List of Solvents PDF

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LIST OF SOLVENTS

Solvent Formula Vacuum (mbar) for bp at 40C 44 556 226 11 25 130 39 36 474 235 atm. press* atm. press* 751 375 107 11 175 240 243 120 335 137 14 337 atm. press* 67 13 35 300 53 271 357 77 183 72 25 Acetic acid Acetone Acetonitrile N-Amylalcohol, n-Pentanol n-Butanol tert. Butanol, 2-Methyl-2-Propanol Butylacetate Chlorobenzene Chloroform Cyclohexane Dichloromethane, Methylenechloride Diethylether 1,2,-Dichloroethylene (trans) Diisopropylether Dioxane Dimethylformamide (DMF) Ethanol Ethylacetate Ethylmethylketone Heptane Hexane Isopropylalcohol Methanol Pentane n-Propylalcohol Pentachloroethane 1,1,2,2,-Tetrachloroethane 1,1,1,-Trichloroethane Tetrachloroethylene Tetrachloromethane Tetrahydrofurane (THF) Toluene Trichloroethylene Water Xylene
*is recommended ~850 mbar

C 2H 4O 2 C 3H 6O C 2H 3N C5H12O C4H10 C4H10O C6H12O2 C6H5CI CHCI3 C6H12 CH2CI2 C4H10O C2H2CI2 C6H14O C 4H 8O 2 C3H7NO C 2H 6O C 4H 8O 2 C 4H 8O C7H16 C6H14 C 3H 8O CH4O C5H12 C 3H 8O C2HCI5 C2H2CI4 C2H3CI3 C2CI4 CCI4 C 4H 8O C 7H 8 C2HCI3 H 2O C8H10

Isoamylalcohol, 3-Methyl-1-Butanol C5H12O

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Chromatography

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Evaporation

Drying

3. Adjust needed vacuum for a boiling point of 40C according to the list of solvents. 2. Cooling water temperature below 20C. 1. Set bath temperature at 60C. The 20 / 40 / 60 rule for ROTAVAPOR

OPTIMAL DISTILLATION PARAMETERS

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