LAB REPORT

CHM 350
EXPERIMENT 4:
PRECIPITATION TITRATION

BY :

BIL NAME GROUP MATRIX NO

1. NATASSHA BT JAMIL ASD4TB 2008218888

LECTURER :
EN. RAFIE BIN DRAMAN
EXPERIMENT 4: PRECIPITATION TITRATION

DATA AND RESULT :

No. of trial 1 2 3
Final buret reading (ml) 47.7 27.6 28.3
Initial buret reading (ml) 0 0 0
Volume of titrant used (ml) 47.7 27.6 28.3

Average volume of KSCN used = ml

REACTION :

HCl + AgNO3 (excess) ----------> AgCl + HNO3

AgNO3 + KSCN -----------> AgCN + KNO3

Fe3+ + SCN- ----------> [FeSCN]++(red)

CALCULATION OF RESULT :

1. Calculate the volume of standard 0.01000 M silver nitrate solution that has
reacted with the hydrochloric.
.....

2. Determine the percentage of pure HCl in the concentrated acid given.

QUESTION :

1. Why must AgNO3 be used in excess ?

2. What is the purpose of washing the ppt with dilute nitric acid ?

CONCLUSION :