Professional Documents
Culture Documents
BS en 196-3, 1995-Cement Setting Time and Soundness
BS en 196-3, 1995-Cement Setting Time and Soundness
porx6sek porx6sek
BRITISH STANDARD
Methods of testing
cement
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
BS EN
196-3:1995
BS EN 196-3:1995
Cooperating organizations
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
Oesterreichisches Normungsinstitut
Institut belge de normalisation
Dansk Standard
Suomen Standardisoimisliito, r.y.
Association franaise de normalisation
Deutsches Institut fr Normung e.V.
Hellenic Organization for Standardization
Technological Institute of Iceland
National Standards Authority of Ireland
Ente Nazionale Italiano di Unificazione
Inspection du Travail et des Mines
Nederlands Normalisatie-instituut
Norges Standardiseringsforbund
Instituto Portugus da Qualidade
Asociacin Espaola de Normalizacin y Certificacin
Standardiseringskommissionen i Sverige
Association suisse de normalisation
British Standards Institution
BSI 01-1999
Amd. No.
Date
Comments
BS EN 196-3:1995
Contents
Cooperating organizations
National foreword
Foreword
Text of EN 196-3
2
3
Inside back cover
Inside back cover
Inside back cover
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
Page
Inside front cover
ii
BSI 01-1999
BS EN 196-3:1995
National foreword
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
This British Standard has been prepared under the direction of Technical
Committee B/516, Cement and lime. It is the English language version
of EN 196-3:1994 Methods of testing cement Part 3: Determination of setting
time and soundness published by the European Committee for Standardization
(CEN). EN 196-3 was drawn up by CEN Technical Committee 51, Cement and
building limes, as Part 3 of a series on testing cement which was originally
accepted by CEN on 15 November 1985 and made available on 12 May 1987. The
UK gave a negative vote at the final voting stage and, under the CEN Rules then
in force, was not obliged to implement this Part. A second formal vote was taken
in November 1992 when the UK again gave a negative vote but, under the CEN
Rules now in force, is obliged to implement this Part. This British Standard
supersedes BS 4550-3.5:1978, BS 4550-3.6:1978 and BS 4550-3.7:1978 which are
withdrawn.
The methods described in this standard retain the use of the familiar Vicat and
le Chatelier apparatus. The UK negative votes on this Part were due to the fact
that the draft European Standard contained certain errors, some of which remain
in the 1994 text, e.g. the minimum laboratory relative humidity in 4.1 should
be 50 % to accord with EN 196-1. Furthermore, the requirement in 7.1.3 for a
minimum relative humidity of 98 % is inappropriate as values at this level can
neither be measured nor controlled with any precision. The lengths of the
standard consistence plunger and of the setting time needles are not critical
where the Vicat apparatus is calibrated in advance of the test (see 5.2.3 and 6.2).
However, for convenience in use, they should be of the same length
within 1 mm. Hence, in the typical illustrations shown in Figure 1, the needle
lengths in (d) and (e) should be shown to the upper shoulder of the cone.
The Vicat mould is specified in 5.1 to be of hard rubber but moulds of metal may
be used provided that .... they can be shown to give the same test results. Such
data are available in the UK enabling metal moulds to be used.
In the test for standard consistence, 5.2.3 requires repeat tests with pastes
containing different water contents until one is found to produce a distance
between plunger and base-plate of (6 1) mm. The UK procedure for meeting
this requirement is given in national annex NA.
BS 4550-3.7:1978 included a soundness test for supersulfated cement, based on
immersion in cold water, which does not appear in EN 196-3. This procedure is
being retained in an appendix to BS 4248:1974.
A British Standard does not purport to include all the necessary provisions of a
contract. Users of British Standards are responsible for their correct application.
Compliance with a British Standard does not of itself confer immunity
from legal obligations.
Summary of pages
This document comprises a front cover, an inside front cover, pages i and ii,
the EN title page, pages 2 to 8, an inside back cover and a back cover.
This standard has been updated (see copyright date) and may have had
amendments incorporated. This will be indicated in the amendment table on
the inside front cover.
ii
BSI 01-1999
EUROPEAN STANDARD
EN 196-3
NORME EUROPENNE
EUROPISCHE NORM
December 1994
ICS 91.100.10
Supersedes EN 196-3:1987
English version
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
Prfverfahren fr Zement
Teil 3: Bestimmung der Erstarrungszeiten und
der Raumbestndigkeit
CEN
European Committee for Standardization
Comit Europen de Normalisation
Europisches Komitee fr Normung
Central Secretariat: rue de Stassart 36, B-1050 Brussels
1994 Copyright reserved to CEN members
EN 196-3:1994
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
Foreword
This European Standard was drawn up by
Technical Committee CEN/TC 51, Cement and
building limes, of which the secretariat is held
by IBN.
The European Standard on the methods of testing
cement comprises the following Parts:
EN 196-1, Methods of testing cement
Part 1: Determination of strength.
EN 196-2, Methods of testing cement
Part 2: Chemical analysis of cement.
EN 196-3, Methods of testing cement
Part 3: Determination of setting time and
soundness.
ENV 196-4, Methods of testing cement
Part 4: Quantitative determination of constituents.
EN 196-5, Methods of testing cement
Part 5: Pozzolanicity test for pozzolanic cements.
EN 196-6, Methods of testing cement
Part 6: Determination of fineness.
EN 196-7, Methods of testing cement
Part 7: Methods of taking and preparing samples of
cement.
EN 196-21, Methods of testing cement
Part 21: Determination of chloride, carbon dioxide
and alkali content of cement.
This European Standard shall be given the status of
a National Standard, either by publication of an
identical text or by endorsement, at the latest by
June 1995, and conflicting national standards shall
be withdrawn at the latest by June 1995.
This European standard supersedes EN 196-3:1987.
According to the CEN/CENELEC Internal
Regulations, the following countries are bound to
implement this European Standard: Austria,
Belgium, Denmark, Finland, France, Germany,
Greece, Iceland, Ireland, Italy, Luxembourg,
Netherlands, Norway, Portugal, Spain, Sweden,
Switzerland, United Kingdom.
Contents
Foreword
1
Scope
2
Normative references
3
Test principles
4
General requirements for testing
5
Standard consistence test
6
Setting time test
7
Soundness test
Figure 1 Vicat apparatus for
determining the standard consistence
and setting time of cement
Figure 2 Le Chatelier apparatus for the
determination of soundness of cements
Page
2
3
3
3
3
3
6
7
4
8
BSI 01-1999
EN 196-3:1994
1 Scope
This European Standard describes the methods for
determining setting time and soundness of cements.
It is applicable to all cements covered by ENV 197-1.
This standard describes the reference procedure; it
allows the use of alternative procedures as indicated
in notes provided that they do not affect the results
significantly. In the event of a dispute, only the
reference procedure described in this standard shall
be used, excluding any alternatives.
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
2 Normative references
This European Standard incorporates by dated or
undated reference, provisions from other
publications. These normative references are cited
at the appropriate places in the text and the
publications are listed hereafter. For dated
references, subsequent amendments to or revisions
of any of these publications apply to this European
Standard only when incorporated in it by
amendment or revision. For undated references, the
latest edition of the publication referred to applies.
EN 196-1, Methods of testing cement
Part 1: Determination of strength.
ENV 197-1, Cement Composition, specifications
and conformity criteria Part 1: Common cements.
3 Test principles
The setting time is determined by observing the
penetration of a needle into cement paste of
standard consistence until it reaches a specified
value.
The soundness is determined by observing the
volume expansion of cement paste of standard
consistence as indicated by the relative movement of
two needles.
Cement paste of standard consistence has a
specified resistance to penetration by a standard
plunger. The water required for such a paste is
determined by trial penetrations of pastes with
different water contents.
5.2 Procedure
5.2.1 Mixing the cement paste
Weigh, to the nearest 1 g, 500 g of cement. Weigh a
quantity of water, e.g. 125 g, in the mixer bowl or
measure the water from the graduated cylinder or
burette and place it into the mixer bowl.
Add the cement carefully to the water in order to
avoid loss of water or cement. The time of addition
shall be not less than 5 s nor more than 10 s. Note
the time of completion of the addition as zero time
from which later measurements of time shall be
made. Start the mixer immediately and run at low
speed for 90 s.
4.2 Apparatus
4.2.1 Balance, capable of weighing to the
nearest 1 g.
BSI 01-1999
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
EN 196-3:1994
NOTE The specified dimensions have to be observed. If the plunger, needle and needle with attachment are all adjusted to have
the same mass, e.g. (9 0,5) g, one correcting weight is sufficient for each apparatus.
BSI 01-1999
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
EN 196-3:1994
NOTE The specified dimensions have to observed. If the plunger, needle and needle with attachment are all adjusted to have the
same mass, e.g. (9 0,5) g, one correcting weight is sufficient for each apparatus.
BSI 01-1999
EN 196-3:1994
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
BSI 01-1999
EN 196-3:1994
7 Soundness test
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
7.1 Apparatus
7.1.1 Le Chatelier apparatus. The mould shall be of
spring brass with indicator needles and shall have
the dimensions shown in Figure 2(a). The resilience
of the mould shall be such that the action of a mass
of 300 g applied as shown in Figure 2(c) shall
increase the distance between the indicator ends of
the needles by (17,5 2,5) mm without permanent
deformation.
A pair of plane glass base and cover plates shall be
provided for each mould. Each plate shall be larger
than the mould. The cover plate shall weigh at
least 75 g; an additional small mass may be placed
on a thin plate to satisfy this requirement.
7.1.2 Water-bath, with means of heating, capable of
containing immersed Le Chatelier specimens and of
raising the temperature of the water
from (20 2) C to boiling in (30 5) min.
7.1.3 Humidity cabinet, of adequate size and
maintained at (20 1) C and not less than 98 %
relative humidity.
7.2 Procedure
Carry out the test simultaneously on two specimens
from the same batch of cement paste.
Prepare a cement paste of standard consistence.
Place a lightly oiled Le Chatelier mould on the
lightly oiled base-plate and fill it immediately
without undue compaction or vibration using only
the hands and a straight-edged implement, if
desired, to level the top surface. During filling,
prevent, the split in the mould from accidentally
opening e.g. by gentle pressure with the fingers or
by tying or by use of a suitable rubber band.
Cover the mould with the lightly oiled cover plate,
add the additional mass, if necessary, and then
immediately place the complete apparatus in the
humidity cabinet. Maintain it for (24 0,5) h
at (20 1) C and not less than 98 % relative
humidity.
7.4 Retest
Should the fresh cement fail to comply with the
specified soundness requirement it may be retested
after storage. For this purpose, spread out the
cement in a layer of 7 cm thickness and store it
for 7 days in an atmosphere maintained
at (20 2) C and not less than 65 % relative
humidity. Then retest the cement according to 7.2.
BSI 01-1999
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
EN 196-3:1994
BSI 01-1999
BS EN 196-3:1995
National annex NA (informative)
Determination of standard consistence
In order to meet the requirement of 5.2.3 to find a paste which produces a distance between plunger and
base-plate of (6 1) mm, the following procedure should be adopted.
Follow the procedure in 5.2 using a paste consisting of 500 g of the cement and a selected. quantity of water,
e.g. 125 g. If this gives a distance from the base-plate of (6 1) mm record the water content of this paste
to the nearest 0.5 % as the water for standard consistence.
If the first paste gives a distance from the base-plate outside the range (6 1) mm, prepare another paste
with a greater or smaller quantity of water as appropriate. If this gives a distance from the base-plate
of (6 1) mm record the water content of this second paste to the nearest 0.5 % as the water for standard
consistence.
If this second paste gives a distance from the base-plate outside the range of (6 1) mm, prepare a third
paste with a greater or smaller quantity of water as appropriate. If this gives a distance from the base-plate
of (6 1) mm record the water content of this third paste to the nearest 0.5 % as the water for standard
consistence.
If this third paste gives a distance from the base-plate outside the range of (6 1) mm, interpolate, from
the three readings already obtained (providing at least one lies at each end of the range of (6 1) mm), the
water content required for a distance from the base-plate of 6 mm and record this value to the nearest 0,5 %
as the water for standard consistence.
NOTE
Any test in which the plunger fails to penetrate the paste, or penetrates the paste to rest on the base-plate, should be ignored.
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
BSI 01-1999
Licensed Copy: porx6sek porx6sek, January 22, 2002, Uncontrolled Copy, (c) BSI
BSI
389 Chiswick High Road
London
W4 4AL
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|