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    Texture Analysis Implementation and Use

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    ronpandolfi
    This document summarizes texture analysis techniques used to study the crystalline structure of materials. Texture refers to the orientation of crystal lattices within a material. Diffraction experiments are used to measure texture by recording how x-rays scatter off of a sample's crystal planes at different rotation angles. These diffraction patterns are represented as pole figures that map the distribution of crystal orientations. The document demonstrates applying these methods to analyze copper samples and identifies plans to automate the technique and compare different algorithms for inverting pole figures into 3D texture models.

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    Texture Analysis Implementation and Use

    Uploaded by

    ronpandolfi
    115 views21 pages
    This document summarizes texture analysis techniques used to study the crystalline structure of materials. Texture refers to the orientation of crystal lattices within a material. Diffraction experiments are used to measure texture by recording how x-rays scatter off of a sample's crystal planes at different rotation angles. These diffraction patterns are represented as pole figures that map the distribution of crystal orientations. The document demonstrates applying these methods to analyze copper samples and identifies plans to automate the technique and compare different algorithms for inverting pole figures into 3D texture models.

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    Texture Analysis  Implementation and Use

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    This document summarizes texture analysis techniques used to study the crystalline structure of materials. Texture refers to the orientation of crystal lattices within a material. Diffraction experiments are used to measure texture by recording how x-rays scatter off of a sample's crystal planes at different rotation angles. These diffraction patterns are represented as pole figures that map the distribution of crystal orientations. The document demonstrates applying these methods to analyze copper samples and identifies plans to automate the technique and compare different algorithms for inverting pole figures into 3D texture models.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    115 views21 pages

    Texture Analysis Implementation and Use

    Uploaded by

    ronpandolfi
    This document summarizes texture analysis techniques used to study the crystalline structure of materials. Texture refers to the orientation of crystal lattices within a material. Diffraction experiments are used to measure texture by recording how x-rays scatter off of a sample's crystal planes at different rotation angles. These diffraction patterns are represented as pole figures that map the distribution of crystal orientations. The document demonstrates applying these methods to analyze copper samples and identifies plans to automate the technique and compare different algorithms for inverting pole figures into 3D texture models.

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    of 21

    Texture Analysis  Implementation and Use

    Ronald J. Pandol
    Mentor: Apurva Mehta
    Stanford Synchrotron Radiation Lightsource, SULI Student

    August 13, 2009


    What is (crystalline) texture?

    Mouse enamel, magnetotactic bacterium, abalone aragonite


    platelets, and sponge spicule each have texture.
    Outline

    Motivation
    Diraction physics
    Representation of texture
    Results from Cu sample
    Plans for future development
    Basic Diraction Physics

    Bragg Diraction
    Basic Diraction Physics
    Outline

    Motivation
    Diraction physics
    Representation of texture
    Results from Cu sample
    Plans for future development
    How is texture represented?
    Pole Figures
    A planar projection of the diraction image
    Superposition of diraction rings recorded at dierent
    goniometer angles, with an equal area projection
    Point intensities proportional to the density of points on the
    reciprocal sphere
    Basic Diraction Physics

    The projection of the diraction rings onto a planar surface, with


    the rotation of the sample, gives a pole gure. Each ring location
    corresponds to a dierent pole gure
    Studying texture at SSRL

    The x-ray sources at SSRL and beamline facilities provide a suitable


    laboratory for texture analysis.

    Experimentation at SSRL would benet from a texture analysis


    system.
    Studying texture at SSRL

    The x-ray sources at SSRL and beamline facilities provide a suitable


    laboratory for texture analysis.

    Experimentation at SSRL would benet from a texture analysis


    system.
    Diraction geometry

    {χ, θ, ∆} → {φ, ψ}
    Pole gures  projections of the reciprocal sphere

    From the 2D pole gures, the 3D texture orientation space must be


    determined. This is a complex mathematical inversion process
    similar to tomogrophy. Solutions are not unique.
    Outline

    Motivation
    Diraction physics
    Representation of texture
    Results from Cu sample
    Plans for future development
    Application of texture analysis procedure

    Example diraction image for Cu target sample


    Application of texture analysis procedure

    Incomplete-interpolated and completed pole gures for Cu


    diraction Data, 111 index.
    Application of texture analysis procedure

    Incomplete-interpolated and completed pole gures for Cu


    diraction Data, 200 index.
    Application of texture analysis procedure

    Incomplete-interpolated and completed pole gures for Cu


    diraction Data, 220 index.
    Application of texture analysis procedure

    Incomplete-interpolated and completed pole gures for Cu


    diraction Data, 311 index.
    Outline

    Motivation
    Diraction physics
    Representation of texture
    Results from Cu sample
    Plans for future development
    What next?

    Plans for further development:


    Other pole gure inversion methods may be used.
    A comparative study may reveal that one algorithm works
    better for this data set.
    Complete automation
    Questions?
    SPECIAL THANKS TO-

    Apurva Mehta

    Matt Bibee

    James (Randy) Groves

    Marc Davidson

    Karen Magid

    Stanford Linear Accelerator Center

    Stanford Synchrotron Radiation Lightsource

    Stanford University

    Science Undergraduate Laboratory Internships

    Department of Energy

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