CNG HA X HI CH NGHA VIT NAM

QCVN 5-4:2010/BYT

QUY CHUN K THUT QUC GIA

I VI CC SN PHM CHT BO T SA
National technical regulation for dairy fat products

H NI 2010

Li ni u
QCVN 5-4:2010/BYT do Ban son tho Quy chun k thut quc gia
v v sinh an ton thc phm i vi sa v sn phm sa bin
son, Cc An ton v sinh thc phm trnh duyt v c ban hnh
theo Thng t s 33/2010/TT-BYT ngy 02 thng 6 nm 2010 ca
B trng B Y t.

QCVN 5-4:2010/BYT

QUY CHUN K THUT QUC GIA

I VI CC SN PHM CHT BO T SA
National technical regulation for dairy fat products

I. QUY NH CHUNG
1. Phm vi iu chnh
Quy chun ny quy nh cc ch tiu an ton thc phm v cc yu cu qun l
i vi cc sn phm cht bo t sa, bao gm cc sn phm cream (ngoi tr
cream bt), b, du b, cht bo sa v cht bo t sa dng pht.
2. i tng p dng
Quy chun ny p dng i vi:
a) Cc t chc, c nhn nhp khu, sn xut, kinh doanh cc sn phm cht
bo t sa ti Vit Nam;
t chc, c nhn c lin quan.
3. Gii thch t ng
Trong Quy chun ny, cc t ng di y c hiu nh sau:
3.1. Cream dng lng
L sn phm giu cht bo, dng nh tng thu c bng cch tch l hc
t sa.
3.2. B
L sn phm cht bo c ch bin t sa hoc sn phm sa, ch yu di
dng nh tng.
3.3. Cht bo sa (milkfat) v du b (butteroil); cht bo sa tch nc
(anhydrous milkfat) v du b tch nc (anhydrous butteroil)
L sn phm cht bo c ngun gc t sa hoc sn phm sa, c ch
bin bng cc phng php sao cho tch c hu ht nc v cht kh khng bo.
3.4. Cht bo t sa dng pht
L sn phm cht bo c ngun gc t sa, dng nh tng hoc dng
mm c th pht c.

QCVN 5-4:2010/BYT
II. QUY NH V K THUT
1. Cc ch tiu lin quan n an ton thc phm i vi cc sn phm
cht bo t sa
1.1. Cc ch tiu l ho c quy nh ti Ph lc I ca Quy chun ny.
1.2. Gii hn ti a cc cht nhim bn c quy nh ti Ph lc II ca Quy chun
ny.
1.3. Cc ch tiu vi sinh vt c quy nh ti Ph lc III ca Quy chun ny.
1.4. Danh mc ph gia thc phm c php s dng ph hp vi quy nh
hin hnh.
1.5. C th s dng cc phng php th c chnh xc tng ng vi
cc phng php quy nh km theo cc ch tiu trong cc Ph lc I, Ph lc II v
Ph lc III ca Quy chun ny.
1.6. S hiu v tn y ca phng php ly mu v cc phng php th
c quy nh ti Ph lc IV ca Quy chun ny.
1.7. Trong trng hp cn kim tra cc ch tiu cha quy nh phng php
th ti Quy chun ny, B Y t s quyt nh phng php th cn c theo cc
phng php hin hnh trong nc hoc ngoi nc c xc nhn gi tr s
dng.
2. Ghi nhn
Vic ghi nhn cc sn phm cht bo t sa phi theo ng quy nh ti Ngh
nh s 89/2006/N-CP ngy 30/8/2006 ca Chnh ph v nhn hng ho v cc
vn bn hng dn thi hnh.
III. QUY NH V QUN L
1. Cng b hp quy
1.1. Cc sn phm cht bo t sa c nhp khu, sn xut, kinh doanh
trong nc phi c cng b hp quy ph hp vi cc quy nh ti Quy chun ny.
1.2. Phng thc, trnh t, th tc cng b hp quy c thc hin theo Quy
nh v chng nhn hp chun, chng nhn hp quy v cng b hp chun, cng
b hp quy c ban hnh km theo Quyt nh s 24/2007/Q-BKHCN ngy 28

QCVN 5-4:2010/BYT
thng 9 nm 2007 ca B trng B Khoa hc v Cng ngh v cc quy nh ca
php lut.
2. Kim tra i vi cc sn phm cht bo t sa
Vic kim tra cht lng, v sinh an ton i vi cc sn phm cht bo t sa
phi c thc hin theo cc quy nh ca php lut.
IV. TRCH NHIM CA T CHC, C NHN
1. T chc, c nhn nhp khu, sn xut cc sn phm cht bo t sa phi
cng b hp quy ph hp vi cc quy nh k thut ti Quy chun ny, ng k bn
cng b hp quy ti c quan qun l nh nc c thm quyn theo phn cp ca B
Y t v bo m cht lng, v sinh an ton theo ng ni dung cng b.
2. T chc, c nhn ch c nhp khu, sn xut, kinh doanh cc sn phm
cht bo t sa sau khi hon tt ng k bn cng b hp quy v bo m cht
lng, v sinh an ton, ghi nhn ph hp vi cc quy nh ca php lut.
V. T CHC THC HIN
1. Giao Cc An ton v sinh thc phm ch tr, phi hp vi cc c quan chc
nng c lin quan hng dn trin khai v t chc vic thc hin Quy chun ny.
2. Cn c vo yu cu qun l, Cc An ton v sinh thc phm c trch nhim
kin ngh B Y t sa i, b sung Quy chun ny.
3. Trong trng hp cc tiu chun v quy nh php lut c vin dn trong
Quy chun ny c s thay i, b sung hoc c thay th th p dng theo vn bn
mi.

QCVN 5-4:2010/BYT
Ph lc I
CC CH TIU L HO CA CC SN PHM CHT BO T SA
Tn ch tiu

Mc quy
nh

Phng php th

Phn loi
ch tiu 1)

10

ISO 2450:1999

1. m, % khi lng, khng ln

hn

16

TCVN 8151-1:2009
(ISO 3727-1:2001)

2. Hm lng cht bo sa, % khi

lng, khng nh hn

80

TCVN 8151-3:2009
(ISO 3727-3:2003);
TCVN 8154:2009
(ISO 17189:2003)

3. Ch s peroxyd, mili ng lng

oxy hot ng/kg cht bo

0,3

ISO 3976:2006

I. Cream dng lng

1. Hm lng cht bo sa, % khi
lng, khng nh hn
II. B

III. Cht bo sa (milkfat) v du b (butter oil)

1. Hm lng cht bo sa, % khi
lng, khng nh hn

99,6

TCVN 8154:2009
(ISO 17189:2003)

2. Ch s peroxyd, mili ng lng

oxy hot ng/kg cht bo

0,6

ISO 3976:2006

IV. Cht bo sa tch nc (anhydrous milkfat) v du b tch nc

(anhydrous butter oil)
1. Hm lng nc, % khi lng,
khng ln hn

0,1

TCVN 7728:2007
(ISO 5536:2002)

2. Hm lng cht bo sa, % khi

lng, khng nh hn

99,8

TCVN 8154:2009
(ISO 17189:2003)

3. Ch s peroxyd, mili ng lng

oxy hot ng/kg cht bo

0,3

ISO 3976:2006

t 10 n
di 80

TCVN 8154:2009
(ISO 17189:2003)

V. Cht bo t sa dng pht

1. Hm lng cht bo sa, % khi
lng
1)

.
,

ch bin cc sn phm cht bo t sa

QCVN 5-4:2010/BYT
Ph lc II
GII HN CC CHT NHIM BN
I VI CREAM V CC SN PHM CHT BO T SA
Tn ch tiu

Gii hn
ti a

Phng php th

Phn loi
ch tiu 2)

1. Ch, mg/kg

0,02

TCVN 7933:2008
(ISO 6733:2006),
TCVN 7929:2008
(EN 14083:2003)

2. Thic (i vi sn phm ng
trong bao b trng thic), mg/kg

250

TCVN 7730:2007
(ISO/TS 9941:2005),
TCVN 8110:2009
(ISO 14377:2002),
TCVN 7788:2007

3. Stibi, mg/kg

1,0

TCVN 8132:2009

4. Arsen, mg/kg

0,5

TCVN 7601:2007

5. Cadmi, mg/kg

1,0

TCVN 7603:2007,
TCVN 7929:2008
(EN 14083:2003)

6. Thu ngn, mg/kg

0,05

TCVN 7993:2008
(EN 13806:2002)

0,5

TCVN 6685:2009
(ISO 14501:2007)

2,5

Thng quy k thut

nh lng melamin
trong thc phm
(Q 4143/Q-BYT)

TCVN 8106:2009
(ISO/TS 26844:2006);

I. Kim loi nng

II. c t vi nm
1. Aflatoxin M1, g/kg
III. Melamin
1. Melamin, mg/kg

IV. D lng thuc th y, g/kg

1. Benzylpenicilin/Procain
benzylpenicilin

AOAC 988.08
2. Clortetracyclin/Oxytetracyclin/
Tetracyclin

100

TCVN 8106:2009
(ISO/TS 26844:2006);
AOAC 995.04

QCVN 5-4:2010/BYT
Tn ch tiu

Gii hn
ti a

Phng php th

Phn loi
ch tiu 2)

3. Dihydrostreptomycin/Streptomycin

200

TCVN 8106:2009
(ISO/TS 26844:2006);
AOAC 988.08;

4. Gentamicin

200

TCVN 8106:2009
(ISO/TS 26844:2006)

5. Spiramycin

200

TCVN 8106:2009
(ISO/TS 26844:2006)

6. Ceftiofur

100

TCVN 8106:2009
(ISO/TS 26844:2006)

7. Clenbuterol

50

8. Cyfluthrin 3)

40

TCVN 8101:2009
(ISO 8260:2008)

9. Cyhalothrin 3)

30

AOAC 998.01

10. Cypermethrin v alphacypermethrin

100

US FDA PAM, Vol. I,

Section 304, E4/C2, C4;

TCVN 8101:2009
(ISO 8260:2008)
11. Deltamethrin 3)

30

12. Diminazen

150

13. Doramectin

15

14. Eprinomectin

20

15. Febantel/ Fenbendazol/

Oxfendazol

100

16. Imidocarb

50

17. Isometamidium

100

18. Ivermectin

10

19. Lincomycin

150

AOAC 988.08

20. Neomycin

1500

TCVN 8106:2009
(ISO/TS 26844:2006)

21. Pirlimycin

200

22. Spectinomycin

200

TCVN 8101:2009
(ISO 8260:2008)

QCVN 5-4:2010/BYT
Tn ch tiu

Gii hn
ti a

Phng php th

Phn loi
ch tiu 2)

23. Sulfadimidin

25

AOAC 992.21

24. Thiabendazol 3)

100

25. Triclorfon (Metrifonat) 3)

50

V. D lng thuc bo v thc vt 4), mg/kg

V.1. i vi thuc bo v thc vt tan trong nc hoc tan mt phn trong cht
bo
1. Endosulfan

0,01

TCVN 7082:2002
(ISO 3890:2000),
phn 1 v phn 2;
TCVN 8170:2009 (EN
1528:1996), phn 1,
2, 3 v 4

2. 2,4-D

0,01

US FDA PAM, Vol. I,

Section 402, E1

3. Abamectin

0,005

4. Acephat

0,02

AOAC 970.52

5. Aldicarb

0,01

US FDA PAM, Vol. I,

Section 401, E1+DL1

6. Aminopyralid

0,02

7. Amitraz

0,01

8. Bentazon

0,05

9. Bifenazat

0,01

10. Bifenthrin

0,05

11. Bitertanol

0,05

12. Carbaryl

0,05

AOAC 970.52

B
B

AOAC 964.18;

US FDA PAM, Vol. I,

Section 401, E1+DL1
13. Carbendazim

0,05

14. Carbofuran

0,05

15. Carbosulfan

0,03

16. Clormequat

0,5

US FDA PAM, Vol. I,

Section 401, E1, DL1

QCVN 5-4:2010/BYT
Tn ch tiu

Gii hn
ti a

Phng php th

Phn loi
ch tiu 2)

0,0005

US FDA PAM, Vol. I,

Section 304, E4, C1C4

18. Clorpyrifos

0,02

TCVN 8101:2009
(ISO 8260:2008)

19. Clorpyrifos-methyl

0,01

TCVN 8101:2009
(ISO 8260:2008)

20. Clethodim

0,05

21. Clofentezin

0,05

22. Cyhexatin

0,05

23. Cyprodinil

0,0004

24. Cyromazin

0,01

25. Diclorvos

0,02

26. Difenoconazol

0,005

27. Dimethenamid-p

0,01

28. Dimethipin

0,01

29. Dimethoat

0,05

30. Dimethomorph

0,01

31. Diquat

0,01

32. Disulfoton

0,01

33. Dithiocarbamat

0,05

34. Ethephon

0,05

35. Ethoprophos

0,01

36. Fenamiphos

0,005

37. Fenbuconazol

0,05

38. Fenbutatin oxid

0,05

39. Fenpropimorph

0,01

40. Fipronil

0,02

41. Fludioxonil

0,01

17. Clorpropham

TCVN 8101:2009
(ISO 8260:2008)

AOAC 970.52

US FDA PAM, Vol. I,

Section 304, E4, C1, C3

US FDA PAM, Vol. I,

Section 304, E4, C1-C4

B
B

QCVN 5-4:2010/BYT
Tn ch tiu

Gii hn
ti a

Phng php th

Phn loi
ch tiu 2)

42. Flutolanil

0,05

43. Glufosinat-amoni

0,02

44. Imidacloprid

0,02

45. Indoxacarb

0,1

46. Kresoxim-methyl

0,01

47. Lindan

0,01

48. Methamidophos

0,02

49. Methidathion

0,001

US FDA PAM, Vol. I,

Section 304, E4, C2, C4

50. Methomyl

0,02

US FDA PAM, Vol. I,

Section 401, E1, DL1

51. Methoxyfenozid

0,01

52. Myclobutanil

0,01

53. Novaluron

0,4

54. Oxamyl

0,02

55. Oxydemeton-methyl

0,01

56. Paraquat

0,005

57. Penconazol

0,01

58. Pirimicarb

0,01

59. Pirimiphos-methyl

0,01

60. Procloraz

0,05

61. Profenofos

0,01

62. Propamocarb

0,01

63. Propiconazol

0,01

64. Pyraclostrobin

0,03

65. Pyrimethanil

0,01

66. Quinoxyfen

0,01

AOAC 970.52

B
B

US FDA PAM, Vol. I,

Section 401, E1, DL1

TCVN 8101:2009
(ISO 8260:2008)

B
B

US FDA PAM, Vol. I,

Section 304, E4, C1, C3

US FDA PAM, Vol. I,

Section 304, E4, C1-C4

B
B

QCVN 5-4:2010/BYT
Tn ch tiu
67. Spinosad

Gii hn
ti a

Phng php th

Phn loi
ch tiu 2)

68. Tebuconazol

0,01

69. Tebufenozid

0,01

70. Terbufos

0,01

71. Thiacloprid

0,05

72. Triadimefon

0,01

73. Triadimenol

0,01

74. Trifloxystrobin

0,02

75. Vinclozolin

0,05

US FDA PAM, Vol. I,

Section 304, C1-C4

B
B

US FDA PAM, Vol. I,

Section 304, C1, C3

US FDA PAM, Vol. I,

Section 304, C1-C3;
E1-E5+C6

V.2. i vi thuc bo v thc vt tan trong cht bo 5)

1. Aldrin v dieldrin

0,006

TCVN 7082:2002
(ISO 3890:2000),
phn 1 v phn 2;
TCVN 8101:2009
(ISO 8260:2008);
TCVN 8170:2009 (EN
1528:1996), phn 1,
2, 3 v 4

2. Cyfluthrin 6)

0,04

TCVN 8101:2009
(ISO 8260:2008)

3. Clordan

0,002

TCVN 7082:2002
(ISO 3890:2000),
phn 1 v phn 2;
TCVN 8170:2009 (EN
1528:1996), phn 1,
2, 3 v 4

4. Cypermethrin

0,05

US FDA PAM, Vol. I,

Section 304, E4/C2, C4;

TCVN 8101:2009
(ISO 8260:2008)

10

QCVN 5-4:2010/BYT
Tn ch tiu

Gii hn
ti a

Phng php th

Phn loi
ch tiu 2)

5. DDT

0,02

TCVN 7082:2002
(ISO 3890:2000),
phn 1 v phn 2;
TCVN 8170:2009 (EN
1528:1996), phn 1,
2, 3 v 4

6. Deltamethrin 6)

0,05

TCVN 8101:2009
(ISO 8260:2008)

7. Diazinon

0,02

TCVN 8101:2009
(ISO 8260:2008)

8. Dicofol

0,1

TCVN 8101:2009
(ISO 8260:2008)

9. Diflubenzuron

0,02

10. Diphenylamin

0,0004

11. Famoxadin

0,03

12. Fenhexamid

0,01

13. Fenpropathrin

0,1

14. Fenpyroximat

0,005

US FDA PAM Vol. I,

Section 304, E4, C1-C4

B
B

15. Fenvalerat

0,1

TCVN 8101:2009
(ISO 8260:2008);
AOAC 998.01

16. Flumethrin

0,05

17. Flusilazol

0,05

18. Heptaclor

0,006

19. Methopren

0,1

20. Permethrin

0,1

TCVN 8101:2009
(ISO 8260:2008)

21. Phorat

0,01

US FDA PAM Vol. I,

Section 304, C2, C4

TCVN 7082:2002
(ISO 3890:2000),
phn 1 v phn 2;
TCVN 8170:2009 (EN
1528:1996), phn 1,
2, 3 v 4

11

QCVN 5-4:2010/BYT
Tn ch tiu

Gii hn
ti a

Phng php th

Phn loi
ch tiu 2)

22. Piperonyl butoxid

0,05

US FDA PAM Vol. I,

Section 401, E1, DL2

23. Propargit

0,1

US FDA PAM Vol. I,

Section 304, E4+C6

2)

, ch bin cc sn phm cht bo t sa

i vi ch tiu

loi B.
3)

Cng c dng lm thuc bo v thc vt.

4)

Tham kho cc phng php th trong TCVN 5142:2008 (CODEX STAN 229-1993,

Rev.1-2003) Phn tch d lng thuc bo v thc vt Cc phng php khuyn co.
5)

Gii hn ny quy nh cho sn phm sa thanh trng v sa tit trng. i vi cream v

cc sn phm cht bo t sa, p dng mc gii hn bng 25 ln quy nh ny, tnh trn c
s cht bo trong sn phm sa.
6)

Cng c dng lm thuc th y.

12

QCVN 5-4:2010/BYT
Ph lc III
CC CH TIU VI SINH VT CA CC SN PHM CHT BO T SA
Tn ch tiu

Gii hn ti a cho php

m 9)

Phng php th

M 10)

Phn
loi ch
tiu 11)

n 7)

c 8)

1. E. coli

2. L. monocytogenes

100 CFU/g

TCVN 7700-2:2007
(ISO 11290-2:1998,
With amd.1:2004)

Khng pht
hin trong 25 g

TCVN 4829:2005
(ISO 6579:2002,
With amd.1:2004)

I. Cream v b
10
100
TCVN 7924-1:2008
CFU/g CFU/g (ISO 16649-1:2001);
TCVN 7924-2:2008
(ISO 16649-2:2001)

(i vi sn phm
dng ngay)
3. Salmonella

II. Cht bo sa (milkfat) v du b (butteroil); cht bo sa tch nc

(anhydrous milkfat) v du b tch nc (anhydrous butteroil) v cht bo
t sa dng pht
L. monocytogenes (i
vi sn phm dng
ngay)

100 CFU/g

TCVN 7700-2:2007
(ISO 11290-2:1998,
With amd.1:2004)

7)

n: s n v mu c ly t l hng cn kim tra.

8)

c: s n v mu ti a c kt qu nm gia m v M, tng s mu c kt qu nm gia m

v M vt qu c l khng t.
9)

m: l mc gii hn m cc kt qu khng vt qu mc ny l t, nu cc kt qu vt

qu mc ny th c th t hoc khng t.
10)

11)

M: l mc gii hn ti a m khng mu no c php vt qu.

.

13

QCVN 5-4:2010/BYT
Ph lc IV
DANH MC PHNG PHP TH CC CH TIU AN TON THC PHM
I VI CC SN PHM CHT BO T SA

I. Ly mu
1. TCVN 6400 (ISO 707) Sa v sn phm sa Hng dn ly mu.
II. Phng php th cc ch tiu l ho
1. ISO 2450:1999 Cream Determination of fat content Gravimetric method
(Reference method) [Cream Xc nh hm lng cht bo Phng php khi
lng (Phng php chun)]
2. ISO 3976:2006 Milk fat Determination of peroxide value (Cht bo sa Xc
nh ch s peroxit)
3. TCVN 7728:2007 (ISO 5536:2002) Sn phm cht bo sa Xc nh hm
lng nc Phng php Karl Fischer
4. TCVN 8151-1:2009 (ISO 3727-1:2001) B Xc nh m, hm lng cht
kh khng bo v hm lng cht bo Phn 1: Xc nh m (Phng php
chun)
5. TCVN 8151-3:2009 (ISO 3727-3:2003) B Xc nh m, hm lng cht
kh khng bo v hm lng cht bo Phn 3: Tnh hm lng cht bo
6. TCVN 8154:2009 (ISO 17189:2003) B, nh tng du thc phm v cht bo
dng pht Xc nh hm lng cht bo (Phng php chun)
III. Phng php th cc cht nhim bn
III.1. Kim loi nng
1. TCVN 6270:1997 (ISO 6732:1985) Sa v cc sn phm sa Xc nh hm
lng st Phng php quang ph (Phng php chun)
2. TCVN 6352:1998 (ISO 8294:1998) Du, m ng vt v thc vt Xc nh
hm lng ng, st, niken Phng php quang ph hp th nguyn t dng
l graphit
3. TCVN 6353:2007 (ISO 12193:2004) Du m ng vt v thc vt Xc nh ch
bng phng php quang ph hp th nguyn t trc tip dng l graphit

14

QCVN 5-4:2010/BYT
4. TCVN 6354:1998 Du, m ng vt v thc vt Xc nh asen bng phng
php dng bc dietyldithiocacbamat
5. TCVN 7601:2007 Thc phm Xc nh hm lng asen bng phng php
bc dietyldithiocacbamat
6. TCVN 7603:2007 Thc phm Xc nh hm lng cadimi bng phng php
quang ph hp th nguyn t
7. TCVN 7730:2007 (ISO/TS 9941:2005) Sa v sa c c ng hp Xc nh
hm lng thic Phng php o ph
8. TCVN 7788:2007 hp thc phm Xc nh hm lng thic bng phng
php quang ph hp th nguyn t
9. TCVN 7929:2008 (EN 14083:2003) Thc phm Xc nh cc nguyn t vt
Xc nh ch, cadimi, crom, molypden bng o ph hp th nguyn t dng l
graphit (GFAAS) sau khi phn hu bng p lc
10. TCVN 7933:2008 (ISO 6733:2006) Sa v sn phm sa
ch

Xc nh hm lng

Phng php quang ph hp th nguyn t dng l graphit

11. TCVN 7993:2008 (EN 13806:2002) Thc phm Xc nh cc nguyn t vt

Xc nh thu ngn bng o ph hp th nguyn t hi-lnh (CVAAS) sau khi
phn hu bng p lc
III.2. c t vi nm
1. TCVN 6685:2009 (ISO 14501:2007) Sa v sa bt Xc nh hm lng
aflatoxin M1 Lm sch bng sc k i lc min dch v xc nh bng sc k
lng hiu nng cao
III.3. Melamin
1. Thng quy k thut nh lng melamin trong thc phm, c c ban hnh
km theo Quyt nh s 4143/Q-BYT ngy 22 thng 10 nm 2008
III.4. D lng thuc th y
1. TCVN 8101:2009 (ISO 8260:2008) Sa v sn phm sa Xc nh thuc bo
v thc vt nhm clo hu c v polyclo biphenyl Phng php sc k kh-lng
mao qun c detector bt gi electron
2. TCVN 8106:2009 (ISO/TS 26844:2006) Sa v sn phm sa
lng khng sinh

Xc nh d

Php th phn tn trong ng nghim

15

QCVN 5-4:2010/BYT
3. AOAC 988.08 Antimicrobial Drugs in Milk. Microbial Receptor Assay (Thuc
khng sinh trong sa)
4. AOAC 992.21 Sulfamethazine Residues in Raw Bovine Milk (D lng
sulfamethazine trong sa b ti)
5. AOAC 995.04 Multiple Tetracycline Residues in Milk. Metal Chelate Affinity-Liquid
Chromatographic Method (D lng tetracycline trong sa. Phng php i lc
chelat kim loi-sc k lng)
6. AOAC 995.09 Chlortetracycline, Oxytetracycline, and Tetracycline in Edible
Animal

Tissues.

Liquid

Chromatographic

Method

(Chlortetracycline,

oxytetracycline v tetracycline trong tht ng vt. Phng php sc k lng)

7. AOAC 998.01 Synthetic Pyrethroids in Agricultural Products Multiresidue. GC
Method (Pyrethroid tng hp trong nng sn. Phng php sc k kh)
8. Pesticide Analytical Manual (PAM), Food and Drug Administration, Washington,
D.C., USA, Vol. I, 3rd edition, Section 304
9. Pesticide Analytical Manual (PAM), Food and Drug Administration, Washington,
D.C., USA, Vol. I, 3rd edition, Section 401
10. Pesticide Analytical Manual (PAM), Food and Drug Administration, Washington,
D.C., USA, Vol. I, 3rd edition, Section 402
III.5. D lng thuc bo v thc vt
1. TCVN 5142:2008 (CODEX STAN 229-1993, Rev.1-2003) Phn tch d lng
thuc bo v thc vt Cc phng php khuyn co
2. TCVN 7082-1:2002 (ISO 3890-1:2000) Sa v sn phm sa Xc nh d
lng hp cht clo hu c (thuc tr su) Phn 1: Xem xt chung v phng
php chit
3. TCVN 7082-2:2002 (ISO 3890-2:2000) Sa v sn phm sa Xc nh d
lng hp cht clo hu c (thuc tr su) Phn 2: Phng php lm sch
dch chit th v th khng nh
4. TCVN 8101:2009 (ISO 8260:2008) Sa v sn phm sa Xc nh thuc bo
v thc vt nhm clo hu c v polyclo biphenyl Phng php sc k kh-lng
mao qun c detector bt gi electron
5. TCVN 8170-1:2009 (EN 1528-1:1996) Thc phm cha cht bo Xc nh
thuc bo v thc vt v polyclo biphenyl (PCB) Phn 1: Yu cu chung

16

QCVN 5-4:2010/BYT
6. TCVN 8170-2:2009 (EN 1528-2:1996) Thc phm cha cht bo Xc nh
thuc bo v thc vt v polyclo biphenyl (PCB) Phn 2: Chit cht bo, thuc
bo v thc vt, PCB v xc nh hm lng cht bo
7. TCVN 8170-3:2009 (EN 1528-3:1996) Thc phm cha cht bo Xc nh
thuc bo v thc vt v polyclo biphenyl (PCB) Phn 3: Cc phng php
lm sch
8. TCVN 8170-4:2009 (EN 1528-4:1996) Thc phm cha cht bo Xc nh
thuc bo v thc vt v polyclo biphenyl (PCB) Phn 4: Xc nh, khng nh,
cc qui trnh khc
9. AOAC 964.18

Carbaryl Pesticide Residues. Colorimetric Method (D lng

thuc bo v thc vt carbaryl. Phng php o mu)

10. AOAC 970.52 Organochlorine and Organophosphorus Pesticide Residues.
General Multiresidue Method (D lng thuc bo v thc vt clo hu c v
phospho hu c. Phng php a d lng)
IV. Phng php th cc ch tiu vi sinh vt
1. TCVN 4829:2005 (ISO 6579:2002, With amd.1:2004)

Vi sinh vt trong thc

phm v thc n chn nui Phng php pht hin Salmonella trn a thch
2. TCVN 7700-2:2007 (ISO 11290-2:1998, With amd.1:2004) Vi sinh vt trong thc
phm v thc n chn nui Phng php pht hin v nh lng Listeria
monocytogenes Phn 2: Phng php nh lng
3. TCVN 7924-1:2008 (ISO 16649-1:2001) Vi sinh vt trong thc phm v thc n
chn nui Phng php nh lng Escherichia coli dng tnh

glucuronidaza Phn 1: K thut m khun lc 44 oC s dng mng lc v 5bromo-4-clo-3-indolyl -D-glucuronid

4. TCVN 7924-2:2008 (ISO 16649-2:2001) Vi sinh vt trong thc phm v thc n
chn nui Phng php nh lng Escherichia coli dng tnh

glucuronidaza Phn 2: K thut m khun lc 44 C s dng 5-bromo-4-clo3-indolyl -D-glucuronid

17