tm Yb
Unit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm
Detection Limit 1 0.5 0.5 3 0.1 0.4 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05 0.1
Analysis Method FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS
GXR-1 Meas 26 122 2.9 8 1380 15.7 8.4 2.9 0.65 3.9 0.8 4.8 0.41 2.3
SY-3 Meas
SY-3 Cert
DR-N Meas
DR-N Cert
DR-N Meas
DR-N Cert
DR-N Meas
DR-N Cert
UB-N Meas
UB-N Cert
NIST 1632c Meas
NIST 1632c Cert
W-2a Meas 6.8 0.9 177 11.2 < 0.4 24.3 12.8 3.3 1.14 0.7 3.9 0.8 2.4 0.35 2.1
W-2a Cert 0.79 0.99 182 10 0.03 23 13 3.3 1 0.63 3.6 0.76 2.5 0.38 2.1
W-2a Meas
W-2a Cert
NIST 696 Meas
NIST 696 Cert
SY-4 Meas 345
SY-4 Cert 340
CTA-AC-1 Meas > 2000 > 3000 1090 162 46.7 124 15.9 11.3
CTA-AC-1 Cert 2176 3326 1087 162 46.7 124 13.9 11.4
BIR-1a Meas <1 3.3 < 0.5 16 0.6 < 0.4 2.1 0.41 2.3 1.1 0.54 1.7 0.4 2.5 0.6 1.8 0.28 1.7
BIR-1a Cert 0.65 0.58 0.005 7 0.62 0.02 1.95 0.38 2.5 1.1 0.54 1.85 0.36 2.5 0.57 1.7 0.26 1.65
JLk-1 Meas
JLk-1 Cert
JSd-1 Meas
JSd-1 Cert
JSl-2 Meas
JSl-2 Cert
SGR-1b Meas
SGR-1b Cert
SGR-1b Meas
SGR-1b Cert
#1 WANNIGRAT/VS (CH) Orig <1 < 0.5 74.2 43 2.4 < 0.4 3.4 0.42 1.4 0.3 0.05 0.2 < 0.1 0.2 < 0.1 0.1 < 0.05 0.1
#1 WANNIGRAT/VS (CH) Dup <1 1.6 76.7 42 2.2 0.5 3.2 0.4 1.3 0.2 0.05 0.2 < 0.1 0.2 < 0.1 < 0.1 < 0.05 0.1
Page 11 of 14
Analyte Symbol Lu Hf Ta W Tl Pb Th U Li Total

Unit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm %
Detection Limit 0.04 0.2 0.1 1 0.1 5 0.1 0.1 1 0.01
Analysis Method FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS TD-ICP FUS-ICP
GXR-1 Meas 0.31 0.9 < 0.1 164 0.6 731 2.6 34.8 15
GXR-1 Cert 0.28 0.96 0.175 164 0.39 730 2.44 34.9 8.2
GXR-1 Meas 14
GXR-1 Cert 8.2
WMG-1 Meas 0.19 1.5 0.3 <1 20 1.2 0.7
WMG-1 Cert 0.21 1.3 0.5 1.3 15 1.1 0.65
NIST 694 Meas
NIST 694 Cert
DNC-1 Meas 0.3 1 0.1 <1 < 0.1 6 0.2 < 0.1 5
DNC-1 Cert 0.32 1.01 0.098 0.2 0.026 6.3 0.2 0.1 5.2
DNC-1 Meas 4
DNC-1 Cert 5.2
GBW 07113 Meas
GBW 07113 Cert
GBW 07113 Meas
GBW 07113 Cert
GXR-4 Meas 10
GXR-4 Cert 11.1
GXR-4 Meas 9
GXR-4 Cert 11.1
GXR-2 Meas 0.27 7.2 0.8 1 0.9 190 8.8 3.1 58
GXR-2 Cert 0.27 8.3 0.9 1.9 1.03 690 8.8 2.9 54
GXR-2 Meas 60
GXR-2 Cert 54
SDC-1 Meas 34
SDC-1 Cert 34
SDC-1 Meas 34
SDC-1 Cert 34
SCO-1 Meas 45
SCO-1 Cert 45
SCO-1 Meas 41
SCO-1 Cert 45
GXR-6 Meas 33
GXR-6 Cert 32
GXR-6 Meas 32
GXR-6 Cert 32
LKSD-3 Meas 0.41 4.5 0.6 <1 15 10.9 4.5
LKSD-3 Cert 0.4 4.8 0.7 2 29 11.4 4.6
MAG-1 (Depleted) Meas 0.38 3.8 1.2 1 0.3 15 12.3 3
MAG-1 (Depleted) Cert 0.4 3.7 1.1 1.4 0.59 24 11.9 2.7
NIST 1633b Meas
NIST 1633b Cert
NIST 1633b Meas
NIST 1633b Cert
SY-2 Meas
SY-2 Cert
Page 12 of 14

Detection Limit 0.04 0.2 0.1 1 0.1 5 0.1 0.1 1 0.01
GXR-1 Meas 0.31 0.9 < 0.1 164 0.6 731 2.6 34.8 15
SY-3 Meas
SY-3 Cert
DR-N Meas
DR-N Cert
DR-N Meas
DR-N Cert
DR-N Meas
DR-N Cert
UB-N Meas
UB-N Cert
NIST 1632c Meas
NIST 1632c Cert
W-2a Meas 0.31 2.6 0.5 <1 0.1 8 2.2 0.5
W-2a Cert 0.33 2.6 0.5 0.3 0.2 9.3 2.4 0.53
W-2a Meas
W-2a Cert
NIST 696 Meas
NIST 696 Cert
SY-4 Meas
SY-4 Cert
CTA-AC-1 Meas 1.09 2.1 2.6 23.3 4.2
CTA-AC-1 Cert 1.08 1.13 2.65 21.8 4.4
BIR-1a Meas 0.25 0.6 < 0.1 <1 < 0.1 <5 < 0.1 < 0.1
BIR-1a Cert 0.26 0.6 0.04 0.07 0.01 3 0.03 0.01
JLk-1 Meas
JLk-1 Cert
JSd-1 Meas
JSd-1 Cert
JSl-2 Meas
JSl-2 Cert
SGR-1b Meas
SGR-1b Cert
SGR-1b Meas
SGR-1b Cert
#1 WANNIGRAT/VS (CH) Orig < 0.04 0.8 0.2 3 0.2 5 1 0.4 83.21
#1 WANNIGRAT/VS (CH) Dup < 0.04 0.6 0.1 2 0.3 <5 0.9 0.3 83.35
Method Blank Method Blank <1
Page 13 of 14

Detection Limit 0.04 0.2 0.1 1 0.1 5 0.1 0.1 1 0.01
GXR-1 Meas 0.31 0.9 < 0.1 164 0.6 731 2.6 34.8 15
Page 14 of 14

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Report: A09-1819 Final Report

Report Date: 15/05/2009 Activation Laboratories

Unit Symbol ppm g % g % % % % % % % % % % % % % %

Analyte Symbol LOI Total Sc Be V Cr Co Ni Cu Zn Ga Ge As Rb Sr Y Zr

Detection Limit 0.01 1 1 5 20 1 20 10 30 1 1 5 2 2 2 4

Analyte Symbol Lu Hf Ta W Tl Pb Th U Li Total

Analyte Symbol Lu Hf Ta W Tl Pb Th U Li Total

Analyte Symbol Lu Hf Ta W Tl Pb Th U Li Total

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