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Permanent Shale

Inhibitors:
PC-1952 & PC-1955
September 2, 2014

Effect of Shale Inhibitors on Viscosity


Inhibition of 50 lb/bbl OCMA clay
10,000

Viscosity (cP)

1,000

6% KCl

100

3% Choline Chloride
3% Jeffamine D-230
3% PC-1955

10

1
1

10
Shear Rate (s-1)

100

MWV Permanent Shale Inhibitors / September 2, 2014

Capillary Suction Time Testing


Inhibition of 50 lb/bbl OCMA clay
60
50

CST (s)

40

30
20
10
0
3% PC-1952

3% PC-1955 3% Jeffamine
D-230

3% Choline
Chloride

6% KCl

3% TMAC

MWV Permanent Shale Inhibitors / September 2, 2014

Shale Dispersion Testing 16 h

Retention (%)

Midway Shale Cuttings rolled at 250 F for 16 h


100
90
80
70
60
50
40
30
20
10
0
3% PC-1952

3% PC-1955 3% Jeffamine
D-230

3% Choline
Chloride

6% KCl

3% TMAC

MWV Permanent Shale Inhibitors / September 2, 2014

Shale Dispersion Testing 5 Day


Cuttings initially rolled at 250 F for 16 h with inhibitor

Retention (%)

Cuttings then washed with water and subjected to 5 days rolling at


250 F in fresh water
100
90
80
70
60
50
40
30
20
10
0
3% PC-1952

3% PC-1955

3% Jeffamine D230

3% Choline
Chloride

6% KCl

MWV Permanent Shale Inhibitors / September 2, 2014

Shale Dispersion Testing 16 h


All products dosed at 2 GPTG

Retention (%)

Midway Shale Cuttings rolled at 250 F for 16 h


100
90
80
70
60
50
40
30
20
10
0
2 GPTG PC-1952

2 GPTG PC-1955

2 GPTG Choline
Chloride

2 GPTG TMAC

MWV Permanent Shale Inhibitors / September 2, 2014

Shale Dispersion Testing 5 Day


All products dosed at 2 GPTG
Cuttings initially rolled at 250 F for 16 h with inhibitor

Retention (%)

Cuttings then washed with water and subjected to 4 days rolling at


250 F in fresh water
100
90
80
70
60
50
40
30
20
10
0
2 GPTG PC-1952

2 GPTG PC-1955

2 GPTG Choline
Chloride

2 GPTG TMAC

MWV Permanent Shale Inhibitors / September 2, 2014

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