(12) INTERNATIONAL APPLICATION PUBLISHED UNDER THE PATENT COOPERATION TREATY (PCT) (19) World Intellectual Property Organization International Bureau (43) International Publication Date 28 June 2007 (28.06.2007) (10) International Publication Number WO 2007/071238 Al 1) International Patent Classification: BOLD 118 (2006.01) 21) International Application Number PCT/DK2005/000820 22 December 2005 (22.12.2005) (25) Filing Language: lish (26) Publication Language: English (71) Applicant (for all designated Staves except US): NIRO AIS [DKIDK]; Gladsaxevej 305, DK-2860 Soborg (DK), m os) Inventors; and wentorsApplicants (for US only): mil [DK/DK]; Ravnsholtvej 22, DK-3450 Allered (DK). ULLUM, Thorvald, Unrskov [DK/DK]; Folkwarsvaj 19, 2nd Floor, DK-2000 Frederiksberg (DK), HANSEN, Ove, (74) Agents: SON, Eva et al; Intemationalt Patent-Bureau AVS, Rigensgade 11, DK-1316 Copea- hagen K (DK), (81) Designated States (uless otherwise indicated. for every ind of national protection available}: AE, AG, AL, AM, AT, AU, AZ, BA, BB, BG, BR, BW, BY, BZ, CA, CH,CN, CO, CR, CU, CZ, DE, DK, DM, DZ, EC, BE, BG, ES, FI, GB, GD, GE, GH, GM, HR, HU, ID, IL, IN, 18, JP, KI KG, KM, KN, KP. KR, KZ, LC. LK, LU, LY, MA, MD, MG, MK, MN, MW, MX, MZ, NA, NG, NI, NO, NZ, OM, PG, PH, PL, PT, RO, RU, SC SK, SL, SM, SY, TJ, TM, TN, TR, TT, TZ, UA, UG, US UZ, VC, VN, YU, ZA, 7M, ZW. ss) Designated States (unless otherwise indicated, for every kind of regional protection available: ARIPO (BW, GH, GM, KE, LS, MW, MZ, NA, SD, SL, SZ, T , ZW), Eurasian (AM, AZ, BY, KG, KZ, MD, RU, TI, TM), European (AT, BE, BG, CH, CY, CZ, DE, DK, EE, BS, FI, FR, GB, GR, HU, IE, I, IT, I, LU, LV, MC, NL,PL, PE RO, SE, Sl, SK, TR), OAPI (BE, BI, CF, CG, C1CM, GA, GN, GQ, GW, ML, MR, NE, SN, TD, TG). Declaration under Rule 4.17: 4s 1 applicant's entilement to apply for and be granted a patent (Rule 4.17(i)) Published: with international search report Fortwo-leter codes and other abbreviations, refer tothe *Guid- ance Notes on Codes and Abbreviations” appearing at the begin- hing of each regular issue of the PCT Gazette 7/071238 At Illll 0 (54) Title: AIR DISPERSER FOR A SPRAY DRYER AND A a i The air disperser (1) comprises an air inlet 2), METHOD FOR DESIGNING AN AIR ISP IRSER pipe (3) defining an air outlet area equipped with one or more & stoning means (4, an oster wall 7) and a space (8) defined by the pipe wall (9 andthe eter wall (7) of he a dispenser. The Sjce hs play ude vanes (1010) posoned sbanilyvereally nh aval ton and substan the © ian te wal) that wal ea see: A os (10s) esi vader ne tt fof the ul rads fom te pipe wal) inthe drction towards the outer wal (7) ofthe ar disperse, and the est of sid guide sens ting ised on ra ong ths creamer of he pe)WO 2007/071238 PCT/DK2005/000820 10 15 20 25 30 Title of the invention Air disperser for a spray dryer and a method for designing an air dis- perser Field of the invention The present invention relates to an air disperser for a spray dryer, comprising an air inlet, a pipe defining an air outlet area equipped with one or more atomizing means, said pipe having a longi- tudinal axis defining an axial direction and a radial direction extending substantially perpendicularly to said axial direction, an outer wall and a space defined by the pipe wall and the outer wall of the air disperser, said space having a plurality of guide vanes. Furthermore, the present invention relates to a method for designing an air disperser. Background of the invention ‘An air disperser must be included in a spray dryer in order to obtain a more uniform drying of the liquid to be atomized. The drying air is brought into contact with the liquid to be atomized through a pipe equipped with one or more nozzles through which the liquid is stream- ing. The drying air is entering the pipe from the air disperser. Hence, it is the aim to obtain a uniform distribution of drying air in the air di perser in order to obtain a uniform and symmetrical downward flow of drying air in the pipe and further into the drying chamber of the spray dryer. In the air dispersers known today it may be difficult to obtain a uniform and symmetrical flow of the drying air. These difficulties are most often due to the construction upstream of the supply pipe for the drying air, but may also be due to the design of the air disperser. If the drying air is not uniformly distributed in the air disperser, then neither the flow of drying air will be uniformly distributed at the point where the drying air and the liquid to be atomized are brought together. Conse- quently, a non-uniform drying process will be performed resulting in for example formation of deposits on the wall inside of the drying chamber, production of a product of less quality and a reduced capacity.WO 2007/071238 PCT/DK2005/000820 10 15 20 25 30 2 For many years it has been known to incorporate guide vanes in air dispersers in order to improve the distribution of drying air inside of the air disperser. For example in US 4,227,896 (Niro) a gas distribu- tion device for the supply of a processing gas to an atomizing chamber is described, said device containing two vane sets positioned opposite to each other in order to obtain a more uniform downwards directed flow of the drying air. However, this design aims at a rotational flow. As an alternative solution perforated plates have been intro- duced in such air dispersers in order to avoid turbulence in the air flow and hence to obtain a more uniform distribution of the air (see for ex- ample FR 1.289.817 (Niro)). However, the use of such perforated plates have shown to cause difficulties in respect of keeping the perforated plates clean. Especially, when the spray dryer is to be used in the food or pharmaceutical industry the sanitary aspects of the production design are very Important. ‘Summary of the invention Tt is an object of the invention to provide an air disperser for a spray dryer having an Improved performance by enabling a substantially symmetrical flow of drying air. In one aspect of the invention this is achieved by the provision of an air disperser for a spray dryer of the kind mentioned in the intro- duction, which is furthermore characterized in that at least one of the guide vanes is covering at least 90% of the full radius from the pipe wall in the direction towards the outer wall of the air disperser, and that the rest of the guide vanes are distributed on radii along the circumference of the pipe. By incorporating a number of guide vanes into the air disperser in the manner provided for by the present invention, the guide vanes distribute the incoming drying air, Doing so in an optimal manner in turn entails that deposits on the Inside of the walls of the drying cham- ber can be avoided and the drying capacity as well as drying economy is markedly improved. Furthermore, as a result of the design of the guide vanes, said guide vanes and the entire air disperser are easy to keepWO 2007/071238 10 15 20 25 30 PCT/DK2005/000820 3 clean and, consequently, such a design is very suitable for use in the food industry as well as in the pharmaceutical industry. Additionally, the pressure drop in the air disperser is less than the pressure drop in known air dispersers and, hence, the energy consumption is markedly decreased in comparison to known air dispersers. By the term “air disperser” as used herein is meant any dis- perser supplied with a drying gas to be used in the spray dryer. A skilled person will know that air is often used as the drying gas when the liquid to be atomized is an aqueous solution, while an inert gas is more likely used, when the liquid to be atomized is a non-aqueous solution, Conse- quently, the term “drying air" covers all types of drying gas, which may be used in the spray drying process. Additionally, the term “spray dry- ing” should be interpreted as embracing any process including drying, cooling and conditioning of a feed Preferably, the guide vanes are spaced from each other in such ‘a way that the length of the curved pipe wall between any two neighbouring guide vanes is substantially identical. Such a symmetrical distribution of the guide vanes has shown to give the best performance of the air disperser when aiming at the uniform and symmetrical down- ward flow of drying air in the pipe. However, in some designs the dis- tance between guide vanes may vary. In one embodiment of the invention the shape of each guide vane is substantially plane, while in another embodiment of the inven- tion the shape of each guide vane is curved in the axial direction and/or in the radial direction. The preferred shape in a given situation depends ‘on the rest of the design of the air disperser, such as the design of the supply pipe for drying air. The drying air may enter the air disperser in different modes. Hence, the drying air may e.g. be provided radially, tangentially or from the top of the air disperser in a downward direction, In one design of the air disperser the air inlet in the air dis- perser is a radial air inlet. In such air dispersers, the number of guide vanes lies between 3 and 20, preferably between 5 and 12. The guide vane positioned at the air inlet may or may not be present in the airWO 2007/071238 PCT/DK2005/000820 10 15 20 25 30 4 jet is not disperser. Hence, when the guide vane positioned at the ai present, the rest of the guide vanes are only positioned in the space be~ tween 10° and 350° from the air inlet. The size of each of the guide vanes depends on the design of the air disperser as well as the air flow needed in order to obtain an ac- ceptable drying. Hence, in one preferred embodiment, the guide vane positioned opposite to the air inlet is covering at least 90% of the full radius from the pipe wall in the direction towards the outer wall of the air disperser. In another preferred embodiment, the guide vane posi- tioned opposite to the air inlet is covering substantially the full radius between the pipe wall and the outer wall of the air disperser. However, the guide vane opposite to the alr inlet may cover any length of the ra- dius in the range of 90% of the radius to the full radius. The purpose of this guide vane is to prevent rotation of the incoming air. In yet another preferred embodiment the guide vanes increase in size in such a way that the guide vane closest to the air inlet is the smallest guide vane covering the smallest part of the radius between the pipe wall and the outer wall of the air disperser and the guide vane opposite to the air inlet is the largest guide vane covering most of the radius between the pipe wall and the outer wall of the air disperser. In cases where the guide vane positioned at the air inlet is not present, the two guide vanes closest to the air inlet are the smallest guide vanes. Al- ternatively, only one of the two guide vanes closest to the air inlet is the smallest one. In the most preferred embodiment, the guide vanes are positioned symmetrically with regard to a vertical plane seen from the air inlet to the guide vane opposite the air inlet in respect of the posi- tions and the sizes of the guide vanes. In another design of the air disperser, the air inlet is a tangen- tial air inlet. In such a design the preferred number of guide vanes lies between 4 and 30, preferably between 12 and 24. Furthermore, in this design the guide vane covering at least 90% of the full radius from the pipe wall in the direction towards the outer wall of the alr disperser is the guide vane positioned at approximately 360° from the air inlet. In another preferred embodiment, the guide vane positioned at approxi-WO 2007/071238 10 15 20 25 30 PCT/DK2005/000820 5 mately 360° from the air inlet is covering the full radius between the pipe wall and the outer wall of the air disperser. The size of each guide vane may vary depending on the design of the air disperser. However, in a preferred embodiment the guide vanes increase in size in such a way that the air coming from the air Inlet first meets the smallest guide vane covering the smallest part of the radius between the pipe wall and the outer wall of the air disperser and the guide vane positioned at approximately 360° from the air inlet is the largest guide vane covering most of the radius between the pipe wall and the outer wall of the air disperser. Such a positioning of the guide vanes has shown to give the best performance of the air disperser when aiming at the uniform and symmetrical downward flow of drying air in the pipe. Independently of the position of the air inlet, in yet another preferred embodiment the size of each guide vane is Identical apart from the one guide vane covering substantially the full radius. The dis tance between guide vanes may be the same or may vary. When performing the spray drying process, the axial velocity of the drying air in the pipe may lie in the range of 1 to 60 m/s. Further more, the overall normalized standard deviation on axial velocities is less than 8%, preferably less than 6%. In another aspect of the invention a method for designing an air disperser is provided. Such a method comprises the steps oft - selecting a number of guide vanes in an air disperser of a cer- tain design, ~ selecting the size of each guide vanes in an air disperser of a certain design, and = selecting the position of each guide vane. A skilled person would recognize that any kind of computational fluid dynamics program (CFD program) may be used as means of aid, when determining the specific best mode of design of the air disperser according to the invention taking upstream ducting and flow into ac- count. As an example of such a computational fluid program suitable for use In the present invention, FLUENT may be mentioned.WO 2007/071238 10 15 20 25 30 PCT/DK2005/000820 6 Furthermore, in a preferred embodiment of the method accord- ing to the present invention, the size of each guide vane is varied by us- ing adjustable guide vanes for testing purposes, before the permanent guide vanes are manufactured and welded into the air disperser. Brief description of the drawings Fig. 1 shows a plane view of an air disperser for a spray dryer having a radial air inlet and an arrangement of guide vanes in a first ‘embodiment of the invention; Fig. 2 shows a side view of the air disperser shown in Fig. 1; Fig. 3 shows a plane view of an air disperser for a spray dryer having a tangential air inlet and an arrangement of guide vanes in a second embodiment of the invention; Fig. 4 shows a side view of the air disperser shown in Fig. 3. Detail description of the invention and of preferred embodiments Fig. 1 and 2 show one preferred embodiment of an air disperser 1 for a spray dryer (not shown), comprising an air inlet 2 (the direction of the flow being indicated by an arrow 2a), which is a radial air inlet, a pipe 3 defining an air outlet area equipped with eight nozzles 4, said pipe having a longitudinal axis defining an axial direction 5 and a radial direction 6 extending substantially perpendicularly to said axial direc- tion. The air disperser 1 has an outer wall 7 and a space 8 defined by the pipe wall 9 and the outer wall 7 of the air disperser, said space hav- ing, in the embodiment shown, eight guide vanes 10 (denoted 10a to 10h). In the air disperser shown in Fig, 1, the guide vanes are posi- tioned substantially vertically in the axial direction and substantially on the radii between the pipe wall 9 and the outer wall 7 of the alr dis- perser. In the embodiment shown in fig. 1 one of the guide vanes 10¢ is covering the full radius between the pipe wall and the outer wall of the ir disperser, and the rest of the guide vanes are distributed on radii along the circumference of the pipe. Eventually, the air disperser Lis provided with a pipe 11 for the return of fines to the drying chamber. The pipe 3, if including more than one nozzle, may be composed of aWO 2007/071238 10 15 20 25 30 PCT/DK2005/000820 7 number of pipes, which encircles a nozzle each. The air disperser 4 Is mounted in the ceiling of the drying chamber of the spray dryer. De- pending on i.a. the size of the drying chamber, there may be more than one, e.g. three such air dispersers mounted in the ceiling of the drying chamber. In the embodiment shown in Fig. 1 the air disperser guide vanes are spaced from each other in such a way that the length a of the curved pipe wall 9 between any two neighbouring guide vanes 10h and 10a is substantially identical. In the embodiment shown In Fig. 1 the shape of each guide vane 10a ~ 10h is substantially plane. ‘As may be seen in Fig. 1, the guide vanes increase in size in such a way that the guide vane 10a closest to the air Inlet 2 Is the smallest guide vane covering the smallest part of the radius between the pipe wall 9 and the outer wall 7 of the air disperser, and the guide vane 10e positioned opposite to the air inlet 2 is the largest guide vane covering the full radius between the pipe wall 9 and the outer wall 7 of the air disperser. Furthermore, the guide vanes are positioned symmet- rically with regard to a vertical plane seen from the air inlet 2 to the guide vane 10e opposite the air inlet in respect of the positions and the sizes of the guide vanes. Fig. 3 and 4 show another preferred embodiment of an air dis- perser 101 for a spray dryer, comprising an air inlet 102, which Is a tangential air inlet, a pipe 103 defining an air outlet area equipped with a rotary atomizer 112, said pipe having a longitudinal axis defining an axial direction 105 and a radial direction 106 extending substantially perpendicularly to said axial direction, The air disperser 101 has an outer wall 107 and a space 108 defined by the pipe wall 109 and the outer wall 107 of the air disperser, sald space having twelve guide vanes 110 (denoted 110a to 1101). In the embodiment of the air dis- perser shown in Fig. 3, the guide vanes are positioned substantially ver- tically in the axial direction and substantially on the radii between the pipe wall 109 and the outer wall 107 of the air disperser. In the em- bodiment shown in Fig. 3 one of the guide vanes 1101 is covering the full radius between the pipe wall 109 and the outer wall 107 of the air dis-WO 2007/071238 PCT/DK2005/000820 10 15 20 25 30 8 perser, and the rest of said guide vanes are distributed on radii along the circumference of the pipe wall 109. The air disperser 101 is mounted in the ceiling of the drying chamber of the spray dryer, e.g. by means of the flange 111. As in the first embodiment, there may be more than one air disperser in the spray dryer. The air disperser shown in Fig. 3 contains twelve guide vanes of various sizes and the shape of each guide vanes is substantially plane. In the embodiment of Fig. 3 the guide vanes are spaced from each other in such a way that the length a of the curved pipe wall between any two neighbouring guide vanes is substantially identical. One guide vane (1101) is covering the full radius between the pipe wall and the outer wall of the air disperser. This is the guide vane positioned at ap- proximately 360° from the ai Inlet. As is shown most clearly in Fig. 3 this guide vane 1101 is secured to the outer wall 107 at the point on which the air inlet 102 intersects the outer wall 107. The air is thus able to flow in the space 108 in counter-clockwise direction until it finally meets the guide vane 110! covering the full radius, but cannot rotate further. The rest of the guide vanes increase in size in such a way that the air coming from the air inlet first meet the smallest guide vane cov- ering the smallest part of the radius between the pipe walll and the outer wall of the air disperser and the guide vane positioned at approximately 360° from the air inlet is the largest guide vane covering most of the ra- dius between the pipe wall and the outer wall of the air disperser. It should be understood that any type of drying air inlet, here shown as radial or tangential, may be combined with any relevant at- omizing means to atomize the feed. Here is shown nozzle means and a rotary atomizer wheel. A person skilled in the art will select between nozzle means, such as e.g. pressure nozzles and two-fluid nozzles, ro- tary atomizers or other droplet generating means e.g. such as using ul- trasound or single droplet generation. For any of the two embodiments described in details above the axial velocity of the drying air in the pipe lie in the range of 1 to 60 m/s, and the overall normalized standard deviation on axial velocities is less than 8%, preferably less than 6%.WO 2007/071238 PCT/DK2005/000820 9 The invention should not be regarded as being limited to the embodiment shown and described in the above but various modifica~ tions and combinations of features may be carried out without departing from the scope of the following claims.WO 2007/071238 10 15 20 25 30 PCT/DK2005/000820 10 A deMas disperser for a spray dryer, comprising an air inlet, a pipe defining an air outlet area equipped with one or more atomizing 1. An means, said pipe having a longitudinal axis defining an axial direction and a radial .ction extending substantially perpendicularly to said ax- jal direction, an outer wall and a space defined by the pipe wall and the outer wall of the air disperser, said space having a plurality of guide vanes, characterized in that the guide vanes are positioned substantially vertically in the axial direction and substantially on the ra- dii between the pipe wall and the outer wall of the air disperser, and that at least one of said guide vanes is covering at least 90% of the full radius from the pipe wall in the direction towards the outer wall of the air disperser, and the rest of said guide vanes being distributed on radii along the circumference of the pipe. 2. An air disperser according to claim 1, wherein the guide vanes are spaced from each other in such a way that the length of the curved pipe wall between any two neighbouring guide vanes is substan- tially identical 3. An air disperser according to any of the claims 1 or 2, wherein the shape of each guide vane is substantially plane. 4, An air disperser according to any of the claims 1 or 2, wherein the shape of each guide vane is curved in the axial direction and/or in the radial direction. 5. An air disperser according to any of the claims 1 to 4, wherein the air inlet is a radial air inlet. 6. An air disperser according to claim 5, wherein the number of guide vanes lies between 3 and 20, preferably between 5 and 12. 7. An air disperser according to any of the claims 5 or 6, wherein the guide vanes are only positioned in the space between 10° and 350° from the air inlet. 8. An air disperser according to any of the claims 5 to 7, wherein the guide vane positioned opposite to the air inlet is covering at least 90% of the full radius from the pipe wall in the direction towards the outer wall of the air disperser.WO 2007/071238 PCT/DK2005/000820 10 15 20 25 30 it 9. An air disperser according to any of the claims 5 to 7, Wherein the guide vane positioned opposite to the air inlet is substan- tially covering the full radius between the pipe wall and the outer wall of the air disperser. 10. An disperser according to any of the claims 5 to 9, wherein the guide vanes increase in size in such a way that the guide vane closest to the air inlet is the smallest guide vane covering the smallest part of the radius between the pipe wall and the outer wall of the air disperser and the guide vane opposite to the air inlet is the larg- est guide vane covering most of the radius between the pipe wall and the outer wall of the air disperser. 11. An air disperser according to any of the claims 5 to 10, wherein the guide vanes are positioned symmetrically with regard to a vertical plane seen from the air inlet to the guide vane opposite the air inlet in respect of the positions and the sizes of the guide vanes. 42. An air disperser according to any of the claims 1 to 4, wherein the air inlet is a tangential air inlet. 13. An air disperser according to claim 12, wherein the number of guide vanes lies between 4 and 30, preferably between 12 and 24. 14, An air disperser according to any of the claims 12 or 13, wherein the guide vane covering at least 90% of the full radius from the pipe wall in the direction towards the outer wall of the air disperser is the guide vane positioned at approximately 360° from the air inlet. 15. An air disperser according to any of the claims 12 or 13, wherein the guide vane covering the full radius between the pipe wall and the outer wall of the air disperser is the guide vane positioned at approximately 360° from the air inlet. 16. An air disperser according to any of the claims 12 to 15, wherein the guide vanes increase in size in such a way that the air com- ing from the air inlet first meets the smallest guide vane covering the smallest part of the radius between the pipe wall and the outer wall of the air disperser and the guide vane positioned at approximately 360° from the air inlet is the largest guide vane covering most of the radius between the pipe wall and the outer wall of the air disperser.WO 2007/071238 PCT/DK2005/000820 12 17. An air disperser according to any of the claims 1 to 8 and 12 to 14, wherein the size of each guide vane apart from one is identi- cal. 18. An air disperser according to any of the claims 1 to 17, 5 wherein the axial velocity of the drying air in the pipe Is in the range of 1 to 60 m/s. 19. An air disperser according to claim 18, wherein the overall normalized standard deviation on axial velocities is less than 8%, pref- erably less than 6% 10 20. A method for designing an air disperser, comprising the steps of: - selecting a number of guide vanes in an air disperser of a cer- tain design, - selecting the size of each guide vanes in an air disperser of a 15 certain design, and - selecting the position of each guide vane. 21. The method according to claim 20, wherein the steps are simulated by use of a computational fluid dynamics program. 22. The method according to any of the claims 20 or 21, 20 wherein the size of each guide vane is varied by using adjustable guide vanes for testing purposes, before the permanent guide vanes are manufactured and welded into the air disperser.WO 2007/071238 PCT/DK2005/000820 1/2 2a Fig. 2 SUBSTITUTE SHEET (RULE 26)