1 3. B lc sch khng kh nn: xem ph lc I, mc 1. 2; TCVN 3740-82.

1.4. B lm kh m : xem ph lc I, mc 1.3. theo TCVN 3740-82.

1.5. m k dng : xem ph lc I. mc 1.4 , theo TCVN 3740-82.
1 6. Bung trn 11 : xem ph lc I, thc 1.6, theo TCVN 3740-82.
1.7. Lu tc k mao qun 14 v mng ngn 18 dng khng ch lu lng kh
c trc bung trn v hn bp khng kh vi kh c cc nhnh trc cc hp th
nghim.
Lu tc k mao qun 14 v mng ngn 18 c chun nh mc 1.7 ph lc 1
TCVN 3740-82.
1.8. Cc u g dng ni hp lc th nghim vo cc ng dn ca thit b.
I 9. Cc bnh c lm lc (hnh 1 v 2 ph lc II) dng ly mu khng kh vi kh
c sau bung trn.
1.10. Bnh ht (hnh 4 ph lc II) dng kim tra kn ca thit b v ly th
tch xc nh nng cht c
1.11. Bnh ch th 23 (hnh 3 ph lc II).
1 12. B hp th 21 dng hp th cht c thi ra.
1 13. Cc kho 1 ng 3, 4, 5 v 17 v kha 3 ng 19 phi c ng knh l khng
nh hn 16m, cn cc kha 1 ng l2 v 16 khng nh hn 5 mm.
2. Chun b thit b cho th nghim
2.1. Cho vo bnh lm kh cht lm kh c sy s b 180 - 2000C.
Cho vo bnh lm m lng than hot tnh c thm t bng nc, cho
vo bnh hp th cht hp th thch hp.
2. 2. Cm vo u ni ca ng m k cc nhit k. hng theo dng khng kh,
nhit k 1 l kh, nhit k th 2 l m bu ca nhit k m c cun cht mt
vng ri bng di vi mm c buc k trong nc ct v buc bng si ch, cn
u kia ca di vi th cho vo bu cha ca m k c nc ct. Mc nc trong

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bu phi cch xa bu thy ngn nhit k khng qu 4 cm. Cc nhit k c t vo

ng m k trn mt nt cao su v gi sao cho bu thy ngn nm trn trc ca ng.
2. 3. Rt du paraphin vo cc ng p lc ti vch (0) (khi th asenhydrua.
sunfuhyrua, amoniac) hoc xt sunfurc c (khi th 1u hunh ioxit).
3- Kim tra kn ca thit b .
3.1. ng kha 17, ni bnh ht vi kha 16 sau bung trn kim tra kn ca
cc phn trc hp lc.
3. 2. ng kha 17, t kha 3 ng 19 v tr hng ti hp lc th nghim, ng
kp vt 22, ln lt kim tra cc nhnh c hp lc. Nu hp lc t trong bung g
trc tin phi kim tra kn ca ch ni hp khi vn cht hp vo u g. ng
kn np y hp, ni bnh ht vi u ni thng dng ni vi bnh ch th. ng
kp vt 22.
3.3. Thit b c coi l kn khi m cc kha ca bnh ht m nc khng chy.
4. Thit lp ch lm vic.
4.1. ng cc kha 12 v 16 m cc kha 17, 3, 4, 5 cn kho 19 t v tr hng
ti bnh hp th. M kp vt 1 v a khng kh vo thit b, khng ch lu lng
khng kh cn thit theo cc lu tc k mng ngn 18 bng cch ng dn kp vt 1
ng thi iu chnh lng khng kh bng cc kha 17.
4. 2. c c m khng kh cho trc, hng mt phn dng khng kh theo
ng dn nh kha 4, cn phn kia ti hnh lm m hay lm kh (ty thuc vo s
cn thit) khi bnh kia (kh hoc m) b kha hon ton. m tng i c xc
nh bng th m (ph lc III TCVN 3740-82).
4. 8. Nhit th nghim c xc nh theo nhit k kh ca m k
4. 4. Ni cc bnh ch th c cht ch th vo thit b.
4. 5. t cc kha 3 ng 19 hng ti hp lc th nghim ni ng h kh hay lu
tc k mao qun ln lt vo tng bnh ch th c cht ch th v iu chnh lu lng
bng kp vt 22 sao cho lu lng qua mi bnh l 1,.5 lt/pht.

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4. 6. To hn hp khng kh vi kh c bng cch m nh kha ca bnh cha kh

v kha 12 n khi lp c hiu s mc xc nh lu tc k mao qun 14.
1.7. Sau khi thit b lm vic 5 pht th tin hnh xc nh nng cht c kim
tra. .
5. Chun lu tc k kh.
Thit lp lu lng khng khi cn thit cho cc hp lc th nghim (cc kha ba
ng t v tr hng ti bnh hp th). a vo thit b cht c v nh.kha 12 xc
lp trn lu tc k kh 14 hiu s mc xc nh. Sau khi lm vic 5 pht th ly mu
hn hp khng kh vi kh c sau bung trn, sau xc nh nng cht c
theo phng php ca tiu chun ny. Tin hnh thit lp thm ln lt 2 - 3 gi tr
hiu s mc khc na, ng thi xc nh mi ln mt nng cht c hn hp
khng kh vi kh c.
Qua cc kt qu thu c, xy dng th chun theo ta :
Hiu s mc cht lng ca lu tc k kh.
Nng cht c trong hn hp khng kh vi kh c.

Cc bnh c tm lc ly mu

15

Hnh 1: Bnh ra kh

Hnh 2 : Bnh ly mu c mng lc

th

16

Hnh 3 : Bnh ch

Hnh 4 : Bnh ht

17