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  • Analisis Instrumental Farmaceutico Practica GC/FID

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    Lorena Avila
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    This document summarizes the results of a gas chromatography/flame ionization detector (GC/FID) analysis of an unknown sample. The GC/FID analysis detected 9 peaks in the sample, including peaks corresponding to benzene and toluene. The document provides information on the sample and method used, a chromatogram showing the separation of components over time, and a peak table summarizing details on each detected peak such as retention time, area, resolution, and signal-to-noise ratio.

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    JUEVES_2016_20

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    This document summarizes the results of a gas chromatography/flame ionization detector (GC/FID) analysis of an unknown sample. The GC/FID analysis detected 9 peaks in the sample, including peaks corresponding to benzene and toluene. The document provides information on the sample and method used, a chromatogram showing the separation of components over time, and a peak table summarizing details on each detected peak such as retention time, area, resolution, and signal-to-noise ratio.

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    © All Rights Reserved
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    23 views2 pages

    Analisis Instrumental Farmaceutico Practica GC/FID

    Uploaded by

    Lorena Avila
    This document summarizes the results of a gas chromatography/flame ionization detector (GC/FID) analysis of an unknown sample. The GC/FID analysis detected 9 peaks in the sample, including peaks corresponding to benzene and toluene. The document provides information on the sample and method used, a chromatogram showing the separation of components over time, and a peak table summarizing details on each detected peak such as retention time, area, resolution, and signal-to-noise ratio.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    of 2

    5/6/2016 9:37:10 AM Page 1 / 2

    Analisis Instrumental Farmaceutico


    Practica GC/FID
    <Sample Information>
    Sample Name
    Sample ID
    Data Filename
    Method Filename
    Batch Filename
    Vial #
    Injection Volume
    Date Acquired
    Date Processed
    0

    : JUEVES
    : Miercoles_G2_01
    : JUEVES_2016_20.gcd
    : solventes1.gcm
    : JUEVES _2016_01.gcb
    : 15
    : 1 uL
    : 5/5/2016 1:51:46 PM
    : 5/5/2016 1:58:02 PM

    Sample Type

    : Unknown

    Acquired by
    Processed by

    : Administrator
    : Administrator

    <Chromatogram>
    uV
    FID1

    1.753

    3000000

    0
    1

    2.339

    FID1
    Peak# Ret. Time
    Area
    Name
    1
    1.547
    158564
    2
    1.753 365255481
    3
    1.907
    1360962 BENCENO
    4
    1.971
    29564 BENCENO
    5
    2.024
    60588
    6
    2.085
    143507
    7
    2.237
    1162
    8
    2.339
    1429026 TOLUENO
    9
    2.556
    7557
    <Peak
    Total Table> 368446410
    Tailing Factor
    2.574
    1.108
    1.386
    -1.342
    1.417
    -1.287
    1.292

    2.556

    1.547

    1000000

    1.971
    2.024
    2.085
    2.237

    1.907

    2000000

    6
    min

    HETP(USP)
    9.995
    16.667
    3.754
    4.903
    4.238
    4.067
    6.747
    3.779
    3.292

    Number of Theoretical Plate(USP)


    15008
    9000
    39962
    30594
    35394
    36880
    22232
    39688
    45560

    Resolution(USP)
    -3.303
    2.748
    1.557
    1.193
    1.417
    2.937
    1.907
    4.572

    Capacity Factor(k') Separation Factor


    S/N
    Tailing Factor(10%)
    --- 2547.18
    1.610
    0.133
    -- ########
    1.058
    0.232
    1.749 32437.47
    1.328
    0.274
    1.180
    654.65
    --

    D:\Project1\Training\data\2016_I\JUEVES_2016_20.gcd

    5/6/2016 9:37:10 AM Page 2 / 2

    Capacity Factor(k') Separation Factor


    S/N
    Tailing Factor(10%)
    0.308
    1.124 1369.06
    1.372
    0.348
    1.128 3158.82
    1.337
    0.446
    1.282
    14.95
    -0.512
    1.148 30482.20
    1.240
    0.652
    1.274
    148.11
    1.252

    D:\Project1\Training\data\2016_I\JUEVES_2016_20.gcd

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