BACKGROUND OF TITRINO 702 AUTOMATIC TITRATOR 1. What is Titrino 702 Automatic Titrator ?

It is an electrical apparatus that can detect Free Hydro and Indigo concentration thru Potentiometric Method. 2. What kind of distilled water will be use for Titrant preparation ? Distilled water should be - 100% purified - pH is 7.0 - Total Hardness is 0 . to avoid sedimentation in Titrino burette that causes clogging in tube line. Effect : Inaccurate result 3. What is the formula use in determining Free Hydro concentration being programmed in the Titrino ? RS 1 = (EP1 x CO1) + CO2 Wherein; RS 1 is the concentration of Free Hydro in grams per liter (g/l) EP 1 is the End point wherein Hydro is completely digested or equal to the volume of 0.1 N Potassium Ferrocyanide consumed in milliliter (ml). CO 1 is the Coefficient Factor 1 or the dilution factor = 0.49 CO 2 - is the Coefficient Factor 2 or the Blank factor = 0 Sample Computation: RS 1 or GPL Hydro = ( 1.202 ml Ferrocyanide consumed x 0.49) + 0 = 0.59 g/l Hydro 4. What is the formula use in determining Indigo concentration being programmed in the Titrino ? (EP2 EP 1) x CO3 RS 2 = ------------------------CO4 Wherein; RS2 is the concentration of Indigo in grams per liter (g/l) EP 1 is the End point wherein Hydro is completely digested or equal to the volume of 0.1 N Potassium Ferrocyanide

consumed in milliliter (ml). EP 2 is the End point wherein Indigo is completely digested or equal to the volume of 0.1 N Potassium Ferrocyanide consumed in milliliter (ml). CO 3 is the Coefficient Factor 3 or the dilution factor for Indigo 0.68. CO 4 - is the Coefficient Factor 4 or the dilution factor for both Free Hydro and Indigo. Sample Computation: (2.698 ml Fe consumed for Indigo - 1.202 ml Fe consumed for Hydro ) x 0.68 RS 2 or GPL Indigo = -------------------------------------------------------------------------0.95 = 1.02 g/l Indigo 5. What is the method use for 5 ml dye liquor sample ( Indigo above 2 gpl) ? Hyd/Ind5 Method - this method is applicable for Slasher dyeing. RS 1 or g/l Hydro = EP 1 x (0.49 x 2) + 0 How to operate the Titrino apparatus ? - Press user meth and then ENTER. - Press Select and find Hyd/Ind5. - Press Enter How to check the constant in Hyd/Ind5 Method ? - Press C-fml : CO 1 value will appear - (0.98) - Press Enter : CO 2 value will appear - (0) - Press Enter : CO 3 value will appear (1.36) - Press Enter : CO 4 value will appear ( 0.95) - Press Enter to go back to method display. How to compute Indigo concentration when Hydro has Missing Endpoint (MEP) ? Calculation for Indigo with Missing Endpoint Hydro: EP1 x CO3 g/l Indigo = ----------------CO4

Or;

Vol. Ferrocyanide consumed for Hydro x 1.36 = -------------------------------------------0.95 = EP1 x 1.4316 = ________ gpl Indigo

6. What is the method use for 10 ml dye liquor sample ( Indigo below 2 gpl) ? Hyd/Ind10 Method - this method is applicable for Rope dyeing. RS 1 or g/l Hydro = EP 1 x (0.49) + 0 How to operate the Titrino apparatus ? - Press user meth and then ENTER. - Press Select and find Hyd/Ind10. - Press Enter How to check the constant in Hyd/Ind10 Method ? - Press C-fml : CO 1 value will appear - (0.49) - Press Enter : CO 2 value will appear - (0) - Press Enter : CO 3 value will appear (0.68) - Press Enter : CO 4 value will appear ( 0.95) - Press Enter to go back to method display. How to compute Indigo concentration when Hydro has Missing Endpoint (MEP) ? Calculation for Indigo with Missing Endpoint Hydro: EP1 x CO3 g/l Indigo = ----------------CO4 Vol. Ferrocyanide consumed for Hydro x 0.68 = -------------------------------------------0.95 = EP1 x 0.7158 = ________ gpl Indigo

Or;

7. What is the function of DOS in the keyboard ? DOS is use only for manual dosage. HOW TO TROUBLESHOOT IF SOME OF THE DISPLAY IN THE KEYBOARD MIGHT BE ACCIDENTALLY PRESS? 1. DOS Action: Press STOP and then ENTER. 2. MODE Action: Press QUIT and then ENTER.

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