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MA 3000 NIC 600 2233 01 Simplified Operation Manual
MA 3000 NIC 600 2233 01 Simplified Operation Manual
NIC-600-2233-01
NIC-600-2233-01
1. Preparation
(1). Open the main valve of the Oxygen gas cylinder
and adjust the pressure to 0.10.5Mpa.
(2). Adjust the regulator pressure to 0.05Mpa on the
backside of MA-3.
2. Start-up
(1). Start-up Windows and boot win by clicking
on the desktop.
and perform the blank measurements at least three times until getting stable. Or set
or press F5 to start.
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NIC-600-2233-01
ABS(HIGH)
0.1ng
0.002
10ng
0.001
1ng
0.02
100ng
0.01
5ng
0.1
1,000ng
0.1
10ng
0.2
5,000ng
0.4
20ng
0.3
10,000ng
0.6
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Calibration curve
y=ax+blank is recommended when
measuring the sample near blank.
6. Measurements
6.1. Registration of standard
Click the tab of "STD.
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Each
instrument
has
its
own
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When you use additive B, please put small amount of additive into sample boat before sample
weighting.
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NIC-600-2233-01
(2) Select the heating method in Method Number. If the moisture content is known as for solid
samples, enter it in MOIST [%] so that the concentration is calculated as dry weight.
(3) After checking Sample Number with
, click
Minerals
Coal, coal ash, metal and mineral
6
7
Waste water
Purge
Heating Method
STD
Typical
amount
~200L
ORGANISM
(SOLID)
SOIL & SLUDGE
URINE & BLOOD
PLASTICS
~200 mg
~200L
~100 mg
MINERAL
~200 mg
WASTE WATER
PURGE
~100L
-
~200 mg
Do not measure the sample digested by HNO3 directly. This sample may generate heat on the
activated carbon filter. Dilute it less than 5wt% of HNO3.
As for HCL solution, dilute it less than 1wt%.
The above Heating Methods may not cover the samples which contain a lot of halogens or burn
quickly.
When the check standard after measuring is lower, reduce the sample size.
Dilute or reduce the sample size if it contains high mercury. Otherwise it contaminates the
plumbing.
As for the liquid samples containing organic mercury, use Additive B on the boat.
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As for the analysis range, the data less than 10ng are applied for LOW range and the data greater than
10ng are applied for HIGH range. An analysis range can be changed and is performed in the Range
column.
If the recovery of the standard solution after the measurement is 90% or less, it might be due to the
interference contamination. Try to reduce the amount of sample or to change the heating conditions.
Inject 200L of Distilled Water for several times, if high concentration samples are measured.
Inject 200L of Standard Solution repeatedly, if the sensitivity reduces. This way recover the
sensitivity and can also confirm.
7. Data Save
() Press
() Select the registered folder and save it with entering the file name.
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8. Printing
() Press
The printing profile's scale is being interlocked with the scale of Profile screen. Set up the scale and
the number of profiles of each range by STD and SMP, respectively.
HIGH
Low
Number
of profile
The row width of printing is being interlocked with a setup of Table screen. If the row width at the time
of printing is narrow, please adjust on the screen. And, the row will not be printed if width of a row is
made into zero.
9. Termination
() Press the upper right button
of MA3win.
() Close the Windows and turn off the power of PC and Printer.
() Power off MA-3000.
() Discharge liquid of a drain tank.
() Close the main cock of the Oxygen gas cylinder.
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NIC-600-2233-01
Technical Center
14-8 Akaoji-cho, Takatsuki-shi, Osaka 569-1146
Japan
Phone: +81-72-693-6820
Fax: +81-72-694-0663
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