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Separation of Substances

~Prelab~

Name___________

Date___________

Purpose:Todeterminetheamountofsodiumchloridepresentinamixtureofsand,iron
filingsandsodiumchloride.
Procedure:
Eachlabgroupwillbegivenabeakercontainingsodiumchloride(NaCl,tablesalt),sand/dirt,
andironfilings.Yourmissionistodeterminethemassofthesodiumchloridepresentinthe
sampleyouaregiven.Youmaydeviseanyprocedureyoufeelwillgiveyouthebestyield
(closestresult).RefertoChapter2andtheglossaryinyourtextforhelpfulvocabulary.
Createalistofnumberedstepsthatyouwillfollowwhenyoudothislab.Basedonyour
proceduredetermineacompletelistofmaterials(bothequipmentandchemicals,ifneeded)you
willuseandrecordthatinformationaswell.Whenyouareready,haveyourteachercheckyour
procedureforsafety(theywillnotcheckitforaccuracy).
Whenyoufeelyouhavesuccessfullycompletedthistask,youwillhavetheopportunityto
comparethemassyoudeterminedwiththeknownmassinordertocalculatethepercenterror.

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Discussion
Belowarequestionstospecificallyaddressafteryourdiscussionparagraph(yourparagraph
shouldmentionatleast5termsfromChapter2).
1. Whateffectwouldaddingfartoomuchwaterhaveonyourresults?Why?
2. Howwouldyouchangeyourprocedureif,afterfiltering,bitsofsandandpaperwerein
thedishwiththesaltsolution?
3. Isitnecessarytoremovetheironfromthesampleinastepseparatefromthesand?Why
orwhynot?
Error Analysis
Asidefromdeterminingtwopotentialproceduralsourcesoferror(noninstrumentalor
calculationbased)andtheirimpact,youwillneedtheinformationbelowtocalculateyour
percenterror.Inaddition,answerthefollowingquestionsinthissection.
Massofsodiumchloride:
1. Describethequalitativewaysinwhichyoudeterminedthatthewaterwascompletely
evaporated.
2. Whatisaquantitativemethodofdeterminingthatevaporationwascomplete?
3. Whatisanexplanationforasodiumchloriderecoverygreaterthan100%?
4. Whatchangeswouldyoumaketoyourprocedureinordertominimizeerrorinthe
future?

275631949.doc

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