Superplastificante HightechPool Melflux-Starvis e

BASF Construction Polymers GmbH
Dr.-Albert-Frank-Strae 32
83308 Trostberg / Germany
P.O. Box 11 16
83302 Trostberg
Tel. +49 8621 86-16
Fax +49 8621 86-29 95
construction-polymers@basf.com
www.construction-polymers.com
Melux
2651 F
Starvis
3003 F
Melux
/Starvis
Hightech Pool
Application Technology Report
Melflux_Starvis englisch_neu.indd 1 10.09.2008 11:18:49 Uhr
Melux
/Starvis
Hightech Pool Application Technology Report

2
Melux
/Starvis
Hightech Pool
for Casein Replacement
Synthetic material / no mold formation
Anti-bleeding and segregation properties
Wide dosage range, easy to dose
Excellent self healing properties
Excellent ow properties
Short mixing times
Safety belt for water and raw
material deviations
Compatible with citric and tartaric acid
and other conventional additives
Better strength development
Constant quality ISO 9001:2000
The high-performance superplasticizer Melux
2651 F and viscosity modifying agent

(stabilizer) Starvis
3003 F are synthetic chemical additives which were developed as a

substitute for casein in cementitious self-levelling underlayments (SLUs).
General
Self-levelling underlayments (SLUs) are fast set-
ting, multi-binder based construction materials
that are commercialized as dry mortars.
Melux
2651 F in combination with viscosity

modifying agent Starvis
3003 F enable the for-

mulator to replace casein by synthetic additives
for developing high quality SLUs.
Dosage
Recommended dosage range
(by total weight of dry mortar - btw):
Melux
2651 F: 0.10 to 0.30% btw

Starvis
3003 F: 0.05 to 0.20% btw

Recommended Fields
of Application
Cementitious self levelling underlayments

Binder
Suitable for all common hydraulic binder
systems based on CEM I, CEM II and
CEM III according to EN 197-1 as well as fast
set cements (e.g. CAC containing blends).
Attainable Effects / Properties and Advantages
2
3
1. Performance Proles
Performance Prole comparing SLUs with Melux
/Starvis
Products
and conventional technologies
1.1 General Properties
1.2 Fresh Mortar Properties
Fig. 1
Depending on the requirements of SLUs,
raw material quality and selection, various
properties can be adjusted by using the
synthetic additives of the Melux
/Starvis

Hightech Pool for casein replacement.
Considerable improvements are achievable
by using a combination of Melux
2651 F
and Starvis
3003 F in comparison to casein

based SLUs.
Products
Case|n +
Convent|ona| Stab|||zer
Po|ycarboxy||c Ether +
Me|f|ux
2651 F +
Starv|s
3003 F
Propert|es
Synthet|c substances/
stab|e qua||ty
Dosage rate/
econom|c eff|c|ency
Low em|ss|ons/no mo|d
= exce||ent = ba|anced = bad = good
Products
Case|n +
Po|ycarboxy||c Ether +
Me|f|ux
2651 F +
Starv|s
3003 F
Propert|es
W|de dosage |nterva|
To|erance aga|nst water +
raw mater|a| dev|at|ons
Short m|x|ng t|me
Pumbab|||ty/
mach|ne app||cab|||ty
In|t|a| f|ow
Workab|||ty/
f|ow over t|me
Se|f hea||ng propert|es
Ant| segregat|on +
ant| b|eed|ng
Compat|b|||ty w|th
c|tr|c ac|d
Compat|b|||ty w|th
tartr|c ac|d
Fig. 2
Melux
/Starvis

4
1.3 Hardened Mortar Properties
2. Mode of Action
2.1 Mode of Action Superplasticizer Molecules (PCE)
2.2 Mode of Action of Stabilizer Molecules (ST)
Products
Case|n +
Po|ycarboxy|ate Ether +
Me|f|ux
2651 F +
Starv|s
3003 F
Propert|es
Strength deve|opment
Fig. 3
+ PCE
(Me|ux
|
cement
particle
Agglomerated cement particles
(with entrapped water)
Sticky cement paste (not owable)
Melux
molecules adsorbed on
cement particles
Dispersed cement particles
Flowable cement slurry
Sedimentation of dispersed
cement particles
Bleeding water on top
Starvis
molecules dissolved in
water (Viscosity enhanced)
No associative thickening
Therefore, owable and stable
mix without sedimentation
+ ST
(Starv|s
|
Fig. 4
Fig. 5
5
3. Application Technology Results
3.1 Test Recipe
Ingredients Amount [% btw]
OPC (CEM I 42.5 R) ___________________ 18.500
CAC (70% CA) ________________________ 11.500
CaSO
4
(Synthetic anhydrite) _____________ 6.500
Quartz sand (0.1 - 0.3 mm) _____________ 40.765 40.615
Limestone powder (20 m) _____________ 19.400
Latex powder __________________________ 2.000
Li
2
CO
3
________________________________ 0.100
Defoamer _____________________________ 0.150
Citric acid * ____________________________ 0.185
Shrinkage reducer ______________________ 0.600
Melux
2651 F _______________________ 0.250

Starvis
3003 F ________________________ 0.05 0.20

Total dry mortar ______________________100.000
Water ________________________________ 20.000
3.2 Fresh Mortar Properties
3.2.1 Dosage range interval and efciency of stabilizer
D|spersant [Stab|||zer]
Case|n
PCE
Me|ux
2651 F Starv|s
3003 F
0.01 0.02 0.03 0.04 0.05 0.06 0.07 0.08 0.09 0.10 0.11 0.12 0.13 0.14 0.15 ...0.20
bleeding slightly bleeding no flow (<14.50cmj good flow, no bleeding
Dosage of stab|||zer [btw|
Casein:
0.30 to 0.40% btw
Conventional Stabilizer:
0.05 to 0.10% btw
Commonly used PCE:
0.30 to 0.40% btw
Conventional Stabilizer:
0.09 to 0.10% btw
Me|f|ux
2651 F:
0.10 to 0.30% btw
Starv|s
3003 F:
0.05 to 0.20% btw
F|ow >14.50 cm, no b|eed|ng
High dispersant dosage
Narrow stabilizer dosage
High dispersant dosage
Extremely narrow
stabilizer dosage
Low dispersant dosage
Wide stabilizer
dosage range
Convent|ona|
Stab|||zer
Fig. 6
N.B.: All tests carried
out at 20C (68F)
temperature and 65%
relative humidity
* or tartaric acid, if
specically mentioned
Melux
/Starvis

6
3.2.2 Water tolerance Anti segregation and bleeding properties
3.2.3 Mixing time
Casein [0.30-40% btw| +
Conventional Stabilizer
[0.05-0.10% btw|
Me|ux
2651 F [0.10-30% btw|

+ Starv|s
3003 F
[0.05-0.20% btw|
Polycarboxylate Ether
[0.30-0.40% btw| + Conventional
Stabilizer [0.09-0.10% btw|
W
a
t
e
r
[
%

b
y

w
e
|
g
h
t

o
f

d
r
y

m
o
r
t
a
r
]
W
a
t
e
r
[
%

b
y

w
e
|
g
h
t

o
f

d
r
y

m
o
r
t
a
r
]
W
a
t
e
r
[
%

b
y

w
e
|
g
h
t

o
f

d
r
y

m
o
r
t
a
r
]
Requ|rement
B|eed|ng and segregat|on
S||ght|y b|eed|ng
No ow, ow < 14.5 cm
No b|eed|ng, ow

14.5 cm, no segregat|on
24
22
20
18
16
14
24
22
20
18
16
14
24
22
20
18
16
14
During mixing (EN 1937) every 15sec a sample
is taken and the ow is measured. Casein based
formulations need approx. 3 times (90sec)
longer mixing time than formulations based on
Melux
2651 F and Starvis
3003 F (30sec).
The short mixing time makes them especially
suitable for machine applied SLUs.
cumulated
real time action (EN 1937)
mixing time
000 030 Add powder to water 0
030 045 Mixing (140rpm) 15
045100 cleaning vessel & blades,
1
st

ow-probe 15
100115 mixing (285rpm) 30
115130 ow-sample 30
iterative con- every 15sec sample etc.
tinuing taken, 15sec mixed
Fig. 7
7
Mixing time
3.2.4 Flowability over Time (EN 12706)

Flow Properties
F
|
o
w

E
N

1
2
7
0
6

[
c
m
|
Tota| e|apsed m|x|ng t|me [sec|

16
15
14
13
12
11
10
9
0
1
5
3
0
4
5
6
0
7
5
9
0
1
0
5
1
2
0
1
3
5
1
5
0
1
6
5
1
8
0
1
9
5
2
1
0
2
2
5
2
4
0
2
5
5
2
7
0
2
8
5
3
0
0

Me|ux
2651 F [0.25% btw| +

Starv|s
3003 F [0.10% btw|

Casein [0.40% btw| +
[0.10% btw|
PCE [0.40% btw| +
[0.10% btw| +
Tartaric Acid [0.14% btw|
Fig. 8
F
|
o
w

E
N

1
2
7
0
6

[
c
m
|
T|me [min|
Me|ux
2651 F [0.25% btw| +

Starv|s
3003 F [0.10% btw|

[0.10% btw|
PCE [0.40% btw| +
[0.10% btw| +

15.5
15
14.5
14
13.5
15 30 45
Flow properties depend on early stiffening
of the binder. The thixotropic effects of
the stabilisers are reduced to an absolute
minimum.
Even at lower dosage rate of Melux
2651F
[0.25 %, btw] ow properties are superior
to regular casein [0.40 % btw] based
formulations.
Fig. 9
Melux
/Starvis

8
3.2.5 Self Healing Properties
Self healing is investigated with a knife-cut test.
The hardened surface can be assessed by a seven-step evaluation scale.
Example:
evaluation of knife cut test:
1 cut heals completely, invisible
2 cut heals, but visible
3 cut heals, but visible edges
4 cut heals, but well visible edges
5 cut heals, but visible scar
6 cut heals, but well visible scar
7 cut does not heal
3.2.6 Setting Time
Vicat Setting Times
1 2 3 6 7
Fig. 10
8m|n 15m|n 30m|n 45m|n 60m|n
Case|n/Convent|ona| Stab|||zer 1 1 2 3 5
PCE/Convent|ona| Stab|||zer 1 1 2 3 5
Me|ux
2651 F/Starv|s
3003 F 1 1 2 2 4
220
200
180
160
140
120
100
80
60
T
|
m
e

[
m
i
n
|
lnitial Final
[0.10% btw|
PCE [0.40% btw| +
[0.10% btw| +
Tartaric acid [0.14% btw|
Me|ux
2651 F [0.25% btw| +

Starv|s
3003 F [0.10% btw|

Retarding effects of casein and conventional stabilizer are eliminated by using Melux
2651 F
and Starvis
3003 F. This accelerates cement hydration during the hardening process resulting
in improved surface properties.
Fig. 11
8
15 30
45
60min
9
3.3 Hardened Mortar Properties
3.3.1 Compressive Strength
Compressive Strength of Mortar Prisms (4cm x 4cm x 16cm)
3.3.2 Flexural Strength
Flexural Strength of Mortar Prisms (4cm x 4cm x 16cm)
Using Melux
2651 F and Starvis
3003 F
provides improved early strength (after 4h)
compared to casein and cellulose ether.
Thus, required time for foot trafc hardness
and oor covering installation is substantially
shortened.
30
20
10
0
[
N
/
m
m
2
|
T|me
4h 24h 7d 28d
[0.10% btw|
PCE [0.40% btw| +
[0.10% btw| +
Me|ux
2651 F [0.25% btw| +

Starv|s
3003 F [0.10% btw|

Fig. 12
8
6
4
2
0
[
N
/
m
m
2
|
T|me
4h 24h 7d 28d
[0.10% btw|
PCE [0.40% btw| +
[0.10% btw| +
Me|ux
2651 F [0.25% btw| +

Starv|s
3003 F [0.10% btw|

Fig. 13
Melux
/Starvis

10
4.1 Storage Instructions
Due to the special polymer properties Melux

powder products have a thermal sensitivity which
may lead to lump formation in case of excessive
heat, humidity and pressure.
Melux
1641 F, 2641 F and 2651 F should be

stored at ambient temperatures below 40 C
(104 F), dry and cool in its unopened original
packaging at relative humidity below 60 %.
Close and reseal opened packages properly. In
any case, please do not double stack the pallets
(reduction of weight exposure).
The shelf life of Melux
1641 F, 2641 F and

2651 F is up to 1 year when stored in the
conditions stated above.
Starvis
3003 F should be protected from

excessive heat and stored in unopened original
packaging. Shelf life for this product is 2 years.
4.2 Others
Furthermore, it is important to obey the
relevant national laws and regulations
concerning safety, environmental protection,
storage and transport.
Beside this we kindly ask to follow the
corresponding advice in technical and
material safety data sheets.
Additional information will gladly be
provided on request.
4.0 Miscellaneous
This information and all further technical advice are based on our current knowledge and experience. However, it implies
no liability or other legal responsibility on our part, including with regard to existing third party intellectual property rights,
especially patent rights. In particular, no warranty, whether expressed or implied, or guarantee of product properties in the
legal sense is intended or implied. We reserve the right to make any changes according to technological progress or further
developments. The customer is not released from the obligation to conduct careful inspection and testing of goods.
Performance and suitability of the product described herein have to be veried by testing, which has to be carried out only
by qualied experts in the sole responsibility of the customer. Reference to trade names used by other companies is neither
a recommendation nor an implementation that similar products could not be used.
In addition our general terms and conditions for sale are valid.
Issue: August 2008
This technical note is valid until replaced by a new issue.
11
For your notes
Marketing/Sales
Tel. + 49 8621 86-16
Fax + 49 8621 86-29 95
Application Technology
Tel. + 49 8621 86-28 55
Fax + 49 8621 86-32 36
How to get through to your Contact Person
BASF Construction Polymers
GmbH is an international
organization providing services
and products as a global
business.
The headquarters and our
regional ofces are located in
the below mentioned countries.
Those countries, which are not
listed below are directly served
by our headquarters in Trostberg,
Germany.
Worldwide Activities
d
e
s
i
g
n
.

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w
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.
s
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p
a
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Germany (Headquarters)
BASF Construction Polymers GmbH
Dr.-Albert-Frank-Strae 32
83308 Trostberg
Germany
P.O. Box 11 16
83302 Trostberg
Tel.: +49 8621 86-16
Fax: +49 8621 86-29 95
www.construction-polymers.com
USA / Canada / Mexico
(Construction Polymers)
BASF Corp.
Construction Polymer Additives
2125 Barrett Park Dr.
Suite 102
Kennesaw, GA 30144-7080
United States of America
Tel.: +1-7 70-9 71 13 17
Fax: +1-7 70-9 71 43 06
info@basf-cop.com
www.basf-cop.com
Australia
ISM International Sales &
Marketing Pty. Ltd.
262 Highett Road
Highett, 3190
Victoria
Australia
Tel.: +61-3-95 32-12 77
Fax: +61-3-95 32-08 02
skelly@ismaus.com
www.ismaus.com
United Kingdom & Ireland
IMCD UK Ltd
(Previous name:
Honeywill & Stein Limited)
Times House
Throwley Way
Sutton, Surrey, SM1 4AF
United Kingdom
Tel.: +44-20-87 70 70 90
Fax: +44-20-87 70 72 95

info@imcd.co.uk
www.imcdgroup.uk
Argentina / Paraguay / Uruguay
Delanta S.A.
Emilio Lamarca 2428, Don Torcuato
Buenos Aires
Argentina
Tel.: +54 11 47 27-03 33
Fax: +54 11 47 27-02 06
ventas@delanta.com.ar
www.delanta.com.ar
Japan (Construction Polymers
and Oileld Polymers)
BASF Pozzolith Ltd.
Polymers Division
Nanbu Bldg. 3-3 Kioicho
Chiyoda-ku
Tokyo 102-8570
Japan
Tel.: +81-3-32 38 22 05
Fax: +81-3-32 38 22 10
bcs-polymers@basf.com
www.pozzolith.basf.co.jp
Italy (Construction Polymers)
Neuchem S.R.L.
Corso Sempione 270/a
20080 San Vittore Olona MI
Italy
Tel.: +39-03 31-42 33 10
Fax: +39-03 31-42 33 03
info@neuchem.it
www.neuchem.it
Russia
EuroHim-1 Ltd.
P.O. Box 33
2a, Tromova
115432 Moscow
Russia
Tel.: +7-4 95 7 81 66 56
Fax: +7-4 95 7 81 66 46
sss@eurohim.ru
www.chem.eurohim.ru
Brazil
Makeni Chemicals Ltd.
Avenida Presidente Juscelino, 570/578
CEP 09950-370 Diadema SP
Brazil
Tel.: +55 11 43 60 64 00
Fax: +55 11 40 71 06 94
Mobile: +55 11 99 18 98 08
makeni@makeni.com.br
www.makeni.com.br

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BASF Construction Polymers GmbH

Hightech Pool Application Technology Report

2651 F and viscosity modifying agent

3003 F are synthetic chemical additives which were developed as a

2651 F in combination with viscosity

3003 F enable the for-

2651 F: 0.10 to 0.30% btw

3003 F: 0.05 to 0.20% btw

Cementitious self levelling underlayments

3003 F in comparison to casein

Hightech Pool Application Technology Report

2651 F _______________________ 0.250

3003 F ________________________ 0.05 0.20

Hightech Pool Application Technology Report

2651 F [0.10-30% btw|

2651 F and Starvis

2651 F [0.25% btw| +

3003 F [0.10% btw|

2651 F [0.25% btw| +

3003 F [0.10% btw|

Hightech Pool Application Technology Report

2651 F [0.25% btw| +

3003 F [0.10% btw|

2651 F and Starvis

2651 F [0.25% btw| +

3003 F [0.10% btw|

2651 F [0.25% btw| +

3003 F [0.10% btw|

Hightech Pool Application Technology Report

1641 F, 2641 F and 2651 F should be

1641 F, 2641 F and

3003 F should be protected from

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