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Polyethylene Bottle Trouble SHooting Guide
Polyethylene Bottle Trouble SHooting Guide
Polyethylene Bottle Trouble SHooting Guide
Terephthalate
(PET)
Processing Guidelines
Troubleshooting Guide
Injection Moulding
Stretch Blow Moulding
Recommended Tests & Equipment
INDEX
PROCESSING GUIDELINES
Drying
Drying Conditions
Dryer Startup
Dryer Specification
Injection Moulding
Resin Inlet Temperature
Barrel Temperature
Nozzle Temperature
Manifold Hot Runner Temperature
Injection Speed
Stretch Blow Moulding
TROUBLESHOOTING GUIDE
Injection Moulding Defects
1) Short Shots
2) Sink Marks
3) Flash
4) Water Marks
5) Black Specs / Contamination
6) Flow Lines
7) Heat Splay
8) PET Inclusion
9) Concentricity
10) Crystalline Gate
11) Long Gate
12) Air Bubbles
13) Stress Pattern
14) Stringing
15) Cloudy Preforms
16) Hollow Gates
17) Discolored Preforms
18) Line Over Finish
19) Burnt Gates
20) Oval Finish
21) Gas Burns
22) High Acetaldehyde
PROCESSING GUIDELINES
THE processing guidelines set out below cover the two major processes involved in the
conversion of PET resin into preforms and containers, namely:
1. INJECTION MOLDING
2. STRETCH BLOW MOLDING.
The resin preparation conditions and barrel temperature profile recommended on the injection
molder could also be used on extrusion barrel, in converting PET resin into amorphous sheet.
DRYING:
Drying Conditions:
This is the first and most crucial step in converting PET resin into perform/container/sheet. If the
drying equipment is not adequate or is not functioning efficiently then it is highly unlikely that
you will produce an acceptable product. The dried resin should have a moisture content not more
than 50 PPM.
Recommended Drying Temperature: 160 - 180 C
Recommended Drying Time
5- 6 hours
Dryer Start-Up :
The time / temperature profile recommended when first starting the dryer or starting from a
major shut down is as below. The first hour at 120 The next two hours 150 The next two hours
180 C
Dryer Specification:
Able to heat air up to 200 C Able to deliver air flow rate in the order of 0.062 metre cube/ min
per kg/ hr of resin being processed. Able to deliver hot dehumidified air with a minimum of
40.0C dew point.
Dryer Resin Level:
To give approximately 5 to 6times the kg/hr capacity of the injection molder or extruder incase
of sheet extrusion.
INJECTION MOLDING PROCESS:
This is the process by which the resin is converted from dried pellets to perform.
Resin Inlet Temperature:
It is better to have a temperature of 160 -170 C on the resin entering the feed zone of the
extruder.
Barrel Temperature Profile:
For other than water grade resin it is recommended to use a temperature of 265C in the feed
zone gradually increasing towards the metering zone 280 C. For the water grade resin however,
it is recommended to use a reverse temperature profile, with highest temperature in the feed
zone, say 280 C and gradually lowering towards the metering zone.
Recommended temperature: 265 - 280 C
Nozzle Temperature:
Recommended temperature: 270 - 280 C
Manifold Hot Runner Temperature:
Recommended temperature: 270 - 280 C
Mold Cooling Water Inlet Temperature:
Recommended temperature: 7 to 8 C
Injection Speed:
As required to fill the cavity with minimum shear and dependent on the gate size.
STRETCH BLOW MOLDING PROCESS:
The most commonly available stretch blow molding machines are the:Single stage stretch blow
molder ( preform & bottle made on the same machine).They are AOKI, NISSEI, UNILOY,
etc.Two stage stretch blow molder (reheating and blowing of preforms made onInjection
molder).They are SIDEL, KRUPP, SIPA, etc.The processing conditions depend on the type of
process used and the mostcommon parametersto be controlled are:
o Preform Temperature.o Re-heating oven profile and over all oven percentage.
o Oven sheilds o Bottle blowing speed, bottles/hour.
o Stretch rod speed
o Air delay time o Pre-blow pressure.
o High blow time.
o High blow pressure.
o Blow mold cooling.
Optimizing of the above parameters depend on several factors such as :
o Preform design.
o Preform intrinsic viscosity.
o Preform infrared absorbing characteristics.
o Bottle design.
TROUBLESHOOTING GUIDE
Injection Moulding
1 Problem: SHORT SHOTS
POSSIBLE CAUSES
o Injection Pressure low
o Barrel temperature low
o Mould manifold temp. low
o Mould cavity temp. low
POSSIBLE SOLUTIONS
oIncrease injection pressure
o Increase barrel temperature
o Increase mould manifold temperature
o Increase mould cavity temperature
o Injection speed low
o Back pressure low
o Increase injection speed
o Increase back pressure
o Clean vent on split, core and cavity
o Check that no foreign object is in gate area.
o Check that the gate pin is moving all the way back
2 Problem: SINK MARKS
POSSIBLE CAUSES
o Holding pressure low
o Holding time low
o High mold temperature
o Inadequate coolant supply
o Cooling time low
o Blocked venting
POSSIBLE SOLUTIONS
o Increase holding pressure
o Increase holding time
o Decrease mould temperature
o Check cooling water
o Increase cooling time
o Clean vents on split, core and cavity
3 Problem: FLASH
POSSIBLE CAUSES
o Injection pressure high
o High injection speed
o Unwanted material in cores
o Unwanted material in splits
o Unwanted material in cavity
TROUBLESHOOTING GUIDE
Stretch Blow Moulding
1 Problem: BLOWN FINISH
POSSIBLE CAUSES
o Overheating of the finish area which allows blow pressure air to stretch the material.
o Oven ambient temperature to high
o Incorrect loading height, too much of the finish is exposed to the elements
POSSIBLE SOLUTIONS
o Move shield away from finish into a thicker part of the preforms taper
o Bring shield close to perform
o Increase oven exhaust
o Reduce neck element heat
2 Problem: SEALING SURFACE DAMAGE
POSSIBLE CAUSES
o Misalignment of the preform, blow mould and blow nozzle usually caused by poor transfer arm
positioning.
o Blow mold position.
o Nozzle position.
POSSIBLE SOLUTIONS
o Realign transfer arm
o Realign blow mould or nozzle if necessary
3 Problem: CHOCKED NECK
POSSIBLE CAUSES
o Over stretching of the preform by the stretch rod prior to blow.
o Low blow delayed or missing
POSSIBLE SOLUTIONS
o Reduce air delay time
o Reduce stretch rod pressure
o Move shield into a thicker part of the taper o Increase heat in the body or base
o Increase low blow pressure
o Reduce heat in the neck
4 Problem: BENT NECK
POSSIBLE CAUSES
o Misalignment of the preform to the mould or nose.
o Distortion below the flange
a) Insufficient mould cooling
b) One mould half with poor cooling
o Excessive material remained in the neck and shoulder.
POSSIBLE SOLUTIONS
o Realignment of the preform to the nose or mould.
o Reduce material thickness in the shoulder by reducing heat in the body
o Increase high blow time
o Improve mould cooling
5 Problem: HARD NECK
POSSIBLE CAUSES
o Initial stretching occurs too lowint
o the preforms taper.
o Preform location incorrectthrough oven.
o Air leak into preform before thestart of low blow.
POSSIBLE SOLUTIONS
o Reduce heat in the body and/ or base until pearlescence occurs then increase neck temperature.
o Increase stretch rod pressure
o Increase air delay time
o Reduce low blow pressure
o Move shield into the thinner part of the taper o Check height of preform though oven.
o Check for air leak through nose
6 Problem: THIN SHOULDER
POSSIBLE CAUSES
o Excessive stretching of the taper. Stations producing a smaller low blow container will be first
withthe fault or the thinnest.
o Poor shield positioning, allowing excessive stretching of the thin part of the taper.
POSSIBLE SOLUTIONS
o Move shield into a thicker part of the preforms taper.
o Reduce air delay time
o Reduce stretch rod pressure
o Increase low blow pressure
o Reduce heat in the neck. If thickening occurs below desired area Increase heat below the neck
element.
7 Problem: HOT BOTTLES
POSSIBLE CAUSES
o Preform temperature above crystalgrowth range for to long
o Insufficient cooling of the outsidesurface for the amount of heatabsorbed by the P.E.T.
o Excessive equilibration time
oPreform wall thickness excessiveblowers.
POSSIBLE SOLUTIONS
o Reduce heat adjacent to the haze untilpearlescence is evident somewhere onthe bottle
o Reduce heat over all until pearlescenceis evident.
o Increase air circulation through oven,increase blower speed, clean blowers.
o Check high pressure. If possible. If station related check for high blow leaks from nozzle or
stretch rod
o Increase high blow time
o Reduce base weight by reducing
16 Problem: HOT SIDES
POSSIBLE CAUSES
o Inconsistent preform rotation through the oven
o Insufficient surface cooling of the preform
POSSIBLE SOLUTIONS
o Check the preform for a drag marl. Ensure oven shields are not touching the preform. Check
collect, spindle or mandrel rotation
o Increase air flow onto the surface of the preform
17 Problem: LOW HEADLOAD
POSSIBLE CAUSES
o Insufficient orientation and/or material thickness to deliver the required physical strength
POSSIBLE SOLUTIONS
o Reduce over all preform temperature
o Reduce heat beside failure point
o Where failures occur between neck and shoulder adjust shield into a thicker part of the taper
18 Problem: LOW BURST PRESSURE (BODY)
POSSIBLE CAUSES
o Insufficient orientation (Too hot)
o Material to thin
o Confirmationo Low IV
POSSIBLE SOLUTIONS
o Reduce preform temperatureo Reduce body heat
19 Problem: LOW BURST PRESSURE (BASE)
POSSIBLE CAUSES
o Base of bottle blown too coldproducing excessive stresso Stretch rod clearance too short
o Excessive crystallinity at the gate
o Low IV
o Excessive stress in preform
POSSIBLE SOLUTIONS
o Increase heat below the perform
o Reset stretch rod clearance
o Reduce stretch rod pressure
20Problem: POOR CLEARANCE
POSSIBLE CAUSES
o Reduce preform temperature to pearlescence, reduce base weight if necessary. Increase high
blow time
o Reduce heat in the preform's lower body
o Line lubricants generally cause severe stress cracking in all feet.
o Increase base weight
26Problem: EXPLOSIONS
POSSIBLE CAUSES
o Hot bottles (Refer Hot Bottles)o Folds in the base
o Light base weight
o Excessive post mould growth
o Low I.V.
o Chemical Reaction (Refer stress Cracking)
o Contamination
o Air bubbles above the gate
POSSIBLE SOLUTIONS
o Refer Causes
o Stress Cracking
o Cracked bases
o Excessive crystallinity
27Problem: DROP TEST FAILURES
POSSIBLE CAUSES
o Preform end cap blown too cold
o Light base weight
o Excessive crystallinity above gate.
o Large air bubbles above the gate
POSSIBLE SOLUTIONS
o Increasing heat at the gate or below without loosing base weight usually improves drop test
failure.
o Increase base weight.