THAI INDUSTRIAL STANDARD

. 2313 2549

BIODIESEL FOR HIGH SPEED ENGINES

ICS 75.160.20

ISBN 978-974-292-275-7

. 2313 2549

6 10400
0 2202 3300

124 37
28 2550

 959

. ()
()

(2)










..2548
BS EN 14214 : 2003
Automotive fuelsFatty acid methyl esters (FAME) for diesel engines
Requirements and test methods
ASTM D 93-02a
Standard Test Methods for FlashPoint by PenskyMartens Closed Cup
Tester
ASTM D 97-02
Standard Test Method for Pour Point of Petroleum Products
ASTM D 13094
Standard Test Method for Detection of Copper Corrosion from Petroleum
Products by the Copper Strip Tarnish Test
ASTM D 44503
Standard Test Method for Kinematic Viscosity of Transparent and Opaque
Liquids (the Calculation of Dynamic Viscosity)
ASTM D 2500-02
Standard Test Method for Clound Point of Petroleum Products
ASTM D 61303b
Standard Test Method for Cetane Number of Diesel Fuel Oil
ASTM D 66401
Standard Test Method for Acid Number of Petroleum Products by
Potentiometric Titration
ASTM D 87400
Standard Test Method for Sulfated Ash from Lubricating Oils and
Additives
ASTM D 116003
Standard Test Method for Distillation of Petroleum Products at Reduced
Pressure
ASTM D 129899
Standard Test Method for Density, Relative Density (Specific Gravity),
or API Gravity of Crude Petroleum and Liquid Petroleum Products by
Hydrometer Method
ASTM D 250002
Standard Test Method for Clound Point of Petroleum Products
ASTM D 262203
Standard Test Method for Sulfur in Petroleum Products by Wavelength
Dispersive Xray Fluorescence Spectrometry
ASTM D 453003
Standard Test Method for Determination of Carbon Residue Micro
Method

(3)

ASTM D 495102

ASTM D 658400
EN 14103 : 2003
EN 14105 : 2003

EN 14108 : 2003
EN 14109 : 2003
EN 14110 : 2003
EN 14111 : 2003
EN 14112 : 2003
pr EN 14538.

.1380-2539

Standard Test Method for Determination of Additive Elements in

Lubricating Oils by Inductively Coupled Plasma Atomic Emission
Spectrometry
Standard Test Method for Determination of Free and Total Glycerine in
B100 Biodiesel Methyl Esters by Gas Chromatography
Fat and oil derivativesFatty acid methyl esters (FAME)Determination
of ester and linolenic acid methyl ester contents
Fat and oil derivativesFatty acid methyl esters (FAME)Determination
of free and total glycerol and mono, di, triglyceride contents (Reference
method)
Fat and oil derivatives-Fatty acid methyl esters (FAME)-Determination
of sodium content by atomic absorption spectrometry
Fat and oil derivatives-Fatty acid methyl esters (FAME)-Determination
of potassuim content by atomic absorption spectrometry
Fat and oil derivativesFatty acid methyl esters (FAME)Determination
of methanol content
Fat and oil derivativesFatty acid methyl esters (FAME)Determination
of iodine value
Fat and oil derivativesFatty acid methyl esters (FAME)Determination
of oxidation stability (accelerated oxidation test)
Fat and oil derivatives-Fatty acid methyl ester (FAME)-Determination
of Ca and Mg content by optical emission spectral analysis with inductively
coupled plasma (ICP OES)

15 .. 2511

(4)


3566 ( .. 2549 )

.. 2511


15 .. 2511

. 23132549
17 .. 2549

(5)

. 23132549

1.
1.1
- B100

2.

2.1

O|
R1COR2
R1

R2
B
B5
5

3.
3.1 2
3.1.1
3.1.2

. 23132549

4.
4.1

4.2
4.2.1



..2548 .

4.2.2

4.3
4.3.1

ASTM D 2500

5.
5.1

6.
6.1

(1)
(2)
(3) () ( )
(4) ( )
(5)

. 23132549

7.
7.1 .

8.
8.1

8.2

. 23132549

.. 2548

1
(Methyl Ester,
2

15 /
(Density at 15 C,

4
5
6
7
8
9
10
11

% wt.)
kg/m 3

96.5

1
EN 14103

860

ASTM D 1298

900

40

3.5

ASTM D 445

(Viscosity at 40 C,

cSt)

5.0
120

ASTM D 93

0.0010

ASTM D 2622

0.30

ASTM D 4530

51

ASTM D 613

0.02

ASTM D 874

0.050

ASTM D 2709

0.0024

ASTM D 5452

C)
(Flash Point,

(Sulphur,
%wt.)

(Carbon Residue, on 10% distillation residue,

%wt.

(Cetane Number)

(Sulfated Ash,
%wt.)

(Water
%wt.)

(Total Contaminate,
%wt.)

(Corrosion Strip Copper )

1 ASTM D 130

. 23132549

12
110

(Oxidation Stability at 110 C, hours)

13 /
(Acid Value,
mg KOH/g)
14
/100
(Iodine Value,
g lodine/100 g)
15

(Linolenic Acid Methyl Ester,

%wt.)
16

(Methanol,
%wt.)
17

(Monoglyceride,
%wt.)
18

Diglyceride,
%wt.)
19

(Triglyceride,
%wt.)
20

(Free glycerin,
%wt.)
21

(Total glycerin,
%wt.)
22 1 (
/
)
(Group I metals (Na+K)
mg/kg)
2 (
/
)
(Group II metals (Ca+Mg)
mg/kg)
23

(Phosphorus,
%wt.)
24 ()
(Additive)

1
EN 14112

0.50

ASTM D 664

120

EN 14111

12.0

EN 14103

0.20

EN 14110

0.80

EN 14105

0.20

EN 14105

0.20

EN 14105

0.020

EN 14105

0.25

EN 14105

5.0

EN 14108
EN 14109

5.0

prEN 14538

0.0010

ASTM D 4951

. 23132549

.

( 7.1)
.1

.2

.2.1
.1380
.2.2
4.1 4.2.1 4.2.2 4.3 5.
6.

. 23132549

..

..
ASTM D 2709 . EN ISO 12937
ASTM D 5452 . EN ISO 12662