Professional Documents
Culture Documents
Phạm Văn Hải
Phạm Văn Hải
KHOA MI TRNG
PHM VN HI
N TT NGHIP
XC NHN GI TR S DNG CA PHNG PHP
XC NH TNG HM LNG ST TRONG NC
BNG PHNG PHP TRC QUANG TI PHNG TH
NGHIM MI TRNG, TRNG I HC TI
NGUYN V MI TRNG H NI
H NI, 2014
PHM VN HI
N TT NGHIP
XC NHN GI TR S DNG CA PHNG PHP
XC NH TNG HM LNG ST TRONG NC
BNG PHNG PHP TRC QUANG TI PHNG TH
NGHIM MI TRNG, TRNG I HC TI
NGUYN V MI TRNG H NI
H NI, 2014
LI CM N
Sau gn 2 thng lm n cng vi s lm vic n lc ca bn thn,
n tt nghip ca ti hon thnh ng thi hn, vi tn ti : Xc nhn
gi tr s dng ca phng php xc nh tng hm lng st trong nc
bng phng php trc quang ti phng th nghim Mi Trng,
Trng i Hc Ti Nguyn V Mi Trng H Ni.
hon thnh kha lun tt nghip ny, li u tin ti xin by t lng
bit n chn thnh v su sc nht ti ngi hng dn l: Thc s Trnh Th
Thy cng tc ti Trng i Hc Ti Nguyn Mi Trng H Ni tn
tnh hng dn ti trong sut qu trnh nghin cu v thc hin ti.
Ti cng xin chn thnh ti ban lnh o nh trng, cc phng ban v
c bit l thy, c trong phng th nghim Mi Trng to mi iu kin
thun li v gip ti hon thnh kha lun tt nghip ny.
Ti xin gi li cm n n cc thy c gio trong khoa Mi Trng
Trng i Hc Ti Nguyn Mi Trng H Ni trang b cho ti nhng
kin thc v kinh nghim qu gi trong qu trnh hc tp ti trng.
Mc d c nhiu c gng, nhng do thi gian c hn, trnh v k
nng ca bn thn cn nhiu hn ch nn chc chn ti tt nghip ny ca
ti khng trnh khi nhng thiu st. Rt mong c s ng gp, ch bo, b
sung thm ca thy c v cc bn.
Ti xin chn thnh cm n!
H Ni, Ngy 09 thng 06 nm 2014
Sinh vin
Phm Vn Hi
MC LC
M U ....................................................................................................... 1
CHNG 1: TNG QUAN .......................................................................... 3
1.1. Tng quan v xc nhn gi tr s dng ca phng php......................... 3
1.1.1. Khi nim v xc nhn gi tr s dng. ................................................. 3
1.1.2. Quy trnh xc nhn gi tr s dng ca phng php ............................ 3
1.1.3. Khi nim cc thng s cn xc nh .................................................... 5
1.2. Tng quan v tiu chun ISO/IEC 17025:2005........................................ 7
1.2.1. Gii thiu v tiu chun ISO/IEC 17025:2005...................................... 7
1.2.2. Cu trc ca tiu chun ISO/IEC 17025:2005 ...................................... 8
1.2.3. Mc ch ca tiu chun ISO/IEC 17025:2005 ..................................... 8
1.3. Tng quan v st ..................................................................................... 9
1.3.1. Tng quan v st trong nc................................................................. 9
1.3.2. nh hng ca st. ............................................................................. 10
1.4. Cc phng php xc nh st ............................................................... 11
1.4.1 Xc nh st bng xphng php trc quang dung thuc th 110phenaltrolin theo TCVN 6177-1996 ......................................................... 11
1.4.2. Xc nh st bng phng php ph hp th nguyn t. ..................... 11
CHNG 2: THC NGHIM ................................................................... 12
2.1. i tng nghin cu ............................................................................ 12
2.2. Phng php nghin cu ....................................................................... 12
2.3. Ly mu v x l mu ........................................................................... 12
2.4. Tin hnh xc nhn gi tr s dng ........................................................ 13
2.4.1. La chn phng php (bc 1) ......................................................... 13
DANH MC CC CH VIT TT
AOAC
KB
khng m bo o
IEC
XNGTSD
Xc nhn gi tr s dng
LOD
LOQ
PTN
Phng th nghim
QA
Bo m cht lng
QC
RSD
SD
lch chun
TCVN
VILAS
WTO
DANH MC CC BNG
DANH MC HNH
M U
pht trin v kin ton h thng quan trc v phn tch mi trng
cho vic pht hin, nh gi nhim, gim st cht lng mi trng phc v
cng tc ging dy v nghin cu khoa hc, hin nay phng th nghim Mi
Trng, Trng i hc Ti Nguyn V Mi Trng H Ni ang tin hnh
xy dng h thng PTN t chun ISO/IEC 17025:2005, xc nhn nng lc
ca PTN, m bo kt qu th nghim/o lng t kt qu ng tin cy nht,
c gi tr v mt k thut.
Xc nhn gi tr s dng ca phng php l mt trong nhng yu cu
v mt k thut trong tiu chun ISO/IEC 17025: 2005, cung cp bng chng
khch quan rng cc yu cu xc nh cho vic la chn v s dng phng
php th c p ng.
Nhiu quyt nh quan trng da vo kt qu phn tch. Trong khi ,
mi php o u c sai s, xc nh cc gi tr sai s ny rt phc tp, i
hi nhiu n lc, sng to, v c trc gic. V vy, kt qu phn tch hon
thnh vi gi tr tin cy cao th phng php phn tch phi m bo. Xc
nh gi tr ca phng php l mt phn khng th thiu nu mun c kt
qu phn tch ng tin cy.
V vy, ti chn ti Xc nhn gi tr s dng ca phng php xc
nh tng hm lng st trong nc bng phng php trc quang ti Phng
th nghim Mi trng, Trng i hc Ti nguyn v Mi trng H Ni.
Mc tiu nghin cu ca ti
Xc nhn gi tr s dng ca quy trnh phn tch chn theo TCVN
6177: 1996.
Ni dung nghin cu:
- Nghin cu ti liu ISO 17025:2005.
2
- Nghin cu kho st cc iu kin ca PTN phc v cho phng php
th.
- Lp k hoch xc nhn gi tr s dng ca phng php bao gm: xc
nh thi gian, ngi thc hin, ch tiu th, mu cn phn tch...
- Xc nh gi tr s dng ca quy trnh phn tch chn bng phng
php tiu chun:
+ Xc nh khong tuyn.
+ Xc nh lp vi quy trnh phn tch chn.
+ Xc nh gii hn pht hin (LOD) v gii hn nh lng (LOQ).
+ Xc nh thu hi.