Professional Documents
Culture Documents
VUV Mirrors TMAE SLD CRID Slac-Pub-5199
VUV Mirrors TMAE SLD CRID Slac-Pub-5199
-.
PRODUCTION OF 400 MIRRORS WITH HIGH REFLECTIVITY FOR USE IN THE SLD CERENKOV RING IMAGING DETECTOR*
VUV
K. Abe, P. Antilogus, D. Astoq2 A. Bean, T. Bienz, F. Bird,2(a) D. Caldwell, P. Co~le,~ D. Co~ne,~ P. Datte,3(b) J. Dubosq3 W. Dunwoodie,2 P. Gagnon: D. Hale,3 G. Hallewell,2 K. Hasegawa, M. Hilton,3(c) J. Hubeq3 P. Jacques5 R. A. Johnsoq6 H. Kawahara,2 Y, Kwoq2 D. W. G. S. Leith,2 A. Lq3 J. Martinez, L. Mathys,3 S. McHugh,3 R. Morrisoq3 D. Muller,2 T. Nagarnine,2 M. Nussbarq6 T. PaveL2 R. P1an0,~ B. Ratcliff, P. Rensing,2 A. K. S. Santha, D. Schultq2 S. Shapiro,2 A. Shoup, C. Sirnopoulos,2 E. Solodov,2(d) P. Stamer,5 I. Stockdahq6 F. Suekane, N. Togq2 J. Va vrq2 J. S. Whitaker,7 D. A. Willianq4 S. H. Williams,2 M. Witherell,3 R. J. Wilson,7 S. Yellin, and H. Yuta
THE SLD
CRID
COLLABORATION
of Physics, Tohoku University, Aramaki, Sendai 980, Japan 2Stanjord Linear Accelerator Center, Stanford University, Stanford, CA 94309, USA Department of Physics, University of California, Santa Barbara, CA 93106, USA 4Santa Cruz Institute for Particle Physics, University of California, Santa Crux, CA 95064, USA cs Laboratory, Rutgers University, 5Serin Phy sa PO Box 849, Piscataway, NJ 08855, USA 6Department of Physics, University of Cincinnati, Cincinnati, OH 45221, USA 7Department of Physics, Boston University, Boston, MA 02215, USA
- Department
Submitted
*
to Nuclear Instruments
and Methods B.
Work supported by Department of Energy contract DE-ACO3-76SFO0515; and National Science Foundation grants PHY88-13669 and PHY88-13018. (a) Present address: EP Division, CERN, CH1211, Geneva 23, Switzerland. (b) Present address: Texas Accelerator Center, 2319 Timberloch Drive, The Woodlands, TX 77380, USA. (c) Permanent address: Applied Magnetics Company, Goleta, CA 93117. (d)
Permanent address:
Institute
of Nuclear
Physics,
Novosibirsk,
630090,
USSR.
.-
ABSTRACT
Large Detector for experimental particle physics detection (CRID). at the
_c
The Stanford
SLAC Linear Collider contains a Cerenkov Ring Imaging Detector -. CRID mirrors have been successfully produced and installed.
The industrial
production
control reflectivity
of the mirrors
produced,
the vacuum ultraviolet An average reflectivity 180-230 nm wavelength of a typical measurements .._ incident
and mirror-shape
of at least 80% for light at 160 nm and 85% for light in the range has been achieved in the production The surface roughness loss due to scattering of over 400 mirrors distortion of the
and optical
is a few percent
.-
1. INTRODUCTION
under construction particle physics
_*
-. A large Cerenkov Ring Imaging Detector (GRID) y2 is currently to be included detection in the Stanford Linear Large Detector Collider (SLC). for experimental This CRID
at the SLAC
consists of a cylindrical
the actual radius of the Cerenkov ring associated with each charged particle along with a momentum In a gas ring imaging charged particle traveling measurement, provides particle identification.
by a relativistic by a mirror to
medium
focus a ring image onto the photosensitive - detector consists of Time Projection tetrakis[dimethylamine]ethylene the photocathode mixed with
position additive
Chambers (TPCs) with the photosensitive with an ionization gas. The TPCs threshold (drift
of 5.4 eV) as
to VUV light.
in three dimensions of the position where the photon ionized a TMAE molecule. The angle of Cerenkov radiation emission, from which the velocity of the relativistic particle can be determined, is found by reconstructing the ring image as registered
by the photodetector
for all the photons associated with a given charged particle. includes both liquid and gas radiators, gaseous TMAE spherical focusing as the photocathode, Each
long drift boxes of the TPC type containing chambers with charge division into 10 azimuthal
and proportional
radiators
and 20 mirrors.
(C5F12)
in which
the Cerenkov
light
is
of wavelengths quantum
h as a significant
to be not less than 85% for light in the range of 180-220 nm. with which the CRID measures the Cerenkov angle of a particle
The accuracy
is determined
by the contributions
aberration
measurement,
and momentum
a small
distortions
of about l-2 mm 3 . The focal properties for ring imaging but cost. 430 were coated, (UCSB)
those for an astronomical quantities A total completed CRID. with thin mirrors of 472 mirror by the University
are difficult
in large
of which
of California,
Santa Barbara
SUBSTRATE
Manufacturing
was required to have a surface finish light. This requirement which would limit
number _c
of photons
produced,
typically
the mirror
substrate were
was required
These requirements
achieved in a two-step
while soft .)
-
(ii)
The spherical blank was ground and polished to produce a substrate roughness After passing mirror 53 nm (rms). visual inspection, the mirror substrate
with surface
was placed into a size gauge to easily verify that the dimensions The 10 mirror
Fixtures
and Epoxy
passed the visual mounting epoxy inspection and dimension check
substrate aluminum
Approximately
0.15 mm of DP190
a gluing
on the use of 3M DP190 epoxy to hold the mirror was carried out. The epoxy was required that absorb
testing
small thermal
expansion
coefficient.
The choice of DP190 was made from a small list of possible adhesives that had been previously tested for outgassing and approved 5 by the SLD CRID group. The epoxy
.-
was further -. f -I
tested at UCSB
substrate,
and hanging
weights from the spool over a long period of time. In the course of production, undergone it was noticed that mirror substrates that had
a normal gluing procedure and had been subjected voids in the epoxy-glass substrate. interface.
._
not controlled
of 0.15 mm using a spacer in the gluing jig. The epoxy temperature (40C) with
weights ranging from 0.91 kg (approximate Small voids (about interface 1 mm*)
mirror substrate weight) to 4.5 kg attached evolved into large voids (about 1 cm*) in
The area of the epoxy was also increased to give further confidence in the mounting spool-mirror substrate connection. To increase this area without system, an epoxy injection a complete redesign method was made
support
Such spools did not develop voids in the injection oven tests.
did develop on the foot regions under low-weight this increased adhesion was provided substrate and subjecting
by taking an injected
and an uninjected
mirror substrate released the spool, while the injected one still remains One cc of epoxy was injected beneath the spool for all mirrors coefficients adhesive
1 year later.
as a result.
protection
against a mirror
detaching
system consisted of four wires connecting spool. This restraint doing further
failed from
sufficiently
-
2.3 Surface
Roughness
of better than 3 nm (rms) is necessary in order to keep the 5%. The surface profile of about 3-D Micro-Surface Measurement
Surface smoothness
of the mirrors
was tested8
a 5x magnification computer
and an online
to provide
using a reference with a known surface roughness of 0.24 nm. Each tested at two or three different locations, and the peak to valley and of the
was measured
were calculated
than 5 nm, was met by 91% of all the tested criterion were repolished
The mirror
or replaced
at no additional
cost.
2.4 Optical
Distortion
distortion of each mirror was measured by placing
a mask with
positioned
holes of a diameter
of 1 cm (made on a numerically
milling
machine)
in front
it with
a point
onto a frosted
10 cm behind ._
This provided
of 10 : 1 of
would produce light spots which fell exactly glass. Departures from the ideal curvature,
1 mrad at the ground glass screen, were easy to see. to the ideal pattern to give Two
averaged
corresponding
The requirement
After
For an ideal mirror the center of curvature create an undistorted imaged pattern centerline computer
by a point
light
source placed
very close to
possible, the point light source was situated and the frosted
The off-axis
glass cause
direction.
criterion
of a maximum
was satisfied
AND
REFLECTIVITY
Before
coating,
the mirror
substrates
were cleaned
by conventional
methods.
After extensive testing of coatings by many vendors, Acton Research Corporation slo standard coating ARC1600 was chosen. purity The mirror aluminum substrates were coated with
80 nm of ultra-high
(approximately
the spool pieces so no shaded areas were left on the mirrors. in a few seconds and followed surface. Figure immediately
The aluminum
The depositions
specifications were
stored in a dry-air
3.2 Reflectivity
Three spherical
Testing
mirror substrates and one planar witness coupon Research Corporation. using the Acton ranging (5.1 x 5.1 cm) of the
were coated in each batch by Acton witness Vacuum coupon was measured
by the vendor
VRTMS-502
Measurement
between
If the reflectivity
of the witness
of the full-size
was assumed to be
were shipped.
Witness
VUV
spectrometer
the full-size
spherical
delivery
to UCSB,
spherical
mirror
ranging
reflectivity
to measure the relative of a large vacuum which permitted small with mirror
reflectivity steering
box with
stands, mirror
of the full-size
in the box.
A McPhearson a narrow
218
a deuterium
lamp l1 directed
the light into a photomultiplier The full-size test mirror about its center point, the motors
to be tested.
and settings
via CAMAC.
At each wavelength,
three positions
of each full-size
test mirror
was compared
standard
to determine
the relative
reflectivity
The absolute
could be calculated
of the witness coupons were measured at in the range 160 to 230 nm. This was to measure down absolute reflectivity vacuum
instrument, This
was built
samples.
was pumped
to a high
(approximately occur.
10 -6 T) so no VUV
absorption
A second McPhearson
218 VUV
10
monochromator
a deuterium
a narrow
beam
of light mirror,
reflected
onto a standard
the light
The light from this measurement standard deuterium standard reflectance mirror was pivoted
into a position
to reflect
beam from
on the
was illuminated
of the mirror
3.3 Reflectivity
Figure coated .steadily
Results
measured at UCSB, of all 430 full-size The reflectivity of all the
mirrors
increases from 84% at 160 nm to 89% at 220 nm. are presented at four wavelengths
in fig. 7 as histograms
of mirrors
N having reflectivity
ranging
the UCSB averages are as much as 3.6% lower than those made by in the range of 160 to 175 nm (as shown in fig. 8). The the measuring measurements errors over all wavelengths. of the witness coupons at
average results are in agreement well within The agreement between the reflectivity
UCSB and those of the associated full-size mirrors (see fig. 5). The average reflectance differ by a maximum of the full-size
11
.-
4. ALIGNMENT .f
-.
4.1 Mounting
The mirror
Spool
alignment process involved the rotating and bending of the mounting and then fully
spools (see fig. 2). The spools were machined from 6061T-6 aluminum annealed.
The purpose of the spool design was to allow the bending of the stem to in any direction with high precision. It had to satisfy the double bumps) but easily position. the amount
of not bending too easily (to prevent droop or accidental without springing
enough to make small adjustments The effect of a variable of deflection . original position
when the torque was applied and the ability when the torque was removed. the elastic limit
of 7.62 mm that
weighed less than 1 kg, this was deemed adequate to prevent droop yet also permit alignment changes of 1 or 2 mrad.
4.2 Mirror
-
Alignment
table was designed to simulate the position of the mirror array as if
An alignment
it were in the SLD CRID vessel. In the CRID each mirror a different position along a drift box. The alignment
array side and the point light source side, as shown in fig. 9. An array consisted of two ladders attached 5 mirrors mounted to a permanently via mirror mounted mirror main channel. Each ladder had
arms onto a side mount channel. The arms were made orient the mirror. The source
table had a point light source-screen assembly, that could be positioned by means of precision alignment holes in the in turn.
and reproducibly
table to bring the source to the center of curvature Each mirror was then illuminated
onto-a
frosted
glass screen.
was measured
by moving
the
screen position
t
until the image reached its smallest point. the spool stem (see sec. 4.1 and fig. 2). The alignment was done to
mrad) from the center of the screen. A secondary at the time of alignment to provide
on each mirror
releasing from its spool (see sec. 2.2). the ladder with its side channel was detached box to
After
all 5 mirrors
in a shipping
boxes were designed and tested in order to comply to transport-environment that driving resistance, cleanliness,
the requirements
--and shock-absorbing affect the alignment. packets filled with The desiccant nitrogen
Tests indicated
The steam-cleaned
aluminum
boxes contained
a desiccating
agent; the boxes were then filled with dry nitrogen. box was purged with dry
packets
Ladder
their arrival
Installation
at SLAC, the mirror Previously, ladders were placed in clean, dry (15% 40 main mirror channels identical to the
RH at 20C)
storage shelves.
one on the alignment argon calorimeter the main channels. on a large turret. instrument
onto the inside surface of the liquid consisted of placing the ladders onto mounted The
vacuum jacket.
This was done by means of a sophisticated The turret allowed access to all positions along three directions to accurately
13
instrument
around
the barrel.
itself permitted
translation
and rotations
about two
was required
channel without _f
bending.
by a compressed
air system which could be remotely step was to wedge a bar between
released after the ladder was in place. The final the ladder and the channel by means of a screw
4.4 In-Place
Alignment f2 mrad.
Mirror
Measurement
to an accuracy barrel of approximately to be considerably of the main or side
We expected contributing
in the CRID
larger-the
by a factor of 100 or so due to the long lever arm. where each mirror pointed onto the particular in mechanical
In addition, drift
we wanted
to determine
tolerances -
at the same three points The device is very which is free to pivot The steering bounces off the position in which the at three wellof fl or
about two axes so as to direct the beam onto the mirror mirror is positioned mirror
being measured.
so that the reflected beam from the measured mirror and back into the laser opening. By determining the direction
the steering
In practice,
was measured
to determine
of the mirror
to an accuracy
indicated
mrad, approximately.
14
now-have _T
-.
of pointing
to an order-of-mag;litude measurement.
better
accuracy,
an in-place
5. CONCLUDING
_ A mirror and a coating to produce quality slumping, grinding, and polishing
REMARKS
process at Lancaster Glass Company implemented counter. The
process at Acton
Research Corp. have been successfully mirrors for the SLD Barrel CRID
performed
is at least 80% for light at range for these mirrors. imply that the scattering The is
160 nm and 85% for light in the 180-230 nm wavelength and optical distortion measurements
to a few percent
of the incident
reflection
error is less
than 1 mrad.
ACKNOWLEDGMENTS
-
Applied
Magnetics
Measurement
15
.-
REFERENCES
(1984); UC-340 (1987); IEEE (May 1984).
-. f
-. 1. SLD Design Report, SLAC-REPORT-273 2. G. Hallewell et al., SLAC-PUB-4405
398 (1988).
3. R. J. Apsimon, 4. P. Baillon et al., Nucl. Instrum.
Methods A241,
339 (1985).
Methods A277,
Bristol, U.K.
338 (1989).
5. I.S.C. Chemicals
Ltd., Avoumouth,
6. F. Bird, SLAC-REPORT-332 7. Mirror 8. Applied 9. WYCO 10. Acton substrates Magnetics manufactured
Corp., 1955 East 6th St., Tucson, AZ, 85719. Research Corp., Acton, MA 01720. Originally both the deuterium lamp
11. Hamamatsu
-
continuous
12. There was a gradual loss of the p-terphenyl window frequently since it was within
16
.-
FIGURE
CAPTIONS
the e* beams of one quadrant of the
1. (a) Vertical
SLD detector.
mounting
substrate.
with a surface roughness of 1.91 nm (rms) and a curvature 4. Bench setup used to measure the optical 5. The average VUV reflectance results distortion
as measured by UCSB
measurement
of the full-size mirrors for all 430 mirrors (a) 160 nm, (b) 180 nm, (c) 200 nm, and
(d) 220 nm. 8. Results of the reflectivity at Acton measurement of the witness coupons for all 430 mirrors 160 thru 230 nm.
17
..f -.
_-
Warm
Iron Calorimeter
(mm)
Fig. la
_-
Gas Radiator
e+
e-
11-89 6507Al
Fig. lb
_-
n \ --w
0
-
I n t\
0 0
> 0
:I>:
-
Side View
Attaches to Arm 0.48 cm 7
\ /
1 t
1 ---I.-
L Attaches to I Mirror
Fig. 2
.f -.
_-
IS:32
E33/~16r89
-Pef
5.
m,<
SURFRCE
cl
0 IFron: 9.8 > 4.9 -
-0.1
-4
-5-u
SIJ 3 a , I nr -9.9nm
c
0
1
496 D1rtanc2 992 Lrllcronr 14aa 1
p1912 1984
-9 u: L:
-.
WYKO
7.6
-7
.o
U: lS.I3rtm L:-14.4nm
WYKO
5-90 6576A5
Fig. 3
_-
MASK
1 1
I
5OURCE
I
-
A
6576~6
RADIUS OF CURVATURE
1110 R
5-90
Fig. 4
.-
0.8
I I I I
160
2-90
220
6576A3
Fig. 5
.-
.-----.-a
\I
MgF2 WINDOW
II
! I/
APERATURE LENS
-a
l--e--------
i \I
iv
&!
FLAT VUV REFLECTIVE MIRROR TM= FULL-SIZE TEST MIRROR or SM=SMALL STANDARD MIRROR
I :________ i TURBO PUMP REGION (n 10M6torr) ---I ,I -1 LARGE MECHANICAL PUMP REGION (- 10e3 torr) 6576A7
Fig. 6a
I
.-
-1
.-CT, LL
-.
.-
Reflectance at 160 nm
I I I I 1 I I 1
Reflectance at 180 nm 80 I 60
60 2 40 2 .k 2 20
n
(a) -
(W
I
0.75
01. 0.75
I 60 i 40 .2 20
(cl
I 2
80 60
00 0.75
2-90
0 0.75
Fig. 7
6576Al
.-
-1
5:
-
I
0.8 160 180 200
PP
220
2-90
Wavelength
Fig. 8
(nm)
6576A2
.-
f -.