UDC 621.643.2-462.31-034.14.018.7 :620.1 been used throughout as the decimal marker, The subclauses marked @ gh ‘specifications which are optional and may be agre 55 Weldability 56 Hot working and heat treatment 57 Surface appearance 5B Leak tightness 59. Imperfections 1 Field of application ‘This standard specifies requirements for seamless circulat tubes manufactured from the steel grades listed in table 1 ‘Such tubes are main intended for use in chemical plants for high pressure applications at service temperatures of 200°C ‘or more and simultaneous exposure to hydrogen (eg. boler (or heat exchanger tubes) 2 Concept ‘Stee! for hydrogen service at elevated temperature and pres- ‘sure is steel that isnot readily susceptibie to decarburization by hydrogen at elevated pressures and temperatures and thus to hydrogen and grain boundary embrittlement. This characteristic is achieved by adding alloying elements that form carbides at the operating temperature Seamless circular steel tubes for hydrogen service at elevated temperatures and pressures Technical delivery conditions "Nahtlose kreistérmige Rohe aus druckwasserstottbestangigen Stahlen; technische Lieferbedingungen |n keeping with current practice in standards published by the International Organization for Standardization (ISO), comma has specifications which are tobe agreed upon atthe time of ordering, and those marked @@ give upon at the time of ordering, Contents 1. Feld of application 1 Pose 530 Dimensions, tolerances and mass per unit 2 Concept 1 bev . rade 1 3 Stool or 8 Testing 3 4. Designation and ordering 1 61 Materais testing certificates 3 4.1 Standard designation 1 62 Test site 3 42 Essontial order details 2 63. Scope of testing 4 43 Optional order details 2 64 Sampling and sample preparation 4 65 Tost procedure, 4 5. Requirements 2 ‘51 Manufacturing process 2 86 Retests . 52 As delivered condition 2 7 Marking 5 53 Chemical composition 2 54 Mechanical properties .. 2 8 Complaints 5 2 3 3 3 3 November 1990 EHOSA ‘Appendix A Estimated creep limit and stress rupture. land elevated temperature tensile strength values 2 ‘Appendix 8 Information on temperatures required for hot working and hes ‘treatment 8 3 Steel grades 3A The specitications of ths standard relate to tubes made from the steel grades listed in table 3.2 @ The selection of the steel grade is at the pur Chaser's discretion, 4 Designation and ordering 41° Standard designation ‘The standard designation of tubes covered In this standard shall give, inthe folowing order = the name of product (tube); ~~ the number of this standard (OIN 17 176) ~ the characteristic dimensions of the tube (outside diam: ter x wall thickness); Continued on pages 2 to 16 127ae Page 2 INIT 176 = the material designation or number denoting the steel grade (ct. table 1); = the symbol denoting the heat treatment condition, for steel grades 12 CrMo 195 and X 12 CrMo 9 1 Example ‘Atube complying wit this standard, with an outside diameter of 127 mm and a wall thickness of 28 mm, made from ste 42 CrMo 195 (material number 1.7362), in the annealed con- ition (G), shall be designated: Tube DIN 17 176 - 127 x 28-12 CrMo195G Tube DIN 17 176-127 x 28 - 1.7362 42 © Essential order details ‘The following order details are essential when ordering tubes fas specified in this standard. 4.24 Quantity (eg. desired total length of tubes in @ con- signment) 4.2.2. Name of product (tube). 42.3 Number of this standard (OIN 17 176). 4.24 Characteristic dimensions of tube (outside diameter wall thickness). 4.2.5 Material designation or number denoting the steel ‘grade (cf, table 1). 4.2.6 Symbol denoting the heat treatment condition on delivery (cf. table 3). 4.2.7 Type of length (ct. table 5), an unt length in the case (of Specified and exact lengths. 428 Type of DIN 50.049 centfica inthe case of third party inspection, the testing agency and ‘any specifications to be complied with, Example of an order: +1000 m tube DIN 17 176-127 x 28-12. CrMo 195, in as manufactured lengths, with DIN 50049 - 3:1 C certificate. 43 @@ Optional order details ‘The essential order detalls may, if so agreed, be supple- mented by one or more of the following items. 434 St making process used (cf. subclause 5.11.2) 4.3.2 Check of chemical composition (by product analysis) (Ct subclause 532). 4.3.3 Hardness testing (of. subclause 635). 4.34 Testing of elevated temperature 0.2 % proof strength (ct subclause 636) 4.35. Non-destructive testing for transverse imperfections ‘andor laminations (cf. subciause 592) 4.3.6 Test pressure if higher than specified here (ct. sub- clause 6561) 5 Requirements 5.1 Manufacturing process 5.1 The steel shall be produced either by an electric pro- cess or by the basic oxygen process. 128 SA1.4 @@ If s0 agreed, a different but equivalent pro: ‘cess may be used. 5.1.1.2 @@ If soagreed, the purchaser shall be informed of the steelmaking process used. 5.1.2 Tubes shall be produced by hot or cold roling, hot pressing, hot or cold drawing, or by a combination of these processes, at the manufacturer's discretion. 5.2 As delivered condition ‘Tubes shall be supplied in one of the heat treatment condi tions sted in table 3. Provided that hot forming ensures an adequately homiogene- ‘ous microstructure, I may be sutficient to temper instead of ‘quenching and tempering tubes made from steel 13 CrMo 4 4 {and 10 CrMo 910, 5:3 Chemical composition 53.1 Ladle analysis ‘The chemical composition as determined by ladle analysis") shall comply with the specifications of table 1. 632 @@ Product analysis Aproduct analysis may be agreed atthe time of ordering ‘see table 7 for scope of testing). When a product analysis 1- ried out, the results may deviate from the values given in table 1 by the amounts listed in table 2 5.33 Deviations With the consent of purchaser or his representative, minor deviations of the chemical composition from the limiting values specified for the ladle analysis and product analysis are permitted provided that they do not adversely affect the ‘mechanical properties, resistance to hydrogen attack and weldabllty of the tube. 5.4 Mechanical properties 54.1 The yield strength, tensile strength, elongation after fracture and impact strength of tubes in their as delivered ‘condition (et. subclause 52) and under the conditions speci- fied in subclauses 64 and 65 shall at ambient temperature, ‘comply with the specifications given in table 3, and the vated temperature proot strength, with those given in table 4 A141 @@ Ahardness test for hocking the homogeneity ‘of the batch in terms of mechanical properties (ct. subclause 635) may be agreed. 54.2 Tables A and A2 give estimated values of 1% creep limit, stress rupture and elevated temperature tensile strength, 64.21 The 1% creep limit and stress rupture values speci fied in table A. for elevated temperatures shall not be t ‘to mean that stee! can be subjected o these temperatures ‘continuous service the imitations in their use being governed by the overall oad inservice and their resistance tohydrogen attack as defined in API Publication 941, 5.5 Weldability 1551 Tubes made from steel as specified here {or arc welding and pressure welding. e suitable +) When sequential castings are supplied, asis possible in the ‘case of continuously cast tubes, the term ‘cast’ should be read as ‘casting unit.ain 5.5.2 However, as set out in DIN 8528 Part 1, weldabilty is ‘ot only a function of the steel grade but also of the welding Conditions, of the design and of the service conditions to ‘which the component willbe submitted, 5.5.3 Any welding filer metal required isto be solected on the basis of DIN 8575 Part 1. 5.6 Hot working and heat treatment ‘Table 8.1 provides information on the temperature for hot working and heat treatment. 5.7 Surface appearance 5.74 Tubes shall have a smooth internal and external sur- face consistent with the manufacturing process. 15.7.2 Slight surtace irregularities such as scabs, seams, sv- fers oF gouges resulting from the manufacturing process ere permitted provided thatthe wall thickness after dressing con- tinues to meet the requirements specified in subclause 5.10.2 {and the performance of the tube isnot adversely affected (cf. subclause 81). 5.7.3 _ Dressing of imperfections by grinding or machining is permitted provided that the wall thickness after dressing con- tinues to meet the requirements specified in subciause 5102. Stopping of surface defects is not permitted, while making {00d of such defects by welding is only permitted with the purchaser's consent, 5.8 Leak tightness Tubes shall remain tight when tested as specified in sub- clause 6586. 5.9 Imperfections 5.9.1 When tubes are checked for longitudinal impe tions by non-destructive methods as specitid in subciaus 1658, the requirements glvenin Stah-Eisen-Prfbltt (iron and steel test sheet) 1915 shall be met 59.2 @@ If s0 agreed at the time of ordering, tubes are tested by non-destructive methods for transverse imperte tions andlor laminations, the requirements given in Stat Eisen-Prifolatter 1918 and 1918 shall be futfiled (ct. sub- clauses 659 and 6.510) 5.10 Dimensions, tolerances and mass per unit length $101 © Dimensions 5.10.14 After consultation with the manufacturer, the pur- ‘chaser is to specty the tube outside diameters and wall thick- esses required, preference being given to the dimensions specified in DIN 2448 and DIN 2391 Part 1 5401.2 Table 5 shall be observed when specifying the tube length. {5.10.2 Dimensional tolerances ‘The outside diameter and wall thickness are subject to the limit deviations specified in table 6. ‘At points where the surface of the tube has been dressed by ‘mechanical means (eg. by grinding), the actual outside diam ‘ter may be less than its lower DIN 17176 Pages 510.3 Geometrical tolerances $10.91 Circularity Tubes shall be as ciccular as possible. For tubes thet are not solution quenched and tempered, the circularity tolerance, R, (of the barrel shall be within the limit deviations specified for ‘the outside diameter (ct. table 6), R being equal to 2% for ‘solution quenched and tempered tubes (cl. subclause 65:12). ‘The circularity tolerance, as a percentage, shall be det mined using the following formula: p20. Samm tanin whore d mass the greatest and dj minis the smallest outside lameter measured. Note. itis permitted that max OF dyin @xC0ed the upper or lower limit of size specified in table 6. 5103.2 Straightness Tubes shall be straight to the eye. 5.10.4 Finish of tube ends all be cut square with the tube axis and be free from 5105 Tolerances on mass per unit length Caleulation ofthe mass per unit length shall bein accordance with 80 4200, taking. however, the density a 7,76 kg/dm® for {rade X 20 CiMoV 12 1 (material number 14822). The actual mass may deviate from the values s0 obtained by 9% fora single tube, and +12% for a consignment of not 85 than 10 6 Testing 6.1 Materials testing certificates Tubes complying with this standard shallbe supplied with one of the DIN 50 049 certificates: ') certificate DIN 50 049 - 31 A (inspection certificate A); ) certificate DIN 60 049 - 31 8 (inspection certificate 8); ©) certificate DIN 50 049 ~ 31. {inspection certificate C). ‘Table 7 summarizes the types and scope of tests to be per: formed as pert of inspection and indicates the associated cortficates. Inspection certificates shall give the following details: @) results of tests as described in subclause 63 and Ccaried out in accordance with subclause 65; 'b) details and reouits of any additional checks or tests ‘agreed (ct. subciause 43); (©) marking (ef, clause 7) Moreover, a DIN 50 049 ~ 22 certificate (test report) giving the results of the ladle analysis forall the elements listod in table 1 forthe steel grade concemed shall be issued. These sults may also be reported in the inspection certificate. Inspection certificates shall cleary correlate tube marking ‘and associated results. 6.2 Test site ‘Tubes shallbe tested at the manufacturer's works Production shall not be unduly disturbed when acceptance inspection is ‘carried out by experts who are not employees of the manu- tacturer. 1295% Page 4 DIN 17176 6.3 Scope of testing 6.31 Tubes shall be inspected by batches, testing of as ‘manufactured lengths being permitted, in which case this shall be indicated in the certificate. Soe table 7 for details. 6.3.1.1. For the purposes of testing, tubes shall be divided according to steel grade, cast and size, into batches each ‘comprising 100 units. Remainders of up to 50 units may be distributed uniformly across the other batches, remainders: ‘over 50 units and consignments of less than 50 units being ‘considered a whole batch. 632 For testing as described in subclauses 651 to 656, ‘wo sample tubes shallbe taken from the frst two batches (ct subclause 63.1) and one sample tube from each further batch, as selected by the inspector taking care to ensure that all casts are represented by the samples taken, 6.3.3 One testtube each shall be taken from consignments fF batches containing not more than ten tubes. 6.3.4 Thefollowing test tubes: 2) tensile test at ambient temperature; ») impact test on tubes made trom grades 25 CrMo 4, X20 CrMoV 121 and 20 CrMoV 188 and having a wal thickness exceeding 10 mm: for the other grades, this test shall be performed on tubes witha wall thickness exceed- ing 30 mm. alle carried out on the sample 635 @@ If Brine hardness testing has been agreed the time of ordering, each tube shall be tested. Where pos- ile, the tube with the minimum hardness shall be subjected toa tensile test and that with the maximum hardness, to an impact test 636 @@ Itvorification ofthe elevated temperature 0.2% root strength has been agreed at the time of ordering, the test temperature shall be stated. Unless otherwise agreed, ‘one sample per cast and size shall be tested 637 @@ It performance of a product analysis has been agreed at the time of ordering, one sample tube shall be ‘checked. 6.3.8 Furthermore, each tube shall be 6.381 tested, at the manufacturer's works, for leak tight- ness, normally by an internal hydrostatic pressure test (ct subclause 65.6); 6.3.82 subjected, at the manufacturer's works, o a mate- ‘als identity test; 6.3.83 inspected for surface appearance; 6.3.84 inspected for its accuracy to size (cf, subclause 5:10); 6.3.85 subjected, at the manufacturer's works, to non-de- structive testing for longitudinal imperfections (ct. subclause 658) 63.851 @@ If so agreed at the time of ordering, each tube shall be tested for transverse impertections andor lam- inations by @ non-destructive method (cf. subclauses 659 ‘and 65.10) 63.86 Both ends of tubes with a wall thickness smaller ‘than 40 mm shall be subjected to a fattening test for each as manufactured length (ct. subclause 654) 6.3.87 Tuboswith awall thickness greater than 40mm shall be subjected to a non-destructive test instead ofa flattening 130 text tostng bog cra out on both tube ends over alenath 28 mms dosed San oer Pian 1D ot sae Giavse 6510) 6.4 Sampling and sample preparation See figure for location and orientation of test pieces. 641 Tensile test 64.11. Forthe tensile test, a plate specimen as specified in DIN "50140 or a cylindrical test piece as specified in DIN 50 125 shall be taken parallel to the tube axis. Test piece land specimen shall not be heat treated nor straightened within the gauge length. For tubes with a wall thickness exceeding 30 mm, the centre line ofthe cylindrica test piece shall run ata distance of one quarter of the wall thickness from the external surface or as close as possible to this point 6.41.2 At the discretion of the manufacturer, samples may bbe taken transverse to the tube axis and machinednto flat or cylindrical test pieces (cf. DIN 50 125) in the case of tubes with fan outside diameter of 200 mm or more, provided that no rior straightening of the material is required. 64.2. Impact test For the impact test, a set of three ISO V-notch test pieces shall be taken transverse to the tube axis provided that no prior straightening of the material is required. Otherwise, the test pieces shall be taken parallel to the tube axis. For tubes with a wall thickness exceeding 30 mm, the centre line of the eylinarcal test pieces shall run ata distance of one quarter of the wall thickness from the external surface or as close as possible to this point. ‘The test pieces shall be taken and prepared so that the notch ‘axis runs at right angles to the tube surface. 64.3 Flattening test The test pieces for the fattening test as described in DIN 50 136 shall be taken from both ends of an as manu: {actured length, the end from which the test piece was taken being clearly identified Ht ends of as manufactured lengths are cut into sections, no further test pieces need be taken from such sections pro vided that these can be traced to the original tube tested by ‘means of suitable marking. 6.44 Chemical composition For performing a product analysis, sample chips shall oe taken at points uniformly distributed over the wall thickness, this also applying where a spectral analysis is to be carried ‘Out. Unless otherwise specified, sampling shall be in accord- ‘ance with StahFEisen-Prifolatt 1808. 6.5 Test procedure 85.1. The tensile test shall be carried out as described in DIN 50 140 or DIN 50 148, 65.2 If determination of the elevated temperature 0,2 % proof strength has been agreed, this shall be determined as oso > ezO LO zzert | bE AOD OX ssonsvo | - | xoacse | ceo ot | ezoo| seo | ovomaco | scomsin | ezoorsso | es) seramoee . ~ | ovveroso | corer ov | cxx0 | seoo| evosreco | coraseo | sroozco | overs | seomozix - - 990 0) S¥'0 09 % OF | oz00 | sto | av0e0E'O oso > s¥0 01800 coeeh S6LOMD TE : ~ | eorerozo | see orsvz | c2x0 | seo} ovoroco | aos | sromeco | seers | orztowors wen] cco> | orveroso | sz ace | sio0| si00| ovosreco | cos | srosare | siees| oreowors ia a 0z't 0 060 sz % 0% | oz0'0 | Sszo'0 | oLOM0r0 oso > s1'001 800 ogelt O16 OD OL - — | sonore zoo | se00 | corsioro | scomorn | Geroooro | seers | — rvomocs - = | ecoersro | orx eroso | eco | seo0 | ofocar | ovos | econo | ors] — swomose a= — wo | A 6 on S iviel = s s\n So oe ‘iehjeue expe} Aq pourwieyep se uojsodulos leoqWweyD seMR PUE SOPEIE JooIs + OIAeL ide 133Page 8 INI7176 ‘Table 2. Amounts by which the chemical analysis as determined by product analysis may deviate from the limiting values specified for ladle analysis: Limi avon ne Tit davnions ho Linking value as Liming vas as tamtng aves as | Groat anaes rom Liming vues as | Groat anasto ce. | etemned by ase | "he tra wales tie. | feterminedbytade | fe tty values, . socchostormetscte | | mont | aaa soccto forte ate ata pecerage | sonia oe ce — eran aon porn eecatage | hay a percent | ey mac) Soe by mace) c| = 028 002 cy = 199 005 > 100 5 1089 oro 3 = 088 008 31000 £ 1280 ois >oas§ $90 doe : oo = 820 208 wn = 190 208 Wo = 088 008 P = 0005 0008 > 095 120 ot s = 0080 2008 w = 080 008 A 20010 08 v 086 008 1) fa number of product analyses are to be carried out, the deviations shown by an element within one cast shall either only ‘above the upper mit or below the lower limit ofthe range specified for the ladle analysis, ut not both at the seme time for fone cast Table 3. Mechanical properties at ambient temperature a Miimum | Misimum impact Net orace von | Wer | vos | tonsa | stonoaton ner | gH, thickness, |strngtn,| strngth, | fracture, As. treatment| NEXr test piece) reatment| "33, Rm | asa percentage Material | Material imme — | in Nienmn?| in Nien? designation | number Long | Trans: | Longi- tudina) | verse") | tucinar 25 GrMos saae |v Z 100, ss | sotoeo | we | 1s | 4 ywomoss | 17335 |v 5 10| 905 sO Stee OE ioe con | eee |e | ao | ae >40< 60| 260 S00 w| 270 yoomes1 | 17360 | Vv = 40| 280 Sao< e0| 270 | 45010600] 2 | 18 | 40 | 2 >e0< 60] 260 vaemoo1 | 17075 | Vv = 100| 955 | Sate | 20 | 168 | 60 a vaemer210 | 173681 | Vv 100] a5s_| saotoeo | 20 | 16 | o | 45 vzemotes | 17362 | 6 e100) 175 | «ws | 2 | 1 | 5 | 09 vi ‘100 275 | «roe | 2 | 7 | ss | ia v2 = 100| 300 | sroto7 | 16 | 16 | o5 | 90 xizemoo1 | 17306 |G S100] 210 | ao< eo) 240 | 298 | 200 | 220 | 205 | 190 | 180 | 170 | 165 | >60< 00| 230 | 225 | 220 | 210 | 195 | 180 | 170 | 160 | 155 | — toeniooro | 17900 | v |< a0] 206 | 250 | 24s | 200 | 200 | 216 | 208 | 15 | 106 | — >40.< 60| 245 | 240 | 235 | 230 | 220 | 205 | 195 | 105 | 175 | — > eo< 00) 295 | 200 | 205 | 220 | 210 | 105 | 106 | 15 | 15 | ‘weaiooie | azar |v | too] sos | sto | sre | aoe | 20 | aoe : zemor210 | 1700 |v |< 100] soo | sto | ove | ao | oot | 200 | 204 | are | | — waeaores | v7ae2 [@ |< 00] 100 | 150 | ae | er | vas | we | vor [v9 | ve | vr |< roo] 248 | 257 | 200 | 208 | 216 | 206 | 16 | ver | ver | — v2 | _< 100] 00s | 360 | so | azz | 00 | 200 | 200 | 200 | zee | — X12CrM0 91 1.7386, Gs 100] 187 | 186 | 178 | 177 | 175 [a7 164 | 153 | 142 | 120 v_[ = too] 76 | oes | a66 | 4s | aa6 | as | axe | 208 | a5 | — poomeves [arm |v |< 00] so | ers | sro | ceo | sso | 210 | «70 | «20 | 0 | - xzocmevi21 | 1402 |v |< 00] 400 | «48 | «0 | 416 | 0 | 320 | aeo | oxo | 220 | 200 1 Key o ambols:G=annosid, = soun or quonched an ompered V1 andV2bang vedo nqush bow tera heat Wana stage esting fron mechrial proper 2) @ @ For greater wall thicknesses, the values of 0,2 % proof strength are to be agreed. Table §. Types of tube length and limit deviations Type ot natn Cin deviations ere a speced natn 500 ‘Up to 6m. +10 e Gg Exact ar 6 up to 12m + ion eee 0 Over fm By aorement *) The ubes re uppiedintheasmanvactred enue tThevolngis vara a trctontovtede dare, ere ele al top Iie in of ondeog 135Page 10 DIN 17176 'BYYE NIQ UI Peyroods ssouyoIN) ITEM PepuEWUODe! OU % o- | — wszs- sesh west — we o- | wor . ests] Se woz+ | *OF este | gezis | *8F | goers | aie | "P%OEF |umozes9H0 Jum oze *peo0< |*pe00>#>"ps00| tpso> | tpwo< | pwoSs>tpsoo | trsoo>| “r< [Yr ss>%s-z| “25 | tPmEOF oda luwooioro} OH : 10H spue wus 099 01 dn ws ze 19H0 wu oze 01 dn ww 061 16H0 uw g€1 Buypee0xe You ‘pewscos [mont | "pio wore *pwsLoF 0} PIED *p oun "Ss@UN9)M) Om Jo UONEEP Ww ‘epjsino jo vonsKep YT [een seeocid upnyoeynuew jo woRouNy 8 ev BUONEMEP MUTT “9 CICEL ia) 136ef DIN 17176 Page 11 Table 7. Scope of testing and DIN 50.049 cartiticates Testing No. Scope of testing Type of certificate ‘Type of testicheck/analysis —_ |Ct. subclause 1 | Ladte analysis 831 All elements for steel grade con- | DIN §0.049-22 ‘cerned as in table 1, per cast or casting unit. 2 | Tensile test at ambient temper- | 63.2 (One test piece each, taken from | DIN S0049-31 A ature 641 two sample tubes of the first two | of DIN 5049-31 B 651 batches and from one sample | or DIN 5049-31 C tube of each further batch, 3 | Impact test 632 For wall thicknesses > 10mm, | DIN 50049-31A 642 fone set of three test pieces per | or DIN 60049-318 653 sample tube specified unter | or DIN 50049-3.1 item No. 2. 4 | Fattening test 6386 For wall thicknesses < 40mm, at | DIN 60049-3.1 A 643 both ends of each as manufac: | or DIN 60049-3.1 8 654 tured length fr DIN 50.049-3.1 C 5 | Non-destructive testing of tube | 6387 For wall thicknesses > 40mm, all | DIN 60049-3.1 B fends for laminations 6510 tubes, over a length of 25 mm, 6 | Non-destructive testing of tube | 6385 AA tubes DIN 50049-3.1 8 fends for longitudinal imoertec- | 658 tons 7 | Leak tightness test 6381 Alltubes: DIN 5049-31 8 656 8 | Visual examination 6383 ‘All tubes DIN 50049-3114 657 or DIN 5049-318 fr DIN 50.049-3.1 C 9 | Materials identity test e382 ‘All tubes DIN 50049-3118 65.14 10. | Dimensional check 6384 ‘All tubes DIN 50.049-3.1 A 6511 for DIN 50.049-3.1 B 6512 for DIN 50.049-3.1 C 11 | @@ Brinot hardness test as a | 635 All tubes, plus one tensile test on | DIN 6049-31 B preliminary stage to establish the | 6513 tube with minimum hardness and homogeneity of the batch in | (6.4.1) fone impact test on tube with maxi- terms of mechanical properties | (651) ‘mum hardness. 642) 683) 12 | @@ Nondestructive testing for | 659 All tubes DIN 50049-2118 transverse imperfections andlor | 65.10 laminations 13 | @@ Hot tensile test 636 Unless otherwise agreed, one test | DIN 0049-31 A 652 Piece per cast and size, ‘or DIN 50049-3118 or DIN 50.049-3.1 C “ Product analysis 532 One test on one sample tube per | DIN 5049-31 B 637 bate, ea 655 137bie Page 12 DIN17176 ‘Appendix A Estimated creep limit and stress rupture, and elevated temperature tensile strength values ‘Table A: gives provisional creep limit and stress rupture values for tubes as specified in this standard, which represent average values deriving from the dispersion of values obtained from tess performed to date. These average values wil be reviewed from Time to time inthe light of new test results, and amended where necessary. Data obtained from creep tests incicate that the lower limit of elspersion of rupture stress values fr the steel grades and temperatures listed lies about 20% below the average values specified here. Til A (tet) ‘Toble At, Estimated creep and stress rupture valves Tem Tom | cep nit), | Rupr sess), 1 eaep Sint), | Rpt ses), suet onde] | in Ninn? or ‘a Winn, fr Steel grade | PE | in Wimm?, tor e Nimen?, for — we, ‘n° | 10000 109000n }10000%) 100000 2200008) ‘eC | 0c00n| eo0c05 | ooo woo | exo © wz | 30 ola] om | a | om o S| i eo] oe | am | on | @ =| m wo | 2a | ws | ae | os a a2 | 2s “ mm | 8 wl] om |u| mw wo | m0 | is | | om @ 7 | mm am |v | i | as | mm romeo | a zs | rscane | wa | soo | ver | me | 2 | | | me | | ow a =| o ms | 8 soli |» | mw we sof io | oa [i | wm wo alae mo] ms | @ || 2 510 m| sf | a | me] ow = wi @ sol a| | s| so | ae | wo | so | me | m |u| 3 | al» wo | 1 | iz | a | as | a7 am | | im | xe | me | ae asa (=) = |S recmows | a0 | ves | wos | zr | oe | a . " amy | mo | 152 | 3) 20 195, wy a eae = wf ia | im joe) mw | w|m| w | as] om | as {im | me | m| mw | wofis | im || a | mm wo [is| im | om) me | so [or | | oo | wr | ns races | so | roo | a | me | 6 | olwliw|os| | m m[im| m)m) a} we wo | co | we | mo | im | || so fm] nm | 2 race195 so| o| e{m| a | # ve [@ [| @ || me | lia] a | w| w | m sof |] » | mw) «| s | wi |e | ms | oi | wi al o|a| a] 2 4 m|s| «|| x | wl) o [wo] w — | @| mj we] w | o | 20 | w | xe) m | m wo | 20 | ss | 6 | me | wla| e)m| «| » ao | m | ws | ae | iw | 10 so| e| a fm] a | 7 w| wo | im || m | m|s| s|m/ mn] @ | 1 | me | 20] we | s|a|o|e| s| 6 so|s| s|e|7| so | | wm | | us | mo so [iz | om [me | ie | ws w| a] «|| »| « womesw |sa| sm) 7m |e | wo | rewns [mo| | | n| au | sola | oe || a | viedvee [so] | oo | ow) oe | m sol a| #jm| a | ow w[a| ala] 2] » m|2| o|o| a| 2 w{e| «lm|a|s w| nj a|s| | ow} a| v[el «| » m|s| s|e| x | 2 es | ee) so) a7) ai| ns) al 9 @|-| 2} a] a] 6 m[a| s[ ol # | 2 m|-| - | a] «|e wl 2) 2 |x| «jo [e[«[e[a[ «T= w|-| -|2| 2] » or) ee ed te For) wd) sn we 138DIN 17176 Page 13 In ti) 1 oe) - io ‘om ta, | an 0, "om to, |p as, stone || “Siti | an tr suet gia |") emer | Wn 1% {nas| ena owes] noo 1 fons] moans os worn 009 wi as) m fa] | a « «| sofa | m fa | a | a = | || or fm] mm | a @ “| in S| im) om fan | ar | a ‘ to | a f/m | | m| m | [m=] w || w | mw 2 =| = wii) || m | a ° | io) || a | a momans | « m | om mii) fm) mo | : wo | elie | mw | om [| || m | 0 w | soli | mw | mr) om | 30 tm | i xacaoes [an | iz |e | mw | ae) is s ts | ' =|) elm) | ww = | o so|'s| @ || om |e 58 tm {on @[s| |e] e| aw [ | m/s) elm) nie mis) a@/m) ge) s {a | mm | | om | a wo} «| » | s| «| a Se | m | me | om | am | mr wlalalal ela m|s) aie) a] a wo] a | w | m | a | as mle) ulal ala sofa | am | me | an | im @|s)sfal a] a a) am |e | a | im | w/a) ef[s| a] e sj m| im |m| om | we so | mm | im | am | ww | tm w[e[»>elm|« anomie wom | « [mlm | m — . Bold (Ebad i 360 | 135 ew | im] ne % bid Ba i finde Bd es sm | 118 TR | 1 6 a mime) of mie | se jm| alo | @ | w : : =|e|2im|n| s w)e|-)mim | - rele elem wl} alm|e| « m| on) ofl es | : wal s|ul| =| 2 xcs fae] | ie] om] wls|a|n| als : soja] > fm| a]: wal s|e| | a wo| | |e) =| 2 w)e]-felel- mw) 3 a. n a es | o w 0 B 8 mla|-falal : m}a| otal a]: fl © Std et es cn he pn ‘raw 000 «oe wfat- fel =| - 2) Smad dc, Wh es gtr ate _ ‘Sam mo mo tre , Fat 139am Page 14 OIN 17 176 Table A2, Estimated elevated temperature tensile strength values (The values given are minimum values established to date) Stesence | eat | Minimum tense strength i Wn Mm Materat| cond |S 5 ansgnaton | rumter| ton) |" |sepsc) 10% 200% 250°C] 900%] 950% 40° 480° 00°C 80° weomos [trae] v_|=100| soo | a0 | «70 | «a0 | so | «ao | ooo | amo | a0 | - wonosa [rraas[ v [s 0o| - | - | avo | aio | ovo | ovo | oes | ass | oo | - weno [sao] v [se] - | - | 20 | aw | a0 | 00 | os | oos | os | - taemooi [sere] v [5100] soo | «00 | ao | «0 | wo | ao | ao | oo] - | - waoniorz10 [tee] v |< 100] soo | «00 | «00 | aso | aso | «a0 | a0 | oo | - | - waemowes | 17002] @ |= 100| 60 | 350 | 200 | oo | oo | o50 | azo | ooo | aro | - vi [= 100 «80 | «2s | «a0 | «00 | avo | amo | ao | as | 10 | v2 [100] ss0 | sas | soo | ao | aco | ao | «15 | ovo | oso | - xizemoet | treee| ¢ |<100| a0 | aco | aso | 250 | ovo | oso | oxo | ans | m0 | - v_|2100| 550 | 525 | s00 | 490 | 480 | 60 | «30 | 405 | 300 | | aooavies [t777@| v_|<100| 00 | o70 | o80 | o20 | oo | ovo | smo | wes | «io | — xaocmovi2%] vaoaa| v |< | 080 | 625 | ooo | soo | soo | os | sio | ass | «oo | as 1) Key to symbols: V= solution or air quenched: G: ‘treatment stages resulting in different mechanical properties. ‘annealed, V 1and V 2 being used to distinguish between diferent heat 140ee DIN 17176 Page 15 Appendix B Table 8.1. Information on temperatures required for hot working and heat treatment : ‘Quenching and tempering eae Heat | Hot working Softening ae treatment| temperature, | (soaking/cooling temperature/ | hardening | Tempering at Material concition’y) inc duration/medium) een |S enpee perature, inC, of designation cecer [25 cro 4 ime |v . 88010 920 | 62010 680 iscrmo44 ass |v - 81010 940 | 66010 730 tocrMos102, | 1.7380/ v - 900t0 960 | 70010 750 rzemos1 | 17375 |v : 90010 960 | 68010 710 facmorz10 | 1.7981 | Vv | sotoason - 900 to 960 | 68010 710 2cmows | 1.7362 | See footnote § for procedure - = vive - 920 t0 980 | 71010 760 xi2cmoo1 | 1.7388 | See footnote 6 for procedure. - - v - 960 to 1000 | 730 to 800" focemevias | a7770 |v : 980 to 1030 | 680 to 730 x20 crmov121 | 1.4922 | v - 1020 to 1070 | 73010 780 ") Key to symbols: G = annealed: V = solution or a quenched 2) This grade may also be subjected tothe following heat treatment: soaking at 900 to 960°C, cooling in a furnace to 700 °C, ‘soaking for not less one hour at 700°C, followed by cooling in ae. 3) In the process, the temperature may drop to 750°C. 4) Tempering should immediately olow quench hardening tr cracking ®) Soaking at 920 to 980°C, cooling in a furnace for 204 hours to 700 to 720°C, followed by cooling in alr. Or, soaking at 950 10 980°C, retarded cooling in @ furnace to 550°C, followed by cooling in ar. ®) Soaking at 950 to 980°C, cooling in a furnace for 2 to 4 hours to 700 to 720°C, tollowed by cooling in ar. Or, soaking at 950 10 980°C, retarded cooling in a furnace to 850°C, followed by cooling in ar. iment since hardened steelis susceptible to stress corrosion 141i 16 INIT 176 Standards and other documents referred to, DIN 2991 Part 1 Seamless precision steel tubes; dimensions DIN. 2448 ‘Seamless steel pipes and tubes; dimensions and mass per unit length DIN 8528 Part 1 Weldabilty of metalic materials; concepts DIN. 8575 Part 1 Filler metals for arc welding of creep resisting steels; classification, designation and technical delivery conditions DIN 1720 Seamless circular tubes made of quenched and tempered steel: technical delivery conditions DIN 50049 Materials testing certificates in an internal pressure test DIN 50 104 Testing the leak tightness of hollow bodies IN 50115, Testing of metalic materials; notched bar impact test DIN 50 125 Testing of metalic materials; tensile test pieces DIN 50 196, Testing of metalic materials; flattening test on tubes DIN 50 140 ‘Testing of metalic materials; tensile testing of tubes and tube sections DIN 50145, Testing of metallic materials; tensile test DIN 50.951 Testing of metalic materials; Brinell hardness test 180 4200:1985 Plain end stee! tubes, welded and seamless; general tables of dimensions and masses per unit length. Stahl-Eisen- Probenahme und Probenvorbereltung fur dle StUckanalyse bel Stuhlen (Sampling and sample preparation for Prifolat 1805") _the product analysis of stee!). ‘StahtEisen- LUtraschallprifung aut Liingsfehler von Rohren aus warmfesten Stahlen (Ultrasonic testing for longitudinal Prifblat 1915") defects in steel tubes with elevated temperature properties) ‘StahlEisen- Utraschallprifung aut Querfehler von Rohren aus warmfesten Stihlen (Ultrasonic testing for trans! -@ Priflatt 1918") defects in steel tubes with elevated temperature properties). Stah-Eisen- Uttraschalpritung aut Doppelungen von Rohven aus warmfesten Stalen (Ultrasonic testing for laminations in Prifolat 1919") _stee! tubes with elevated temperature properties) ‘Stabi-Eisen- EleKiromagnetische Pritung von Rohren zum Nachwels der Dichthelt (Electromagnetic testing of tubes for Prifolat 1925") verification of leak tightness). stoffblatt $90-61*) Druckwasserstoftbestindige Stinle (Steels for hydrogen service at elevated temperatures and pressures) Handbuch fur das Eisenhuttenlaboratorium*) (Loose-teaf collection) ‘API Publication 941%) Steels for hydrogen service at elevated temperatures and pr petrochemical plants sures In petroleum refineries. and Explanatory notes This standard Is based on Stehi-Eisen-Werkstofflat (Iron and steel materials sheet) 590-61 Druckwasserstoffbestindige Stahle sued by the Verein Deutscher Eisenhittenleute (Society of German Ferrous Metallurgy Engineers). However, only grades 125 CrMo 4, 20 CrMoV 19 5 and X 20 CrMoV 12 1 have been adopted from this materials sheet. To meet current demands, six fur- ther grades have been included in this standard, should be noted that grade 25 CrMo 4is also covered in DIN 17 204, However, since the stests specified here are to comply with ‘more stringent requirements regarding resistance to hydrogen, the specifications regarding mechanical properties and heat treat~ ‘ment ag given in this standard, itfer trom those of DIN 17 204. As the strength values given inthis standard have proved adeouate in plezochemistry for more than fy years t has been considered inappropriate to adopt specifications from DIN 17 2 International Patent Classification 8 21.37/00 8220 czcsae © 22.¢ 38/22 6018 21/00 G01 L 5100 G 0133/20 *) Obtainable from Verlag Stahleisen mbH, Postfach 82 28, D-4000 Disseldort 1 ‘Obteinable from the American Petroleum Insitute, 2101 L Street, Washington, D.C, 20037. 142