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Coeus.vn a5.CHẤT LÀM BÓNG
Coeus.vn a5.CHẤT LÀM BÓNG
Coeus.vn a5.CHẤT LÀM BÓNG
H NI - 2011
Li ni u
QCVN 4-20:2011/BYT do Ban son tho quy chun k thut
quc gia v Ph gia thc phm v cht h tr ch bin bin
son, Cc An ton v sinh thc phm trnh duyt v c ban
hnh theo Thng t s 01/2011/TT-BYT ngy 13 thng 01 nm
2011 ca B trng B Y t.
I. QUY NH CHUNG
1. Phm vi iu chnh
Quy chun k thut quc gia (sau y gi tt l Quy chun) ny quy nh cc yu cu
k thut v qun l v cht lng, v sinh an ton i vi cc cht lm bng c s dng
vi mc ch lm ph gia thc phm.
2. i tng p dng
Quy chun ny p dng i vi:
2.1. T chc, c nhn nhp khu, xut khu, sn xut, bun bn v s dng cc
cht lm bng lm ph gia thc phm (sau y gi tt l t chc, c nhn).
2.2. C quan qun l nh nc c lin quan.
3. Gii thch t ng v ch vit tt:
3.1. Cht lm bng: l ph gia thc phm c cho thm vo b mt pha
ngoi ca thc phm nhm to bng hoc to lp bo v.
3.2. JECFA monograph 1 - Vol. 4 (JECFA monographs 1 - Combined
compendium of food additive specifications; Joint FAO/WHO expert committee on
food additives; Volume 4 - Analytical methods, test procedures and laboratory
solutions used by and referenced in the food additive specifications; FAO, 2006): Cc
yu cu k thut i vi ph gia thc phm, Tp 4 Cc phng php phn tch, quy
trnh th nghim, dung dch th nghim c s dng (hoc tham chiu) trong yu
cu k thut i vi ph gia thc phm; JECFA bin son; FAO ban hnh nm 2006.
3.3. M s C.A.S (Chemical Abstracts Service): M s ng k ha cht ca
Hip hi Ha cht Hoa K.
3.4. TS (test solution): Dung dch thuc th.
3.5. ADI (Acceptable daily intake): Lng n vo hng ngy chp nhn c.
3.6. INS (International numbering system): H thng m s quc t v ph gia
thc phm.
Ph lc 1:
1.2.
Ph lc 2:
1.3.
Ph lc 3:
1.4.
Ph lc 4:
1.5.
Ph lc 5:
Beeswax
INS 901
2. nh ngha
M s C.A.S.
3. Cm quan
4. Chc nng
5. Yu cu k thut
5.1. nh tnh
tan
62 65C
Ch s acid
17 24
Ch s peroxyd
Ch s x phng ha
87 104
Sp carnauba
Ch
6. Phng php th
6.1. tinh khit
Ch s peroxyd
Ch s peroxyd =
(a
b) N 1000
m
Trong :
a = s mL natri thiosulfat dng cho mu th
b = s mL natri thiosulfat dng cho mu trng
N = nng ng lng ca natri thiosulfat
m = khi lng mu (g)
Sp carnauba
Ch
INS 902
2. nh ngha
M s C.A.S.
8006-44-8
3. Cm quan
4. Chc nng
5. Yu cu k thut
5.1. nh tnh
tan
hp th hng
ngoi
68,50 72,50
Ch s acid
T 12 n 22
Ch s x phng ha
T 43 n 65.
Ch
Khng c qu 2 mg/kg.
6. Phng php th
tinh khit
Ch
INS 904
2. nh ngha
M s C.A.S
9000-59-3
3. Cm quan
4. Chc nng
5. Yu cu k thut
5.1. nh tnh
Phn ng mu
tan
Khng tan trong nc; tan chm trong ethanol; t tan trong
aceton v ether.
Ch s acid
Rosin
Sp
Ch
6. Phng php th
6.1. nh tnh
Phn ng mu
Sp
Ch
2. nh ngha
M s C.A.S
8012-95-1
3. Cm quan
4. Chc nng
5. Yu cu k thut
5.1. nh tnh
tan
Khng tan trong nc, t tan trong ethanol, tan trong ether
t chy
Khng nh hn 11 cSt
S carbon im
chng ct 5%
Khng nh hn 28
im si im chng ct 5% cao hn 4220C
Khng nh hn 500
t yu cu.
Cc cht d than ho
t yu cu.
Hydrocarbon a vng
thm
t yu cu.
Parafin rn
Ch
6. Phng php th
tinh khit
12
Parafin rn
Ch
13
Petroleum wax;
INS 905c
2. nh ngha
3. Cm quan
4. Chc nng
5. Yu cu k thut
5.1. nh tnh
tan
Ch s khc x
Ph hp th hng ngoi
Khng c nh hn 11 mm2/giy
Xem m t trong phn Phng php th
S carbon im
chng ct 5%
Khng nh hn 500
Xem m t trong phn Phng php th
Khng c qu 0,1%
Xem m t trong phn Phng php th
Mu sc
Lu hunh
Khng c qu 0,4%
Xem m t trong phn Phng php th
Ch
Hydrocarbon a vng
thm
hp th cc i/chiu di
ng truyn (cm)
14
0,15
290 - 299
0,12
300 - 359
0,08
360 - 400
0,02
6. Phng php th
tinh khit
nht 1000C
S carbon im
chng ct 5%
25
30
15
15
knh
trong
0,32
0,53
0,25
DB-1
methyl
silicon
RTX-1
methyl
silicon
DB-5 5%
phenyl
methyl
silicon
dy lp phim mng
(m)
0,25
0,25
0,25
Kh mang
heli
heli
heli
Tc dng (ml/pht)
1,56
5,0
2,3
Tc tuyn (cm/giy)
33
35
60
800C
800C
800C
10
3800C
3400C
3500C
ngui trn
ct
ngui
trn ct
ngui
trn ct
Detector
FID
FID
FID
Nhit
3800C
3400C
3750C
1,0
1,0
1,0
Pha tnh
nng
nhit
16
Trong :
CISTP: Nng ca n C16 trong dung dch ni chun long
(% theo khi lng)
WS: Khi lng dung dch gc (g)
Kim tra mu trng:
Bm 1 l dung mi. Khng c pick no c pht hin trong
khong thi gian lu m sp ra gii.
phn gii ct:
Bm 1 l dung dch 0,05% mi n C20 v n C24 trong
cyclohexan. phn gii ct R khng c nh hn 30 c
tnh ton theo cng thc sau:
Trong :
d: Khong cch gia cc i pic ca n C20 v n C24 (mm)
W1: Pic bng mt na chiu cao ca n C20 (mm)
W2: Pic bng mt na chiu cao ca n C24 (mm)
tuyn tnh:
Phn tch chun tuyn tnh. Cc h s p ng khi lng
tnh ton lin quan n hexadecan phi trong khong 0,90
1,10.
lp li thi gian lu:
Phn tch chun tuyn tnh 2 ln. Cc thi gian lu i vi
17
Trong :
i: S carbon
Ci: Hm lng cc thnh phn c s carbon i (%)
19
Mu sc
Lu hunh
Trong :
A: S m ca nhy chun c xc nh ti thi im
hiu chnh
B: S m ca nhy chun c xc nh ti thi gian
phn tch
Cch tin hnh:
mu trong cng o thch hp. Mc d bc x lu hunh
xuyn qua ch mt khong nh trong mu, phn tn t cc
mu v mu c th khc nhau n mc m mt lng c th
hoc mt lng ti thiu mu phi c s dng.
t mu trong chm tia X v cho php kh quyn quang hc
tia X n trng thi cn bng. Xc nh cng ca bc
x K lu hunh ti 5,373 bng cch o tc m ti
nhng ch gc chnh xc t cho bc sng ny. o tc
m nn ti 5,190 .
Tnh kt qu:
Hm lng lu hunh trong mu c tnh theo cng thc
sau:
Trong :
R: Tc m thc c hiu chnh
CK: Tng s m thu c ti 5,373 i vi mu
S1: Thi gian cn thit thu c cc s CK (giy)
CB: Tng s m thu c ti 5,190 i vi nn
S2: Thi gian cn thit thu c cc s CB (giy)
F: Tc m ti 5,373 / tc m ti 5,190 i vi
mu khng cha lu hunh
F: H s hiu chnh i vi cc thay i nhy thit b hng
ngy.
S dng tc m thc hiu chnh, c nng lu
hunh t ng chun.
21
25
Ph hng ngoi
Sp vi tinh th
29