CNG HA X HI CH NGHA VIT NAM

QCVN 4-2 : 2010/BYT

QUY CHUN K THUT QUC GIA

V PH GIA THC PHM - CHT LM M

National technical regulation on Food Additive - Humectants

H NI - 2010

Li ni u
QCVN 4-2:2010/BYT do Ban son tho quy chun k thut
quc gia v Ph gia thc phm v cht h tr ch bin
bin son, Cc An ton v sinh thc phm trnh duyt v
c ban hnh theo Thng t s 19/2010/TT-BYT
ngy 20 thng 5 nm 2010 ca B trng B Y t.

QUY CHUN K THUT QUC GIA

V PH GIA THC PHM - CHT LM M
National technical regulation on food additive - Humectants
I. QUY NH CHUNG
1. Phm vi iu chnh
Quy chun k thut quc gia (sau y gi tt l Quy chun) ny quy nh cc yu cu
k thut v qun l v cht lng, v sinh an ton i vi cc cht lm m c s dng
vi mc ch lm ph gia thc phm.
2. i tng p dng
Quy chun ny p dng i vi:
2.1. T chc, c nhn nhp khu, xut khu, sn xut, bun bn v s dng cc
cht lm m lm ph gia thc phm (sau y gi tt l t chc, c nhn).
2.2. C quan qun l nh nc c lin quan.
3. Gii thch t ng v ch vit tt:
3.1. Cc cht lm m: l ph gia thc phm c s dng vi mc ch ngn
nga s mt nc ca cc sn phm thc phm.
3.2. JECFA monograph 1 - Vol. 4 (JECFA monographs 1 - Combined
compendium of food addiditive specifications; Joint FAO/WHO expert committee on
food additives; Volume 4 - Analytical methods, test procedures and laboratory
solutions used by and referenced in the food additive specifications; FAO, 2006): Cc
yu cu k thut i vi ph gia thc phm, Tp 4 Cc phng php phn tch, quy
trnh th nghim, dung dch th nghim c s dng (hoc tham chiu) trong yu
cu k thut i vi ph gia thc phm; JECFA bin son; FAO ban hnh nm 2006.
3.3. M s C.A.S. (Chemical Abstracts Service): M s ng k ha cht ca
Hip hi Ha cht Hoa K.
3.4. TS (test solution): Dung dch thuc th.
3.5. MTDI (Maximum Tolerable Daily Intake): Lng n vo hng ngy ti a
chu ng c.
3.6. INS (International numbering system): H thng m s quc t v ph gia
thc phm.
II. YU CU K THUT, PHNG PHP TH V LY MU
1. Yu cu k thut v phng php th i vi cht lm m l calci dihydro
diphosphat c quy nh ti ph lc ban hnh km theo Quy chun ny.

QCVN 4-2 : 2010/BYT

2. Cc yu cu k thut quy nh trong Quy chun ny c th theo JECFA
monograph 1 - Vol. 4, ngoi tr mt s php th ring c m t trong cc ph lc.
Cc phng php th c hng dn trong Quy chun ny khng bt buc phi
p dng, c th s dng cc phng php th khc tng ng.
3. Ly mu theo hng dn ti Thng t 16/2009/TT-BKHCN ngy 02 thng 6
nm 2009 ca B Khoa hc v Cng ngh v hng dn kim tra nh nc v cht
lng hng ha lu thng trn th trng v cc quy nh khc ca php lut c lin
quan.
III. YU CU QUN L
1. Cng b hp quy
1.1. Cc cht lm m phi c cng b ph hp vi cc quy nh ti Quy
chun ny.
1.2. Phng thc, trnh t, th tc cng b hp quy c thc hin theo Quy
nh v chng nhn hp chun, chng nhn hp quy v cng b hp chun, cng
b hp quy ban hnh km theo Quyt nh s 24/2007/Q-BKHCN ngy 28 thng 9
nm 2007 ca B trng B Khoa hc v Cng ngh v cc quy nh ca php lut.
2. Kim tra i vi cht lm m
Vic kim tra cht lng, v sinh an ton i vi cc cht lm m phi thc
hin theo cc quy nh ca php lut.
IV. TRCH NHIM CA T CHC, C NHN
1. T chc, c nhn phi cng b hp quy ph hp vi cc quy nh k
thut ti Quy chun ny, ng k bn cng b hp quy ti Cc An ton v sinh thc
phm v bo m cht lng, v sinh an ton theo ng ni dung cng b.
2. T chc, c nhn ch c nhp khu, xut khu, sn xut, bun bn v s dng
cc cht lm m sau khi hon tt ng k bn cng b hp quy v bo m cht lng,
v sinh an ton, ghi nhn ph hp vi cc quy nh ca php lut.
V. T CHC THC HIN
1. Giao Cc An ton v sinh thc phm ch tr, phi hp vi cc c quan chc
nng c lin quan hng dn trin khai v t chc vic thc hin Quy chun ny.
2. Cn c vo yu cu qun l, Cc An ton v sinh thc phm c trch nhim
kin ngh B Y t sa i, b sung Quy chun ny.
3. Trng hp hng dn ca quc t v phng php th v cc quy nh
ca php lut vin dn trong Quy chun ny c sa i, b sung hoc thay th th
p dng theo vn bn mi.
2

QCVN 4-2 : 2010/BYT

Ph lc
YU CU K THUT V PHNG PHP TH
I VI CALCI DIHYDROGEN DIPHOSPHAT
1. Tn khc, ch s

Monocalcium dihydrogen pyrophosphate, Acid calci

pyrophosphat
INS 450vii
MTDI=70mg/kg th trng tnh cho phospho t cc ngun
thc phm

2. nh ngha
Tn ha hc

Monocalci dihydrogen diphosphat

M s C.A.S.

14866-19-4

Cng thc ha hc

CaH2P2O7

Khi lng phn t

215,97

3. Cm quan

Tinh th trng hoc bt trng

4. Chc nng

Cht lm m, n nh, bt ni, cht nh ha, cht dinh

dng.

5. Yu cu k thut
5.1. nh tnh
Calci

Phi c phn ng c trng ca calci

Phosphat

Phi c phn ng c trng ca phosphat.

5.2. tinh khit

Gim khi lng khi sy
kh

Khng c qu 1,0 % (105 oC trong 4 gi).

Cc cht khng tan trong

acid

Khng c qu 0,4%.

Florid

Khng c qu 30 mg/kg.

Arsen

Khng c qu 3,0 mg/kg.

Ch

Khng c qu 4,0 mg/kg.

5.3. Hm lng CaH2P2O7 Khng c qu 64,0% quy ra P2O5 tnh theo ch phm
kh.
6. Phng php th
6.1. tinh khit
Florid

- Th theo hng dn ti JECFA monograph 1 - Vol. 4.

- Phng php III; s dng c mu v cc th tch dung
dch chun ph hp xy dng ng chun.
3

QCVN 4-2 : 2010/BYT

Arsen

- Th theo hng dn ti JECFA monograph 1 - Vol.4 ,

phng php II.

Ch

- Th theo hng dn ti JECFA monograph 1 - Vol.4 .

- Xc nh bng k thut hp th nguyn t thch hp
cho hm lng quy nh. La chn c mu th v
phng php chun b mu da trn nguyn tc ca
phng php m t ti JECFA monograph 1 - Vol.4
phn cc phng php phn tch cng c.

6.2. nh lng
Cn khong 200 mg (chnh xc n mg) mu th, ha
tan trong 25 ml nc v 10 ml dung dch acid nitric long
(TS) v un si trong 30 pht. Lc nu cn v ra kt
ta sau ha tan ta bng cch thm 1 ml dung dch
acid nitric long (TS). un nng n 50 oC, thm 75 ml
dung dch amoni molybdat (TS) v gi 50 oC trong 30
pht, thnh thong khuy. yn 16 gi hoc qua m
nhit d phng. Gn phn dch pha trn qua giy lc,
ra ta bng nc 1 hoc 2 ln, mi ln 30 - 40 ml, gn
b dch ra ln giy lc nu trn, Cho kt ta vo giy
lc va gn dch ra, ra ton b bng dung dch kali
nitrat (1/100) n khi dch ra khng cn acid khi th vi
qu tm. Cho giy lc cha ta vo bnh kt ta ban u,
thm 50ml dung dch natri hydroxyd 1N, lc n khi ta
tan hon ton, thm 3 git dung dch phenolphtalein (TS)
v chun lng natri hydroxyd d bng acid sulfuric
1N.
Mi ml dung dch natri hydroxyd 1 N tng ng vi
3,088 mg P2O5.