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WJ - 1975 - 01 - s12 Purging With Nitrogen
WJ - 1975 - 01 - s12 Purging With Nitrogen
WJ - 1975 - 01 - s12 Purging With Nitrogen
12-s I J A N U A R Y 1 9 7 5
Back Purging
Experimentation
Butt welds were made with 4 mm
thick AISI type 316 austenitic stainless steel plates using GTA welding.
The root welds were made without
any filler and the second pass of the
two-pass butt welds was made with
AISI type ER 316 L filler wire. The
composition of the base plate and
filler metal is given in Table 1. The
welding conditions are given in Table
2. The weld root and adjacent plate
showed no discoloration on the surface in both the argon and nitrogen
purged joints.
Results and Discussion
1. Radiographic Tests. X-ray ,radiographs of the joints revealed the
joints to be sound without any porosity and cracking both in argon as well
as in nitrogen purged joints.
6.65
6.25
Ni
Mo
Si
11.45
13.025
2-3
2-3
0.3
0.41
Mn
1.61
2 Max.
0.09
0.14
0.03 Max. 0.17
Sr.
no.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
Joint
no.
1
2
3
4
5
6
7
10
10
11
11
12
12
13
13
14
15
16
16
17
18
19
20
Open clr.
voltage,
V
Arc
voltage,
V1
Current,
A
10
10
10
10
10
10
10
10
10
10
10
11
11
11
11
11
11
11
11
11
11
11
11
66
85
77
77
102
86
86
82
77
82
77
82
77
82
77
83
82
84
82
130
130
120
120
63
62
58.5
58.5
63
63
62.5
60
60
62
62
60
60
60
60
60
60
62
62
56.5
56.5
62
61
N
N
Ar
N
N
Ar
Ar
Ar
N
N
N
N
Ar
Ar
N
N
N
N
Ar
N
N
Ar
Welding
speed
mm/min
25
34.3
65
60
117
89
62.25
61
41.6
61
40
58
45
44.5
38.8
46.8
40.75
18.35
20.10
166.4
144.3
162
133.5
Heat
input
kJ/mm
1.584
1.4875
0.714
0.77
0.525
0.58
0.82
0.806
1.11
0.806
1.155
0.9325
1.131
1.23
1.31
1.157
1.33
3.02
2.69
0.515
0.594
0.489
0.593
Sr.
no.
Joint
no.
Delta-Ferrlte,
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
1
2
3
4
5
6
7
10
10
11
11
12
12
13
13
14
15
16
16
17
18
19
20
1 to 1.5
1 to 1.5
0.6 to 1
0to1
0to1
0 to 0.6
0 to 0.6
0 to 0.6
Nil
0 to 0.6
0 to 0.6
0 to 0.6
Nil
0 to 0.6
Nil
0to1
0to1
0.9 to 1.5
0 to 0.6
0to1
0to1
0to1
Oto 1
N
N
N
Ar
N
N
Ar
Ar root pass
A r 2 n d pass
N root pass
N 2nd pass
N root pass
N 2nd pass
Ar root pass
Ar 2nd pass
N
N
N root pass
N 2nd pass
Ar
N
N
Ar
% <>
Proof
stress
kg/mm2
Joint
no.
12 N<a>
13 Ar (a >
12 N
13 Ar
Base plate
Base plate
Tensile
strength
kg/mm2
60.075
61.05
59.5
58.6
59.1
52.8
38.3
39.55
35.5
33.3
33.7
Elongation,
Remarks< b )
FR
FR
FB
FB
52.125
49.4
49.0
47.5
54.0
From
standards
(a) Average of two close values
(b) FR = Failure in weld zone, reduced section test; FB
<
o
or
<
or
UJ
10
DISTANCE
5
FROM
0
WELD
10
15
CENTRE (mm)
Fig- 1 Hardness variation across the joint for nitrogen and argon purged welds
WELDING
13-s
"
A
0
A
1 N -10 V
2 N - 1 0 V , SS A
.X
5N-I0V
66 A
K N - 1 1 V , 83 A
15 N - 11 V
I 6 N - 11 V , 82 A
-2
<
*-
82 A
-20
o
10
DEPTH
X
V
'
A
0
.14
O
V
.12
(Ar J
6 N 1
10
a
Ott
06
'
10 V , 7 7 A
10 V
7ArJr
10A r l
I
J
11 N
17 A r l
18 N J
86A
10 V , 8 2 A
11 V , 130 A
19 N
20 A r
11 V , 120 A
+
B
DEPTH
"
1
ROOT
"J
0<
ID
11-
mm
Fig. 2(b) - Comparison between nitrogen content variation in nitrogen and argon purged
weld roots made with equal heat inputs
Table 5 Carbide Precipitation
Sr.
no.
Joint
no.
1 N ^
2 N -'
10 Ar \
12 N
13 Ar
15 N
7
8
Microstructural observations
7 Ar
11 N /
16 N
14 N
Other
joints
14-8 I J A N U A R Y
o o
mm.
IB
V
B
-8
X
A
- \"
0-04
O-OS
-6
1
6
e
8
Fig. 2(a) Nitrogen content variations in weld root passes for six nitrogen purged joints
.'
ARGON P SGED
ROOT
NITROGEN PURGED
OS.
.*,
102A
1 975
p r o p e r t i e s of t h e n i t r o g e n a n d a r g o n
p u r g e d j o i n t s a n d h e n c e it c a n b e
c o n c l u d e d that nitrogen can very well
b e u s e d a s a p u r g i n g g a s in t h e
w e l d i n g of a u s t e n i t i c
unstabilized
stainless steels.
2. W e l d i n g s h o u l d b e p e r f o r m e d
with the m i n i m u m specific heat input
possible.
Sr.
no.
Joint
no.
1 N '
2 N
2
Acknowledgments
The authors are thankful to Messers
Larsen and Toubro Ltd., Powai, for providing stainless steel material and filler
wires.
3
4
5
6
N, 17
Ar,18
N, 19
N, 20
7 Ar
References
1. A m e r i c a n Society for Metals, Metals
Handbook,
Vol. 6, Welding and Brazing,
8th Edition.
2. A m e r i c a n Welding Society, Welding
of Austenitic Cr-Ni Steel Piping and Tubing, A W S D10.4-66.
3. Gooch, T. G., "The corrosion beh a v i o u r of w e l d e d n i t r o g e n b e a r i n g
austenitic stainless steels," Met. Const,
and Br. W. J., 1, D e c , 1969, 0569.
4. Lapsatre, J., Hubert, M. and Messag e s C , "Contribution A L'etude du s o u dage des aciers austenitiques du type 1810 A L' azote," Revue de Metallurgia,
66,
Nov., 1969, p 7 7 1 .
5. P a s c a r e l , L., H u b e r t , M . a n d
Messager, C , "Aspect particuliers de la
fissuration a chaud par soudage d'aciers
austenitiques influence de L' azote." Rev.
de Met, 68, D e c , 1971, p809.
6. Borland, J. C. and Yonger, R. N.,
"Some aspects of cracking in welded Cr-Ni
austenitic steels," B.W.R.A. Report, Br.
W.J., 7, 1960, p22.
7. Gooch, T. G., "Welding metallurgy of
Microstructural observations
Ar
N
N
Ar
10 Ar
11 N
HAZ attack, ditch structure, one or two grains completely surrounded by ditches, weld attack, interdendritic ditches, more in second pass
12 N
13 Ar
HAZ attack, ditch structure, more than one grain completely surrounded by ditches, weld attack, interdendritic ditches, more in second pass
14 N
15 N
HAZ attack, ditch structure, m o r e than one grain completely surrounded by ditches, weld attack, interdendritic ditches
16 N
by
WRC Bulletin
No. 185
July 1973
"Improved Discontinuity Detection Using ComputerAided Ultrasonic Pulse-Echo Techniques"
by J. R. Frederick and J. A. Seydel
The purpose of this project, sponsored by the Pressure Vessel Research Committee of the Welding Research Council, was to investigate means for obtaining
improved characterization of the size, shape and location of subsurface discontinuities in metals. This objective was met by applying computerized dataprocessing techniques to the signal obtained in conventional ultrasonic pulseecho systems. The principal benefits were improved signal-to-noise ratio and
resolution.
The price of WRC Bulletin 185 is $3.50 per copy. Orders should be sent to the
Welding Research Council, 345 East 47th Street, New York, N.Y. 10017.
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