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  • Determination of SO in Tape Water

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    niazmn
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    This document provides procedures for determining the concentrations of sulfate and residual chlorine in tap water. For sulfate, the sample is boiled with acid to precipitate barium sulfate, which is then filtered, dried, weighed, and calculated based on its molecular weight. For chlorine, the sample is titrated with sodium thiosulfate using starch as an indicator, and the concentration is calculated based on the volume used and molarity of the thiosulfate solution. Reagents including methyl red indicator, hydrochloric acid, barium chloride solution, and a silver nitrate solution are also described.

    Original Description:

    Laboratory manual for sulphates in water

    Original Title

    Sulphates Water

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    This document provides procedures for determining the concentrations of sulfate and residual chlorine in tap water. For sulfate, the sample is boiled with acid to precipitate barium sulfate, which is then filtered, dried, weighed, and calculated based on its molecular weight. For chlorine, the sample is titrated with sodium thiosulfate using starch as an indicator, and the concentration is calculated based on the volume used and molarity of the thiosulfate solution. Reagents including methyl red indicator, hydrochloric acid, barium chloride solution, and a silver nitrate solution are also described.

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    © All Rights Reserved
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    14 views4 pages

    Determination of SO in Tape Water

    Uploaded by

    niazmn
    This document provides procedures for determining the concentrations of sulfate and residual chlorine in tap water. For sulfate, the sample is boiled with acid to precipitate barium sulfate, which is then filtered, dried, weighed, and calculated based on its molecular weight. For chlorine, the sample is titrated with sodium thiosulfate using starch as an indicator, and the concentration is calculated based on the volume used and molarity of the thiosulfate solution. Reagents including methyl red indicator, hydrochloric acid, barium chloride solution, and a silver nitrate solution are also described.

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    © All Rights Reserved
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    of 4

    DeterminationofSO42 intapewater:

    1) AddafewdropsMethyle redandafewdropsofConc.HCl to150mL


    samplewaterinabeaker.(toapHof44.5,checkthroughmethyle red)
    2) Boilsoln forabout3minutes
    3) Add1520mlof10%BaCl2 solutionslowlytothesample.(checkiffullppts
    areformedbyaddingafewmoredropsofBaCl2 andnoticingppt
    formation)
    4) Heatagainfor2minutesandkeepthesamplefor24hoursforprecipitates
    formation

    Determinationofresidualchlorineintapewater:
    1. Prepare0.01Msodiumthiosulphate solution(Na2S2O3.5H2O)
    2. RinsetheburettewithSTSandfilltheburettewithit
    3. Take200mLoftapewaterandadd5mLAceticacid(pHbetween3
    and4
    4. Add1gofKIandmixitbystirringrod
    5. QuicklytitrateagainstSTSuntiltheyellowcolorbecomespale
    yellow
    6. Add1mLofstarchsolution.ContinueTitrationuntill bluecolor
    disappearsandnotetheburettereading
    7. 1mlof0.01MSTS=0.354mgchlorine

    DeterminationofSO42 intapewater:
    1) After24hours,filterthroughashlessfilterpaperandwashwith50mL
    distilledwaterandcheckCl withAgNO3Solution.
    2) Dryandignitetheppt onthefilterpaepr (onapreweighedcrucible)at
    8500Cfor20minutes
    3) Shiftthecrucibletoadessicator andweighthesolid
    4) CalculateasSO42 formthesolidBaSO4 solid
    Thereactionisasfollowing:
    Ba2+ (aq)+SO42 (aq)>BaSO4 (s)
    Mol.WtofBaSO4 =233
    While233gofBaSO4 contains96gofSO4

    Reagentpreparation
    1. Methylredindicatorsolution:Dissolve100mgmethylredsodiumsaltin
    distilledwateranddiluteto100mL.
    2. b.Hydrochloricacid,HCl,useconcentratedone,foundinthebottle
    3. c.Bariumchloridesolution:Dissolve100gBaCl2.2H2Oin1Ldistilledwater.
    Filterthroughanashlessfilterpaperbeforeuse;
    4. d.Silvernitratenitricacidreagent:Dissolve8.5gAgNO3 and0.5mLconc.
    HNO3 in500mLdistilledwater.

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