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List of Solvents PDF
List of Solvents PDF
List of Solvents PDF
Solvent Formula Vacuum (mbar) for bp at 40C 44 556 226 11 25 130 39 36 474 235 atm. press* atm. press* 751 375 107 11 175 240 243 120 335 137 14 337 atm. press* 67 13 35 300 53 271 357 77 183 72 25 Acetic acid Acetone Acetonitrile N-Amylalcohol, n-Pentanol n-Butanol tert. Butanol, 2-Methyl-2-Propanol Butylacetate Chlorobenzene Chloroform Cyclohexane Dichloromethane, Methylenechloride Diethylether 1,2,-Dichloroethylene (trans) Diisopropylether Dioxane Dimethylformamide (DMF) Ethanol Ethylacetate Ethylmethylketone Heptane Hexane Isopropylalcohol Methanol Pentane n-Propylalcohol Pentachloroethane 1,1,2,2,-Tetrachloroethane 1,1,1,-Trichloroethane Tetrachloroethylene Tetrachloromethane Tetrahydrofurane (THF) Toluene Trichloroethylene Water Xylene
*is recommended ~850 mbar
C 2H 4O 2 C 3H 6O C 2H 3N C5H12O C4H10 C4H10O C6H12O2 C6H5CI CHCI3 C6H12 CH2CI2 C4H10O C2H2CI2 C6H14O C 4H 8O 2 C3H7NO C 2H 6O C 4H 8O 2 C 4H 8O C7H16 C6H14 C 3H 8O CH4O C5H12 C 3H 8O C2HCI5 C2H2CI4 C2H3CI3 C2CI4 CCI4 C 4H 8O C 7H 8 C2HCI3 H 2O C8H10
Chromatography
Synthesis BCHI Labortechnik AG P.O. Box 9230 Flawil Switzerland Telephone Telefax Internet E-Mail +41 71 394 63 63 +41 71 394 65 65 www.buchi.com buchi@buchi.com
Evaporation
Drying
3. Adjust needed vacuum for a boiling point of 40C according to the list of solvents. 2. Cooling water temperature below 20C. 1. Set bath temperature at 60C. The 20 / 40 / 60 rule for ROTAVAPOR