LOT NUMBER 0001

DATE:
NEW BATCH RECORD
REPEAT BATCH RECORD
REVISED BATCH RECORD

[X]
[ ]
[ ]

REVISION OF

PRODUCT TITLE:

PRODUCT STRUCTURE

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===============================================================================================
===============================================================================================
APPROVALS
NAME
DATE

ORIGINATOR (PRINTED)

ROSE AULT

05/04/2015

ORIGINATOR

JACOB DONDERS

05/04/2015

DIRECTOR OF OPERATIONS

KIM KOZLOFF AND SARA HEINES

05/04/2015

ENVIRONMENTAL OFFICER

KATIE YEACKER AND KATIE GERHARDT

05/04/2015

PILOT PLANT MANAGER

BEN ECKERT AND ANDREW KEATING

05/04/2015

CHIEF ENGINEER

SARAH BURGESS AND WADE MURPHY

05/04/2015

CLIENT
CLIENT

REPRESENTATIVE (PRINTED)
REPRESENTATIVE (SIGNATURE)

MSU SR. ASSOC. VICE PRESIDENT

BRANDON HIGH SCHOOL

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MICHIGAN STATE UNIVERSITY

BIOECONOMY INSTITUTE
BATCH RECORD

THEOR. YIELD:
EXPECTED YIELD:
EXPECTED MOLE % YIELD:
DATE STARTED:

160.9

KG

NET WEIGHT:

KG

149.31

KG

ACTUAL YIELD:

KG

ACTUAL MOLE % YIELD:

92.8

DATE COMPLETED:

=================================================================
BRIEF DESCRIPTION OF CHANGE AND REASONS FOR PROPOSED CHANGE:
(ADDITIONAL DETAILS AND SUPPORTING DATA MAY BE ATTACHED)
THIS IS A NEW BATCH RECORD.

BRANDON HIGH SCHOOL

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RAW MATERIALS
ITEM
NUMBE
R

MATERIAL DESCRIPTION
CANOLA OIL (MW XX.X)
METHANOL (MW XX.X)
CATALYST NAOH
WATER

BRANDON HIGH SCHOOL

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KMOLE
S

PLANNED
QUANTITY

0.1821
1.642
.0266
1.346

159.62 KG
52.61 KG
1.064 KG
24.25 KG

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CHEMICAL EQUATIONS

WASTE TREATMENT AND DISPOSAL

SPENT / DISTILLED SOLVENTS:

N/A

MOTHER LIQUORS AND WASHES:

CONSIDERING THE WASH IS BETWEEN 6 AND 8 PH WE WILL DISPOSE OF IT IN THE PROVIDED SEWER

FACILITY.
WASTE SOLIDS:

GLYCERIN WASTE WILL BE PUT INTO A DRUM AND SOLD.

BRANDON HIGH SCHOOL

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INCREMENT SECTION:

COMPLETE THE TABLE BELOW WITH THE RAW MATERIAL LOTS AND QUANTITIES. CONFIRM THAT THE
MATERIALS HAVE BEEN RELEASED FOR USE BY QUALITY ASSURANCE.

ITEM NUMBER

BRANDON HIGH SCHOOL

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MATERIAL DESCRIPTION

LOT
NUMBER

LOT RELEASE
CONFIRMED
BY

PLANNED
QUANTITY

CANOLA OIL

0001

159.62

METHANOL

0002

52.61

CATALYST NAOH

0003

1.064

K
G
K
G
K
G

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MATERIAL SAFETY PRECAUTIONS

INPUT MATERIAL
CANOLA OIL
NAOH SOLUTION
METHANOL
OUTPUT MATERIALS
BIODIESEL
GLYCEROL
WASTE WATER
THE GLYCEROL AND THE BIODIESEL WITH BOTH BE PLACED IN BARRELS. THE GLYCEROL WILL BE SOLD IN THE BARRELS.
MSDS MATERIAL SAFETY SHEETS AVAILABLE UPON REQUEST

BRANDON HIGH SCHOOL

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GENERAL CHEMICAL SAFETY PRECAUTIONS

LAST UPDATE: 01/20/10
THE FOLLOWING SAFETY PRECAUTIONS APPLY TO ALL PROCESS CHEMICALS UNLESS A SPECIFIC CHEMICAL MSP PROVIDES DIFFERENT
OR ADDITIONAL INFORMATION.
USE LOCAL EXHAUST VENTILATION WHEN AVAILABLE.
MINIMIZE OPEN TRANSFERS. AVOID TRANSFERS OF HOT SOLUTIONS ABOVE 37.8 C (100 F) USING NORMAL CHEMICAL HOSES.
INSPECT ALL CHEMICAL TRANSFER HOSE FOR INTEGRITY.
PRACTICE GOOD PERSONAL HYGIENE. WASH PRIOR TO LUNCH AND BREAKS. DO NOT CONSUME FOOD OR BEVERAGES IN
MANUFACTURING AREAS.
FLUSH EYES OR SKIN AFTER CHEMICAL EXPOSURE WITH WATER IN AN EMERGENCY EYEWASH OR SHOWER STATION FOR 15 MINUTES
AND SEEK MEDICAL ATTENTION.
IMMEDIATELY REPORT ALL CHEMICAL EXPOSURES, SYMPTOMS OF EXPOSURE, ILLNESSES AND INJURIES TO THE AREA SUPERVISOR OR
SEEK MEDICAL ATTENTION.
FLUSH SMALL LIQUID SPILLS TO THE CHEMICAL SEWER WITH EXCESS WATER. SWEEP UP DRY POWDER SPILLS AND PLACE IN A
SUITABLE CONTAINER FOR FUTURE DISPOSAL OR FLUSH WITH EXCESS WATER TO THE CHEMICAL SEWER. USE APPROPRIATE PERSONAL
AND RESPIRATORY PROTECTIVE EQUIPMENT. REPORT ALL SPILLS TO THE PILOT PLANT MANAGER. RESPOND ONLY TO SPILLS
THAT ARE WITHIN YOUR RESPONSE CAPABILITIES. REPORT L
ARGER SPILLS TO ENVIRONMENTAL COMPLIANCE MANAGER.
USE WATER, CARBON DIOXIDE, DRY CHEMICAL, OR FOAM ON MOST INCIDENTAL FIRES UNLESS SPECIFIC FIRE FIGHTING MEDIA IS
RECOMMENDED IN THE CHEMICAL MSP (I.E., FOR PYROPHORIC AND WATER REACTIVE CHEMICALS). REPORT ALL FIRES TO PILOT
PLANT AND ENVIRONMENTAL COMPLIANCE MANAGERS.
IN EVENT OF AN EMERGENCY, OPERATORS SHOULD SAFETY SHUTDOWN CHEMICAL CHARGES AND HOSE
TRANSFERS ONLY IF NO HAZARD TO PERSONNEL. OTHERWISE EVACUATE.
EQUIPMENT STARTUP FOLLOWING A CHEMICAL RELEASE, FIRE, EXPLOSION, EMERGENCY EVACUATION OR OTHER EMERGENCY
EQUIPMENT SHUTDOWN MUST BE CONDUCTED UNDER THE DIRECTION OF THE PILOT PLANT MANAGER. CHEMICAL OPERATORS MUST
USE APPROPRIATE CARE NOT TO INTRODUCE A HAZARD INTO THE PROCESS DURING EQUIPMENT RESTART PROCEDURES.
DO NOT LIFT OR HANDLE HEAVY DRUMS OR BAGS ALONE. IF DRUM OR BAG WEIGHS MORE THAN 55 POUNDS, ASK FOR HELP OR USE
AVAILABLE MECHANICAL ASSIST DEVICES. USE LIFT TRUCKS, DRUM HANDLERS OR OTHER EQUIPMENT TO MOVE HEAVY LOADS. AVOID
AWKWARD POSITIONS WHEN HANDLING AND CHARGING MATERIALS.

BRANDON HIGH SCHOOL

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FLAMMABLE MATERIAL SAFETY PRECAUTIONS

LAST UPDATE: 11/15/09
CHEMICALS THAT HAVE A FLASH POINT LESS THAN OR EQUAL TO 37.8 C (100 F) ARE FLAMMABLE AND THOSE WITH A FLASH POINT
BETWEEN 37.8 C (100 F) AND 115.5 C (240 F) ARE COMBUSTIBLE.
TRANSFER FLAMMABLE CHEMICALS ONLY IF FIRE PROTECTION SYSTEMS ARE FUNCTIONAL.
MAINTAIN 35 FEET BETWEEN ALL TYPE I HOT WORK AND ALL OPEN TRANSFERS OR HOSE TRANSFERS OF FLAMMABLE AND
COMBUSTIBLE CHEMICALS.
MAINTAIN 10 FEET BETWEEN ALL TYPE II HOT WORK AND ALL OPEN TRANSFERS OR HOSE TRANSFERS OF FLAMMABLE AND
COMBUSTIBLE CHEMICALS.
FOLLOW PROPER INERTION AND GROUNDING PROCEDURES WHEN HANDLING FLAMMABLE AND COMBUSTIBLE CHEMICALS.
USE AN EAGLE MONITOR TO EVALUATE OXYGEN AND LEL CONCENTRATIONS.
IF A LARGE SPILL OCCURS, ISOLATE AREA AND EVACUATE. IF NO RISK, STOP LEAK (BY CLOSING VALVE, STOPPING SOLVENT PUMPS,
ETC.) AND ELIMINATE IGNITION SOURCES. CALL 911 TO OBTAIN ASSISTANCE FROM OTTAWA COUNTY HAZMAT TEAM OR THE

HOLLAND TOWNSHIP FIRE DEPARTMENT.

PPE REQUIREMENTS
LAST UPDATED: 11/15/09
EMPLOYEES MUST WEAR THE SPECIFIED PPE. EMPLOYEES MAY ALWAYS WEAR ADDITIONAL PPE PROVIDING A HIGHER LEVEL OF
PROTECTION. ENGINEERING CONTROLS, SUCH AS SPRAY BALLS, SHOULD ALWAYS BE USED TO MINIMIZE THE NEED FOR PPE.
PPE REQUIRED FOR ROUTINE ACTIVITIES INCLUDES: UNIFORM, SAFETY SHOES, SAFETY GLASSES, BUMP CAP OR HARD HAT.
EYE PROTECTION WHEN HANDLING HAZARDOUS CHEMICALS INCLUDES THE FOLLOWING OPTIONS: (1) GOGGLES; (2) FACE SHIELD
OVER SAFETY GLASSES; (3) FULL FACE RESPIRATOR
GLOVE PROTECTION IS NORMALLY THE BLACK PVC (BLACK KNIGHT) UNLESS ANOTHER GLOVE IS SPECIFIED.
EYE PROTECTION AND GLOVES MUST BE USED WHENEVER OPENING OR CLOSING HAND VALVES OR WHEN DISCONNECTING FITTINGS OR
CHEMICAL TRANSFER HOSE.
A RUBBER APRON, EYE PROTECTION AND GLOVES MUST BE USED WHEN COLLECTING SAMPLES THAT MAY BE AT HIGH TEMPERATURE
(> 50 C) OR THAT MAY BE CORROSIVE (PH < 4; PH > 10).

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INERTION PROCEDURES
LAST UPDATE: 11/15/09
PRESSURE/VACUUM UNIT CONVERSION
1 ATMOSPHERE = 14.7 PSIA = 0 PSIG = 760 MM MERCURY (HG) ABSOLUTE = 29.92 IN HG ABSOLUTE
VACUUM PURGE PROCEDURE
THIS PROCEDURE WILL REDUCE OXYGEN CONTENT TO LESS THAN 5%. IT IS NOT INTENDED TO REMOVE ALL SOLVENT VAPOR FROM A
VESSEL. TO INERT, SEAL THE VESSEL, AND:
1. PULL VACUUM TO 24 INCHES HG; OR
2. PULL VACUUM UNTIL PRESSURE IN VESSEL IS 150 MM HG ABSOLUTE.
IF NECESSARY, BREAK VACUUM WITH FILTERED NITROGEN.
IF SUFFICIENT VACUUM IS NOT AVAILABLE TO ACHIEVE THE ABOVE VACUUM CONDITIONS, SEAL THE VESSEL, AND:
1. PULL VACUUM TO AT LEAST 15 INCHES OF HG. BREAK VACUUM WITH FILTERED NITROGEN. THEN PULL VACUUM TO AT LEAST 15
INCHES OF HG; OR
2. PULL VACUUM UNTIL PRESSURE IN VESSEL IS 300 MM HG ABSOLUTE. BREAK VACUUM WITH FILTERED NITROGEN. THEN PULL
VACUUM UNTIL PRESSURE IN VESSEL IS 300 MM HG ABSOLUTE.
IF NECESSARY, BREAK VACUUM WITH FILTERED NITROGEN.
FLOW-THROUGH PURGE PROCEDURE
THIS PROCEDURE WILL REDUCE OXYGEN CONTENT TO LESS THAN 5%. IT IS NOT INTENDED TO REMOVE ALL SOLVENT VAPOR FROM A
VESSEL. TO INERT, SEAL THE VESSEL, OPEN VESSEL VENT, ASSURE OTHER VENTS ARE CLOSED, APPLY FILTERED NITROGEN THROUGH
THE BOTTOM VALVE UNTIL ABOUT FOUR VESSEL VOLUMES OF NITROGEN HAVE FLOWED THROUGH THE VESSEL. MONITOR THE
OXYGEN CONCENTRATION AND CONTINUE THE FLOW-THROUGH PURGE UNTIL THE OXYGEN CONCENTRATION IS LESS THAN 5%.

MANUAL PRESSURE PURGE PROCEDURE

THIS PROCEDURE WILL REDUCE OXYGEN CONTENT TO LESS THAN 5%. IT IS NOT INTENDED TO REMOVE ALL SOLVENT VAPOR FROM A
VESSEL. TO INERT, SEAL THE VESSEL AND PRESSURIZE WITH FILTERED NITROGEN TO AT LEAST 15 PSIG. VENT VESSEL TO LESS THAN
1 PSIG. REPEAT THIS PROCEDURE TWO MORE TIMES.

SOLIDS CHARGING PROCEDURE (APPLIES TO EITHER WET OR DRY SOLIDS)

INERT THE VESSEL. INITIAL INERTION SHOULD ACHIEVE AN OXYGEN CONCENTRATION OF 1% OR LESS. CHARGING MUST BEGIN
IMMEDIATELY. MAINTAIN A SLOW FILTERED NITROGEN PURGE WITH THE SCRUBBER VENT OFF TO RETAIN INERT CONDITIONS DURING
SOLIDS CHARGING. IF DELAYS ARE ENCOUNTERED, THE INERTION MUST BE RE-CHECKED. MONITOR THE OXYGEN CONCENTRATION AT
LEAST EVERY FIVE MINUTES AND RE-INERT IF OXYGEN CONTENT IS 5% OR HIGHER.

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SOLVENT RINSE FOR VESSELS PROCEDURE

WHENEVER POSSIBLE, AVOID CLEANING OPEN VESSELS WITH FLAMMABLE SOLVENTS. WHEREVER POSSIBLE, USE CLEAN IN PLACE
(CIP) TECHNOLOGY SUCH AS SPRAYBALLS.
THE FOLLOWING PROCEDURE APPLIES WHEN CLEAN IN PLACE TECHNOLOGY IS NOT FEASIBLE. THIS PROCEDURE APPLIES TO VESSEL
RINSING CONDUCTED THROUGH AN OPEN HATCH USING A POLAR SOLVENT SUCH AS ACETONE OR METHANOL. RINSING WITH A NONPOLAR SOLVENT SUCH AS TOLUENE IS NOT PERMITTED. INERT THE VESSEL. MAINTAIN A SLOW FILTERED NITROGEN PURGE WITH THE
ROTOCLONE OFF, USING LOCAL EXHAUST VENTILATION JUST OUTSIDE THE HATCH. MONITOR THE VESSEL TO ASSURE THAT THE
OXYGEN CONCENTRATION IS LESS THAN 5%. WEAR A SUPPLIED AIR RESPIRATOR AND PROCEED WITH VESSEL RINSING WITHOUT
DELAY. MONITOR THE OXYGEN LEVEL ABOUT EVERY FIVE MINUTES DURING VESSEL RINSING. THE OXYGEN CONCENTRATION MUST
REMAIN BELOW 5%.
SOLVENT RINSE FOR CENTRIFUGES PROCEDURE
THIS PROCEDURE APPLIES TO CENTRIFUGE RINSING WITH A POLAR SOLVENT SUCH AS ACETONE OR METHANOL. RINSING WITH A NONPOLAR SOLVENT SUCH AS TOLUENE IS NOT PERMITTED. DO NOT USE MORE SOLVENT THAN IS REQUIRED FOR ADEQUATE CLEANING.
WEAR A SUPPLIED AIR RESPIRATOR AND PROCEED WITH CENTRIFUGE RINSING WITHOUT DELAY.

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EQUIPMENT REQUIREMENTS & LIMITATIONS

80 L GLASS LINED REACTOR (#333) - 150 PSI MAWP RATED VESSEL EQUIPPED WITH A 2 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 75 PSI RUPTURE DISK.
120 L GLASS LINED/STAINLESS POT/FRACTIONATING STILL (#334) - 150 PSI MAWP RATED VESSEL EQUIPPED WITH A 2 INCH
EMERGENCY RELIEF VENT TO CONTAINMENT AND 75 PSI RUPTURE DISK.
120 L GLASS LINED REACTOR (#351) - 150 PSI MAWP RATED VESSEL EQUIPPED WITH A 2 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 130 PSI RUPTURE DISK.
200 L GLASS LINED STILL (#331) - 150 PSI MAWP RATED VESSEL EQUIPPED WITH A 3 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 90 PSI RUPTURE DISK.
200 L GLASS LINED REACTOR (#332) - 150 PSI RATED VESSEL EQUIPPED WITH A 3 INCH EMERGENCY RELIEF VENT TO CONTAINMENT
AND 90 PSI RUPTURE DISK. .
400 L GLASS LINED STILL (#324) - 150 PSI MAWP RATED VESSEL EQUIPPED WITH A 3 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 90 PSI RUPTURE DISK.
400 L GLASS LINED REACTOR (#325) - 150 PSI RATED VESSEL EQUIPPED WITH A 3 INCH EMERGENCY RELIEF VENT TO CONTAINMENT
AND 90 PSI RUPTURE DISK.
400 L HASTELLOY REACTOR (#261) - 100 PSIG MAWP RATED VESSEL EQUIPPED WITH A 3 INCH EMERGENCY RELIEF VENT TO ROOF
AND 100 PSIG RUPTURE DISK.
400 L HASTELLOY REACTOR (#262) - 100 PSIG MAWP RATED VESSEL EQUIPPED WITH A 2 INCH EMERGENCY RELIEF VENT TO ROOF
AND 100 PSIG RUPTURE DISK.
800 L STAINLESS STEEL STILL (#352) - 150 PSIG MAWP RATED VESSEL EQUIPPED WITH A 4 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 100 PSIG RUPTURE DISK.
800 L STAINLESS STEEL STILL (#353) - 150 PSIG RATED VESSEL EQUIPPED WITH A 4 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 100 PSIG RUPTURE DISK.
800 L GLASS LINED STILL (#121) - 150 PSI MAWP RATED VESSEL EQUIPPED WITH A 4 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 100 PSI RUPTURE DISK.
800 L GLASS LINED REACTOR (#122) - 150 PSI RATED VESSEL EQUIPPED WITH A 4 INCH EMERGENCY RELIEF VENT TO CONTAINMENT
AND 100 PSI RUPTURE DISK.
2,000 L GLASS LINED STILL (#131 OR #134) - 100 PSI RATED VESSEL EQUIPPED WITH A 6 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 100 PSI RUPTURE DISK.
2,000 L GLASS LINED REACTOR (#132 OR #135) ) - 100 PSI RATED VESSEL EQUIPPED WITH A 6 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 100 PSI RUPTURE DISK.

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4,000 L GLASS LINED STILL (#141 OR #143) - 100 PSI MAWP RATED VESSEL EQUIPPED WITH AN 8 INCH EMERGENCY RELIEF VENT
TO CONTAINMENT AND 100 PSI RUPTURE DISK.
4,000 L GLASS LINED REACTOR (#142) - 100 PSI MAWP RATED VESSEL EQUIPPED WITH AN 8 INCH EMERGENCY RELIEF VENT TO
CONTAINMENT AND 100 PSI RUPTURE DISK.
40 INCH HASTELLOY CENTRIFUGES
ATMOSPHERIC SCRUBBER;

BRANDON HIGH SCHOOL

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(#137 OR #144),

PROCESS

TOP UNLOADING

SCRUBBER

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EMERGENCY RELIEF VENT SIZING

EMERGENCY RELIEF VENT SIZING HAS BEEN PERFORMED FOR THE VESSELS LISTED ABOVE FOR PROCESS CONDITIONS
DESCRIBED IN THE BATCH RECORD. IT IS CRITICAL TO PERFORM BATCH CARD ACTIVITIES AS DESCRIBED. CHARGING THE WRONG
MATERIAL OR CHARGING MATERIALS IN THE WRONG ORDER OR TOO QUICKLY COULD CAUSE VESSEL HEATING AND/OR GAS
GENERATION THAT MAY EXCEED THE EMERGENCY VENTING CAPABILITIES OF THE VESSEL. WHEN CHOOSING ALTERNATE VESSELS
DIFFERENT FROM THOSE LISTED IN THE BATCH RECORD, ASSURE THAT A VESSEL OF EQUAL OR LARGER SIZE IS CHOSEN.
DEFLAGRATIONS INVOLVING FLAMMABLE VAPOR CAN NOT BE VENTED SAFELY. PROPER VESSEL INERTION MUST BE
PROVIDED TO PREVENT THE POTENTIAL FOR DEFLAGRATIONS WHEN USING FLAMMABLE LIQUIDS OR GASES.
SEE

PSM GUIDELINE 116 EMERGENCY RELIEF VENT SIZING FOR MORE INFORMATION.

CHEMICAL PROCESS HAZARDS EVALUATION

NO PRECAUTIONS BEYOND THOSE NOTED IN THE GENERAL CHEMICAL SAFETY PRECAUTIONS

ABOVE.

PERSONAL SAFETY
NO PRECAUTIONS BEYOND THOSE NOTED IN THE SAFETY PRECAUTION SECTIONS ABOVE.
EQUIPMENT SAFETY
SEE OTHER PERTINENT INFORMATION IN THE SAFETY PRECAUTION SECTIONS ABOVE.

WASTE DISPOSAL
SPENT / DISTILLED SOLVENTS:

N/A

MOTHER LIQUORS AND WASHES:

CONSIDERING THE WASH IS BETWEEN 6 AND 8 PH WE WILL DISPOSE OF IT IN THE PROVIDED SEWER

FACILITY.
WASTE SOLIDS:

GLYCEROL WASTE WILL BE PUT INTO A DRUM AND SOLD.

SAMPLE HANDLING
USE SAFETY PRECAUTIONS NOTED IN SECTIONS ABOVE.
CHEMICAL REACTION HAZARD LAB REVIEW

REF:

REACTION CALORIMETRY FOR ALL SYNTHESIS REACTIONS;

DSC FOR ALL RAW MATERIALS, INTERMEDIATES, FINAL PRODUCTS, WASTE PRODUCTS THAT WILL BE
HEATED/DISTILLED/CONCENTRATED, ETC.

OTHER PERTINENT INFORMATION

BRANDON HIGH SCHOOL

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MATERIAL FLOW BALANCE SHEET

KGS
159.62

INPUT
CANOLA OIL

OPERATION
START UP

KGS

52.61

METHANOL

REARRANGEMENT

31.68

1.064

NAOH

24.25

WATER

PHASE SEPARATION
PACKAGE PRODUCT

29.02
176.8
237.5

237.5

TOTAL INPUT

BRANDON HIGH SCHOOL

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OUTPUT

REMARKS

DRUM PRODUCT

GLYCEROL

WATER/WASTE
BIODIESEL
TOTAL OUTPUT

DRUM PRODUCT

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CHEMICAL PROCESS PROJECT TEAM

THE MEMBERS OF THE PROJECT TEAM, LISTED BELOW REVIEWED THE PROCESS AND THE SUITABILITY OF THE
EQUIPMENT FOR ITS INTENDED USE PRIOR TO INITIATION OF WORK IN THE PRODUCTION AREA.

CUSTOMER REPRESENTATIVE

DATE

PILOT PLANT MANAGER

DATE

PROCESS TECHNICIAN

DATE

PROCESS TECHNICIAN

DATE

PROCESS TECHNICIAN

DATE

PROCESS TECHNICIAN

DATE

BRANDON HIGH SCHOOL

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THE PROCESS:
1. PREPARE REACTOR #325 FOR HEATING AND STIRRING CANOLA OIL. BY
A.

BE SURE THAT THE REACTOR IS DRY CK

2. PREPARE 159.62 KG CANOLA OIL BY

3. PREPARE REACTOR #333 FOR MIXING METHANOL AND NAOH. BY
4. ADD NAOH TO METHANOL BY A INTEGRAL CHARGING FUNNEL WITH THE TANK INERTED WITH NITROGEN GAS. BY

CK

5. HEAT THE OIL IN REACTOR #325 TO 45C NOT EXCEEDING 50C WHILE RAPIDLY STIRRING. WHEN THE CORRECT TEMPERATURE HAS
BEEN REACHED, TURN OFF THE HEAT.

BY

6. ADD THE NAOH/METHANOL MIXTURE TO REACTOR #325 BY

7.

STIR FOR

CK

3 HOURS BY

8. STOP STIRRING BY
9.

AGITATE THE MIXTURE FOR TO ALLOW IT TO SEPARATE BY

10. AFTER ALLOWING THE MIXTURE TO SEPARATE, YOU SHOULD NOTICE 2 DISTINCT LAYERS. SEPARATE THE BOTTOM LAYER. STORE
EXCESS GLYCEROL IN DRUM TANK.

11. POUR BIODIESEL LAYER INTO A TANK WITH A LOCAL EXHAUST SYSTEM.
12. STIR/HEAT BIODIESEL. HEAT BIODIESEL TO 80C FOR 100 MINUTES, WHILE STIRRING.
13. WHEN BIODIESEL HAS COOLED, STORE IN DRUM TANK.

BRANDON HIGH SCHOOL

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BRANDON HIGH SCHOOL

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