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  • MB Acetone

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    Fahad Rocking
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    This document summarizes a distillation process using a GC/KF combo. It provides details on the feed material composition, mass balance, cut identification and results. The feed is composed primarily of acetone (92.84%), with smaller amounts of water, ethyl acetate, ethanol, methanol and chloroform. The distillation produced three cuts - an intercut fraction, main cut 1 and main cut 2, as well as residue and remaining feed. The intercut was collected at 11.3 hours as an impure fraction, while the main cuts were taken at 13:30 and 14:30 hours respectively.

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    This document summarizes a distillation process using a GC/KF combo. It provides details on the feed material composition, mass balance, cut identification and results. The feed is composed primarily of acetone (92.84%), with smaller amounts of water, ethyl acetate, ethanol, methanol and chloroform. The distillation produced three cuts - an intercut fraction, main cut 1 and main cut 2, as well as residue and remaining feed. The intercut was collected at 11.3 hours as an impure fraction, while the main cuts were taken at 13:30 and 14:30 hours respectively.

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    5 views2 pages

    MB Acetone

    Uploaded by

    Fahad Rocking
    This document summarizes a distillation process using a GC/KF combo. It provides details on the feed material composition, mass balance, cut identification and results. The feed is composed primarily of acetone (92.84%), with smaller amounts of water, ethyl acetate, ethanol, methanol and chloroform. The distillation produced three cuts - an intercut fraction, main cut 1 and main cut 2, as well as residue and remaining feed. The intercut was collected at 11.3 hours as an impure fraction, while the main cuts were taken at 13:30 and 14:30 hours respectively.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as xlsx, pdf, or txt
    of 2

    Batch Size

    Feed Material
    Feed Composition
    a
    b
    c
    d
    e
    f

    GC/KF combo
    Component 1
    Acetone
    Component 2
    Water
    Component 3 Ethyle Acetate
    Component 4
    Ethanol
    Component 5
    Methanol
    Component 6
    Chloroform

    Feed Mass Balance


    a
    b
    c
    d
    e
    f

    Component 1
    Component 2
    Component 3
    Component 4
    Component 5
    Component 6

    Cut Identification
    Intercut F-1
    Mian Cut F-2
    Main Cut F-3
    Residue (Reboiler)
    Feed Remaining

    Litres

    165

    98.06
    5.32
    1.49
    0.02
    0.03
    0.2

    %
    w/w %
    %
    %
    %
    %
    Wt %

    By GC Method
    By KFR
    By GC Method
    By GC Method
    By GC Method
    By GC Method
    Description Of feed
    Acetone in feed (100% basis)
    water in feed (100% basis)
    Ethyle Acetate in feed (100% basis)
    Ethanol in feed (100% basis)
    Methanol in feed (100% basis)
    Chloroform in feed (100% basis)
    TOTAL

    Acetone
    Water
    Ethyle Acetate
    Ethanol
    Methanol
    Chloroform
    TOTAL

    92.84
    5.32
    1.411
    0.019
    0.028
    0.19
    100

    %
    w/w %
    %
    %
    %
    %
    %

    Volume

    Mass

    Time

    KFR

    Density

    Lit
    30
    85
    40
    15
    30

    Kgs
    24.3
    67.15
    31.6
    15.75
    24.3

    Hrs.
    11.3
    13:30
    14:30
    15:00

    %
    6.9
    2
    1
    84
    5.32

    g/cc
    0.81
    0.79
    0.79
    1.05
    0.81

    Remarks

    Intercut as impure fraction


    Mian cut -1
    Mian cut -2
    Left over material
    Feed not consumed for Distill

    Description Of feed
    ne in feed (100% basis)
    er in feed (100% basis)
    cetate in feed (100% basis)
    nol in feed (100% basis)
    nol in feed (100% basis)
    orm in feed (100% basis)
    TOTAL

    Qty.
    124.08
    7.11
    1.885
    0.025
    0.038
    0.25
    133.7

    UOM
    Kg
    Kg
    Kg
    Kg
    Kg
    Kg
    Kg

    Results
    Remarks
    Intercut as impure fraction
    Mian cut -1
    Mian cut -2
    Left over material
    Feed not consumed for Distill

    GC
    %
    98.95
    99.65
    98.06

    KFR
    %
    6.9
    2
    1
    84
    5.32

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