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    Tasya Diah Rachmadiani
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    This document contains data from observations of mixing patterns and times using different mixing speeds for both dilute and concentrated solutions. For the dilute solution, the Reynolds number and blending time factor were calculated for mixing times of the base and acid. Reynolds numbers ranged from 1115 to 1833 and blending times from 51.97 to 61.33 seconds. For the concentrated solution, calculations showed Reynolds numbers from 558 to 916 and blending times from 86.62 to 255.56 seconds. Higher mixing speeds produced higher Reynolds numbers and shorter blending times.

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    This document contains data from observations of mixing patterns and times using different mixing speeds for both dilute and concentrated solutions. For the dilute solution, the Reynolds number and blending time factor were calculated for mixing times of the base and acid. Reynolds numbers ranged from 1115 to 1833 and blending times from 51.97 to 61.33 seconds. For the concentrated solution, calculations showed Reynolds numbers from 558 to 916 and blending times from 86.62 to 255.56 seconds. Higher mixing speeds produced higher Reynolds numbers and shorter blending times.

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    14 views13 pages

    Data Pengamatan

    Uploaded by

    Tasya Diah Rachmadiani
    This document contains data from observations of mixing patterns and times using different mixing speeds for both dilute and concentrated solutions. For the dilute solution, the Reynolds number and blending time factor were calculated for mixing times of the base and acid. Reynolds numbers ranged from 1115 to 1833 and blending times from 51.97 to 61.33 seconds. For the concentrated solution, calculations showed Reynolds numbers from 558 to 916 and blending times from 86.62 to 255.56 seconds. Higher mixing speeds produced higher Reynolds numbers and shorter blending times.

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    of 13

    I.

    DATA PENGAMATAN
    A. Pola aliran hasil pengadukan
    Tipe pengaduk yang digunakan : Tree Blade/Marinne Propeller
    Diameter pengaduk (Da)
    : 11 cm = 0,11 m
    Diameter tangki (Dt)
    : 30 cm = 0,3 m
    Kalibrasi Kecepatan Putar Propeller
    0.5 50
    10
    1.5 50
    20
    2.5 50
    30
    3.5 50
    40
    4.5 50
    50

    39.8 rpm
    65.9 rpm
    94.4 rpm
    121.3 rpm
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm
    267.9 rpm (Bergolak)

    Kecepatan yang digunakan :


    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm
    B. Waktu pengadukan
    Data Pengamatan Kecepatan 1: Larutan Encer
    Kecepatan
    putaran (rpm)
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm

    t1
    (t NaOH,detik)
    14.38
    11.18
    08.79
    08.56
    06.96

    t2
    (t H2SO4,detik)
    10.34
    08.39
    09.77
    16.41
    16.77

    Temperature
    (oC)
    26,8
    26,2
    26,2
    26
    26

    Densitas
    (gr/ml)
    1,228
    1,240
    1,236
    1,236
    1,234

    Temperature
    (oC)
    26,8
    26,2
    26,2
    26
    26

    Densitas
    (gr/ml)
    1,228
    1,240
    1,236
    1,236
    1,234

    Data pengamatan Kecepatan 2 : Larutan Encer


    Kecepatan
    putaran (rpm)
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm

    t1
    (t NaOH,detik)
    13.83
    11.00
    08.99
    08.44
    07.11

    t2
    (t H2SO4,detik)
    10.11
    08.20
    09.09
    12.40
    11.86

    Data Kecepatan Pengadukan Rata-rata : Larutan encer


    Kecepatan
    putaran (rpm)
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm

    t1
    (t NaOH,detik)
    14.10
    11.09
    08.89
    08.50
    07.03

    t2
    (t H2SO4,detik)
    10.22
    08.29
    08.90
    14.40
    14.31

    Temperature
    (oC)
    26,8
    26,2
    26,2
    26
    26

    Densitas
    (gr/ml)
    1,228
    1,240
    1,236
    1,236
    1,234

    t2
    (t H2SO4,detik)
    13.00
    11.81
    07.81
    07.02
    06.30

    Temperature
    (oC)
    28,8
    28,2
    28,2
    28
    28

    Densitas
    (gr/ml)
    1,128
    1,140
    1,136
    1,136
    1,134

    t2
    (t H2SO4,detik)
    12.36
    10.75
    07.71
    06.65
    05.23

    Temperature
    (oC)
    28,8
    28,2
    28,2
    28
    28

    Densitas
    (gr/ml)
    1,128
    1,140
    1,136
    1,136
    1,134

    Temperature
    (oC)
    28,8
    28,2
    28,2
    28
    28

    Densitas
    (gr/ml)
    1,128
    1,140
    1,136
    1,136
    1,134

    Data Kecepatan 1 : Larutan Pekat


    Kecepatan
    putaran (rpm)
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm

    t1
    (t NaOH,detik)
    14.84
    10.84
    08.71
    08.04
    07.16

    Data Kecepatan 2 : Larutan Pekat


    Kecepatan
    putaran (rpm)
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm

    t1
    (t NaOH,detik)
    13.18
    09.77
    08.59
    08.06
    07.87

    Data Kecepatan Pengadukan Rata-rata :


    Kecepatan
    putaran (rpm)
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm
    II.

    t1
    (t NaOH,detik)
    14.01
    10.30
    8.65
    8.05
    7.51

    t2
    (t H2SO4,detik)
    12.68
    11.28
    7.76
    6.83
    5.76

    PENGOLAHAN DATA

    1) SLURRY ENCER
    encer : 2,6 x 10-3 kg/ms
    encer : 1,2345 kg/L
    1. Menghitung bilangan Reynold ( ENCER )
    t 1 (t NaOH)
    kecepatan putaran 148.9 rpm

    Nre=

    D N

    (0.1274 m)2 ( 148.9 rpm ) (1,2

    2,6 x 10

    kg
    )
    m3

    kg
    ms

    1115,43

    kecepatan putaran 174,6 rpm

    D 2 N
    Nre=

    (0.1274 m)2 ( 174,6 rpm ) (1,2

    2,6 x 10

    kg
    )
    m3

    kg
    ms

    1307,95

    kecepatan putaran 196,8 rpm

    Nre=

    D 2 N

    (0.1274 m)2 ( 196,8 rpm ) (1,2

    2,6 x 10

    kg
    )
    m3

    kg
    ms

    1474,25

    kecepatan putaran 223,5 rpm

    Nre=

    D 2 N

    (0.1274 m) ( 223,5 rpm ) (1,2

    2,6 x 10

    kg
    )
    m3

    kg
    ms

    1674,26

    kecepatan putaran 244,7 rpm


    2

    Nre=

    D N

    (0.1274 m) ( 244,7 rpm ) (1,2

    2,6 x 10

    kg
    ms

    kg
    )
    m3

    1833,08
    t 2 (t H2SO4)
    kecepatan putaran 148,9 rpm

    Nre=

    D 2 N

    (0.1274 m)2 ( 148,9 rpm ) (1,84

    2,6 x 10

    kg
    )
    m3

    kg
    ms

    1710,32

    kecepatan putaran 174,6 rpm

    Nre=

    D 2 N

    (0.1274 m)2 ( 174,6 rpm ) (1,84

    2,6 x 10

    kg
    )
    m3

    kg
    ms

    2005,52

    kecepatan putaran 196,8 rpm


    2

    Nre=

    D N

    (0.1274 m) ( 196,8 rpm ) (1,84

    2,6 x 10

    kg
    )
    m3

    kg
    ms

    2260,52

    kecepatan putaran 223,5 rpm


    2

    Nre=

    D N

    (0.1274 m) ( 223,5 rpm ) (1,84

    2,6 x 10
    2567,20

    kecepatan putaran 244,7 rpm

    Nre=

    D 2 N

    kg
    ms

    kg
    )
    m3

    (0.1274 m)2 ( 244,7 rpm ) (1,84

    2,6 x 10

    kg
    )
    m3

    kg
    ms

    2810,72

    2. Menghitung Blending time factor


    Dari grafik didapatkan ntT = 1200 (digunakan untuk semua kecepatan karena perbedaan Nre
    yang terlalu sedikit )
    t 1 (t NaOH)
    kecepatan putaran 148,9 rpm

    = 61,33

    kecepatan putaran 174,6 rpm

    = 58,16

    kecepatan putaran 196,8 rpm

    = 55,89

    kecepatan putaran 223,5 rpm

    = 53,56

    kecepatan putaran 244,7 rpm

    = 51,97
    t 2 (H2SO4)
    ntT = 1000 (digunakan untuk semua kecepatan putar kecuali kecepatan 148,9 rpm )

    kecepatan putaran 148,9 rpm

    = 61,33

    kecepatan putaran 174,6 rpm

    = 48,46

    kecepatan putaran 196,8 rpm

    =46,57

    kecepatan putaran 223,5 rpm

    = 44,64

    kecepatan putaran 244,7 rpm

    = 43,32
    Kecepata
    n putar
    (rpm)
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm

    Reynold Number

    Blending time

    t1

    t2

    t1

    t2

    1115,43
    1307,95
    1474,25
    1674,26
    1833,08

    1710,32
    2005,52
    2260,52
    2567,20
    2810,72

    61,33
    58,16
    58,16
    53,56
    51,97

    61,33
    48,46
    46,57
    44,64
    43,32

    2) SLURRY PEKAT

    t1
    (t NaOH,detik)

    t2
    (t H2SO4,detik)

    14.10
    11.09
    08.89
    08.50

    10.22
    08.29
    08.90
    14.40

    07.03

    14.31

    pekat : 5,2 x 10-3 kg/ms


    pekat : 1,2345 kg/L
    Menghitung bilangan Reynold
    t 1 (t NaOH)
    kecepatan putaran 148.9 rpm

    Nre=

    D 2 N

    (0.1274 m)2 ( 148.9 rpm ) (1,2

    5,2 x 10

    kg
    )
    m3

    kg
    ms

    557,71

    kecepatan putaran 174,6 rpm

    Nre=

    D 2 N

    (0.1274 m)2 ( 174,6 rpm ) (1,2

    5,2 x 10

    kg
    )
    m3

    kg
    ms

    653,97

    kecepatan putaran 196,8 rpm

    Nre=

    D 2 N

    (0.1274 m)2 ( 196,8 rpm ) (1,2

    5,2 x 10

    kg
    )
    m3

    kg
    ms

    737,12

    kecepatan putaran 223,5 rpm


    2

    Nre=

    D N

    (0.1274 m) ( 223,5 rpm ) (1,2

    5,2 x 10

    kg
    ms

    837,13

    kecepatan putaran 244,7 rpm


    2

    Nre=

    D N

    kg
    )
    m3

    (0.1274 m)2 ( 244,7 rpm ) (1,2

    5,2 x 10

    kg
    )
    m3

    kg
    ms

    916,54
    t 2 (t H2SO4)
    kecepatan putaran 148,9 rpm
    2

    Nre=

    D N

    (0.1274 m)2 ( 148,9 rpm ) (1,84

    5,2 x 10

    kg
    )
    m3

    kg
    ms

    855,16

    kecepatan putaran 174,6 rpm


    2

    Nre=

    D N

    (0.1274 m) ( 174,6 rpm ) (1,84

    5,2 x 10

    kg
    )
    m3

    kg
    ms

    1002,76

    kecepatan putaran 196,8 rpm

    D 2 N
    Nre=

    (0.1274 m)2 ( 196,8 rpm ) (1,84

    5,2 x 10

    kg
    )
    m3

    kg
    ms

    1130,26

    kecepatan putaran 223,5 rpm

    Nre=

    D 2 N

    (0.1274 m)2 ( 223,5 rpm ) (1,84

    5,2 x 10
    1283,60

    kecepatan putaran 244,7 rpm

    kg
    ms

    kg
    )
    m3

    Nre=

    D N

    (0.1274 m)2 ( 244,7 rpm ) (1,84

    5,2 x 10

    kg
    )
    m3

    kg
    ms

    1405,40
    Menghitung Blending time factor
    t 1 (t NaOH)
    kecepatan putaran 148,9 rpm

    = 255,56

    kecepatan putaran 174,6 rpm

    = 193,88

    kecepatan putaran 196,8 rpm

    = 139,72

    kecepatan putaran 223,5 rpm

    = 111,6

    kecepatan putaran 244,7 rpm

    = 86,62
    t 2 (H2SO4)
    ntT = 1000 (digunakan untuk semua kecepatan putar kecuali kecepatan 148,9 rpm )

    kecepatan putaran 148,9 rpm

    = 127,78

    kecepatan putaran 174,6 rpm

    = 72,70

    kecepatan putaran 196,8 rpm

    =55,89

    kecepatan putaran 223,5 rpm

    = 53,56

    kecepatan putaran 244,7 rpm

    = 51,97
    Kecepata
    n putar
    (rpm)
    148.9 rpm
    174.6 rpm
    196.8 rpm
    223.5 rpm
    244.7 rpm

    Reynold Number

    Blending time

    t1

    t2

    t1

    t2

    557,71
    653,97
    737,12
    837,13
    916,54

    855,16
    1002,76
    1130,26
    1283,60
    1405,40

    255,56
    193,88
    139,72
    111,6
    86,62

    127,78
    72,70
    55,89
    53,56
    51,97

    t1
    (t NaOH,detik)

    t2
    (t H2SO4,detik)

    14.10
    11.09
    08.89
    08.50
    07.03

    10.22
    08.29
    08.90
    14.40
    14.31

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