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Thi Nghiem Hoa Ly Bai 5 Va 6
Thi Nghiem Hoa Ly Bai 5 Va 6
Bi 5:
IU CH CC H KEO V KHO ST MT S
TNH CHT CA CHNG
Tin hnh th nghim:
1. Ch to Son S v Son colophan (nha thng rn) bng phng
php th dung mi.
a) Ch to mt dung dch bo ho lu hunh trong ru etylic
bng cch lc mnh cho S ho tan n bo ho ri lng phn S
cn tha. Ly 5 ml dung dch ny nh chm (va nh va khuy) vo
20ml nc ct. S khng tan trong nc, nn khi phn tn vo nc,
cc phn t lu hunh s ngng t li thnh nhng ht c kch thc
c ht keo. Cht lm bn l mt sn phm oxi ho ru v nhng tp
cht vi lng c sn trong lu hunh. Ht keo lu hunh tch in m
v rt d keo t bng cc cht in li (dng dung dch mt cht in li
no , th xem!).
b) Ch to mt dung dch 2% clphan trong ru. Nh t t 2 ml
dung dch ny (va nh va khuy mnh) vo 20 ml nc ct, ta s
c Son clphan trong nc. Ht ko clphan tch in m.
Phng php ch tao Son S v Son clphan nh trn gi l
phng php thay th dung mi, trong nc thay th cho ru
lm dung mi cho Son hnh thnh. Phng php thay th dung mi
thuc loi phng php ngng t.
hoc
Khi dng d
ht keo s
lm ion quyt nh th
3. Ch to keo
Da vo phn ng:
un nng (n khong 900C) 120ml nc ct trong mt cc 250ml, nh
vo cc tng git cho n ht 45ml dung dch
2%. un thm vi
c mu nu
K2SO4)
Ly 12 ng nghim nh s ng t 1 n 12, cho vo mi ng
5ml dung dch Son Fe(OH)3. T dung dch Na2SO4 ban u c nng
0,01N pha thnh c dung dch long dn theo th t sau:
ng s
2 3 4 5 6 7 8 9 10 11
2 3 4 5 6 7 8 9 10 11
Dung dch
S ml Na2SO4
0.01N
S ml nc ct
11 10 9 8 7 6 5 4 3 2
10 11 12
(-)..(+)....(+)
Bi 6: NG HP PH NG NHIT
Tin hnh th nghim:
Phng th nghim c sn dung dch CH3COOH vi nng gn
ng 1N, hy pha c 100ml cc dung dch c nng gn ng sau
y:
0.025N ;
0.05N ;
0.1N ;
0.2N ;
0.4N ;
0.5N
trong
y:
l hp th
STT
Nng ban
u
Nng
sau
th no?
2) ng ng nhit Langmuir c dng th no nng
tht nh?
MTTCQ
Bi 5:
IU CH CC H KEO V KHO ST MT S
TNH CHT CA CHNG
Kt qu th nghim:
Th nghim 1: Ch to Son S v Son colophan bng phng php th dung
mi.
1. Son S.
Khi cho dung dich bo ha S trong ru etylic vo nc th to thnh h
keo, mang in tch m (-) v h keo c ht keo bm ln cc Cu, h keo c
mu vng c.
2. Son colophan
Khi cho colophan pha trong ru vo nc to thnh h keo, mang in
tch m (-) v h keo c ht keo bm ln cc Cu, h keo c mu en xm.
Th nghim 2: Ch to Son AgI bng phn ng trao i.
AgNO3 + KI = AgI + KNO3
Ly vo bnh tam gic 20 ml dung dch AgNO3 0.01N. Nh t t vo
bnh 2 ml dung dch KI 0.01N.
Hin tng dung dch mu tm c. Dng que d in th ht keo bm
xung quanh Zn nn ht keo mang in tch m (+).
10
11
S ml Na2SO4 0.01N
10
11
S ml nc ct
11
10
Dung dch
10
11
12
Ngng keo t:
o S ml nc ct cn ly:
ng 7 dng pha dung dch long hn.
o S ml Na2SO4 cn ly:
o S ml nc ct cn ly:
Kt qu thu c:
ng s
10
11
12
Bi 6: NG HP PH NG NHIT
kt qu th nghim:
STT
Nng ban
u
Nng
sau
0.02525
0.0235
0.0875
0.0875
-1.06
-1.63
0.270
0.05050
0.0450
0.2750
0.2750
-0.56
-1.35
0.164
0.11700
0.1050
0.6000
0.6000
-0.22
-.098
0.175
0.25100
0.2290
1.1000
1.1000
0.04
-.064
0.210
0.47750
0.4325
2.2500
2.2500
0.35
-0.36
0.190
0.57250
0.5350
1.8750
1.8750
0.27
-0.27
0.290
Series1
Linear (Series1)
0.024
0.045
0.105
0.229
0.433
0.535
T l C/
Dng my tnh b ti bm ta c:
Langmuir:
C
A
0.05
1.04
0.10
1.90
0.20
3.24
0.40
4.99
0.50
5.59
Series1
-1.63
-1.35
-0.098
-0.064
Linear (Series1)
LogC
Dng my tnh b ti bm ta c:
-0.36
-0.27
0.6
0.4
0.2
0
-0.2
-0.4
-0.6
-0.8
-1
-1.2
LogA
Freundlich:
C
A
0.05
0.44
0.10
0.76
0.20
1.29
0.40
2.20
0.50
2.62
Series1
1
0.5
0
0.05
0.1
0.2
0.4
0.5