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HPLC 2013 Amsterdam Program
HPLC 2013 Amsterdam Program
HPLC 2013 Amsterdam Program
39th International Symposium on High Performance Liquid Phase Separations and Related Techniques
HPLC 2013
Final Program
Dionex Corona
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Contents
Welcome Message ...................................................................................................................................................... 4 Sponsors ...................................................................................................................................................................... 5 Media Partners ........................................................................................................................................................... 8 Supporting Organizations ........................................................................................................................................... 9 Committees ............................................................................................................................................................... 10 History and Future Meetings .................................................................................................................................... 12 Awards ...................................................................................................................................................................... 16 Short Courses ............................................................................................................................................................ 18 Lecture Program ....................................................................................................................................................... 21 Lunch & Breaks Scheme/Special Events ................................................................................................................... 23 List of Posters ............................................................................................................................................................ 55 Vendor seminars ..................................................................................................................................................... 147 Symposium proceedings ......................................................................................................................................... 152 Information for Speakers and Poster Presenters .................................................................................................... 153 Exhibition ................................................................................................................................................................ 155 Exhibitors ................................................................................................................................................................ 158 Exhibition Area ........................................................................................................................................................ 166 Social Events ........................................................................................................................................................... 169 General Information ............................................................................................................................................... 170
Welcome Message
Welcome to Amsterdam and the 39th International Symposium on High-Performance Liquid-Phase Separations and Related Techniques. HPLC2013 Amsterdam is the third meeting in this series that is held in The Netherlands after 1987 (Amsterdam) and 2001 (Maastricht). Not bad for a country with mostly baseline and very few peaks. Throughout the last fifty or sixty years many chromatographers gathered in our country, starting with van Deemter and following on with the likes of Carel Cramers, Udo Brinkman, and the brilliant Hans Poppe, as well as imported talent, such as Joseph Huber and Roland Frei. Like painters in the 17th century they all found their way to Amsterdam.
Amsterdam is one of the natural hubs of the old and the new Europe. Odds are that you found it easy to get here. In fact, odds are that you have been here before and that you will come back. Although us Dutch can be impolite and ill-mannered (not only the cab drivers), we do appreciate you being here. To demonstrate our hospitality, just about everyone in Amsterdam can communicate with you in English. We offer you a generous amount of separation science this week. We have three hours of lectures on a typical morning or afternoon, plus posters, technical seminars and tutorials. We offer you generous amounts of coffee, food, and drinks (on four occasions during the week). We offer you free internet at the conference and Petras posse is offering all the help you need. And, yes, we are frugal! I have great memories of the incredible HPLC1987 Amsterdam. Our aim is to give you a week that you will treasure until at least 2040. On behalf of the entire team of HPLC2013 Amsterdam, welcome! Peter Schoenmakers
The organization of the HPLC symposium would not have been possible without the generous and invaluable support of the following companies and organizations.,
Sponsors
Agilent Technologies
Platinum Sponsors
Agilent Technologies is a global provider of leading measurement technology for evaluating the environment, foods, pharmaceuticals, industrial processes, and biological samples for over 40 years and has 19,0000 employees worldwide. A leader in GC and GC/MS, Agilent also makes some of the world's bestselling liquid chromatography and LC/MS systems and holds leadership positions in consumables, software, genomics, reagents, lab automation, support and compliance services.
Shimadzu is one of the worldwide leading manufacturers of analytical instrumentation for consumer protection, product and environmental safety. Latest developments include the Nexera X2 UHPLC system, which targets routine analysis and applications in highly regulated environments, the LCMS-8040, the worlds fastest LCMS/MS tandem mass spectrometer, the Perfinity iDP* (integrated Digestion Platform) online enzyme digestion HPLC system and the Nexera MP, which is perfect as a Front End system for LC/MS analysis conducted in pharmacokinetics and synthesis stages in drug detection processes. Its new SIL-30ACMP Multiplate Autosampler provides industry-leading features.
Shimadzu Europe
Thermo Scientific
Thermo Fisher Scientific Inc. is the world leader in serving science. Our mission is to enable our customers to make the world healthier, cleaner and safer. We serve customers within pharmaceutical and biotech companies, hospitals and clinical diagnostic labs, universities, research institutions and government agencies, as well as in environmental and process control industries. Our three premier brands are Thermo Scientific, Fisher Scientific and Unity Lab Services, which offer a unique combination of innovative technologies, convenient purchasing options and a single solution for laboratory operations management. Our products and services help our customers solve complex analytical challenges, improve patient diagnostics and increase laboratory productivity.
Waters Corporation
Waters Corporation, the premium brand in the analytical instruments industry, creates business advantages for laboratory-dependent organizations by delivering practical and sustainable scientific innovation to enable significant advancements in healthcare delivery, environmental management, food safety, and water quality worldwide. Bringing keen understanding and deep experience to those responsible for laboratory infrastructure and performance, Waters helps customers make profound discoveries, optimize laboratory operations, deliver product performance, and ensure regulatory compliance. Pioneering a connected portfolio of separations and analytical science, laboratory informatics, mass spectrometry, as well as thermal analysis, Waters technology breakthroughs and laboratory solutions provide an enduring platform for customer success.
Gold Sponsors
AB SCIEX AB SCIEX is a global leader in the development of best-in-class technologies that help answer complex scientific challenges and improve our world. We create scientific instrumentation, software and services for the life science, clinical research and industrial markets, empowering you with technologies that are used in drug discovery and manufacturing, food and environmental
Merck Millipore
Molnr-Institute for applied chromatography For over 30 years, Molnr-Institute has delivered chromatography modeling solutions to the pharmaceutical, chemical, food, biotech and research industries. Our UHPLC modeling software DryLab is used worldwide and offers an intuitive and visual solution for the creation of fast, robust and high quality methods. With its comprehensive resolution and robustness mapping abilities, DryLab enables scientists to easily determine their optimal working space, and to gain unprecedented insight into the effects of various parameters on the resolution and selectivity of the separation. We look forward to meeting you at our booth E18!
Sigma-Aldrich is a leading Life Science and High Technology company committed to enabling Science to improve the quality of Life. Supelco, Fluka, Cerilliant and RTC are the analytical brands of Sigma-Aldrich. Supelcos innovative chromatography products together with Flukas high quality analytical solvent, reagents and standards are used for research and control in Pharmaceutical, Food, Environmental, Clinical and many others areas. Recently Cerilliant and RTC joined the Sigma-Aldrich family to further increase the quality offering of Certified Reference Materials and Proficiency testing. Sigma-Aldrich operates in 40 countries and has over 9,600 employees providing excellent service worldwide. Welcome to visit us in person at Booth A10 during HPLC 2013 in Amsterdam to discuss the latest in particle technology/phase chemistry or let us know how we can make you more successful.
Sigma-Aldrich International
Silver Sponsors
Knauer - Wissenschaftliche Geraetebau Dr. Ing. H. Knauer KNAUER manufactures UHPLC and HPLC systems for the analytical up to the preparative range of applications. The instruments are used in science, quality control, and test laboratories worldwide. KNAUER is a competent partner for continuous chromatography using SMB and MCSGP technologies. For high resolution analysis or purification of proteins and other biomolecules KNAUER offers perfectly matched biochromatography systems, pressure stable glass columns, and separation media. LC columns, UV/VIS/NIR and RI detection systems, as well as appropriate software complete the choice of high quality LC products. KNAUER also supplies osmometers for chemistry and clinical use. KNAUER is certified ISO 9001/14001 Restek Corporation
Phenomenex Phenomenex is a global leader committed to developing novel analytical chemistry solutions that solve the separation and purification challenges of researchers in industrial, government and academic laboratories. The companys core technologies include products for liquid chromatography, gas chromatography, sample preparation, bulk purification chromatographic media, and chromatography accessories and equipment. Phenomenex is responsible for many HPLC innovations over the years, most recently including the award-winning Kinetex Core-Shell Technology.
Bronze Sponsors
SCAT Europe
Media Partners
Supporting Organizations
CASSS - An International Separation Science Society Arbeitskreis Separation Science Association Francophone des Sciences Sparatives Austrian Society of Analytical Chemistry (ASAC) Czech Chemical Society - Chromatography & Electrophoresis Group Deutschen Gesellschaft fr Massenspektrometrie (DGMS) Divisioni di Chimica Analitica Hungarian Society for Separation Sciences Koninklijke Vlaamse Chemische Vereniging (KVCV) KNCV Sectie Analytische Chemie (SAC) Nederlandse Vereniging voor Massaspectrometrie (NVMS) Polska Akademia Nauk (PAN) Sociedad Espaola de Cromatografa y Tcnicas Afines (SECyTA) The Chromatographic Society (ChromSoc) University of Amsterdam
Committees
Scientific Committee
Permanent members Atilla Felinger (Hungary) John Frenz (USA) Georges Guiochon (USA) Bill Hancock (USA) Grard Hopfgartner (Switzerland) Barry Karger (USA) Wolfgang Lindner (Austria) Koji Otsuka (Japan) Peter Schoenmakers (The Netherlands) Guowang Xu (China) Ed Yeung (USA) Ad hoc members Gert Desmet (Belgium) Monika Dittmann (Germany) Paola Dugo (Italy) Emily Hilder (Australia) Michael Lmmerhofer (Germany) David McCalley (UK) Michel Nielen (The Netherlands) J. Michael Ramsey (USA) Marja-Liisa Riekkola (Finland) Ulrich Tallarek (Germany)
Chairmen
Local Organizers
Tom Aalbers Petra Aarnoutse Peter Verschuren Gabriel Viv Truyols
PCO
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The International Symposium on High Performance Liquid Phase Separations (HPLC) is an international forum for the scientific discussion of the methods of high performance liquid chromatography in its various forms, along with the complementary separation techniques such as electrophoresis, electrochromatography, field-flow fractionation, supercritical fluid chromatography and hyphenated techniques, such as LC/MS and CE/MS. In addition, microfluidics, separations on chips, diagnostic systems, and other leading technologies are also considered. This conference originated in 1973. Advances in the field of liquid-phase separations are highlighted at each meeting. The meetings alternate between Europe and the United States with even years being in the US. Since 2008 additional meetings are held in Asia and other continents.
Chair(s) Willy Simon Jack J. Kirkland Joseph F.K. Huber Barry L. Karger Georges Guiochon Robert Bardford Klaus Peter Hupe Csaba Horvath John H. Knox Ronald E. Majors Hans Poppe Georges Guiochon Douglas Westerlund Barry L. Karger Fritz Erni
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Year 1992 1993 1994 1995 1996 1997 1998 1999 2000 2001 2001 2002 2003 2004 2005 2006 2007 2008 2008 2009 2010 2011 2011 2012 2013 2013 2014 2015 2016 2017
Location Baltimore, USA Hamburg, Germany Minneapolis, USA Innsbruck, Austria San Francisco, USA Birmingham, UK St. Louis, USA Granada, Spain Seattle, USA Maastricht, The Netherland Kyoto, Japan Montreal, Canada Nice, France Philadelphia, USA Stockholm, Sweden San Francisco, USA Gent, Belgium Baltimore, USA Kyoto, Japan Dresden, Germany Boston, USA Budapest, Hungary Dalian, China Anaheim, USA Amsterdam, The Netherlands Hobart, Australia New Orleans, USA Geneva, Switzerland San Francisco, USA Prague, Czech Republic
Chair(s) Fred E. Regnier Klaus K. Unger Larry D. Bowers and Peter W. Carr Wolfgang Lindner William S. Hancock Anthony F. Fell Daniel W. Armstrong Emilio Gelpi Edward S. Yeung Hans Poppe and Henk Lingeman Nobuo Tanaka and Shigeru Terabe Irving W. Wainer Antoine M. Siouffi Mark R. Schure Douglas Westerlund John H. Frenz Jacques Crommen and Pat Sandra Georges Guiochon and Steven Jacobson Koji Otsuka and Nobuo Tanaka Christian Huber Steven A. Cohen Attila Felinger Guowang Xu Frantisek Svec Peter Schoenmakers and Wim Kok Paul Haddad and Emily Hilder J. Michael Ramsey Grard Hopfgartner Robert T. Kennedy Michal Holapek and Frantisek Foret
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Awards
Eligibility Criteria All presenters of oral contributions (excepting past winners) who are less than 35 years of age at the time of their lecture are eligible for consideration. Candidates will be required to provide evidence of eligibility (e.g., passport, driver's license). Selection Process The Scientific Committee selects abstracts for inclusion in the oral program. An Award Jury judges the eligible th presentations and chooses a winner. The winner will be announced at the closing ceremony, Thursday, June 20 at 16:40 in the Auditorium.
Uwe Neue was an outstanding liquid chromatographer. Two-and-a-half years after he passed away the first award that carries his name will be presented to an industrial scientist who like Uwe has made significant contributions to the field of separation science and has strived to see these implemented in commercial products. The award underlines what Uwe Neue has amply demonstrated. Great scientists can make great contributions and have great careers in industry.
th
The award will be presented on Tuesday, June 18 at 8:40 in the Auditorium by Martin Gilar of Waters and Georges Guiochon on behalf of the permanent scientific committee to Dr. J.J. Kirkland, vice president of R&D Technologies, Advanced Materials Technology, for his advancements in chromatography and dedication to separation science.
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Agilent Technologies is the long-standing sponsor of the poster awards at the HPLC meetings. Also this year, Agilent are generously sponsoring ten awards of 500 each for the best posters. Expert Review Gerard Rozing will lead a jury consisting of a large number of recognized international experts on liquid phase separations. The jury will publically nominate up to 30 posters on Wednesday evening. Posters are reviewed based on excellence in terms of three criteria Inspiration (creativity, novelty, uniqueness, originality) Transpiration (experimental execution, completeness of the work) Presentation (overall readability of the poster, visual impression, objectives and conclusions, author's explanations) In the final round on the last day of the conference, seven of these nominated posters will be selected to receive Agilent Technologies best-poster awards. Public poll Statistician Martin Lopatka organizes the public vote. All participants (industrial and academic scientists, students and exhibitioners) are urged to vote. The public voting will take place at Poster Headquarters in the exhibition area. Poster HQ is also the home of the expert jury and the place where jurors report for duty. The three highest scoring posters in the public poll will also receive Agilent Technologies best-poster awards. Qualification To qualify for a poster award you must have declared yourself a candidate upon submitting your abstract. To th qualify for the public poll you should have submitted a pdf copy of your poster by June 7 2013.
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All short courses take place in parallel on Sunday, June 16, from 9:00 to 16:00 in the RAI Congress Centre, Amsterdam. Sample Preparation in HPLC Lourdes Ramos and Mara Luz Sanz Dpt. Anlisis Intrumental y Qumica Ambiental, IQOG-CSIC, ES Lecture Hall G104
Short Courses
Short course 1
Short course 2
Comprehensive Two-Dimensional Liquid Chromatography (LCLC) 1 2 Dwight Stoll and Xiaoli Wang 1 2 Gustavus Adolphus College, US; Agilent Technologies, Wilmington, DE, US Lecture Hall G105
Short course 3
Short course 4
Retention Mechanisms in HPLC Mara Celia Garca-lvarez-Coque and Jos Ramn Torres Lapasi University of Valencia, ES Lecture Hall G107
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Lecture Program
Sunday, June 16, 2013 Plenary Session
16:15 17:00 17:00 17:40 Opening Ceremony PL1 Fight against Cancer Jos Beijnen Slotervaart Hospital, Amsterdam, NL Introduced by Wim Kok PL2 Top Ten HPLC Column Myths Ron Majors Wilmington, DE, US Introduced by Peter Schoenmakers and Laura Bush PL3 Forget Everything, Except Mass Spectrometry Michel Nielen Wageningen University and RIKILT, Wageningen, NL Introduced by Grard Hopfgartner
17:40 18:10
18:10 18:40
18:40 19:00
PL4 From Pore Level Reconstruction to Morphological Analysis of Eddy Dispersion Stefan Bruns, Tibor Mllner, Ulrich Tallarek Philipps Universitt Marburg, Marburg, DE Introduced by John Frenz ChromSoc Awards Presented by Paul Ferguson Welcome Reception Sponsored by Shimadzu Corporation
19:00 19:10
19:15 21:00
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Thursday, June 20
11:00 11:30 12:30 13:30 14:30 14:50 Coffee-Tea break / Exhibition & Posters Lunch / Exhibition & Posters Coffee-Tea break
Special Events
Tuesday, June 18, Auditorium
8:40 9:00 Uwe D. Neue Award (sponsored by Waters Corporation) Presented by Martin Gilar and Georges Guiochon
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9:30 10:00
KN2 Monolithic Columns in Thin Layer Format for TLC-MS Separations Frantisek Svec, Alexandros Lamprou, Zhixing Lin, Yongqin Lu LBNL, The Molecular Foundry, Berkeley, CA, US OR1 New Developments in Chromatographic Applications for the Enrichment and Separation of Biological Molecules Gnther Bonn Institute of Analytical Chemistry and Radiochemistry, Innsbruck, AT OR2 Mashmallow Gels: Monolithic Macroporous PDMS Analogue for Versatile Separations 1 1 1 2 Kazuki Nakanishi , Gen Hayase , Kazuyoshi Kanamori , Kei Morisato 1 2 Kyoto University, Graduate School of Science, Kyoto, JP; GL Sciences/Kyoto University, Graduate School of Science, Kyoto, JP OR3 HYPERperformance Carbon Phases for Ion Chromatography and Hydrophilic Interaction Liquid Chromatography Charles A. Lucy, M. Farooq Wahab, Mohammed E.A. Ibrahim Department of Chemistry/University of Alberta, Edmonton, Alberta, CA
10:00 10:20
10:20 10:40
10:40 11:00
Emerald
KN7 Improving Patient Outcome by Strategic Build within the Healthcare Sector Gyorgy Marko-Varga Lund University, Lund, SE KN8 State-of-the-art Liquid Chromatography for (Bio)Pharmaceutical Analysis Pat Sandra, Koen Sandra Research Institute for Chromatography, Kortrijk, BE OR10 Combining Three HPLC Modes and Polysaccharide-Based Chiral Stationary Phases in One Generic Separation Strategy 1 2 1 1 Debby Mangelings , Ahmed Younes , Hasret Ates , Yvan Vander Heyden 1 2 Vrije Universiteit Brussel - FABI, Brussels, BE; Helwan University, Cairo, EG OR11 Enantioselective Ultrahigh-Pressure Liquid Chromatography and UltrahighPerformance Supercritical Fluid Chromatography in the Chiral Science Separation Scenario: Ultra-Fast Separations on a New Sub-2-m Whelk-O 1 Stationary Phase 1 1 1 2 3 4 Dorina Kotoni , Alessia Ciogli , Marco Pierini , Jelena Kocergin , Ted Szczerba , Harald Ritchie , 1 1 Claudio Villani , Francesco Gasparrini 1 2 3 Sapienza University of Rome, Rome, IT; Regis Technologies, Morton Grove, Illinois, US; Regis 4 Techn., Morton Grove, Illinois, US; Thermo Fisher Scientific, Runcorn, GB OR12 Identification of Drug Target Spectrum by Monolith Affinity Chromatography and HPLC-Mass Spectrometry Jingwu Kang, Xuepei Zhang Shanghai Institute of Organic Chemistry, CAS, Shanghai, CN
9:30 10:00
10:00 10:20
10:20 10:40
10:40 11:00
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OR20 Novel Isotope Dimethyl Labeling-Based Methods for Quantitative Proteomics Study with High Accuracy and Precision Yuan Zhou, Yichu Shan, Lihua Zhang, Zhang Yukui Dalian Institute of Chemical Physics, CAS, Dalian, CN OR21 LC-MS: A Delivery Platform for Drug Targets and Biomarkers Iulia M. Lazar Virginia Polytechnic Institute and State University, Blacksburg, VA, US OR22 Clean-Up Strategies to Overcome the Matrix Effect in the Determination of Polyether Ionophores in Sewage Sludge by Liquid Chromatograpy-Tandem Mass Spectrometry Pol Herrero, Francesc Borrull, Eva Pocurull, Rosa Maria Marc Universitat Rovira i Virgili, Tarragona, ES KN11 Ionization Methods in Liquid Chromatography-Mass Spectrometry Risto Kostiainen University of Helsinki, Faculty of Pharmacy, Helsinki, FI KN12 New Ionization Methods for Use in Mass Spectrometry Sarah Trimpin Wayne State University, Detroit, MI, US
9:20 9:40
9:40 10:00
10:00 10:30
10:30 11:00
Tutorials
9:30 10:10 TU1 The Role of the Column in Modern HPLC/UHPLC Ron Majors Wilmington, DE, US Introduced by Katya Davydova TU2 Microfluidic Chemical Separations Devices J. Michael Ramsey University of North Carolina, Chapel Hill, NC, US Introduced by Sebastian Thrmann
G104-105
10:30 11:10
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OR4 Sample Trapping in Microfluidic LC: Theoretical and Practical Considerations Martin Gilar, Gregory Roman, Jay Johnson, Jim Murphy Waters Corp., Milford, MA, US OR5 Reaching Sub-m Plate Heights in HPLC by Radial Extension of the Support Structures 1 1 1 1 2 Wim De Malsche , Jeff Op De Beeck , Manly Callewaert , Heidi Ottevaere , Han Gardeniers , 1 Gert Desmet 1 2 Vrije Universiteit Brussel, Brussels, BE; UTwente, Enschede, NL OR6 Two-Photon Excited Fluorescence Detection in Chip Electrochromatography Claudia Ernst, Reinhild Beyreiss, Detlev Belder University of Leipzig, Institute of Analytical Chemistry, Leipzig, DE
11:50 12:10
12:10 12:30
Emerald
OR13 Applications of Two-Dimensional Liquid Chromatography in Pharmaceutical Analysis C.J. Venkatramani, James Girotti, Larry Wigman, Nik Chetwyn Genentech Inc, South San Francisco, US OR14 Method Development and Application of Ultra-Fast Supercritical Fluid Chromatography in Pharmaceutical Analysis 1 2 2 1 Lucie Novkov , Michal Doua , Josef Reitmajer , Petr Solich 1 2 Charles University in Prague, Faculty of Pharmacy, Hradec Krlov, CZ; Zentiva a.s., Prague, CZ DI1 Discussion on needs for pharmaceutical analysis
11:50 12:10
12:10 12:30
G102-103
KN13 Reactions of Gadolinium Chelates in Biological Matrices and the Environment Unraveled by Hyphenated Analytical Techniques Uwe Karst, Lena Telgmann, Marvin Birka, Christoph Wehe, Michael Sperling University of Mnster, Mnster, DE KN14 Feasibility of Direct-EI LC-MS as a Tool for Food Safety Applications: Identification and Quantitation of Environmental Contaminants in Milk and Nutritional Drink 1 1 1 1 Achille Cappiello , Pierangela Palma , Giorgio Famiglini , Veronica Termopoli , Fabiana 1 2 Capriotti , Nick Cellar 1 2 University of Urbino, Urbino, IT; Abbott Nutrition, Columbus, OH, US
12:00 12:30
Tutorial
11:50 12:30 TU3 Ultra High Performance Liquid Chromatography (UHPLC) Monika Dittmann, Agilent Technologies, Waldbronn, DE Introduced by Sandra Pous Torres
G104-105
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KN3 A New Procedure for Predictions of Overloaded Profiles in Gradient Elution 1 1 2 1 1 Torgny Fornstedt , Dennis sberg , Marek Lesko , Martin Enmark , Patrik Forssn , Jrgen 1 2 Samuelsson , Krzysztof Kaczmarski 1 2 Karlstad University, Karlstad, SE; Rzeszow University of Technology, Rzeszw, PL KN4 Time Scales in Liquid Chromatography from Picoseconds to Kiloseconds Attila Felinger University of Pcs, Pcs, HU OR7 Highly Efficient Capillary Columns Packed with Sub-2 Micron Superficially Porous Particles James Treadway, James Jorgenson University of North Carolina - Chapel Hill, Chapel Hill, NC, US OR8 One Step Further on the Way Toward the Ultimate Stationary Phase: Analysis of Efficiency of Bi-Layer Core-Shell Particles Krisztin Horvth, Pter Hajs University of Pannonia, Veszprm, HU OR9 Perfluorinated Adsorbents for UHPLC and Environmental Applications: Geometrical Properties, Wetting Behavior and New Insights into Retention Mechanisms 1 1 2 1 2 Alberto Cavazzini , Nicola Marchetti , Alessia Ciogli , Francesco Dondi , Francesco Gasparrini , 2 3 Aldo Lagan , Donatella Capitani 1 2 3 University of Ferrara, Ferrara, IT; University of Rome, Rome, IT; Istituto Metodologie Chimiche CNR Area Ricerca, Monterotondo, Rome, IT
14:30 15:00
15:00 15:20
15:20 15:40
15:40 16:00
Emerald
KN9 Analytical Challenges Related to the Elucidation of the Chemical Compounds Taken Part in Atmospheric Aerosol Formation 1 1 1 1 1 Marja-Liisa Riekkola , Jose Ruiz-Jimenez , Jevgeni Parshintsev , Totti Laitinen , Kari Hartonen , 2 2 Tuukka Petj , Markku Kulmala 1 2 University of Helsinki, Department of Chemistry, Helsinki, FI; University of Helsinki, Department of Physics, Helsinki, FI KN10 High Resolution Mass Spectrometry (LC/Q-TOF-MS) for the Identification of Emerging Contaminants in Water Imma Ferrer, Michael Thurman University of Colorado, Boulder, CO, US OR15 Miniaturization of Selective Extraction Sorbents for their On-Line Coupling with Capillary Chromatography or their Introduction on Chip Valerie Pichon, Fabien Brothier, Wassim Hadj Ali LSABM, ESPCI -UMPC -CNRS, Paris, FR OR16 Development of a Comprehensive Two-Dimensional Nano-/Capillary-LC system with Mass-Spectrometric Detection for the Screening Analysis of Complex Samples Thorsten Teutenberg, Jakob Haun, Juri Leonhardt, Christoph Portner Institut fr Energie- und Umwelttechnik e. V., Duisburg, Duisburg, DE OR17 Evaluation of Quantitation in Two Dimensional Liquid Chromatography Catherine Rimmer, Mallory Morris, Melissa Phillips, Benjamin Place, Lane Sander National Institute of Standards and Technology, Gaithersburg, MD, US 28
14:30 15:00
15:00 15:20
15:20 15:40
15:40 16:00
14:20 14:40
OR24 Parallel Artificial Liquid Membrane Extraction Micro-Scale Liquid-LiquidLiquid Extraction in the 96-Well Format Astrid Gjelstad, Knut Einar Rasmussen, Marthe Petrine Parmer, Stig Pedersen-Bjergaard School of Pharmacy, University of Oslo, Oslo, NO OR25 A Microchip Emitter for Solid Phase Extraction Gradient Elution Mass Spectrometry Natalia Gasilova, Liang Qiao, Dmitry Momotenko, Mohammad Reza Pourhaghighi, Hubert Girault EPFL, LEPA, Lausanne, CH KN15 Capillary Electrophoresis Mass Spectrometry, the Nerdy Brother of a Giant, Can Be the Answer for Your Next Analytical Challenge David Chen University of British Columbia, Vancouver, CA KN16 Capillary Electrophoresis-Mass Spectrometry: Towards Comprehensive Characterization of Intact Biomacromolecules 1 2 2 2 Govert Somsen , Rob Haselberg , Elena Dominguez Vega , Gerhardus de Jong 1 2 VU University, Amsterdam, NL; Utrecht University, Utrecht, NL
14:40 15:00
15:00 15:30
15:30 16:00
Tutorials
14:00 14:40 TU4 Monolithic Silica Columns Nobuo Tanaka GL Science, Tokyo, JP Introduced by Axel Vaast TU5 Polymer Monoliths Emily Hilder University of Tasmania, Hobart, AU Introduced by Eva Tyteca
G104-105
15:00 15:40
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KN5 Properties of the Water-Rich Layer at the Stationary Phase in HILIC A Molecular Dynamics Study 1 1 1 2 Ulrich Tallarek , Alexandra Hltzel , Sergey Melnikov , Andreas Seidel-Morgenstern 1 2 Department of Chemistry, Philipps-Universitt Marburg, Marburg, DE; Max-Planck-Institut fr Dynamik komplexer technischer Systeme, Magdeburg, DE KN6 Nanoparticles as Probes for Chromatography 1 1 1 1 2 2 Edward Yeung , Gufeng Wang , Rui Han , Lehui Xiao , Dong Xu , Yan He 1 2 Iowa State University, Ames, Iowa, US; Hunan University, Changsha, Hunan, CN
17:30 18:00
Emerald
OR18 Separation and Identification of New POPs by Liquid Chromatography and Mass Spectrometry Guibin Jiang, Ting Ruan Chinese Academy of Sciences, Beijing, CN OR19 Novel Single and Multi-Dimensional Chromatographic Approaches to a Better Understanding of Dissolved Organic Matter (DOM) 1 2 1 3 3 Sara Sandron , Brian Kelleher , Ekaterina Nesterenko , Pavel Nesterenko , Brett Paull 1 2 3 DCU-ISSC, Dublin, Ireland; DCU-School of Chemistry, Dublin, Ireland; ACROSS, Hobart, AU DI2 Discussion on needs for environmental analysis
17:20 17:40
17:40 18:00
G102-103
OR26 Characterization of Allergens by Various Capillary Electrophoresis Modes 1 1 1 2 2 Hanno Stutz , Sergey Gusenkov , Lorenz Stock , Chlo Ackaert , Gertie Janneke Oostingh 1 2 Division of Chemistry and Bioanalytics/University of Salzburg, Salzburg (Austria), AT; Division of Allergy and Immunology/University of Salzburg, Salzburg (Austria), AT OR27 Development of Microfluidic Device Combined with Mass Spectrometer for Study of Cell Drug Metabolism Jin-Ming Lin, Qiushui Chen, Dan Gao, Huibin Wei Tsinghua University, Beijing, CN OR28 Chip Chromatography in Microfluidic Glass Chips with Optical and Mass Spectrometric Detection Detlev Belder, Claudia Ernst, Sebastian Thrmann Universitt Leipzig, Leipzig, DE
17:20 17:40
17:40 18:00
Tutorial
17:00 17:40 TU6 Nanofluidics and its Applications to Separations and Sensing Stephen Jacobson Indiana University, Bloomington, IN, US Introduced by Robert-Jan Raterink
G104-105
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8:40 11:00
8:40 9:00 Uwe D. Neue Award
Auditorium
KN17 Optimized Superficially Porous Particles for Protein Analysis Joseph Kirkland, Stephanie Schuster, Brian Wagner, Barry Boyes, Joseph DeStefano Advanced Materials Technology, Inc., Wilmington, DE, US KN18 Understanding the Fine Details of the Band Broadening Processes in Liquid Chromatography Gert Desmet, Sander Deridder Vrije Universiteit Brussel, Brussels, BE OR29 Active Flow Technology Presenting the Infinite Diameter Column in a Curtain Flow Mode of Operation 1 2 Ross Shalliker , Harald Ritchie 1 2 University of Western Sydney, North Parramatta, Australia; ThermoFisher, Runcorn, GB OR30 The New Cutting Edge in Reversed-Phase UHPLC Performance: 1.3 m CoreShell Particles Tivadar Farkas, Mike Chitty, Jeff Layne, Jason Anspach, Carl Sanchez Phenomenex, Inc., Torrance, CA, US OR31 A New Particle for Liquid Chromatography 1 1 1 2 Peter Myers , Haifei Zhang , Adham Ahmed , Antony Edge 1 2 Department of Chemistry, Liverpool, GB; ThermoFisher, Runcorn, GB
9:30 10:00
10:00 10:20
10:20 10:40
10:40 11:00
High-Impact LC Proteomics
9:00 9:30
Chair: William Hancock and Alexander Leitner KN25 Pre-Fractionation and MS; Condemned to Each Other in Proteomics? Albert J.R. Heck Biomolecular Mass Spectrometry, Utrecht University, Utrecht, NL
Emerald
9:30 10:00
KN26 High-Efficiency and High Peak Capacity Chromatographic Separation Methods for Proteome Analysis 1 1 2 1 2 Christian G. Huber , Silke Ruzek , Katja Melchior , Lisa Weilnbck , Nathanale Delmotte , 2 2 Hansjrg Toll , Sascha Quinten 1 2 Department of Molecular Biology, University of Salzburg, Salzburg, AT; Department of Chemistry, Instrumental Analysis and Bioanalysis, Saarland University, Saarbrcken, DE OR35 In-House Construction of a UHPLC System Enabling the Identification of over 4,000 Protein Groups in a Single Analysis Alba Cristobal, Marco Hennrich, Piero Giansanti, Soenita S. Goerdayal, Albert J.R. Heck, Shabaz Mohammed Utrecht University, Utrecht, NL OR36 Simultaneous Peptide Mapping, Posttranslational Modifications and Major NGlycosylation Characterization of Trastuzumab by Sheathless Capillary Electrophoresis - Tandem Mass Spectrometry 1 1 2 3 3 Rabah Gahoual , Alicia Burr , Jean-Marc Busnel , Lauriane Kuhn , Phillipe Hammann , Alain 4 1 1 Beck , Yannis-Nicolas Francois , Emmanuelle Leize-Wagner 1 2 LSMIS, UMR 7140, University of Strasbourg, Strasbourg, FR; Beckman Coulter Inc., Brea, US; 3 4 Proteomics Facility, IBMC, University of Strasbourg, Strasbourg, FR; Centre d'Immunologie Pierre Fabre, St Julien-en-Genevois, FR OR37 Discovery and Validation of Serum Biomarkers for Cervical Cancer by LCMS/MS 1 1 2 1 Alexander Boichenko , Natalia Govorukhina , Ate van der Zee , Rainer Bischoff 1 2 University of Groningen, Groningen, NL; University Medical Centre Groningen, Groningen, NL 32
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OR46 The Contribution of High-End Analytical Technology to an Integrated Workflow for Valorisation of Bio-Waste Streams Sebastiaan Bijttebier, Els D'Hondt, Stefan Voorspoels VITO NV, Mol, BE OR47 Efficiently Combining HPLC, NMR and MS Ulrich Braumann Bruker BioSpin, Rheinstetten, DE KN29 Novel Analytical Methods of HPLC-MS Based Metabolomics Xu Guowang, Weidong Dai, Qiang Huang, Shili Chen, Guozhu Ye, Lina Zhou, Peiyuan Yin, Xin Lu Dalian Institute of Chemical Physics, Chinese Academy of Sci, Dalian, CN KN30 New Approaches in Nontargeted Lipidomic Quantitation of Biological Samples by LC/MS Michal Holapek, Eva Cfkov, Miroslav Lsa, Blanka erven University of Pardubice, Pardubice, CZ
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Tutorials
9:30 10:10
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TU7 MALDI, other Matrix Assisted Ionization Methods, and Nonconventional Approaches to LC/MS Sarah Trimpin Wayne State University, Detroit, MI, US Introduced by: Karli Reiding TU8 Quantitative LC-MS Uwe Karst University of Mnster, Mnster, DE Introduced by: Andjoe Sampat
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KN19 Designing Polymer Monoliths for the Efficient Chromatography of Small and Large Molecules Emily Hilder, Dario Arrua, Mohammad Talebi, Paul Haddad, Chris Desire University of Tasmania, Hobart, Tasmania, AU KN20 On the Morphology, Porous Properties, Polymer Nano-Scale Gel Structure and Related Chromatographic Performance of Porous Polymer Monoliths Ivo Nischang Johannes Kepler University Linz, Leonding, AT
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High-Impact LC Proteomics
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Emerald
OR38 Immunohistochemical Staining, Laser Capture Microdissection and FASP Assisted Proteomic Analysis of Cancer Stem Cells within Tissue Samples David Lubman, Jintang He, Jianhui Zhu, Xing Fan University of Michigan, Ann Arbor, MI, US OR39 Solid-Phase Based Technologies and Methods for Glycoproteome and Phosphoproteome Analysis Zou Hanfa, Fangjun Wang, Mingliang Ye, Jun Zhu, Zhen Sun, Hongqiang Qin, Junfeng Huang Dalian Institute of Chemical Physics, Dalian, CN DI3 Discussion on needs for proteomics
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OR48 Improvement of 2D (NP/RP) LC-QToF MS Method and its Application in Lipid Profiling of Human Plasma from Peritoneal Dialysis Patients Huwei Liu, Min Li, Yu Bai, Yiping Liao Peking University, Beijing, CN OR49 Enantiomeric Characterization of Triacylglycerols and Other Nonpolar Lipids Using Chiral HPLC/MS Miroslav Lisa, Michal Holapek University of Pardubice, Pardubice, CZ OR50 HPLC and MS as Tools for Determination of Stabilizers in Synthetic Polymers: A Way to Improve Quality and to Understand the Performance of Plastic Materials Wolfgang Buchberger, Susanne Beissmann, Ingrid Hintersteiner, Michael Reisinger, Lucas Sternbauer, Martin Stiftinger Institute of Analytical Chemistry, University Linz, Linz, AT
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Tutorial
11:50 12:30 TU9 Comprehensive Two-Dimensional Liquid Chromatography Paola Dugo University of Messina, Messina, IT Introduced by: Anna Baglai
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KN21 Theoretical and Practical Performance Limits of High Efficiency Small-Bore UHPLC Columns in Isocratic and Gradient Separations 1 1 2 2 2 Monika Dittmann , Bernd Hoffmann , William Barber , Xiaoli Wang , Ta-Chen Wei 1 2 Agilent Technologies, Waldbronn, DE; Agilent Technologies, Wilmington, US KN22 Nanopore Devices for Virus Particle Characterization Stephen Jacobson, Zachary Harms, Laurence Kohler, Lisa Selzer, Lye Siang Lee, Adam Zlotnick Indiana University, Bloomington, IN, US OR32 High-Pressure Miniaturized Electro-Osmotic Pump for Capillary HPLC 1 Shaorong Liu, Congying Gu, Zaifang Zhu, Wei Wang, Aaron Morgan, Joann Lu University of Oklahoma, Norman, US OR33 Half-Width Plots: A Simple Tool to Reveal Column Kinetics and Characterize Chromatographic Columns Mara Celia Garca-lvarez-Coque, Juan Jos Baeza-Baeza, Mara Jos Ruiz-ngel, Jos Ramn Torres-Lapasi, Samuel Carda-Broch University of Valencia, Burjassot (Valencia), ES OR34 Characterizing Extra-Column Effects in Ultra-High Pressure Liquid Chromatography 1 2 2 1 James Grinias , Martin Gilar , Jeremy Rose , James Jorgenson 1 2 UNC Chapel Hill, Chapel Hill, NC, US; Waters Corp., Milford, MA, US
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Emerald
KN27 Challenging the Present State of the Art of Polymer Separations 1 2 Mark Schure , Wei Gao 1 2 Superon GmbH and Kroungold Analytical, Inc., Blue Bell, PA 19422, US; The Dow Chemical Company, Springhouse, PA 19477, US KN28 SEC-Gradients: A New Approach to the Separation of Polymers by Chemical Composition Wolfgang Radke Fraunhofer Institute for Structural Durability and System Reliability, Darmstadt, DE OR40 Efficiency in (Ultra-High-Pressure) Size-Exclusion Chromatography 1 2 3 Elena Uliyanchenko , Sjoerd van der Wal , Peter Schoenmakers 1 2 3 SABIC, Bergen op Zoom, NL; DSM Resolve, Geleen, NL; University of Amsterdam, Amsterdam, NL OR41 Advances in Size Characterization of Synthetic Polymers Edouard Bouvier, Bonnie Alden, Mia Summers, Jeremy Shia, Jessica Wilson, Michael Savaria, Kevin Wyndham, Thomas Walter Waters Corporation, Milford, US OR42 Enabling Polymer Characterization via Unique Separation Selectivities and Mechanisms 1 2 2 3 3 1 Rob Edam , Rongjuan Cong , Willem deGroot , Dean Lee , John Lyons , Edwin Mes , David 3 3 3 4 2 2 Meunier , Randy Pell , Ted Stokich Jr. , Peter Schoenmakers , Bill Winniford , Matthew Miller 1 2 3 Dow Benelux B.V., Terneuzen ZE, NL; Dow Chemical, Freeport, US; Dow Chemical, Midland, 4 US; University of Amsterdam, Amsterdam, NL
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OR51 Recent Progress in Core-shell and Embedded Nanoparticle Layers for the Separation and Sensing of Biomarkers and Cell Signalling Molecules 1,2 2 3 1,2 Lin Zhou , Gerard P. McGlacken , John H.T. Luong , Jeremy D. Glennon * 1 2 Innovative Chromatography Group, Irish Separation Science Cluster (ISSC), Department of Chemistry and the Analytical &Biological Chemistry Research Facility (ABCRF), University College 3 Cork, IE; Biotechnology Research Institute, National Research Council Canada, Montreal, Quebec, CA OR52 Vitamin-D Metabolite Metrology Lane Sander, Karen Phinney, Mary Bedner, Johanna Camara, Katrice Lippa, Susan Tai, Stephen Wise National Institute of Standards and Technology, Gaithersburg, MD, US OR53 Combined SPE-LC-MS/MS Analysis of Small Molecules Directly in Blood and Blood Plasma Karl-Siegfried Boos, Qianqian Yu, Sena Caglar, Rosa Morello Laboratory of BioSeparation, Medical Center LMU, Munich, DE KN31 The Role of Mass Spectrometry in Post-Column On-Line/At-Line Bioactivity Screening Wilfried Niessen VU University Amsterdam, Amsterdam, NL KN32 Strategy for Chromatographic Analysis of Glycans in Medicinal Plants Shaoping Li University of Macau, MO
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Tutorials
14:00 14:40 TU10 Chiral Separations Michael Lmmerhofer University of Tbingen, Tbingen, DE Introduced by: Debby Mangelings TU11 Column Efficiency Fabrice Gritti The University of Tennessee, Knoxville, TN, US Introduced by: Michelle Camenzuli
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KN23 On the Use of Bayesian Statistics for the Analysis of Chromatographic Data: A New Generation of Data-Treatment Methods? Gabriel Vivo-Truyols University of Amsterdam, Amsterdam, NL KN24 Herbal Fingerprints: Extraction of Information, Focussing on Similarity Analyses Yvan Vander Heyden, Goedele Alaerts, Melanie Dumarey, Mohammad Goodarzi, Christophe Tistaert, Bieke Dejaegher: Vrije Universiteit Brussel (VUB), Brussels, BE
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Emerald
OR43 Separation and Characterization of Targeting Biomedical Polymers by HPLC 1 1 1 1 2 Xulin Jiang , Yanfeng Chu , Jia Liu , Renxi Zhuo , Peter J. Schoenmakers 1 2 Wuhan University, Wuhan, CN; University of Amsterdam, Amsterdam, NL OR44 Understanding Retention of Block Co-Polymers in SEC and LCCC 1 1 1 2 J. Ilja Siepmann , Kim Struk , Tim Lodge , Mark Schure 1 2 University of Minnesota, Minneapolis, US; Kroungold Analytical Inc, Blue Bell, US DI4 Discussion on needs for polymer analysis
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OR54 LCxLC Hyphenated to Q-TOF MS for the Characterization of Protein Biopharmaceuticals 1 2 2 1 1 Gerd Vanhoenacker , Koen Sandra , Isabel Vandenheede , Frank David , Pat Sandra 1 2 Research Institute for Chromatography, Kortrijk, BE; Metablys, Kortrijk, BE OR55 Synthesis of a Neo-Glyco-Vaccine against Tuberculosis: The Key Role of Liquid Chromatography-Mass Spectrometry Caterina Temporini, Teodora Bavaro, Immacolata Serra, Sara Tengattini, Enrica Calleri, Marco Terreni, Gabriella Massolini Dept. Drug Sciences University of Pavia, Pavia, IT OR56 Rapid qualitative and Quantitative Characterization of Antibody Glycosylation Profiles by Native Mass Spectrometry Using an Orbitrap Mass Analyzer 1 2 2 2 1 Sara Rosati , Ewald T.J. van den Bremer , Paul Parren , Janine Schuurman , Albert J. R. Heck 1 2 Utrecht University, Utrecht, NL; Genmab, Utrecht, NL
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Tutorial
17:00 17:40 TU12 Towards Quantitative Morphology-transport Relationships for Chromatographic Stationary Phases Ulrich Tallarek Philipps-Universitt Marburg, Marburg, DE Introduced by: Henrik Cornelisson van de Ven
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Moving faster
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HPLC 2013
Visit us at booth U7 and enter for a free iPad!
High-Performance Lindner Chromatography (sessions sponsored by Millipore) Presented by Michael Lmmerhofer and Barry Karger KN33 The Integration of Liquid Chromatography and Mass Spectrometry for Ultratrace Analysis Barry Karger Barnett Institute/Northeastern University, Boston, US KN34 Studying Protein Complexes and Biological Networks by Chemical CrossLinking and Mass Spectrometry Alexander Leitner, Thomas Walzthoeni, Franz Herzog, Abdullah Kahraman, Ruedi Aebersold ETH Zurich, Institute of Molecular Systems Biology, Zurich, CH OR57 Ion-Exchange, Hydrophilic and Hydrophobic Interactions Affecting Selectivity for Neutral and Charged Solutes on Agglomerated Ion-Exchange and Commercial Mixed-Mode Stationary Phases 1 1 1 1 2 Brett Paull , Artaches Kazarian , Paul Haddad , Pavel Nesterenko , Mark Taylor 1 2 Australian Centre for Research on Separation Science, Hobart, Australia; Pfizer Global Research and Development, Sandwich, GB OR58 Polymer-Coated Or Not? A Simple Test Method to Categorize Hydrophilic Interaction Chromatography (HILIC) Phases Based on their Structural Selectivity 1 2 Tohru Ikegami , Nobuo Tanaka 1 2 Kyoto Institute of Technology, Kyoto, JP; GL Science, Iruma, JP OR59 The Impact of Imidazolium Substituents on the Retention Properties of Surface-Confined Ionic Liquid Stationary Phases for HPLC Revisited Apryll M. Stalcup: Irish Separation Science Cluster/Dublin City University, Dublin 9, IE
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High-Impact LC Food
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Emerald
KN41 Food Analysis: A Challenging Area for Liquid Chromatography and Mass Spectrometry Hans-Gerd Janssen Unilever Research Vlaardingen, Vlaardingen, NL KN42 Advanced Liquid Chromatography and Mass Spectrometry Techniques for Lipid Analysis 1 2 1 1 Paola Dugo , Paola Donato , Francesco Cacciola , Luigi Mondello 1 2 University of Messina, Messina, IT; University Campus Biomedico, Rome, IT OR63 Orbitrab vs QTOF to Determine Pesticide Residues in Fruit and Vegetable Extracts 1 2 2 Yolanda Pic , Marinella Farr , Dami Barcel 1 2 Faculty of Pharmacy, University of Valencia, Burjassot, ES; IDAEA/CSIC, Barcelona, ES OR64 The Serial RP-HPLC/HILIC/API-MS Coupling: An Easy, Robust and Versatile Technique Giorgia Greco, Thomas Letzel Technische Universitt Mnchen, Garching, DE OR65 Discovery of Multiple Sites of Intra-Molecular Protonation and Different Fragmentation Patterns within the Fluoroquinolone Class of Antibiotics in Porcine Muscle Extracts Using Ion Mobility Mass Spectrometry 1 1 1 2 2 Sara Stead , Mike McCullagh , Antonietta Gledhill , Wouter deKeizer , Aldert Bergwerff 1 2 Waters corp, Manchester, GB; RnAssays, Utrecht, NL 40
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OR73 Glycosylation Analysis of Enriched Immunoglobulin A 1 2 1 1 1 Dennis Blank , Albert Bondt , Simone Nicolardi , Yuri E.M. Burgt , Andr M. Deelder , Manfred 1 Wuhrer 1 2 Leiden University Medical Center - LUMC, Leiden, NL; Erasmus University Medical Center, Rotterdam, NL OR74 Use of Liquid Chromatography- High Resolution Mass spectrometry (LC-HRMS) in Bioanalytical Assays in Combination with Micro-sampling of Biological Fluids Monica P. Cala Molina, Juan P. Rincon Pabon, Roland J.W. Meesters Universidad de los Andes, Bogota D.C., CO OR75 At the Edge of One-Dimensional HT-UHPLC-MS in an Industrial Environment Ron Peters, Ynze Mengerink, Sjoerd van der Wal DSM Resolve, Geleen, NL KN45 The Role of Molecular Flash Photography in Desorption, Detection and Disease Ron M.A. Heeren FOM-AMOLF, Amsterdam, NL KN46 Orbitrap Mass Spectrometry: Past, Present and Future Alexander Makarov ThermoFisher Scientific (Bremen), Bremen, DE
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Tutorials
9:30 10:10 TU13 System Performance Gert Desmet Free University Brussels, Brussels, BE Introduced by: Rudy Vonk TU14 Role of the Stationary Phase in HPLC Attila Felinger University of Pcs, Pcs, HU Introduced by: Daniela Peroni
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KN35 Influence of Phase Type and Solute Structure on Changes in Retention with Pressure in Reversed-Phase High Performance Liquid Chromatography 1 2 3 1 David McCalley , Stephan Buckenmaier , Nobuo Tanaka , Morgane Fallas 1 2 University of the West of England, Bristol, Bristol, GB; Agilent Technologies, Waldbronn, DE; 3 GL Sciences, Kyoto, JP KN36 Effect of Pressure on Retention and Selectivity of Polymeric ODS and C30 Stationary Phase in Reversed-Phase HPLC. Increased Separation of Isomeric Fatty Acids, Fatty Acid Methyl Esters, Triacylglycerols, and Tocopherols at High Pressure 1 2 2 2 3 Nobuo Tanaka , Kensuke Okusa , Ikuma Kuroda , Masayoshi Ohira , Toshiharu Nagai , Hoyo 3 4 5 6 Mizobe , Naohiro Gotoh , Tohru Ikegami , David V. McCalley 1 2 3 GL Sciences, Inc., Kyoto, JP; GL Sciences, Inc., Iruma, JP; Tsukishima Foods Industry, Toyko, JP; 4 5 Tokyo University of Marine Science and Technology, Tokyo, JP; Kyoto Institute of Technology, 6 Kyoto, JP; University of the West of England, Bristol, GB
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High-Impact LC Food
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Emerald
OR66 Recent Developments in the Liquid Chromatographic Analysis of Anthocyanins Andr de Villiers, Chandr Willemse, Philippus Alberts, Maria Stander Stellenbosch University, Stellenbosch, SA OR67 The Analysis of Natural Products Using Active Flow Technology with Multiplexed Detection 1 2 1 Michelle Camenzuli , Harald Ritchie , R. Andrew Shalliker 1 University of Western Sydney, Parramatta, NSW, Australia; 2Thermo Fisher Scientific, Runcorn, WA7 1TA, GB DI5 Discussion on needs for food analysis
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KN47 Signal Processing - The Missing Link in Analysis of LC, LC-MS and LCLC Data 1 1 1 1 2 Jan Christensen , Nikoline Nielsen , Rune Grsbl , Sren Furbo , Giorgio Tomasi 1 Plant and Environmental Sciences, University of Copenhagen, Frederiksberg C, Denmark; 2 European Commission Joint Research Centre, Institute for Health and Consumer Protection, ISPRA, IT KN48 Recent Developments and Applications of Metalign-Based Data Processing in Chromatography Combined with Full Scan Mass Spectrometry Arjen Lommen, Paul Zomer, Michel Nielen, Hans Mol RIKILT - Institute of Food Safety, Wageningen UR, Wageningen, NL
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Tutorial
11:50 12:30 TU15 Supercritical Fluid Chromatography Isabelle Francois Waters, Brussels, BE Introduced by: Hanneke Brust
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OR60 HPLC Performance of Zwitterionic Chiral Stationary Phases in Direct Enantiomer Separation of Amino Acids and Other Ionisable Compounds 1 1 1 2 Pilar Franco , Tong Zhang , Emilie Holder , Wolfgang Lindner 1 2 Chiral Technologies Europe, Illkirch, FR; University of Vienna, Department of Analytical Chemistry, Vienna, AT OR61 Chiral Amino Acid Metabolome Analysis for Biomarker Assay in Clinical Diagnosis Using Enantioselective 2D-HPLC 1 1 1 2 3 3 Kenji Hamase , Yurika Miyoshi , Nao Kusano , Jumpei Sasabe , Yosuke Tojo , Masashi Mita , 2 4 Sadakazu Aiso , Wolfgang Lindner 1 2 3 Kyushu University, Fukuoka, JP; Keio University, Tokyo, JP; Shiseido Co., Ltd., Tokyo, JP; 4 University of Vienna, Vienna, AT OR62 Optimizing Selectivity for HPLC Separations of Charged and Neutral Polar Compounds Egidijus Machtejevas: Merck Millipore / MM-L Lab Essentials, Darmstadt, DE KN37 Purification of Baculovirus and Influenza VLP by Monoliths Alois Jungbauer, Petra Gerster, Reingard Grabherr: BOKU, Vienna, AT KN38 Nanoparticle-Based Selective Sample Preparation for HPLC-MS/MS Analysis of Oxidized Phospholipids as Biomarkers for Oxidative Stress 1 2 3 3 Michael Lmmerhofer , Helmut Hinterwirth , Elisabeth Haller , Wolfgang Lindner 1 2 Institute of Pharmaceutical Sciences, Univ. of Tuebingen, Tuebingen, DE; Institute ofAnal. 3 Chem., Univ. of Vienna, Vienna, AT; Institute of Anal. Chem., Univ. of Vienna, Vienna, AT
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High-Impact LC Metabolomics
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Chair: DavidMcCalley and Sebastiaan Eeltink KN43 Metabolomics Hannelore Daniel: Technische Universitt Mnchen, Freising-Weihenstephan, DE
Emerald
KN44 Analytical Solutions to Address the Challenges of Mass-Spectrometry Based Metabolomics Thomas Hankemeier: Netherlands Metabolomics Centre/Leiden University, Leiden, NL OR68 State-Of-The-Art LC-MS Based Lipidomics Applied in The Study of Lung Diseases 1 1 2 1 2 Koen Sandra , Ruben t'Kindt , Eef Telenga , Lucie Jorge , Antoon van Oosterhout , Nick ten 2 1 1 2 Hacken , Pat Sandra : RIC/Metablys, Kortrijk, BE; UMCG, Groningen, NL OR69 Evaluation of Different Column Chemistries for Fast Urinary Metabolic Profiling 1 1 2 1 2 Martin Giera , Dick-Paul Kloos , Henk Lingeman , Andr Deelder , Wilfried Niessen , Oleg 1 Mayboroda 1 2 Leiden University Medical Center (LUMC), Leiden, NL; VU University, Amsterdam, NL OR70 Molecular Cartography in Acute Chlamydia Pneumoniae Infections A NonTargeted Metabolomics Approach 1 2 3 4 5 Constanze Mller , Inga Dietz , Dimitrios Tziotis , Franco Moritz , Jan Rupp , Philippe Schmitt4 Kopplin 1 2 Research unit Analytical BioGeoChemistry, Helmholtz Zentrum, Neuherberg, DE; University of 3 Lbeck, Lbeck, DE; Institute for Medical Research unit Analytical BioGeoChemistry, Helmholtz 4 Zentrum Mnchen, Neuherberg, DE; Research unit Analytical BioGeoChemistry, Helmholtz 5 Zentrum Mnchen, Neuherberg, DE; Institute for Medical Microbiology and Hygiene, University of Lbeck, Lbeck, DE 44
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OR76 How to Assess Uncertainties in the Mass Spectrometric Confirmation 1 1 2 Bjorn Berendsen , Linda Stolker , Michel Nielen 1 2 RIKILT, Wageningen UR, Wageningen, NL; Wageningen University, Wageningen, NL OR77 Parallel LC-MALDI and MALDI Imaging Workflow for Direct Identification of Biomarkers from Tissue 1 1 1 1 2 Michael Becker , Martin Schuerenberg , Rainer Paape , Detlev Suckau , Axel Walch , Sandra 2 Rauser 1 2 Bruker Daltonik GmbH, Bremen, DE; Helmholtz Zentrum Mnchen, Institut fr Pathologie, Munich, DE OR78 Full plasma N-Glycoproteomics Using GlycoFrag and HILIC Micro-SPE Enrichment Bas Jansen, Leonardo Lenoci, Maurice Selman, Dennis Blank, Gerhild Zauner, Magnus Palmblad, Andr Deelder, Manfred Wuhrer Leiden University Medical Center, Leiden, NL KN49 New Approaches to High-Throughput Protein and Protein-Protein Interaction Analysis Using Capillary and Microchip Electrophoresis Robert Kennedy University of Michigan, Ann Arbor, MI, US KN50 Bigger is Better: Challenges in Pharmaceutical Microtechnology John Frenz GlobeImmune, Inc., Louisville, CO, US
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Tutorials
14:00 14:40 TU16 Environmental Analysis Marja-Liisa Riekkola University of Helsinki, Helsinki, FI Introduced by: Alexander Boichenko TU17 Lipidomic Analysis Michal Holapek University of Pardubice, Pardubice, CZ Introduced by: Jana Krlov
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KN39 The impact of Quality by Design on Chromatography Method Development Fritz Erni Dornach, CH KN40 Selectivity Tuning of Chiral Ion Exchanger Type Stationary Phases via Chemical Structure and Mobile Phase Variations in HPLC and SFC Mode 1 1 2 Wolfgang Lindner , Denise Wolrab , Michal Kohout 1 2 University of Vienna, Vienna, AT; Dept. of Organic Chemistry, Prague, CZ
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Emerald
OR71 State-Of-The-Art Hyphenated Techniques HPLC/DAD-MS/SPE/NMR Interface for New Approches by High Throughput Sensitivity Medicinal Chemistry, Pharmacognosy, Metabolomic and Translational Projects Cyril Antheaume, Nicole Rimlinger, Veronika Cakova Universit de Strasbourg, Illkirch, FR OR72 3-Phase Electroextraction: A New (Online) Sample Purification and Enrichment Method for Bioanalysis Robert-Jan Raterink, Peter Lindenburg, Rob Vreeken, Thomas Hankemeier Leiden University, LACDR, NMC, Leiden, NL DI6 Discussion on needs for metabolomics
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OR79 Sample Displacement Chromatography for Protein Purification Hartmut Schlter, Marta Kotasinska, Verena Richter, Robert Ahrends, Diana Hildebrand, Maria Trusch University Medical Center Hamburg-Eppendorf, Hamburg, DE OR80 Coupling of Protein Prefractionation with LC-MS/MS Using Electrospun Nanofibers Wenwan Zhong, Hui Wang, Samantha Schachermeyer University of California, Riverside, Riverside, US OR81 Electrochemically Initiated Reactions Upfront MS - EC/MS an Unknown Panacea? Jean-Pierre Chervet, Agnieszka Kraj, Hendrik-Jan Brouwer, Martin Eysberg Antec, Zoeterwoude, NL
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Tutorial
17:00 17:40 TU18 Residue Analysis Yolanda Pic University of Valencia, Valencia, ES Introduced by: Petra Dinisova
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KN51 Comparison of Selective and Fully Comprehensive Two-Dimensional HPLC 1 1 2 Dwight Stoll , David Harmes , Joe Davis 1 2 Gustavus Adolphus College, St. Peter, MN, US; Southern Illinois University, Carbondale, Carbondale, IL, US KN52 The Quest for Ultra-High Peak Capacities - Spatial Three-Dimensional Chromatography Bert Wouters, Jelle De Vos, Axel Vaast, Sebastiaan Eeltink Vrije Universiteit Brussel, Brussels, BE OR82 Comprehensive Two-dimensional LCxLC Using Combinations of Monolithic Capillary Columns and Short Core-Shell Columns Pavel Jandera, Magda Stankova, Tomas Hajek, Petr Cesla, Katerina Vynuchalova University of Pardubice, Pardubice, CZ OR83 Ultrafast 2D-RPLC: Superficially-porous 2.7 m Particles versus 1.8 m Fully Porous Particles for Use in Second Dimension Imad Haidar Ahmad, Peter Carr University of Minnesota, Minneapolis/Minnesota, US OR84 Rigorous Optimization of LCLC With Gradient Elution in Both Dimensions 1 2 1 Sandra Pous Torres , Gabriel Viv Truyols , Jos Ramn Torres Lapasi , Mara Celia Garca 1 2 lvarez-Coque , Peter Schoenmakers 1 2 Analytical Chemistry Department. University of Valencia, Burjassot, ES; Analytical Chemistry Group, Van 't Hoff Institute for Molecular Sciences, University of Amsterdam, Amsterdam, NL
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High-Impact LC Forensics
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Chair: Emily Hilder and Bjorn Berendsen KN55 Forensic Challenges for LC and LC-MS Arian van Asten, John Gonsalvez, Bas Teunissen, Xiaoma Xu Netherlands Forensic Institute, The Hague, NL
Emerald
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KN56 Modern Forensic Applications of LC and LC-MS Emmie Ho, W.H. Kwok, David Leung, Gary Leung, April Wong, Colton Wong, Jenny Wong, Nola Yu, Terence Wan The Hong Kong Jockey Club, Sha Tin, N.T., HK OR88 Determination of 2-Methylthiazolidine-4-carboxylic acid (MTCA) a Potential Marker for Ethanol Consumption by HPLC-ESI-MS/MS 1 2 1 3 Roland Reischl , Wolfgang Bicker , Thomas Keller , Wolfgang Lindner 1 2 Paris Lodron University Salzburg, Salzburg, AT; FTC Forensic Toxicology Lab Ltd, Vienna, AT; 3 University of Vienna, Vienna, AT OR89 Gas-Phase Separation of Drugs of Abuse and their Metabolites from Tissue Sections by Differential Ion Mobility Spectrometry Tiffany Porta, Emmanuel Varesio, Grard Hopfgartner University of Geneva, Geneva, CH OR90 Information Dependent Acquisition with LC-MS/MS as a Tool for Screening of 453 Compounds in Forensic Urine and Whole Blood Samples Ruth Verplaetse, Sylvie Decabooter, Eva Cuypers, Jan Tytgat KU Leuven, Laboratory Toxicology, Leuven, BE
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OR93 A Linear pH Gradient Separation Platform for Monoclonal Antibody (MAb) Charge Variant Analysis 1 2 1 1 1 1 Shanhua Lin , Wim Decrop , Julia Baek , Srinivasa Rao , Yury Agroskin , Chris Pohl 1 2 Thermo Fisher Scientific, Sunnyvale, US; Thermo Fisher Scientific, Amsterdam, NL OR94 Studying the MMP-9 TIMP-1 Protease-Inhibitor System by Activity-Based Enrichment and Selected Reaction Monitoring (SRM) Nano-LC-MS/MS 1 1 1 1 2 Laurette Prely , Anouk Oldenburger , Jos Hermans , Krisztina Paal , Riccardo Castelli , Nico C. 1 1 3 1 van de Merbel , Antoon J.M. van Oosterhout , Herman S. Overkleeft , Martina Schmidt , Rainer 1 Bischoff 1 2 3 University of Groningen, Groningen, NL; Leiden University, Groningen, NL; Leiden University, Leiden, NL OR95 Peptide Behaviour in RP-HPLC Coupled to MS: Practical Considerations Based on a Quantitative Structure-Retention Relationship Study Virginie Houbart, Anne-Catherine Servais, Jacques Crommen, Marianne Fillet University of Lige, Lige, BE KN59 Protein Glycosylation Analysis by LC-MS Manfred Wuhrer, Maurice H.J. Selman, Cees Bruggink, Crina I.A. Balog, Zauner, Carolien A.M. Koeleman, Paul J. Hensbergen, Andr M. Deelder Leiden Univ. Medical Center, Leiden, NL KN60 Genome-Wide Proteomics: Gastric Cancer Transcriptomics/Proteomic Signatures William Hancock Northeastern University, Boston, MA, US
9:20 9:40
9:40 10:00
10:00 10:30
10:30 11:00
Tutorials
9:30 10:10
G104-105
TU19 The Nanoliter Lab: Using Droplets in Analytical and Separation Science Robert Kennedy University of Michigan, Ann Arbor, MI, US Introduced by: Marija Mladic TU20 How to Understand and Accomplish Separations Using Hydrophilic Interaction Chromatography (HILIC) David McCalley University of Western England, Bristol, UK Introduced by: Blanka erven
10:30 11:10
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KN53 Determination of Equilibrium Isotherms in Supercritical Fluid Chromatography Georges Guiochon, Fabrice Gritti, Abhijit Tarafder, Fahimeh Kamarei University of Tennessee, Knoxville, TN, US KN54 Towards a Better Understanding of Enantioselective SFC Caroline West, Syame Khater ICOA, CNRS UMR 7311, University of Orlans, Orlans, FR
12:00 12:30
High-Impact LC Forensics
11:30 11:50
Emerald
OR91 Rapid Separations of Improvised Explosives Michael Breadmore, Cameron Johns, Adam Gaudry, Parvez Mahbub, Phil Zakaria, Joseph Hutchinson, Emily Hilder, Greg Dicinoski, Rosanne Guijt, Pavel Nesterenko, Mirek Macka, Paul Haddad University of Tasmania, Hobart, Tasmania, AU OR92 Accurate Quantitation of Explosive Residues by Liquid Chromatography-Mass Spectrometry (LC-MS) to Investigate Possible Crime-Scene Presence 1 2 2 2 Hanneke Brust , Arian van Asten , Mattijs Koeberg , Chris-Jan Kuijpers , Antoine van der 3 1 Heijden , Peter Schoenmakers 1 2 University of Amsterdam, Amsterdam, NL; Netherlands Forensic Institute, The Hague, NL; 3 TNO Technical Sciences, Rijswijk, NL DI7 Discussion on needs for forensics
11:50 12:10
12:10 12:30
HPLC-MS LCxLC-MS
Chair: Michal Holcapek 11:30 11:50
G102-103
OR96 Analysis of Chinese Herbal Medicine with LCLC-MS 1 2 1 Oliver Schmitz , Roman Dck , Duxin Li 1 2 University of Duisburg-Essen, Essen, DE; University of Wuppertal, Wuppertal, DE OR97 Two-dimensional HPLC with Hyphenated UV-MS-CAD Detection in Pharmaceutical Analysis Kelly Zhang; Genentech Inc., South San Francisco, CA, US OR98 Combining Different Analytical Methods for Glycan Characterization of Cancer Tissues 1 1 1 1 Stephanie Holst , Crina I. A. Balog , Kathrin Stavenhagen , Carolien A. M. Koeleman , Liam M. 1 1 1 2 2 McDonnell , Oleg A. Mayboroda , Aswin Verhoeven , Wilma E. Mesker , Rob A. E. M. Tollenaar , 1 1 Andr M. Deelder , Manfred Wuhrer 1 2 LUMC, Center for Proteomics and Metabolomics, Leiden, NL; LUMC, Department of Surgery, Leiden, NL
Tutorial
11:50 12:30
G104-105
TU21 LC x LC of Polymers Wolfgang Radke Fraunhofer Institute for Structural Durability and System Reliability LBF, Darmstadt, DE Introduced by: Maria Marioli
50
- Direct Linearity. - 4 Orders of Magnitude Dynamic Range. - Picogram Level Sensitivities. - Truly Universal for U-HPLC, SFC, -HLPC...
OR85 Possibilities and Limitations of SFC and SFC-MS/MS Using State-Of-The-Art Instrument and Innovative Stationary Phases Davy Guillarme, Alexandre Grand-Guillaume Perrenoud, Szabolcs Fekete, Jean-Luc Veuthey University of Geneva, Geneva, CH OR86 Packed Column SFC: 1 or 2 Powerful Dimension(s) in 2D Separation Techniques Didier Thiebaut, Pierre Guibal, Orjen Petkovic, Patrick Sassiat, Jerome Vial ESPCI Paristech - LSABM, Paris Cedex 05, FR OR87 Production Rate Optimization in (Semi-)Preparative Chromatography via Chiral and Achiral Stationary Phase Optimized LC and SFC Frederic Lynen, Sander Delahaye, Kai Chen Ghent University, Ghent, BE
13:50 14:10
14:10 14:30
Emerald
14:00 14:30
KN58 Towards High-Sensitive Detection in Microscale Electrophoresis Using On-Line Sample Concentration 1 1 1 1 2 1 Koji Otsuka , Hiroshi Koino , Saeko Kinami , Hiroya Ota , Takayuki Kawai , Kenji Sueyoshi , 1 3 Takuya Kubo , Fumihiko Kitagawa 1 2 Kyoto University, Kyoto, JP; National Institute of Advanced Industrial Science and Technology, 3 Osaka, JP; Hirosaki University, Aomori, JP
G102-103
KN61 Advances and Applications of UPLC-MS to Endogenous and Drug Metabolite Profiling Ian Wilson Imperial College, London, GB KN62 Making an Integrated, Versatile Microfluidic UHPLC System Reality Steven Cohen, Paul Rainville, Jay Johnson, Angela Doneanu, Jim Murphy Waters Corporation, Milford MA, US
14:00 14:30
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PL5 Interfacing Liquid Chromatography with Mass Spectrometry: From Zero Plate Chromatography to Multidimensional Approaches Grard Hopfgartner, Emmanuel Varesio University of Geneva, Geneva, CH PL6 Microfluidic Separation Devices Coupled to Mass Spectrometry J. Michael Ramsey University of North Carolina at Chapel Hill, Chapel Hill, NC, US PL7 Developments in the Design and Usage of High Performance Ion-Exchange Columns Paul Haddad Australian Centre for Research on Separation Science, Hobart, Tasmania, AU PL8 High-Impact Liquid Chromatography Peter Schoenmakers University of Amsterdam, Amsterdam, NL Closing Ceremonies (including Award Presentations) Farewell Reception Location: First Floor restaurant
15:20 15:50
15:50 16:20
16:20 16:40
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MEET OUR SPECIALISTS AT HPLC 2013, JUNE 16-20 IN AMSTERDAM, THE NETHERLANDS, TO FIND OUT MORE ABOUT OUR NEW SOLUTIONS FOR SEC/GPC, HPLC, UHPLC AND DOWNSTREAM PROCESSING OR VISIT OUR WEBSITE WWW.TOSOHBIOSCIENCE.COM.
BIOM BIOP BIOT CEFF CEMS CEPH CHIP CHIR CMTR COLS ENVI FOOD FORC FUND GLYC HILC HRMS INST LCLC LCMS LCSM LPDS MASS META MONO MSDA NANO PHAR POLY PROT QTMS RMEC SAMP SELE SSFC STPH MO TU WE
List of Posters
List of Abbreviations
Biomedical Biopharmaceutical Biotechnology Column efficiency CE-MS Capillary electrophoresis Chip-based separations Chiral separations Chemometrics Columns Environmental Food Forensic Fundamentals Glycans HILIC High-resolution MS Instrumentation LCLC LC-MS principles LC-MS of small molecules Lipids Mass spectrometry Metabolomics Monoliths MS data analysis Nanomaterials Pharmaceutical Polymers Proteomics Quantitative MS Retention mechanisms Sample preparation Selectivity Sub- and supercritical-fluid chromatography Stationary phases Presented on Monday Presented on Tuesday Presented on Wednesday
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Method Validation for the Analysis of Citrulline and Related Amino Acids in Plasma by Using the Last Generation Monolithic Column in RP-HPLC Mode 1 1 1 2 Agustn Acquaviva , Lilian Romero , Cecilia Castells , J. Manuel Herrero Martinez 1 2 LIDMA, La Plata, AR; Departamento de Qumica, Valencia, ES Sensitive Analysis of 5-Nitroimidazoles by Cation-Selective-Exhaustive-Injection and Sweeping-Micellar-Electrokinetic-Chromatography in Untreated Clinical Samples Diego Airado-Rodrguez, Maykel Hernndez-Mesa, Carmen Cruces-Blanco, Ana Mara GarcaCampaa Department Analytical Chemistry, University of Granada, Granada, ES LC-MS Quantification of 6-Methylmercaptopurine to Determine Thiopurine SMethyltransferase Activity in Red Blood Cells 1 1 2 2 1 Joseph Bailey , Molly Zaman , Christopher Titman , Alan Barnes , Sally Benton 1 2 Clinical Biochemistry Department, Barts Health NHS Trust, London, GB; Shimadzu Corporation, UK, Milton Keynes, GB Separation and Isolation of Pure and Active Antimicrobial Peptide of Bacteriocin Class Using HPLC for Modeling of Preparative Scale Separation 1 2 2 2 Beata Furmanek-Blaszk , Joanna Gazowska , Daniel Jastrzbski , Mariusz Jaszczot , Micha 2 2 2 Laskowski , Grzegorz Boczkaj , Marian Kamiski 1 2 University of Gdask, Biology Faculty, Department of Microbiology, Gdansk, PL; Gdansk University of Technology, Gdansk, PL Development of the Isolation of Whey Proteins Using High Performance Liquid Chromatography on Preparative Scale Mariusz Jaszczot, Joanna Gazowska, Karol Kadlec, Grzegorz Boczkaj, Marian Kamiski Gdansk University of Technology, Gdansk, PL Analytical Power of LC-UV-MS/MS in Drug Metabolism Studies: Phase I and II Gentamicin Metabolites Produced by Human Liver Microsomal Fractions 1 1 2 2 Bogusaw Buszewski , Magorzata Szultka , Rafa Krzemiski , Marek Jackowski 1 2 Nicolaus Copernicus University, Faculty of Chemistry, Toru, PL; Nicolaus Copernicus University, Collegium Medicum, Bydgoszcz, PL Ultra High Performance Liquid Chromatography and High Resolution Mass Spectrometric Detection in the Clinical Laboratory Use of 2u Particle Packed Reversed Phase Columns Karin Cabrera, Michael Schulz, Anita Piper, Petra Lewits, Patrik Appleblad Merck KGaA, Darmstadt, DE Study of Inhibitors of Abl1 Tyrosine Kinase by an Indirect Pulsed Electrochemical Detection Method Hui Chen, Erwin Adams, Ann Van Schepdael KU Leuven, Leuven, BE Protein Unbound Pharmacokinetic Interaction of a Traditional Chinese Medical Formulation, Jia-Wei-Xiao-Yao-San, on 5-Fluorouracil in Rats Blood and Brain by Microdialysis 1 2 1 Meng-Hsuan Chiang , Lie-Chwen Lin , Tung-Hu Tsai 1 2 National Yang-Ming University, Taipei, TW; National Research Institute of Chinese Medicine, Taipei, TW A Simplified and Sensitive Strategy for the Determination of Plasma Total Homocysteine and Metabolic Related Vitamins B6, B9 and B12 Using MEPS-UHPLCPDA Analysis Hugo Cmara, Jorge Pereira, Jos S. Cmara CQM, UMa, Funchal, PT 56
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Aptamers Sieving for Protein, Bacteria and Cell Based on Capillary Electropohresis Feng Qu, Xinying Zhao, Xiaomei Zhou, Zhaoyang Meng, Beilei Lou School of Life Science, Beijing Instititu of Technology, Beijing, CN Determination of Warfarin and Warfarin Alcohols in Saliva and Plasma by High Performance Liquid Chromatography with Fluorimetric Detection 1 1 1 1 2 Silvia Ghimenti , Tommaso Lomonaco , Isabella Piga , Denise Biagini , Massimo Onor , Fabio Di 1 3 4 4 5 Francesco , Aldo Paolicchi , Lucia Ruocco , Giovanni Pellegrini , Maria Giovanna Trivella , Roger 1 Fuoco 1 2 University of Pisa, Dept of Chemistry and Ind. Chemistry, Pisa, IT; Institute of Chemistry of 3 Organometallic Compounds, CNR, Pisa, IT; University of Pisa, Dept of Translational Research 4 and New Technologies in Medicine and Surgery, Pisa, IT; Chemical-Clinical Analysis Laboratory, 5 AOUP, Pisa, IT; Institute of Clinical Physiology, CNR, Pisa, IT Development and Validation of UHPLC-MS/MS Method for the Quantification of Cortisol and 6-Hydroxycortisol in Human Urine as Biomarker of CYP3A Activity Kim Hor Daryl Hee, Lawrence Soon-U Lee National University of Singapore, Singapore, SG Rational Design and Affinity Evaluation of Polyvalent Peptide Probes for Tumor Biomarker Targeting Yanyan Huang, Rui Zhao Institute of Chemistry, Chinese Academy of Sciences, Beijing, CN Developing High Throughput 2D-LC-MS/MS Method for Quantification of Vitamin D Which Overcomes Challenges of Chemiluminescent Immunoassay 1 2 1 2 2 Siji Joseph , Sreekala K.N , Sudha Rajagopalan , Anura Kurpad , Amit Mandal 1 2 Agilent Technologies, Bangalore, IN; St. Johns Research Institute, Bangalore, IN Biomarkers Determination in Exhaled Breath Condensate, Plasma and Urine by Liquid ChromatographyTandem Mass Spectrometry with Simple Sample Preparation Agata Kot-Wasik, Monika Janicka, Andrzej Wasik, Jacek Namienik Gdask University of Technology, Gdask, PL Development of New HPLC Method for Determination of Retinol, Alpha- and GammaTocopherol Using High Resolution Monolithic Column for Bioanalysis 1 1 2 1 Barbora Kuerov , Lenka Krmov , Dagmar Solichov , Petr Solich 1 2 Charles University, Faculty of Pharmacy, Hradec Krlov, CZ; University Hospital, III. Internal Gerontometabolic Clinic, Hradec Krlov, CZ Assessment of Urinary Biomarkers of Oxidative Stress in Cancer and Cardiovascular Pathologies Using a Semi-Automatic Micro-Extraction Technique Combined with UHPLC-PDA System 1 1 1 2 1 Berta Mendes , Pedro Silva , Jorge Pereira , Fernando Aveiro , Isabel Mendona , Jos S. 1 Cmara 1 2 CQM, UMa, Funchal, PT; SESARAM, Hospital Dr. Nlio Mendona, Funchal, PT Rapid Quantitation of Five Immunosuppresants from Body Fluids Siji Joseph, Sreelakshmy Menon Agilent Technologies, Bangalore, IN Exploring the Potential of Microextraction by Packed Sorbent (MEPS) Combined with Ultrahigh Pressure Liquid Chromatography to Quantify the Urinary Leukotriene B4 Levels in Asthmatic Patients Rosa Perestrelo, Catarina L. Silva, Jorge Pereira, Jos S. Cmara CQM, UMa, Funchal, PT
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Development and Validation of a Chromatographic Method for Determination of Allopurinol and its Derivatives 1 1 2 2 Mnica Raviolo , Margarita Brin , J. Peris-Vicente , Samuel Carda-Broch , Enrique Ochoa3 2 Aranda , Josep Esteve-Romero 1 2 3 Universidad Nacional Crdoba, Crdoba, AR; University Jaume I, Castell, ES; Hospital Provincial, Castell, ES Determination of Tamoxifen and its Main Metabolits in Plasma Samples from Breast Cancer Patients 1 2 2 3 Enrique Ochoa-Aranda , Juan Peris-Vicente , Samuel Carda-Broch , Mnica-Ana Raviolo , Josep 2 Esteve-Romero 1 2 3 Hospital Provincial, Castell, ES; University Jaume I, Castell, ES; Universidad Nacional Crdoba, Crdoba, ES Chromatographic Determination of Lipophilicity of Potential Antitrypanosomal Compounds 1 1 1 2 Mnica Raviolo , Margarita Brin , Mara S. Gualdesi , Juan Peris-Vicente , Samuel Carda2 2 Broch , Josep Esteve-Romero 1 2 Universidad Nacional Crdoba, Crdoba, AR; University Jaume I, Castell, ES Relationships between the Dose of Tamoxifen and CYP2D6 Phenotype 1 1 1 Enrique Ochoa-Aranda , Eduardo Martnez-Dueas , Teresa Ferrer-Magdalena , Juan Peris2 2 2 3 Vicente , Samuel Carda-Broch , Josep Esteve-Romero , Mnica-Ana Raviolo 1 2 3 Hospital Provincial, Castell, ES; University Jaume I, Castell, ES; Universidad Nacional Crdoba, Crdoba, AR Hospitalary Monitorization in Blood of an Highly Active Antiretroviral Therapy Regime 1 2 1 1 Juan Peris-Vicente , Inmaculada Casas-Breva , Samuel Carda-Broch , Mnica Villarreal-Traver , 1 1 1 1 David Fabregat-Safont , Noelia Fuentes-Navarro , Ester Peris-Garca , Josep Esteve-Romero 1 2 University Jaume I, Castell, ES; Hospital la Plana, Castell, ES Simultaneous Determination of Three Traditional and Two Novel Antiepileptic Drugs Using Micellar Liquid Chromatography 1 2 3 4 Swati Dubey , Sudhir Kumar Shukla , Abhilasha Durgbanshi , Josep Esteve-Romero , Devasish 1 4 4 Bose , Juan Peris-Vicente , Samuel Carda-Broch 1 2 Dr. H.S.Gour University, Sagar, IN; Central Forensic Science Laboratory (CFSL), Chandigarh, IN 3 4 Regional Forensic Science Laboratory, Dharamshala, IN; University Jaume I, Castell, ES Determination of Glutathione and Glutathione Disulfide in Mouse Brain Using High Performance Liquid Chromatography with Post-Column Chemiluminescence Detection 1 1 1 2 1 Zoe M. Smith , Jessica M. Terry , Laura J. Gray , Dean J. Wright , Neil W. Barnett , Paul S. 1 Francis 1 2 Deakin University, Geelong, VIC, AU; University of Melbourne, Melbourne, VIC, AU The Use of Linear Ion Trap for Qualitative and Quantitative Analysis of Phytochemicals in Ginseng Samples Andrey Stavrianidi, Igor Rodin, Arkady Braun, Oleg Shpigun Moscow State University, Moscow, RU UHPLC with Electrochemical Detection for the Quantitative Determination of Picomolar Concentrations of Monoamines in Microdialysis Samples 1 2 1 2 Jolien Van Schoors , Hendrik-Jan Brouwer , Katrien Maes , Lusi Van Heerwaarden , Nico 2 1 1 Reinhoud , Yvette Michotte , Ann Van Eeckhaut 1 2 Vrije Universiteit Brussel, Jette, Brussels, BE; Antec BV, Zoeterwoude, NL
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Pharmacokinetics of Alkaloids Isolated from a Traditional Antimalarial Decoction of Argemone Mexicana L. in CD1 Mice and in Humans 1 2 2 1 3 Amina Haouala , Jacques Falquet , Bertrand Graz , Claudia Simoes-Pires , Issaka Sagara , 3 4 5 5 6 Ogobara K. Doumbo , Rokia Sanogo , Santiago Ferrer , Adolfo Garcia , Xavier Ding , Muriel 1 1 Cuendet , Philippe Christen 1 2 3 Geneva University, Geneva, CH; Lausanne University, Lausanne, CH; Malaria Research and 4 5 Training Center, Bamako, ML; Dpartement De Mdecine Traditionnelle, Bamako, ML; GSK, 6 Madrid, ES; Medicines for Malaria Venture, Geneva, CH Neonatal Screening Using Shimadzu LCMS-8040 1 2 3 Giancarlo La Marca , Sabrina Malvagia , Stefano Zaza 1 2 Mass Spectrometry and Pharmacology Laboratory, A. Meyer Chil, Florence, IT; Mass Spectrometry and Pharmacology Laboratory, A. Meyer Childrens Hospital Pediatric Neurology 3 Unit and Laboratories, University of Florence, Florence, IT; Shimadzu Italia, Milan, IT
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Biopharmaceutical
The Role of Internal Standards in High-Sensitivity Protein Quantifications with LCMS/MS 1 1 2 Kees Bronsema , Rainer Bischoff , Nico van de Merbel 1 2 University of Groningen, Groningen, NL; PRA-International EDS laboratory, Assen, NL Multidimensional LC/UV-BChE-ICER Method for Ligand Screening Carmen Lucia Cardoso Universidade de So Paulo-USP, Ribeiro Preto- SP, BR Metallic Derivatives as Potential Cholinesterase Inhibitors: Comparative Studies Using On-Flow Inhibitors Screening Assay 1 1 2 Adriana Ferreira Lopes Vilela , Brbara Mammana Frugeri , Kenia Loureno Vanzolini , Andr 2 2 2 Lcio Franceschini Sarri , Joo Baptista Fernandes , Quezia Bezerra Cass , Carmen Lucia 1 Cardoso 1 2 Universidade de So Paulo-USP, Ribeiro Preto- SP, BR; Universidade Federal de So CarlosUFSCar, So Carlos - SP, BR Orthogonal Peptide Mapping Analysis of Erythropoietin (EPO) Protein by HILIC and Reversed-Phase Chromatography 1 2 2 2 2 Andrew Coffey , Alex Zhu , James Martosella , Phu Duong , Maureen Joseph 1 2 Agilent Technologies UK Ltd, Church Stretton, GB; Agilent Technologies Inc, Wilmington, US Reversed-Phase LC/MS Characterization of Glycosylation in the Fc Region of a Therapeutic Recombinant Monoclonal Antibody (mAb) 1 2 2 2 2 Andrew Coffey , Alex Zhu , James Martosella , Phu Duong , Maureen Joseph 1 2 Agilent Technologies UK Ltd, Church Stretton, GB; Agilent Technologies Inc, Wilmington, US The Impact of Amino Acids on Analytical SEC of mAb Aggregates Judith Vajda, Werner Conze, Egbert Mller Tosoh Bioscience, Stuttgart, DE Fast and Robust Direct Infusion ESI-MS Method for the Characterization of PEGylated Proteins 1 2 2 2 Ines C. Forstenlehner , Johann Holzmann , Wolfgang Wieder , Hansjrg Toll , Christian G. 1 Huber 1 2 University of Salzburg, Salzburg, AT; Sandoz, Kundl, AT Considerations in the HPLC Analysis of Biomolecules Sandra Hanson, Mark Woodruff Fortis Technologies Ltd, Neston, GB 59
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Cation-Exchange Chromatography with Conductivity Detection for the Analysis of Cations in Human Saliva 1 2 3 2 2 2 Kyung Suk Hwang , Yooseok Kim , Su Min Yoo , Chang Seon Yoo , Ji Eun Kim , Ha Jeong Kwon 1 Department of Dental Technology, Shinheung University, Uijeongbu, Kyunggido, KR; 2 Department of Preventive Social Dentistry School of Dentistry, Kyung Hee University, Seoul, 3 KR; Department of Dental Hygiene, Dong-Woo College, Sokcho, KR Analytical Challenges in Analysis of Peptides & Proteins in Oral Solide Dose Formulations Babak Jamali Novo Nordisk, Maaloev, DK High Resolution Analysis of High Molecular Weight Components Contained within Igg Using the Latest Silica-Based SEC Columns Yasutoshi Kawai, Hiroyuki Yamasaki, Shigeru Nakatani Tosoh corporation, Shunan, Yamaguchi, JP Pharmacokinetics and Bioavailability of Epimedin C in Rat after Oral Administration of Herba Epimedii Extract Measured by Liquid Chromatography Coupled to Tandem Mass Spectrometry 1 1 1 2 1 Chia-Jung Lee , Thomas Y. Hsueh , Wan-Ning Tseng , Lie-Chwen Lin , Tung-Hu Tsai 1 2 National Yang-Ming University, Taipei, TW; National Research Institute of Chinese Medicine, Taipei, TW Determination of Oseltamivir and Oseltamivir Carboxylic Acid in Rat Brain after Oseltamivir Intravenous Administration and its Neurochemical Interaction 1,2 1 2 2,3 2,4 Chia-Chun Lin , Jiin-Cherng Yen , Yu-Tse Wu , Lie-Chwen Lin , Tung-Hu Tsai
1
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Institute of Pharmacology, 2Institute of Traditional Medicine, School of Medicine, National Yang-Ming University, Taipei, TW
BIOP14_TU Development of a Cation-Exchange Ph Gradient Separation Platform Shanhua Lin, Wim Decrop, Julia Baek, Srinivasa Rao, Yury Agroskin, Chris Pohl Thermo Fisher Scientific, Sunnyvale, US High-Speed, High Resolution Oligonucleotide Separations Using Small Particle Anion-Exchangers 1 1 2 1 Shanhua Lin , J. R. Thayer , Ken Cook , Sinivasa Rao 1 2 Thermo Scientific, Sunnyvale, CA, US; Thermo Scientific, Hemel Hempstead, GB Advantages of Small Particle High Resolution Separation Media for Monoclonal Antibody Analysis. Srinivasa Rao, Yuanxue Hou, Julia Baek, Shanhua Lin, Hongmin Zhang, Yury Agroskin, Chris Pohl Thermo Fisher Scientific, Sunnyvale, US Elimination Or Isolation of Phospholipids from Biological Matrices before HPLC/MS Analysis Using Zirconia-Based Adsorbents 1 2 2 2 Frank Michel , Craig R. Aurand , Xiaoning Lu , David S. Bell 1 2 Sigma-Aldrich, Taufkirchen, DE; Supelco/Sigma-Aldrich, Bellefonte, US Fabrication of Large-Sized Silica Monolith Exceeding 1000 Ml with High Structural Homogeneity and the Chromatographic Performances 1 2 2 2 1 Riichi Miyamoto , Yukiko Ando , Chie Kurusu , Hong-zhi Bai , Kazuki Nakanishi , Masamichi 3 Ippommatsu 1 2 Graduate School of Science, Kyoto University, Kyoto, JP; Renaissance Energy Investment Co., 3 Ltd., Kyoto, JP; New Industry Creation Hatchery Center, Tohoku University, Miyagi, JP QA/QC of Monoclonal Antibodies: Charge Variants and Disulfide Linkage Analysis Sundaram Palaniswamy, Ravindra Gudihal, Siji Joseph Agilent Technologies Pvt Ltd, Bangalore, IN 60
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Purification and Characterization of Lysozyme Modified with Poly Ethylene Glycol (PEG) 1 2 1 Sundaram Palaniswamy , Lakshmi NS , Ravindra Gudihal 1 2 Agilent Technologies India, Bangalore, IN; Amrita University, Kollam, IN Use of Entrapment and High-Performance Affinity Chromatography to Compare the Binding of Drugs and Site-Specific Probes with Normal and Glycated Human Serum Albumin Abby Jackson, Jeanethe Anguizola, Erika Pfaunmiller, David Hage University of Nebraska-Lincoln, Lincoln, US Soy Isoflavones: An Automated and Validated UHPLCMS/MS Method for the Determination of the Phase II Metabolites in Blood Plasma and Urine 1 2 Sebastian Soukup , Sabine E. Kulling 1 2 Max Rubner-Institut,, Karlsruhe, DE; Max Rubner-Institut, Karlsruhe, DE Global Analytical Strategy to Characterize Drug-Plasma Protein Interactions: from High Throughput to In-Depth Analysis. Karine Vuignier, Jean-Luc Veuthey, Pierre-Alain Carrupt, Julie Schappler University of Geneva, Switzerland, Geneva, CH Silica-Based Monolithic Capillary Columns Modified by Liposomes for Characterization of Analyte-Liposome Interactions by Capillary Liquid Chromatography 1 2 2 Susanne Wiedmer , Dana Moravcov , Josef Planeta 1 2 University of Helsinki, Department of Chemistry, Helsinki, FI; Institute of Analytical Chemistry of the ASCR, Brno, CZ High-Performance Liquid Chromatography (HPLC) in Non-Clinical Toxicology Research of Pharmaceutical Proteins Shishan Zhao Charles River Laboratories, Montreal, CA Development of an Accurate HP-SEC Method for the Quantification of Polio Virus in (Partially) Purified In-Process Samples. Jonathan Knibbe, Annemiek Y. W. Verwilligen, Pascal de Raadt, Harold H.J. Backus Crucell Holland BV, Leiden, NL
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Biotechnology
Orthogonal Ion-Pairing Reversed Phase Liquid Chromatography Purification of TaqMan Probes with Bulky Fluorophores Concordio Anacleto, Nancy Schoenbrunner Roche Molecular Diagnostics, Pleasanton, CA, US Linear and Non Linear Zonal Bioaffinity Chromatography: A Tool for Ligand Characterization 1 1 1 2 2 3 Quezia Cass , K.L. Vanzolini , L.C.C. Vieira , A.G. Corra , C.L. Cardoso , R. Moaddel 1 2 Universidade Federal de So Carlos, So Carlos - SP, BR; Departamento de Qumica, USP3 Ribeiro Preto, BR; Biomedical Research Center, NIA-NIH, Baltimore, MD, US A Multidimensional Chromatography Method for on Line Cathepsin D Ligands Screening in Natural Products 1 2 1 1 Vivian Cornelio , Marcela Moraes , Quezia Cass , Paulo Cezar Vieira 1 2 Department of Chemistry, University of Sao Carlos, Sao Carlos - SP, BR; Instituto de Bioqumica Mdica, Ncleo de Pesquisas de Produtos Naturais, Universidade Federal do Rio de Janeiro, Rio de Janeiro - RJ, BR
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High Performance Anion Exchange Chromatography (HPAEC)-Mass Spectrometry (MS): Analysis of Complex Mixtures of Oligosaccharides in Biomass Hydrolysates Leon Coulier, Wibo van Scheppingen, Rob van der Hoeven, Jort Gerritsma DSM Biotechnology Center, Delft, NL Automated, Unattended Purification of Beta-Galactosidase, Trypsines, and Proteases with a Single, High Pressure LC Purification System Markus Fuchs Wissenschaftliche Geraetebau Dr. Ing. H. KNAUER GmbH, Berlin, DE Confirmation of the Nature of Solid Residue from Beff Tallow Biodiesel Used as Fuel by LC-MS-IT-TOF Paulo Pivesso Petroleum, Natural Gas and Biofuels National Agency Brazil, Brasilia / DF, BR Direct LC-MS Analysis of Reduced and Oxidized Cysteine and Glutathione in Microbiological Sample Matrices Pieter Stam, Ilco Boogers, Alexander L.L. Duchateau DSM Biotechnology Center, Delft, NL Process of Extration, Purification, Isolation of Epiisopiloturine Alkaloid and its Antiparasitic Activity against Schistosoma Mansoni 1 1 1 1 1 Leiz Vras , Maria Adelaide Guimares , Marianne Vieira , Yuri Campelo , David Lima , Paulo 2 2 3 4 1 Silva , Luciene Vasconcelos , Markus Godejohann , Josu Moraes , Jos Roberto Leite 1 2 3 Federal of Piau University, Parnaba - PI, BR; Anidro do Brasil, Parnaba - PI, BR; Bruker 4 BioSpin, Rheinstetten, DE; Vigilncia Sanitria em Sade, So Paulo - SP, BR Development of Robust Platform High-Throughput Ion Exchange Chromatography for Charge Heterogeneity Analysis of Therapeutic Proteins Jennifer Wang, Tony Moreno, Dan McDonald, Dell Farnan Genentech, Inc., South San Francisco, US High Performance Liquid Chromatography Detection of Products Formed by Recombinant Carotenoid Biosynthesis Pathways Astrid Wirtz, Anita Loeschcke, Annette Markert, Susanne Wilhelm, Frank Rosenau, Karl-Erich Jaeger, Thomas Drepper Institut fr Molekulare Enzymtechnologie, Juelich, DE Novel Sample Preparation Strategy for High Efficient Integral Membrane Protein Analysis Qun Zhao, Lihua Zhang, Yukui Zhang Dalian institute of chemical physics, CAS, Dalian, CN Analysis of Mannosylerythritol Lipids by Normal Phase Liquid Chromatography Atmospheric Pressure Photo Ionization Mass Spectrometry Wilma du Chatinier, Hans-Gerd Janssen Unilever R&D Vlaardingen, Vlaardingen, NL
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Column Efficiency
Evaluation of Fused Core Silica Stationary Phases for the Chromatographic Analysis of Different Pharmaceutical Drugs 1 2 Amal Ammar , Peter Surmann 1 2 Faculty of Pharmacy, University of Tripoli, Tripoli, LY; Faculty of Pharmacy, Free University, Berlin, DE
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Chromatographic Method Development Using a Design Approach for the Quantification of Metabolites in Ilex Paraguariensi 1 1 1 1 Flvio Beltrame , Rodrigo M. C. Pinto , Bruna M. Lemes , Fernanda M. Kreutz , Accio A. F. 1 1 1 2 2 Zielinski , Traudi Klein , Airton V. Pereira , Tiago Campos , Fernando de Paula 1 2 State University of Ponta Grossa, Ponta Grossa, BR; Waters Technologies - Brazil, So Paulo, BR Comparison of the Separation Performance Limits of Small and Large Fully Porous and Superficially Porous Particles 1 2 1 1 Yoachim Vanderheyden , Deirdre Cabooter , Gert Desmet , Ken Broeckhoven 1 2 Vrije Universiteit Brussel, Brussels, BE; K.U.Leuven, Leuven, BE High Speed Separation of Nucleosides in UHPLC Ken Butchart, Neil Mcgrath Fortis Technologies Ltd, Neston, GB Towards a Generic Variable-Length Method Development Strategy for Samples with a Large Variety in Polarity. Pharmaceuticals in Waste Water: a Case Study 1 1 2 3 1 Deirdre Cabooter , Yves Loyson , Franois Lestremau , Monika Dittmann , Kris Wolfs , Gert 4 Desmet 1 2 3 K.U.Leuven, Leuven, BE; INERIS, Verneuil-en-Halatte, FR; Agilent Technologies, Waldbronn, 4 DE; V.U.B., Brussel, BE Fused Core Particles An Assessment of their Practical Daily Use within the Pharmaceutical Industry 1 1 2 Barbara Channer , Sabrina Lisandrin , Mel Euerby 1 2 Actelion Pharmaceuticals Ltd., Allschwil, CH; Strathclyde Institute of Pharmacy and Biomedical Sciences, University of Strathclyde, Glasgow, GB Development of an NARP-UHPLC-MS Method for the Analysis of Milk Triacylglycerols Marco Beccaria, Giuseppe Sullini, Paola Donato, Carla Ragonese, Marina Russo, Francesco Cacciola, Paola Dugo, Luigi Mondello University of Messina, Messina, IT Synthesis of Superficially Porous Particles via Coacervation and the Benefits of Using this Method of Particle Manufacture Wu Chen, Ta-Chen Wei, William Long Agilent Technologies, Wilmington, Delaware, US Speed and Resolution with 5-Micron Superficially Porous Particles 1 1 1 1 2 Joseph DeStefano , Joseph Kirkland , Stephanie Schuster , William Johnson , Thomas Waeghe 1 2 Advanced Materials Technolgy, Inc., Wilmington, Delaware, US; Mac-Mod Analytical, Inc., Chadds Ford, Pennsylvania, US A Simple Multi-Residue Method for Analysis and Quantification of Fluoroquinolones Antibiotics in Wastewater and Surface Water by LC-MS/MS Marina Denadai, Quezia Cass Universidade Federal de So Carlos - UFSCar, SO CARLOS, BR Evaluation of Ultra-High Performance Size Exclusion Chromatography for Protein Aggregates, Using Sub-2 m Particles 1 2 1 Szabolcs Fekete , Katalin Ganzler , Davy Guillarme 1 2 University of Geneva, Geneva, CH; Gedeon Richter Plc, Budapest, HU Development of an SPE-LC/MS/MS Method for Simultaneous Quantification of Intact Human Insulin and 5 Analogs in Human Plasma 1 1 2 2 Kenneth Fountain , Erin Chambers , Norman Smith , Cristina Legido-Quigley 1 2 Waters Corporation, Milford, MA, US; Kings College London, London, GB 63
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The Development and Application of new Fused-Core HPLC Particle 1 1 1 2 Parmar Gaurang , Wayne Way , Richard Henry , Jens Boertz 1 2 Sigma-Aldrich, Bellefonte, US; Sigma-Aldrich, Buchs, CH Methods for Improving Laboratory Productivity by Reducing UHPLC and LC/MS System Downtime 1 1 1 1 2 Maureen Joseph , Anne Mack , William Long , Jason Link , Norwin von Doehren , Wilroy 2 3 Bennen , Andrew Coffey 1 2 3 Agilent Technologies Inc, Wilmington, US; Agilent Technologies BV, Middelburg, NL; Agilent Technologies UK Ltd, Church Stretton, GB Morphology Transport Relations for Packed Beds: From Metric Properties to Structural Descriptors of Diffusion and Hydrodynamic Dispersion Siarhei Khirevich, Stefan Bruns, Alexandra Hltzel, Ulrich Tallarek Philipps-Universitt Marburg, Marburg, DE A Challenge for Visualization of Kinetics on Separation Parameters in High Performance Liquid Chromatography Hiroshi Kobayashi Shinwa Chemical Industries Ltd., Kyoto, JP Comparison of Measured Peak Capacity Using HPLC, UHPLC and LCLC Systems for Analysis of Complex Samples of PAH Biodegradation Products Mie Kristiansen, Jan Christensen, Rune Grsbll, Esther Boll, Nikoline Nielsen University of Copenhagen, Frederiksberg, DK Trends in HPLC Column Technology and their Application: From Small Particles and Long Columns Stefan Lamotte BASF SE, Ludwigshafen, DE Synthesis of Stationary Phase for Reverse-Phase High-Performance Liquid Chromatography Based on Thermal Immobilization of PMDTS(polymethyltetradecylsiloxane) onto Aluminized Silica Renata Nome, Carol Collins UNICAMP, Campinas, BR HPLC Determination of Agomelatine in Tablets Using Different Types of Stationary Phases Mehmet Emre zdemirhan, Nafiz nc Can Anadolu University, Eskisehir, TR Advances in Column Technology for Pharmaceutical Applications Mia Summers, Kenneth Berthelette, Kenneth Fountain Waters Corp, Milford, MA, US Rapid HPLC Method for Estimation of Catechin from Albizia Lebbeck Bark Extracts 1 1 2 3 Pratima Tatke , Sonal Desai , S.Y. Gabhe , Vinay Gaitonde 1 2 C. U. Shah College of Pharmacy, Mumbai, MS, IN; Poona College of Pharmacy, Pune, MS, IN; 3 Biotech India Pvt. Ltd., Mumbai, MS, IN Packing Efficient Capillary Columns with Sub-2 Micron Superficially Porous Particles James Treadway, James Jorgenson University of North Carolina - Chapel Hill, Chapel Hill, NC, US UHPLC Analysis of Biomolecules Mark Woodruff, Neil McGrath Fortis Technologies Ltd, Neston, GB
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Use of UPLC as a Fast and Efficient Approach to Determine the Log Kow Martien van der Meijden, Rob Beks, Erik Baltussen, Theo Noij WIL Research Europe, 's-Hertogenbosch, NL Advances in Particle and Packing Technology for Higher Efficiency UltraPerformance LC Columns Thomas Walter, Kevin Wyndham, Steve Shiner, Daniel Walsh, Michael Savaria, Pamela Iraneta, Jonathan Turner, Cheryl Boissel, Scott McCall Waters Corporation, Milford, MA, US Development and Validation of New HPLC Method for Fast Analysis and High Separation Efficiency with Low Back Pressure 1 1 1 2 Amal Ammar , Mohamed El-Attug , Anisa Elhamili , Peter Surmann 1 2 Faculty of Pharmacy, University of Tripoli, Tripoli, LY; Faculty of Pharmacy, Free University, Berlin, DE How to Optimise Your UHPLC Performance Connect Properly! Ken Butchart, Neil Mcgrath Fortis Technologies Ltd, Neston, GB Experimental Investigation of the Possibilities of Ultra-Performant Chromatographic Columns Ken Broeckhoven, Yoachim Vanderheyden, Gert Desmet Vrije Universiteit Brussel, Brussel, BE Characterization of a New 1.3 m Core-Shell Material 1 2 1 Szabolcs Fekete , Tivadar Farkas , Davy Guillarme 1 2 University of Geneva, Geneva, CH; Phenomenex, Torrance, US Optimal Method Development Utilizing Modern UHPLC Columns via a QualityByDesign (Qbd) Methodology 1 1 1 2 Maureen Joseph , Jason Link , William Long , Andrew Coffey 1 2 Agilent Technologies Inc, Wilmington, US; Agilent Technologies UK Ltd, Church Stretton, GB Performance of High Efficiency Columns and the Impact of System Dispersion Jonathan Turner, Pamela Iraneta, Bonnie Alden, Daniel Walsh, James Cook, Steven Shiner, Michael Savaria, Kevin Wyndham, Thomas Walter Waters Corp, Milford, Ma, US
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CEMS01_MO
CE-MS
CE-UV/MALDI-MS: A New Platform Using an Integrative Matrix Delivery System for Proteomics and Intact Proteins Applications Michael Biacchi, Jasmine Hertzog, Cyril Adolf, Yannis-Nicolas Francois, Emmanuelle LeizeWagner LSMIS, UMR 7140, University of Strasbourg, Strasbourg, FR Development of an Immunoaffinity Sorbent with Fab Antibody Fragments for the Analysis of Neuropeptides by IA-SPE-CE-MS Fernando Benavente, Silvia Medina-Casanellas, Jos Barbosa, Victoria Sanz-Nebot Department of Analytical Chemistry, University of Barcelona, Barcelona, ES Analysis of Glycopeptide Glycoforms of Human Transferrin by Capillary Liquid Chromatography-Mass Spectrometry. Application to Alcoholism Diagnosis Fernando Benavente, Albert Barrroso, Estela Gimnez, Jos Barbosa, Victoria Sanz-Nebot Department of Analytical Chemistry, University of Barcelona, Barcelona, ES
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Capillary Electrophoresis-Triple-Quadrupole Mass Spectrometry Based Peptide Quantification 1 2 3 Suresh Babu C.V. , Martin Greiner , Sundaram Palaniswamy 1 2 Agilent Technologies India Pvt. Ltd., Bangalore, IN; Agilent Technologies R&D and Mktg. 3 GmbH & Co.KG,, Waldbronn, DE; Agilent Technologies, Bangalore, IN Analysis of the sPRG PTM Peptide Standard Using Sheathless Capillary Electrophoresis Electrospray Mass Spectrometry (CESI-MS) Klaus Faserl, Bettina Sarg, Herbert Lindner Innsbruck Medical University, Innsbruck, AT A Next Generation Mass Spectrometry Platform for the Rapid Identification of (Multi-)Drug Resistant Gram-Negative Bacteria Frank Fleurbaaij Leiden University Medical Center, Leiden, NL Characterization of Nitrated Allergens by CZE-ESI-TOF MS Sergey Gusenkov, Chlo Ackaert, Gertie Oostingh, Hanno Stutz University Salzburg, Salzburg, AT Ultra-Low Flow CE-ESI-MS as an Analysis Tool for Post Translational Modifications 1 1 2 1 Anton Heemskerk , Bart Schoenmaker , Jean-Marc Busnel , Paul Hensbergen , Manfred 1 1 1 Wuhrer , Andr M. Deelder , Oleg A. Mayboroda 1 2 Leiden University Medical Center, Leiden, NL; Beckman Coulter Inc., Brea, CA, US Online Coupling of Capillary Electrophoresis with Direct Analysis in Real Time Mass Spectrometry Huwei Liu, Cuilan Chang, Yu Bai Peking University, Beijing, CN Sensitivity Enhancement in Capillary ElectrophoresisMass Spectrometry Using LVSEP. 2 1 2 3 1 4 1 Hiroya Ota , Takayuki Kawai , Kenji Sueyoshi , Takuya Kubo , Fumihiko Kitagawa , Koji Otsuka 1 2 Kyoto University, Kyoto, JP; National Institute of Advanced Industrial Science and Technology, 3 4 Osaka, JP; Osaka Prefecture University, Osaka, JP; Hirosaki University, Hirosaki, JP Investigation of the Oxidative Metabolism of the Alkaloid Harmane by Electrochemistry, Non-Aqueous Capillary Electrophoresis and Mass Spectrometry Jrg Roscher, Oliver Hachmller, Jana Happe, Uwe Karst University of Mnster, Mnster, DE Electrophoretic and Mass Spectrometric Analysis of Bacterial Endotoxins 1 1 2 3 1 3 Viktor Sndor , Dalma Scheffer , Bla Kocsis , Ferenc Kilr , Anik Kilr , gnes Drnyei 1 2 Dept. of Anal. and Envir. Chem., University of Pcs, Pcs, HU; Dept. of Med. Microb. and 3 Immun., University of Pcs, Pcs, HU; Inst. of Bioanalysis, University of Pcs, Pcs, HU Determination of Harmala Alkaloids in Edible Algae by Capillary Electrophoresis Mass Spectrometry 1 1 2 2 Marcos Tascon , Leonardo Gagliardi , Fernando Benavente , Jose Barbosa , Victoria Sanz2 Nebot 1 2 Universidad Nacional de La Plata, La Plata, AR; Universidad de Barcelona, Barcelona, ES Detemination of Eight Fluoroquinolones in Domestic Sewage by OffLine Immunoaffnity SolidPhase Extraction Coupled with Electrospray Ionization Mass Spectroscopy 1 1 1 1 2 Xin-Xiang Zhang , Deng Yan , Zhou Yinglin , Zhang Xiao-Hui , Li Peiwu 1 2 Peking University, Beijing, CN; the Oil Crops Research Institute (OCRI) of the Chinese Academy of Agricultural Sciences (CAAS), Wuhan, CN 66
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CEPH01_MO
Capillary Electrophoresis
The Use of Discontinuous Buffers in Capillary Electrophoresis Analysis of Biopharmaceuticals 1 2 Hytham Ahmed , Wael Ebied 1 2 Faculty of Pharmacy, Damanhour University, Damanhour, EG; SEDICO Pharmaceutical Company, 6th October, EG Off-Line Comprehensive IP-RPLC X CE and IEX-LC X CE for Oligonucleotide Impurity Mapping Piotr Alvarez, Frederic Lynen Ghent University, Gent, BE Application of Various On-Capillary Stacking Techniques for Determination of Homocysteine-Thiolactone Kamila Borowczyk, Paulina Furmaniak, Pawe Kubalczyk, Rafa Gowacki University of Lodz, Faculty of Chemistry, Dep. Env. Chem., Lodz, PL Accelerating Drug Discovery: Electrophoretic Front-End Library Screening for Biological Relevance 1 1 2 Christa Colyer , Kathryn Riley , Shingo Saito 1 2 Wake Forest University, Winston-Salem, NC, US; Saitama University, Saitama, JP Interinstrumental Transfer of a Chiral CE Method Using Precision Studies and Robustness Testing Data Bart De Cock, Birgit De Meuter, Bieke Dejaegher, Debby Mangelings, Yvan Vander Heyden Vrij universiteit Brussel, Jette, BE Kinetic Performance Evaluation and Perspectives of Packed Column Capillary Electrochromatography Seppe De Smet, Frdric Lynen Ugent, Gent, BE Hydrophilic Interaction Capillary Electrochromatography (HICEC) Applied in Packed and Open-Tubular Capillaries Seppe De Smet, Frdric Lynen Ugent, Gent, BE New Developments for In-Situ Electrokinetic Preconcentration Techniques for Trace Analysis in Capillary Electrophoresis Nathalie Delaunay, Philippe Anres, Pierre Gareil PECSA, Chimie ParisTech, Paris, FR Capillary Zone Electrophoresis for the Characterisation and Separation of Detonation Nanodiamond Emer Duffy, Dimitar Mitev, Pavel N. Nesterenko, Brett Paull Australian Centre for Research on Separation Science, Hobart, TAS, AU Sweeping as a Multistep Enrichment Procedure in Cyclodextrin-Modified Micellar Electrokinetic Chromatography of Hydrophobic Basic Analytes: Application to Pharmaceuticals 1 2 1 Mohamed El-Awady , Fathalla Belal , Ute Pyell 1 2 University of Marburg, Department of Chemistry, Marbrug, DE; University of Mansoura, Faculty of Pharmacy, Mansoura, EG Enhancement of Coating Stability for Capillary Zone Electrophoresis of Proteins in DDAB Modified Surfaces 1 1 1 1 2 Anisa Elhamili , Amal Ammar , Mohamed El-attug , Shaban Saad , Douglas Westerlund , Jonas 2 2 Bergquist , Stellan Hjerten 1 2 Tripoli University, Tripoli, LY; Uppsala University, Uppsala, SE 67
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Experimental Design Based Strategies to Optimize Capillary Electrophoresis Methods for the Separation of Polycyclic Aromatic Hydrocarbons 1 1 2 3 4 Ludivine Ferey , Nathalie Delaunay , Douglas Rutledge , Alain Huertas , Yann Raoul , Pierre 1 5 1 Gareil , Isabelle Rivals , Jrme Vial 1 2 Laboratory PECSA, Chimie ParisTech, ESPCI ParisTech, Paris, FR; Laboratory IAQA, 3 4 5 AgroParisTech/INRA, Paris, FR; Lesieur, Asnires sur Seine, FR; Sofiprotol, Paris, FR; Equipe de Statistique Applique, ESPCI ParisTech, Paris, FR IEF-CGE as a Highly Selective Quantitative Approach for the Quantitation and Characterisation of Proteins Thomas Hahne, Hermann Wtzig Institute of Med. and Pharmaceut. Chemistry, TU Braunschweig, Braunschweig, DE Development of a Capillary Electrophoretic Method for Determination of Plasma Clearance of Iohexol in Dogs and Cats 1 2 3 3 1 Alexander Hellqvist , Reidun Heiene , Siska Croubels , Siegrid De De Baere , Ylva Hedeland 1 2 3 Uppsala University, Uppsala, SE; Norwegian School of Veterinary Science, Oslo, NO; Ghent University, Merelbeke, BE Evaluation of Electro-Osmotic Markers in Aqueous and Non-Aqueous Capillary Electrophoresis Alexander Hellqvist, Ylva Hedeland, Curt Pettersson Uppsala University, Uppsala, SE Determination of 5-Nitroimidazoles in Environmental Waters by Cation-SelectiveExhaustive-Injection and Sweeping-Micellar-Electrokinetic-Chromatography Using Dispersive-Liquid-Liquid-Microextraction for Sample Treatment Maykel Hernndez-Mesa, Diego Airado-Rodrguez, Ana Mara Garca-Campaa, Carmen CrucesBlanco University of Granada, Granada, ES Anion Analysis in Wine by Capillary Zone Electrophoresis John C. Hudson, Jim Thorn and Hans Dewald Beckman Coulter Inc., Brea, CA, US Label-free Electrophoretic Analysis of Carbohydrates Using Complexation with Quinolineboronic Acids. 2 1 2 3 1 4 Koichi Kanemori , Takayuki Kawai , Kenji Sueyoshi , Takuya Kubo , Fumihiko Kitagawa , Koji 1 Otsuka 1 2 Kyoto University, Kyoto, JP; National Institute of Advanced Industrial Science and Technology, 3 4 Osaka, JP; Osaka Prefecture University, Osaka, JP; Hirosaki University, Hirosaki, JP Classification of Dickeya and Pectobacterium Species by HPLC and Gel Isoeletric Focusing 1 1 1 2 1 Anna Kubesov , Dana Moravcov , Ji alplachta , Jaroslav Hork , Marie Hork 1 2 Institute of Analytical Chemistry of the ASCR, Brno, CZ; State Phytosanitary Administration, Division of Diagnostics, Olomouc, CZ Capillary Electrophoresis Applications for the Separation and Quantification of Resin Acids Present in Rosin Samples 1 1 2 2 Louise Mckeon , Fiona Regan , Ray Leonard , Barry Burns 1 2 Dublin City University, Dublin, IE; Henkel, Dublin, IE Molecularly Imprinted Monolithic Hydrophobic Polymers as a Tool for Separation in Capillary Electrochromatography 1 2 1 1 Recep Uzek , Fatma Mutlu , Ali Derazshamshir , Adil Denizl 1 2 Hacettepe University, Ankara, TR; Abant zzet Baysal University, Bolu, TR
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Separation by a Dual Mixture of Cyclodextrins Described by Overall Complexation Parameters Ludmila Mllerov, Pavel Dubsk, Bohuslav Ga Charles University in Prague, Faculty of Science, Prague, CZ Miniaturization of Enzymatic Assays by Capillary Electrophoresis: Application to Human Kinases Implicated in Cancer and Neurodegeneration Hala Nehme, Reine Nehme, Pierre Lafite, Emilie Destandau, Sylvain Routier, Philippe Morin Institute of Organic and Analytical Chemistry, Orlans cedex 2, FR Monitoring of -Galactosidase and Glycerol Kinase Activity and Inhibition Using Capillary Electrophoresis Hala Nehme, Reine Nehme, Pierre Lafite, Sylvain Routier, Philippe Morin Institute of Organic and Analytical Chemistry, Orlans cedex 2, FR Evaluation of Capillary Gel Electrophoresis for the Development of Analytical Fingerprints for the Control of Complex Protein Mixtures of Therapeutic Interest Randa Ben Ameur, Galle Coussot, Catherine Perrin Institut des Biomolcules Max Mousseron, Montpellier, FR SweepingLarge Volume Sample Stacking (LVSS) as Two Sequential Steps for Online Enrichment of Some Cancer Biomarkers Azza Rageh, Achim Kaltz, Ute Pyell University of Marburg, Marburg, DE Performance of Chromatographic Systems to Estimate Biopartitioning Properties Mart Ross, Clara Rfols, Elisabet Fuguet, Marta Hidalgo-Rodrguez Universitat de Barcelona, Barcelona, ES Protein-Copper Ion Mapping of Human Serum Using a Novel Metal Ion Contaminant Sweeping Technique and Fluorescent Metal Probe in Polyaminocarboxylate Gel Electrophoresis 1 1 2 1 Shingo Saito , Mitsuyoshi Kawashima , Makoto Sato , Masami Shibukawa 1 2 Saitama University, Saitama, JP; Sino-Test Corporation, Sagamihara, JP Multiple Stacking Preparative Capillary Electrophoresis Using Transient Isotachophoresis 1 2 2 1 1 Hiroto Tsujimura , Tomoko Haraga , Kuniaki Takahashi , Masami Shibukawa , Shingo Saito 1 2 Saitama University, Saitama, JP; Japan Atomic Energy Agency, Ibaraki, JP Evaluation of CYP3A4 Enantioselective Metabolism of Verapamil by Electrophoretically Mediated Microanalysis 1 1 1 Lucia Asensi-Bernardi , Yolanda Martn-Biosca , Laura Escuder-Gilabert , Sagrario Torres2 3 1 Cartas , Salvador Sagrado , Maria Jos Medina-Hernndez 1 2 Dep. Qumica Analtica, Facultad de Farmacia, Univ. Valncia, Burjassot, ES; IGIC-Universitat 3 Politcnica de Valncia, Gandia, ES; IDM. Unitat mixta UPV-UV, Valencia, ES Electrophoretically Mediated Microanalysis for the Evaluation of Enantioselective Metabolism of Fluoxetine by CYP2D6 1 1 1 Lucia Asensi-Bernardi , Yolanda Martn-Biosca , Laura Escuder-Gilabert , Sagrario Torres2 3 1 Cartas , Salvador Sagrado , Maria Jos Medina-Hernndez 1 2 Dep. Qumica Analtica. Facultad de Farmacia. U. Valncia, Burjassot, ES; IGIC-Universitat 3 Politcnica de Valncia, Gandia, ES; IDM. Unitat mixta UPV-UV, Burjassot, ES On-Line Capillary Electrophoresis for Studying Carboxylic Acid Production During Bioreactor Cultivation of Yeast 1 2 1 Heidi Turkia , Heli Sirn , Juha-Pekka Pitknen 1 2 VTT Technical research centre of Finland, Espoo, FI; Lappeenranta University of Technology, Lappeenranta, FI 69
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Separation of Antibiotics Present in Biological Fluids by Capillary Isoelectric Focusing and High-Performance Liquid Chromatography with UV Detection 1 1 2 1 1 1 Marie Vykydalov , Marie Hork , Filip Rika , Filip Dua , Dana Moravcov , Vladislav Kahle , 1 Karel lais 1 2 Institute of Analytical Chemistry of the ASCR, v. v. i., Brno, CZ; Department of Microbiology, Faculty of Medicine, Masaryk University, Brno, CZ Fast and Validated Affinity Capillary Electrophoresis for Routine Binding Screening Assays 1 1 1 2 1 Hermann Wtzig , Hassan Alhazmi , Markus Nachbar , Deia Abd El-Hady , Sabine Redweik 1 2 Univ. of Braunschweig, Braunschweig, DE; Assiut University, Assiut, EG CEtoolbox: Specialized Calculator for Capillary Electrophoresis Users as an Android Application 1 2 2 2 Jrome Pansanel , Michael Biacchi , Rabah Gahoual , Emmanuelle Leize-Wagner , Yannis 2 Francois 1 2 IPHC, UMR 7178, Universit de Strasbourg, Strasbourg, FR; LSMIS, UMR 7140, University of Strasbourg, Strasbourg, FR Viral Vaccine Characterization with Capillary Electrophoresis 1 1 1 2 Ewoud van Tricht , Marta Germano , Harold Backus , Cari Snger-van de Griend 1 2 Crucell Holland B.V., Leiden, NL; Kantisto B.V., Baarn, NL
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Chip-Based Separations
Ion-Pair Reversed-Phase Chromatography of Short Double Stranded DNA in Silicon Micro-Pillar Array Columns: Retention Model and Applications 1 1 1 2 Lei Zhang , Bivragh Majeed , Chris Van Hoof , Wim De Malsche 1 2 Imec, Leuven, BE; Vrije Universiteit Brussel, Brussels, BE High Sensitive Quantitative Analysis: The Promise of Chip Based Micro LC/MS Lieve Dillen, Willy Cools, Filip Cuyckens Janssen Research and Development, Beerse, BE Chip Electrochromatography Coupled to Mass-Spectrometric Detection by Monolithically Integrated Nanospray Emitter Claudia Ernst, Fabian Schwarzkopf, Detlev Belder University of Leipzig, Institute of Analytical Chemistry, Leipzig, DE Considerations in Developing a Prototype Microfluidic Trapping Column to Improve Mass and Volume Capacity in an Integrated LC/MS System Jay Johnson, Jim Murphy, Angela Doneanu, Bob Jencks, Bob Collamati Waters Corporation, Milford, MA, US Separation of Macromolecules by Miniaturized Asymmetrical Flow Field Flow Fractionation 1 2 1 2 1 Jana Kralova , Manly Callewaert , Peter Schoenmakers , Wim De Malsche , Wim Kok 1 2 University of Amsterdam, Amsterdam, NL; Vrije Universiteit Brussel, Brussels, BE Monitoring Enzymatic Oxidation of Polycyclic Aromatic Hydrocarbons by Microchip Electrochromatography 1 1 2 2 1 Karin M. Krone , Claudia Ernst , Carlos G. Acevedo-Rocha , Manfred T. Reetz , Detlev Belder 1 2 Institute for Analytical Chemistry, University of Leipzig, Leipzig, DE; Max Planck Institute of Coal Research, Mlheim an der Ruhr, DE Ultra-High Throughput Approach for Single Cell Genomics with Novel Agarose-based Microfluidic Comet Array Electrophoresis Bi-Feng Liu, Yiwei Li Huazhong University of Science and Technology, Wuhan, CN 70
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Research-Flexible vs. Commercial Fixed-Purpose Microfluidic Chip Platforms: Can We Have the Best of Both Worlds for Flexible Field Deployable Electrodriven Analysis? Chip-ITP with Indirect Fluorescence Detection 1 1 2 3 4 1 Petr Smejkal , Michael Breadmore , Rosanne Guijt , Frantisek Foret , Fritz Bek , Mirek Macka 1 2 University of Tasmania, School of Chemistry, Hobart, AU; University of Tasmania, School of 3 Pharmacy, Hobart, AU; Institute of Analytical Chemistry, Academy of Sciences of the Czech 4 Republic, Brno, CZ; Agilent Technologies, Waldbronn, DE Capillary Scale LC/MS/MS for High Sensitivity Bioanalysis Is This a Reality and Where Are the Pit Falls Paul Rainville, James Murphy, Thomas Wheat, Robert Plumb Waters Corporation, Milford, US Liquid Chromatography in Extended Nanospace: Development of Micellar Liquid Chromatography for Dansyl Amino Acids Separation Adelina Smirnova, Kazuma Mawatari, Takehiko Kitamori The University of Tokyo, Tokyo, JP Towards Iso-Electric Focussing of Proteins on a Chip for Potential Use in MultiDimensional Separations 1 1 2 2 1 1 R.J. Vonk , B.W.J. Pirok , B. Wouters , S. Eeltink , W.Th. Kok , P.J. Schoenmakers 1 2 Universiteit van Amsterdam, Amsterdam, NL; Vrije Universiteit Brussel, Brussel, BE High Pressure Chip Chromatography with Variable On-Chip Injection and CustomBuilt Particulate Columns for Void-Volume-Free Performance Sebastian Thrmann, Detlev Belder Institute of Analytical Chemistry, University of Leipzig, Leipzig, DE Centrifugal Microfluidic Disc Integrating Carbon Monoliths for Solid-Phase MicroExtraction 1 2 1 1 1 Mercedes Vazquez , Emer Duffy , Xiaoyun He , Elizaveta Vereshchagina , Jens Ducre , 1 2 1 2 Ekaterina Nesterenko , Pavel Nesterenko , Dermot Brabazon , Brett Paull 1 2 Dublin City University, Dublin, IE; University of Tasmania, Hobart, AU On-Chip Peptide Screening towards Beta-Endorphin Antibody Based on Reverse Affinity Chromatographic Microarray Rui Zhao, Weizhi Wang, Yanyan Huang, Yulong Jin Institute of Chemistry, Chinese Academy of Sciences, Beijing, CN On-line Chip-based Strategy for 2D Fractionation Comparing Peptides Found between 1D and 2D Proteomic Analysis 1 1 1 2 3 Remco van Soest , Xiang Zhu , Tina Settineri , Christie Hunter , Jenny Albanese 1 2 3 Eksigent, part of AB SCIEX, Dublin, US; AB SCIEX, Foster City, US; AB SCIEX, Dublin, US Design of Cyclic Olefin Copolymer-Based Microfluidic Devices Designed for Spatial Two- and Three-Dimensional Chromatography 1 1 1 2 1 Bert Wouters , Sander Jespers , Gert Desmet , Peter Schoenmakers , Sebastiaan Eeltink 1 2 Vrije Universiteit Brussel, Brussel, BE; Universiteit van Amsterdam, Amsterdam, NL
CHIP09_WE
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CHIP11_TU
CHIP12_WE
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CHIP14_TU
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CHIR01_MO
Chiral Separations
Optimization and Validation of a GC-MS Method for Determination of Free D-Amino Acids Ratio in Human Urine in a Type 1 Diabetes Study 1 2 2 1 1 MPaz Lorenzo , Manuel Gibellini , Federica Pellati , Coral Barbas , Garcia Antonia 1 CEMBIO, Facultad de Farmacia, Universidad CEU San Pablo, Boadilla del Monte, ES; 2 Department of Life Sciences, University of Modena and Reggio Emilia, Modena, IT
71
CHIR02_TU
A Novel Approach in HPLC Chiral Method Development: Dealing with Multiple Chiral Centers 1 2 1 David Bell , Anders Fridstrom , Gaurang Parmar 1 2 Sigma-Aldrich/Supelco, Bellefonte, PA, US; Sigma-Aldrich/Supelco, St Gallen, CH A New Enantioselective HPLC Method for Analysis of Ketorolac: Application to Pharmacokinetic Study Sunil Kumar Dubey, R. N. Saha, Amit Anand Department of Pharmacy, Birla Institute of Technology & Science, Pilani, IN Enantioselective Separation of Profens Using Immobilized Polysaccharide-Based Columns in Reverse Phase Separation Systems Radim Geryk, Denisa Plecita, Kvta Kalkov, Eva Tesaov Faculty of Science, Charles University in Prague, Prague, CZ Preparation and Characterization of 4-Isopropylcalix[4]Arene-Capped (3-(2-O-Cyclodextrin)-2-Hydroxypropoxy)-Propylsilyl-Appended Silica Particles as Chiral Stationary Phase for High-Performance Liquid Chromatography S.K. ThamaraiChelvi, Jia Zhao, E.L. Yong, Yinhan Gong National University of Singapore, Singapore, SG Pharmacokinetics Behaviour of Verapamil after Intravenous and Oral Administration of Valproic Acid in Rats by HPLC 1 2 3 Habiba Rechak , Mesbah Lahouel , Abderrazak Hamdi 1 2 3 Jijel University, JIjel, DZ; Jijel University, Jijel, DZ; USTHB University, Faculty of Chemistry, Bab Ezzouar, DZ Chiral Determination of Carvedilol and Baclofen in Plasma Samples by HighThroughput Methods Based on Ion Mobility Spectrometry (IMS)-MS-MS with HPLC Separation 1 2 1 1 2 Adriana Iordachescu , Luigi Silvestro , Adelina Ciuciuleaca , Dan Peru , Simona Rizea-Savu 1 2 Pharma Serv International, Bucharest, RO; 3S-Pharmacological Consultation & Research GmbH, Harpstedt, DE Simultaneous Quantification of Mefloquine (+)- and (-)-Enantiomers and the Carboxy Metabolite in Dried Blood Spots by LC-MS/MS Using a New Chiral Separation Approach on the Stationary Phase CHIRALPAK ZWIX(-) 1 2 3 1 4 Mirjam Kasel , Wolfgang Lindner , Michael Lmmerhofer , Reinhold Kerb , Michael Ramharter , 1 1 Matthias Schwab , Ute Hofmann 1 2 Dr.Margarete Fischer-Bosch Institute of Clin. Pharmacology, Stuttgart, DE; Department of 3 Analytical Chemistry, University of Vienna, Vienna, AT; Institute of Pharmaceutical Science, 4 University of Tuebingen, Tuebingen, DE; Division of Infectious Diseases and Tropical Medicine, Medical University Vienna, Vienna, AT Simultaneous Two-Dimensional High-Performance Liquid Chromatographic Determination of All Proteinogenic Amino Acid Enantiomers in Human Serum Using High Performance Pirkle-Type Chiral Stationary Phases 1 2 1 1 3 Nao Kusano , Jumpei Sasabe , Hirohisa Onigahara , Yurika Miyoshi , Masashi Mita , Sadakazu 2 4 1 Aiso , Wolfgang Lindner , Kenji Hamase 1 2 3 Kyushu University, Fukuoka, JP; Keio University School of Medicine, Tokyo, JP; Shiseido Co., 4 Ltd, Tokyo, JP; University of Vienna, Vienna, AT Approach to Enhance the Enantioseparation of Basic Drugs Using Clarithromycin as a Chiral Selector Margarita V. Lebedeva, Aleksandra F. Prokhorova, Elena N. Shapovalova, Oleg A. Shpigun Lomonosov Moscow State University, Moscow, RU
CHIR03_WE
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CHIR05_TU
CHIR06_WE
CHIR07_MO
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72
CHIR11_TU
Design and Synthesis of a Novel Reagent with 6-MOQ Moiety for Amino Acid Labeling and Chiral Separations of All Proteinogenic Amino Acids 1 2 1 1 1 Tsubasa Oyama , Eiichi Negishi , Nao Kusano , Hirohisa Onigahara , Yurika Miyoshi , Masashi 3 1 4 1 5 1 Mita , Manabu Nakazono , Sumio Ohtsuki , Akio Ojida , Wolfgang Lindner , Kenji Hamase 1 2 3 Kyushu University, Fukuoka, JP; Shiseido Irica Technology Inc., Kyoto, JP; Shiseido Co., Ltd., 4 5 Tokyo, JP; Kumamoto University, Kumamoto, JP; University of Vienna, Vienna, AT Evaluating the Effects of Altering the Polymerization Conditions for Organic Based Monoliths on the Immobilization of Human Serum Albumin as a Binding Agent for Various Chiral Solutes in High Performance Affinity Chromatography Applications 1 1 1 1 1 Erika Pfaunmiller , Zhao Li , Mahli Hartman , Courtney Dupper , Marie Laura Paulemond , 2 2 1 Shannon Lum , Stephen Gross , David Hage 1 2 University of Nebraska-Lincoln, Lincoln, NE, US; Creighton University, Omaha, NE, US D- Or L-Glutamine? What Are Bacteria Using for Making Them Resistant to their Own Produced Antibiotics? A Stereochemical Identification Stefan Polnick, Orwah Saleh, Tobias Bonitz, Lutz Heide, Michael Lmmerhofer University of Tuebingen, Tuebingen, Germany, DE Enantioselective Determination of Fluoxetine and Norfluoxetine in Wastewater by HPLC-FD Using SPE 1 2 3 4 5 Ana R Ribeiro , Alexandra S Maia , Irina S Moreira , Carlos M Afonso , Paula ML Castro , Maria E 6 Tiritan 1 2 CICS-ISCSN-CESPU, CBQF-ESB-UCP, CEQUIMED-UP, Gandra - Paredes, PT; CICS-ISCSN-CESPU, 3 4 CBQF-ESB-UCP, Gandra - Paredes, PT; CBQF-ESB-UCP, CEQUIMED-UP, Porto, PT; CEQUIMED5 6 UP, Porto, PT; CBQF-ESB-UCP, Porto, PT; CICS-ISCSN-CESPU, CEQUIMED-UP, Gandra - Paredes, PT Continuous Preparative Chromatography to Obtain Enantiomers of Verapramil Using Simulated Moving Bed (SMB) 1 2 3 Cesar Santana , Rafael Perna , Marco Cremasco 1 2 3 UNIT, Aracaju- SE, BR; UNICAMP, Campinas - SP, BR; UNICAMP, Campinas-SP, BR Continuous Chromatographic Process for Production of Secnidazole Enriched Enantiomers 1 1 2 Ana Nascimento , Marco Cremasco , Cesar Santana 1 2 Unicamp - University of Campinas, Campinas - SP, BR; Unit, Aracaju, BR Development and Validation of a LC Method for the Stability Study of a Pharmaceutical Formulation Containing Voriconazole Using Cellulose Tris(4-Chloro3-Methylphenylcarbamate) as Chiral Selector and Polar Non-Aqueous Mobile Phase 1 1 1 2 1 Anne-Catherine Servais , Radu Moldovan , Elena Farcas , Isabelle Roland , Marianne Fillet 1 2 University of Lige, Lige, BE; CHU, Lige, BE Investigation of the Retention Phenomena of Mefloquine Enantiomers 1 1 2 Csaba Szmolnik , Attila Felinger , Wolfgang Lindner 1 2 University of Pcs, Pcs, HU; University of Vienna, Vienna, AT Chiral Discrimination by High-Performance Liquid-Chromatography with Joint Use of Ion Interaction Reagents with Cyclodextrins as Additives to the Mobile Phase Kamila Szwed Institute of Physical Chemistry PAN, Warsaw, PL
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CHIR14_TU
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73
CHIR20_TU
Optical Isomer Separation of Flavanones and Flavanone Glycosides by Nano-Liquid Chromatography Using a Phenyl-Carbamate-Propyl-Beta-Cyclodextrin Chiral Stationary Phase 1 1 1 2 Fairouz Tazerouti , Kahina Si-Ahmed , Ahmed Y Badjah-Hadj-Ahmed , Zeineb Aturki , Giovanni 2 2 2 Dorazio , Anna Rocco , Salvatore Fanali 1 2 University of Science and Technology Houari Boumedien Usthb, Algiers, Algeria, Dz; a Institute of Chemical Methodologies, Italian National Council of Research, Rome, IT Enantioselective Degradation of Enantiomers of Fluoxetine Followed by HPLC- FD 1 2 3 4 5 Ana R Ribeiro , Alexandra S Maia , Irina S Moreira , Carlos M Afonso , Paula ML Castro , Maria E 6 Tiritan 1 2 CICS-ISCSN-CESPU, CBQF-ESB-UCP, CEQUIMED-UP, Gandra - Paredes, PT; CICS-ISCSN-CESPU, 3 4 CBQF-ESB-UCP, Gandra - Paredes, PT; CBQF-ESB-UCP, CEQUIMED-UP, Porto, PT; CEQUIMED5 6 UP, Porto, PT; CBQF-ESB-UCP, Porto, PT; CICS-ISCSN-CESPU, CEQUIMED-UP, Gandra - Paredes, PT Dress-Up Chiral Columns for the Enantioseparation of Amino Acids Based on Fluorous Separation 1 1 1 1 1 1 Kenichiro Todoroki , Yasuhiro Ishii , Koji Toyoda , Takashi Ikawa , JunZhe Min , Koichi Inoue , Shuji Akai, Toshimasa Toyo'oka University of Shizuoka, Shizuoka, JP Electrophoretic and Molecular Docking Data Connection on the Enantioselective Binding of ()-Catechin to Human Serum Albumin 1 2 2 3 Njabulo J. Gumede , Myalowenkosy I Sabela , Khirsna Bisetty , Lucia Asensi-Bernardi , Yolanda 3 3 3 4 Martn-Biosca , Laura Escuder-Gilabert , Maria Jos Medina-Hernndez , Salvador Sagrado , 5 Sagrario Torres-Cartas 1 2 Departament of Chemistry. Mangosuthu University of Technology, Jacobs, ZA; Departament 3 of Chemistry. Durban University of Technology, Durban, ZA; Departamento Qumica Analtica. 4 Facultad de Farmacia. Universitat de Valncia, Burjassot, ES; Centro de Reconocimiento Molecular y Desarrollo Tecnolgico (IDM), Unidad mixta Universitat Politcnica de 5 ValnciaUniversitat de Valncia, Valencia, ES; IGIC. Universitat Politcnica de Valncia, Gandia, ES Potential of Highly Sulfated -Cyclodextrin as Chiral Selector of Neutral and Basic Drugs in Capillary Electrophoresis 1 1 1 Lucia Asensi-Bernardi , Yolanda Martn-Biosca , Laura Escuder-Gilabert , Sagrario Torres2 3 1 Cartas , Salvador Sagrado , Maria Jos Medina-Hernndez 1 Departamento Qumica Analtica. Facultad de Farmacia. Universitat de Valncia, Burjassot, ES; 2 3 IGIC. Universitat Politcnica de Valncia, Gandia, ES; Centro Interuniversitario de Reconocimiento Molecular y Desarrollo Tecnolgico, Unidad Mixta Universitat Politcnica de Valencia-Universitat de Valncia, Valencia, ES
CHIR21_WE
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CMTR01_MO
Chemometrics
Impact of the Nature of the Set of the Probe Solute on Orthogonality Evaluation in RPLC 1 2 2 2 2 Ramia Al Bakain , Isabelle Rivals , Patrick Sassiat , Didier Thiebaut , Marie-Claire Hennion , 2 2 Guillaume Euvrard , Jrme Vial 1 2 The University of Jordan, Department of Chemistry, Amman, JO; ESPCI Paristech, Paris, FR Characterization of Stationary Phases Based on Polysiloxanes Thermally Immobilized onto Silica and Metalized Silicas Using Supercritical Fluid Chromatography 1 1 2 2 Carla Grazieli Azevedo Da Silva , Carol Collins , Eric Lesellier , Caroline West 1 2 University of Campinas (UNICAMP), Campinas, BR; Universit DOrlans, Orlans, FR 74
CMTR02_TU
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Chromatographic Determination of SSRIs with Fluorescence Detection in Plasma and Urine 1 1 2 3 Nitasha Agrawal , Devasish Bose , Neeti Prakesh Dubey , Juan Peris-Vicente , Samuel Carda3 3 Broch , Josep Esteve-Romero 1 2 dr. H.S.Gour University, Sagar, In; Regional Forensic Science Laboratory, Dharamshala, In 3 University Jaume I, Castell, ES Determination of Distribution Coefficients of Non Steroidal Anti-Inflammatory Drugs (NSAID) by HPLC on Immobilized Artificial Membrane Columns with Current Silica Platforms Owen Foley, Dara Fitzpatrick Irish Separation Science Cluster - University College Cork, Cork, IE General Solution of the Plate Model Including Longitudinal Diffusion and Slow Transfer Kinetics for Isocratic Chromatographic Elution Mara Celia Garca-lvarez-Coque, Juan Jos Baeza-Baeza University of Valencia, Burjassot (Valencia), ES Application of the Artificial Neural Network in Quantitative Structure Retention Relationship Modeling of Liquid Chromatography Separation of Candesartan Cilexetil and its Degradation Products Jelena Golubovic, Biljana Otasevic, Ana Protic, Mira Zecevic University of Belgrade-Faculty of Pharmacy, Belgrade, RS Stability Studies in Different Matrices of Novel Derivatives of Allopurinol 1 1 1 2 Mnica Raviolo , Margarita Brin , Christian Muoz Sosa , Juan Peris-Vicente , Samuel Carda2 2 Broch , Josep Esteve-Romero 1 2 Universidad Nacional Crdoba, Crdoba, AR; University Jaume I, Castell, ES Multivariate Characterisation of Chromatographic Drug-Protein Interactions 1 1 1 2 Tomas Leek , Magnus Klarqvist , Karin Danielsson , Johan Gottfries 1 2 Astrazeneca R&D Mlndal, Mlndal, SE; Gothenburg University, Gothenburg, SE Probabilistic Peak Detection in One and Two Dimensional First-Order Chromatograms 1 1 1 2 2 Martin Lopatka , Andjoe Sampat , Gabriel Vivo-Truyols , Marjan Sjerps , Arian Van Asten , 1 Peter Schoenmakers 1 2 University of Amsterdam, Amsterdam, NL; Netherlands Forensic Institute, the Hague, NL Fast Determination of Saponins in Three Medicinal Plants of Panax Genus Using UPLC-DAD-CAD and Microwave-Assisted Extraction Guang-Ping Lv, De-Jun Hu, Wan-Rong Zong, Jing Zhao, Shao-Ping Li State Key Laboratory of Quality Research in Chinese Medicine, Macao, MO A Monte Carlo Look at Multipoint Linear Calibration Veronika R. Meyer EMPA St. Gallen, St. Gallen, CH Single and Combined HILIC and RPLC for the Separations of Polyphenols 1 1 2 Casandra Ortiz Bolsico , Sandra Pous Torres , Gabriel Viv Truyols , Jos Ramn Torres 1 1 2 Lapasi , Mara Celia Garca lvarez-Coque , Peter J. Schoenmakers 1 2 University of Valencia, Burjassot, ES; University of Amsterdam, Amsterdam, NL Development of a Chromatographic Method to Quantify Melamine in Swine 1 1 1 Beatriz Beltrn-Martinavarro , Juan Peris-Vicente , Samuel Carda-Broch , Josep Esteve-Romero, Sergio Marco-Peir University Jaume I, Castell, ES
CMTR04_MO
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CMTR11_TU
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CMTR14_TU
Isocratic HPLC Optimization for Serially-Coupled Columns Considering Mobile Phase Composition, Column Nature and Length Casandra Ortiz-Bolsico, Jos Ramn Torres-Lapasi, Mara Celia Garca-lvarez-Coque University of Valencia, Burjassot (Valencia), ES Enantiomeric Composition Determination of Highly Overlapped Chromatographic Profiles by Combination of Chromatography and Chemometric Methods. Application to the Analysis of Enantiomeric Drugs 1 1 2 2 Jaiver Osorio , Cecilia Castells , Juan Arancibia , Alejandro Olivieri 1 2 Universidad Nacional De La Plata, La Plata, AR; Instituto De Qumica De Rosario, Rosario, AR Intelligent Peak Deconvolution Analysis Through in Depth Integration of Data Matrix from Liquid Chromatography Coupled with Novel Photo-Diode Array Detector for Pharmaceutical Analysis 1 1 2 2 2 Kanta Horie , Takashi Kato , Yasuhiro Mito , Toshinobu Yanagisawa , Masatoshi Takahashi , 3 Naoki Asakawa 1 2 3 Eisai Co., Ltd., Kakamigahara, JP; Shimadzu Corporation, Kyoto, JP; Eisai Co., Ltd., Tsukuba, JP Development of Analytical Fingerprints for the Control of Complex Protein Mixtures of Therapeutic Interest Using Capillary Zone Electrophoresis 1 2 1 2 1 Randa Ben Ameur , Christelle Reynes , Galle Coussot , Robert Sabatier , Catherine Perrin 1 2 Institut Des Biomolcules Max Mousseron, Montpellier, FR; EA2415 Epidemiology Biostatistics Clinical Research, Montpellier, FR Validation of Human Clinical Genetic Tests: The State of the Art 1 2 2 3 Enrique Ochoa-Aranda , Juan Peris-Vicente , Samuel Carda-Broch , Mnica-Ana Raviolo , Maria 2 2 Rambla-Alegre , Josep Esteve-Romero 1 2 3 Hospital Provincial, Castell, ES; University Jaume I, Castell, ES; Universidad Nacional Crdoba, Crdoba, AR Elution and Peak Width Triangles: a Schematic Representation of the Chromatographic Behavior in Linear Gradient Liquid Chromatography Casandra Ortiz-Bolsico, Jos Ramn Torres-Lapasi, Juan Jos Baeza-Baeza, Mara Celia Garcalvarez-Coque University of Valencia, Burjassot (Valencia), ES Determination of Fungicides in Seed, Formulation, Plant Material, Soil and Water Samples 1 2 3 1 Sandeep K. Mourya , Abhilasha Durgabanshi , Josep Esteve-Romero , Devasish Bose , Juan 3 3 3 Peris-Vicente , Samuel Carda-Broch , Khaled Tayeb-Cherif 1 2 3 dr. H.S.Gour University, Sagar, In; Banaras Hindu University, Vanarasi, In; University Jaume I, Castell, ES A Universal Comparison Study of Chromatographic Response Functions used in Automated Method Development Eva Tyteca, Gert Desmet Vrije Universiteit Brussel, Elsene, BE New Challenges in Developing Robust Criteria in Comprehensive Two-Dimensional Liquid Chromatography Methods Pascale Vanbel University of Amsterdam, Amsterdam, NL Effectual Optimization Strategy for Ternary-Solvent Composition on Reversed Phase Liquid Chromatography Utilizing the Retention Prediction Models Tsukasa Sasaki, Takefumi Kawabe, Eiji Obara, Nobuyuki Suzuki, Toshiaki Tomitsuka Aqerl, Pt Division, Daiichi-Sankyo Co., Ltd., Hiratsuka, Kanagawa, JP
CMTR15_WE
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CMTR24_WE
Linear Modeling of Ligand-Receptor Binding in Enantioselective Liquid Chromatography 1 2 1 Adrian Sievers-Engler , Wolfgang Lindner , Michael Lmmerhofer 1 2 University of Tbingen, Institute for Pharmacy, Tbingen, DE; University of Vienna, Institute for Analytical Chemistry, Tbingen, DE How to Choose the Appropriate Class of Stationary Phases in Relation to the Nature of the Solutes to be Analyzed 1 2 3 3 1 Alain Tchapla , Claire Bordes , Didier Charbonneau , Benjamin Chabot , Sylvie Heron , Jean- Luc 4 4 2 Veuthey , Serge Rudaz , Pierre Lanteri 1 2 Univ.Paris Sud/Groupe De Chimie Analytique De Paris-Sud, Orsay, FR; ISA/Laboratoire Des 3 Sciences Analytiques/ CNRS, Villeurbanne, FR; Interchim R & D, Montluon, FR; 4 Univ.Genve/Laboratoire De Chimie Analytique Pharmaceutique, EPGL, Genve, CH Single Injections in Coupled Columns at Varying Solvent Content Versus Complementary Resolution Systems in the Separation of Complex Mixtures Jos Ramn Torres-Lapasi, Casandra Ortiz-Bolsico, Mara Celia Garca-lvarez-Coque University of Valencia, Burjassot (Valencia), ES SPME-LC/MSn for the Analysis of Selected Biologically Active Compounds Bogusaw Buszewski, Magorzata S Nicolaus Copernicus University, Faculty of Chemistry, Toru, PL Adaption of Retention Models to Allow Optimisation of Peptide and Protein Separations 1 1 2 3 3 Patrik Petersson , Jette Munch , Andrey Vazhentsev , Michael McBrien , Karim Kassam , Mel 4 Euerby 1 2 Novo Nordisk A/S, Mlv, DK; Advanced Chemistry Development (ACD/Labs), Moscow, RU 3 4 Advanced Chemistry Development (ACD/Labs), Toronto, CA; Strathclyde Institute of Pharmacy and Biomedical Sciences, Glasgow, GB Chemometrics in the Development of Analytical Separation Techniques in Medicinal Plant Materials Pascale Vanbel, Jolle Quetin-Leclercq Universit catholique de Louvain, Brussels, BE Development of an Automatic Peak Detection Algorithm for Use in Liquid Chromatography Yoachim Vanderheyden, Eva Tyteca, Gert Desmet VUB, Brussel, BE Identification, Discrimination and Classification of Curcuma Samples Using their Chromatographic Fingerprints Johan Viaene, Goedele Alaerts, Bieke Dejaegher, Yvan Vander Heyden Vrije Universiteit Brussel, Jette, BE
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COLS01_MO
Columns
A Comparison of HPLC Analyses of -Blockers on C18 and C28 Reversed Phases Silica Gel Columns 1 2 3 4 1 Imran Ali , Norikaju Nagae , Vinay Gaitonde , Javed Farooqi , Dilshad Alam 1 2 Jamia Millia Islamia, New Delhi, IN; ChromaNik Technologies Inc.,, 552-0001 Japan, Osaka, JP 3 4 Prochrome India, Mumbai, IN; Indhira Gandhi National Open University, New Delhi, IN
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Analysis of Silicone Oils by High Performance Liquid Chromatography and Corona Charged Aerosol Detection Bruce Bailey, Ian Acworth, Marc Plante Thermo Fisher Scientific, Chelmsford, US Use of Limonene in Countercurrent Chromatography: a Green Alkane Substitute Alain Berthod, Karine Faure, Suchet Pauline, Bouju Elodie University of Lyon 1 - Institute of Analytical Science, Villeurbanne, FR Comparison of HPLC Core-Shell Columns for Isocratic Separation of Selected Xanthophylls in Egg Yolk 1 1 2 Luka Brulc , Breda Simonovska , Irena Vovk 1 2 National Institute of Chemistry, Ljubljana, SI; National Institute of Chemistry; EN-FIST Centre of Excellence, Ljubljana, SI Effect of Sample and Matrix Loading on Signal Response in LC-MS Bioanalysis Ken Butchart, Helen Lomax Fortis Technologies Ltd, Neston, GB Precision and Reliability - An Intercontinental Study of Curtain Flow Chromatography 1 1 2 1 1 Anthony Edge , Dominic Foley , Michelle Camenzuli , Luisa Pereira , Harald Ritchie , 2 Andrew Shalliker 1 2 Thermo Fisher Scientific, Runcorn, GB; University of Western Sydney, Sydney, AU Comparison of Different Types of Frits in Packed Capillary Columns Martin Franc, Pavel Coufal Charles University in Prague, Faculty of Science, Prague, CZ Reverse Phase HPLC Retention Behavior of Four Poteins on Different Stationary Phases 1 2 2 Jelena Golushko , Oksana Rotkaja , Edzus Picka 1 2 Institute of Chromatography, Riga, LV; University of Latvia, Riga, LV Optimization of LC Method for Simultaneous Determination of Active Compounds in Milk Thistle Dry Extract and Transfer to UPLC on Sub -2 m and Superficially Porous Phases Natalia Halatcheva, Alexander Stoyanov, Vesela Andreeva, Stefan Avramov Sopharma JSC, Sofia, BG UPLC Performance on a Shoestring, the Adaption of an AOAC LC Method to Rapid Analysis in the Absence of UPLC Hardware Robert Hatfield, Andrew Turner Cefas, Dorset, GB The Development of a Novel Hydrolytically Stable Silica Based Stationary Phase for HPLC 1 2 3 2 Matthias Ide , Frdric Lynen , Pat Sandra , Pascal Van Der Voort 1 2 3 University Ghent/Mesosol, Ghent, BE; University Ghent, Ghent, BE; University Ghent/RIC, Ghent, BE Faster and Improved HPLC Separations within Pharmacopeia Guidelines 1 2 Siji Joseph , Udo Huber 1 2 Agilent Technologies, Bangalore, IN; Agilent Technologies, Waldbronn, DE High Temperature Water Chromatography a Green Method for the Analysis of Bioactive Compounds in Birch Bark extracts Firas Jumaah, Charlotta Turner, Margareta Sandahl Lund University, Lund, SE 78
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Separation of Compounds of Biological Interest on the Diamond Analytics Flare Mixed Mode Column 1 1 2 2 2 Supriya S. Kanyal , Bhupinder Singh , Michal A. Vail , Andrew E. Dadson , Andrew J. Miles , 1 2 Matthew R. Linford , David Jensen 1 2 Brigham Young University, Provo, US; Diamond Analytics, Orem, US A Mix-model HPLC Stationary Phase with Reverse-phase Adsorption and Anionexchange mechanisms Yin Lei, Yang Zhao, Wan Wang Bonna-Agela Technologies, Tianjin, CN An Affinity Protein a Column for Monoclonal Antibody (MAb) Titer Analysis Shanhua Lin, Kelly Flook, Yuanxue Hou, Hongmin Zhang, Charanjit Saini, Srinivasa Rao, Yury Agroskin, Chris Pohl Thermo Fisher Scientific, Sunnyvale, US Silica Surface Hybrid Material with Chemical Stability over a Wide pH Range for Reversed Phase Chromatography Cecilia Mazza, Fredrik Lim, Robert Fredriksson, Emelie hgren, Bernt Larsson Akzo Nobel PPC AB, Bohus, SE High Performance Chelation Ion Chromatography of Alkaline Earth, Transition and Lanthanide Metal Cations Using a New IDA-Silica Core-Shell Stationary Phase 1 1 2 3 Nicola McGillicuddy , Ekaterina Nesterenko , Pavel N. Nesterenko , Jesse O. Omamogho , 3 4 Jeremy D. Glennon , Brett Paull 1 2 Irish Separation Science Cluster, Dublin City University, Dublin, IE; Australian Centre for 3 Research on Separation Science, University of Tasmania, Hobart, IE; Irish Separation Science 4 Cluster, University College Cork, Cork, IE; Australian Centre for Research on Separation Science, University of Tasmania, Hobart, AU Bed-Extrusion Based Method for the Evaluation of Packing Morphology in Analytical UHPLC Columns Tibor Mllner, Kristof Hormann, Ulrich Tallarek Philipps-Universitt Marburg, Marburg, DE Development of Core Shell Particle with Large Pore for Separation of Peptides and Proteins 1 1 2 3 4 Norikazu Nagae , Tomoyasu Tsukamoto , Alessandro Baldi , Anders Grahn , Ralf Jutvik 1 2 3 ChromaNik Technologies Inc., Osaka, JP; Protea Biosciences, Morgantown, US; Biotech AB, 4 Onsala, SE; Biotech AB, Insala, SE Synthesis and Use of a Thiol Terminated Reaction Column for the Determination of Iodine Catherine Rimmer, Peter Howell National Institute of Standards and Technology, Gaithersburg, US Post Column Derivatisation Using Reaction Flow Chromatography 1 1 1 1 1 Andrew Shalliker , Arianne Soliven , Maryanne Selim , Michelle Camenzuli , Gary Dennis , 2 Harald Ritchie 1 2 University of Western Sydney, North Parramatta, AU; ThermoFisher Scientific, Runcorn, GB Preparation of Crown-Ether Derivatives with Allylsilylated H8-BINOL Skeleton Acting as Chiral Stationary Phases for HPLC and their Applications to Optical Resolution of Amino Acids 1 2 1 Shunsuke Hirata , Keiji Nishihara , Toyoshi Shimada 1 2 Nara National College of Technology, Nara, JP; Daicel Corporation, CPI Company, Hyogo, JP
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An Extensive Characterization of the Diamond-Based Flare Mixed-Mode Column 1 2 2 2 2 Bhupinder Singh , David S. Jensen , Andrew E. Dadson , Michael A. Vail , Andrew J. Miles , 1 Matthew R. Linford 1 2 Brigham Young University, Provo, Utah, US; Diamond Analytics, Orem, Utah, US Tri-Peptide Based Stationary Phases for Separation of Bio-Molecules: Chromatographic Insight with Structure Function Relation Makoto Takafuji, Sudipta Ray, Hirotaka Ihara Kumamoto University, Kumamoto, JP A Qbd Approach to Eprosartan Mesylate and its Related Impurities by a Coreshell-LC Method for Ultra Fast, High Resolution, Efficient and Reproducible Analysis 1 1 2 M V N Kumar Talluri , Pradip Kalariya , Vinay D. Gaitonde 1 2 National Institute of Pharmaceutical Education and Research, Hyderabad, IN; Biotech India Pvt. Ltd, Mumbai, IN On-Line Post-Column Derivatization of Amino Acids in Capillary Liquid Chromatography 1 2 2 2 Ji Vojta , Anna Kubkov , Martin Franc , Pavel Coufal 1 2 Charles University in Prague, Faculty of Science, Prague, CZ; Charles University in Prague, Faculty of Science, Department of Analytical chemistry, Prague, CZ Separation of Different Classes of Herbicides at pH 2 and pH 12 on the Diamond Analytics Flare Mixed-Mode Column 1 1 2 2 2 Landon A. Wiest , Bhupinder Singh , David S. Jensen , Andrew E. Dadson , Michael A. Vail , 1 Matthew R. Linford 1 2 Brigham Young University, Provo, UT, US; Diamond Analytics, Orem, UT, US Detection and Quantification of Inorganic Arsenic in Fruit Juices by Capillary Ion Chromatography Using 4 m Columns Hua Yang, Linda Lopez ThermoFisher Scientific, Synnyvale, CA, US Development of a High Temperature LC Method for Estrogens and Androgens for LCIRMS Eva de Rijke, Paul Zoontjes, Hennie van Rossum, Saskia Sterk RIKILT Wageningen UR, Wageningen, NL The Utility of 2.5m UHPLC/HPLC Columns for Laboratory Performance Emelie hgren, Cecilia Mazza, Luba Nilsson, Terese Tran Akzo Nobel PPC AB, Bohus, SE Evaluation of Five Core Shell Columns Based on Both Separation Behavior and Physical Property 1 1 1 2 2 Nagae Norikazu , Tomoyasu Tsukamoto , Vinay Gaitonde , Anders Grahn , Ralf Jutvik 1 2 ChromaNik Technologies Inc., Osaka, JP; Biotech AB, Onsala, SE Active Flow Management Coupled to Monolithic Columns 1 1 2 1 1 Luisa Pereira , Dominic Foley , Arianne Soliven , Anthony Edge , Harald Ritchie , Andrew 2 Shalliker 1 2 Thermo Fisher Scientific, Runcorn, GB; University of Western Sydney, Sydney, AU A Novel Approach for Preparation of Porous Layer Open Tubular Capillary Columns Using Polymerisation Mixture Displacement with an Immiscible Liquid Radim Knob, Michael C. Breadmore, Rosanne M. Guijt, Jan Petr, Mirek Macka University of Tasmania, Hobart, AU
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80
ENVI01_MO
Environmental
Optimization of a Solid Phase Extraction Combinated with Liquid Chromatography Tandem Mass Spectrometry Procedure to Simultaneous Determination of Pharmaceuticals Compounds in Water Samples Cristina Afonso-Olivares, Zoraida Sosa-Ferrera, Cristina Fernndez-Rodrguez, Jos Miguel DoaRodrguez, Jos Juan Santana-Rodrguez Universidad de Las Palmas de Gran Canaria, Las Palmas de G.C., ES Semi-Targetted Screening of Pharmaceutically-Related Contaminants in the Thames Tideway Using Liquid Chromatography-High Resolution Mass Spectrometry 1 1 2 3 3 3 Edge Anthony , Luisa Pereira , Claudia Martins , Kelly Munro , Leon Barron , David Cowan 1 2 3 Thermo Fisher Scientific, Runcorn, GB; Thermo Fisher Scientific, Villebon, FR; King's College London, London, GB Hydrophilic Interaction Liquid Chromatography in Very Sensitive HPLC-MS/MS Methods for the Determination of Neurotoxic Domoic Acid in Lagoon Samples 1 2 2 2 1 Elena Barbaro , Roberta Zangrando , Silvia Rossi , Carlo Barbante , Andrea Gambaro 1 2 University Ca' Foscari Venice, Venice, IT; Institute for the Dynamics of Environmental Processes CNR, Venice, IT Comparison of the Efficiency of Three Extraction Techniques for the Determination of Quinolone Antibiotic Derivatives in Sewage Sludge Samples Noem Dorival-Garca, Alberto Zafra-Gmez, Francisco Javier Camino-Snchez, Alberto Navaln, Jos Luis Vlchez University of Granada, Granada, ES Silica Supported Fe3O4 Magnetic Nanoparticles for Magnetic Solid Phase Extraction and Magnetic In-Tube Solid Phase Microextraction: Application to Organophosphorus Compounds Rodrigo Gonzlez Fuenzalida, Yolanda Moliner Martnez, Carmen Molns Legua, Helena Prima Garca, Antonio Ribera, Pilar Campns Falc, Eugenio Coronado Universitat de Valncia, Burjassot, ES Improved PAH Analysis with an Automated Sample Pretreatment On-Line SPE Method Vincent Goudriaan Shimadzu Benelux BV, 's-Hertogenbosch, NL Trace Level Analysis of Herbicides in Drinking and Surface Water by Online-SPE LC/Triple Quadrupole MS to the Lower ppt Range Angelika Gratzfeld-Huesgen, Edgar Naegele Agilent Technologies, Waldbronn, DE Ultra-High Performance Chromatography with Mass Spectrometry Detection (UHPLC-MS/MS) for the Determination of Fifteen Hormonal Compounds in Sewage from Wastewater Treatment Plants of Gran Canaria (Spain) Rayco Guedes-Alonso, Zoraida Sosa-Ferrera, Jos Juan Santana-Rodrguez Universidad de Las Palmas de Gran Canaria, Las Palmas de G.C., ES Study of Photocatalytic Degradation of a Non-Ionic Surfactant (Triton X-100) by Ultrahigh-Performance Liquid Chromatography Erzsebet Szabo-Bardos, Peter Hegedus, Krisztian Horvath, Zoltan Zsilak, Otto Horvath, Peter Hajos University of Pannonia, Veszprem, HU
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ENVI10_MO
Determination of Endocrine Disrupting Compounds in Fish from Mediterranean Rivers Using Quechers-UPLC-MS/MS 1 2 1 1 2 Anna Jakimska , Belinda Huerta , aneta Bargaska , Agata Kot-Wasik , Sara Rodrguez-Mozaz , 2 Dami Barcel 1 2 Gdask University of Technology, Faculty of Chemistry, Gdask, PL; Catalan Institute for Water Research, Girona, ES UPLC-MS/MS Analysis in Support of Ecotoxicity Studies Ivonne Lammers, Erik Baltussen Theo Noij WIL Research Europe B.V., 's-Hertogenbosch, NL Determination of Inorganic Anions in Municipal Drinking and Waste Water Using High-Pressure Modular Capillary Ion Chromatography Linda Lopez, Carl Fisher, Fei Pang, Terri Christison Thermo Fisher Scientific, Sunnyvale, US Miniaturized Procedure for Estimating DEHP in Sediments Maria Muoz Ortuo, Yolanda Moliner Martinez, Rosa Herraez Hernandez, Jorge Verdu Andres, Javier Pla Tolos, Pilar Campins Falco Universitat De Valencia, Burjassot (Valencia), ES Degradation of Fluoroquinolone Antibiotics and Identification of Metabolites/Transformation Products by LC-MS/MS 1 2 3 4 Alexandra S Maia , Ana R Ribeiro , Catarina L Amorim , Juliana C Barreiro , Quezia B 4 5 6 Cass , Paula ML Castro , Maria Elizabeth Tiritan 1 2 CICS-ISCSN-CESPU, CBQF-ESB-UCP, Gandra - Paredes, PT; CICS-ISCSN-CESPU, CBQF3 ESB-UCP, CEQUIMED-UP, Gandra - Paredes, PT; CBQF-ESB-UCP, CEQUIMED-UP, Porto, 4 5 6 PT; DQ-UFSCar, So Carlos - SP, BR; CBQF/ESB-UCP, Porto, PT; CICS-ISCSN-CESPU, CEQUIMED-UP, Gandra - Paredes, PT Matrix Effect and Sorption Studies of Norfloxacin on Soils Livia Maniero Peruchi, Susanne Rath University of Campinas, Campinas / So Paulo, BR Determination of Personal Care Products and Pharmaceuticals in Reservoir Water in Colombia by Ultra-High Performance Liquid-ChromatographyTandem Mass Spectrometry Carolina Aristizabal-Ciro, Marian Martinez-Zapata, Gustavo Peuela-Mesa Grupo de Diagnstico y Control de la Contaminacin GDCON, Medellin, Antioquia, CO Screening, Quantitation and Confirmation of Pesticide Residues in Environmental Samples by UHPLC-Quadrupole Time-Of-Flight Mass Spectrometry Ana Masi Reyes, Julian Campo, Cristina Blasco, Yolanda Pic University of Valencia, Burjassot, ES LC-MS/MS Analysis of Pharmaceuticals in the Irish Aquatic Environment and their Potential to Bioaccumulate Up the Food Chain 1 1 2 3 4 Gillian McEneff , Brian Kelleher , Leon Barron , Brett Paull , Brian Quinn 1 2 3 Dublin City University, Dublin, IE; Kings College, London, GB; University of Tasmania, 4 Hobart, AU; Galway Mayo Institute of Technology, Galway, IE Multi-Analyte Imprinted Polymer for the Selective Determination of Estrogens in Water Samples Gema Paniagua Gonzlez, Juan Carlos Bravo, M Dolores Picn, Pilar Fernndez National University of Distance, Madrid, ES
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82
ENVI20_TU
Amines in Ultrafine Atmospheric Aerosols: Determination by Liquid Chromatography-Triple Quadrupole Mass Spectrometry Jevgeni Parshintsev, Luis Barreira, Kari Hartonen, Marja-Liisa Riekkola University of Helsinki, University of Helsinki, FI Ultra High Performance Separation of PAHs, Harnessing the Technological Advances of a Novel UHPLC System Wilhad Reuter, Joseph DiCesare PerkinElmer Inc., Shelton, CT, US Two Step Pre-Concentration at Fully Microscale Column Switching Capillary Liquid Chromatography-Mass Spectrometry Allowing Versatile and Sensitive Analysis of Sulfonamides in Aqueous Environmental Samples Lucas Carvalho, Adriel Lima, Rodrigo Padovan, Fernando Lanas, Alvaro Santos-Neto Institute of Chemistry of So Carlos, University of So Paulo, So Carlos, SP, BR Simultaneous Separation of Aliphatic and Aromatic Organic Acids by IonExclusion Chromatography with Photodiode Array Detection and Atmospheric Pressure Chemical Ionization Mass Spectrometry Ludovit Schreiber, Iveta Hukelova, Radoslav Halko Faculty of Natural Sciences Comenius University in Bratisl, Bratislava, SK Determination of Carbonyl Compounds in Biological Samples of Medical Students Population in the Context of Life Style and Tobacco Smoke Exposure Magdalena Szumska, Tomasz Wielkoszyski, Krystyna Tyrpie Medical University of Silesia, Katowice, PL Development and Optimization of an Online SPE-HPLC-FD Method for Quantification of Fluoroquinolones in Wastewater Effluents 1 2 1 3 4 Bernardo Meira , Alexandra S Maia , Virgnia MF Gonalves , Ana R Ribeiro , Maria E Tiritan 1 2 CICS-ISCSN-CESPU, Gandra - Paredes, PT; CICS-ISCSN-CESPU, CBQF-ESB-UCP, Gandra 3 4 Paredes, PT; CICS-ISCSN-CESPU, CBQF-ESB-UCP, CEQUIMED-UP, Gandra - Paredes, PT; CICSISCSN-CESPU, CEQUIMED-UP, Gandra - Paredes, PT Sorption of Enrofloxacin in Sub-Tropical Brazilian Soils Alessandra Vieira, Anne Hlne Fostier Unicamp, Campinas, BR Simulation and Analysis of Xenon Outflow Behavior Under Multi-Pulse Injection in Dimensional Chromatography ShuJiang Liu, ZhanYing Chen, YinZhong Chang, ShiLian Wang, Qi Li, YuanQing Fan CTBT Beijing National Data Center &Radionuclide Laboratory, Beijng, CN LC-MS/MS Method for the Determination of Parabens in Compost Samples. Comparison of the Efficiency of Two Extraction Techniques Noem Dorival-Garca, Julio Csar Bentez-Villalba, Alberto Zafra-Gmez, Francisco Javier Camino-Snchez, Jos Luis Vlchez University of Granada, Granada, ES Study of the Influence of Temperature and Precipitations on the Levels of BETX in Natural Waters Rodrigo Gonzlez Fuenzalida, Yolanda Moliner Martnez, Rosa Herrez Hernndez, Jorge Verd Andrs, Pilar Campns Falc, Cristina Garrido Palanca, Carmen Molns Legua Universitat de Valncia, Burjassot, ES
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High- and Ultra-High-Performance Chromatography with Mass Spectrometry Detection Method for the Determination of Pharmaceutical Compounds in Wastewater Effluents from Wastewater Treatment Plants of Gran Canaria (Spain) Rayco Guedes-Alonso, Cristina Afonso-Olivares, Sarah Montesdeoca-Esponda, Zoraida SosaFerrera, Jos Juan Santana-Rodrguez Universidad de Las Palmas de Gran Canaria, Las Palmas de G.C., ES Sorption of Sulfonamides on Brazilian Soils Livia Maniero Peruchi, Keity Margareth Doretto, Susanne Rath University of Campinas, Campinas, So Paulo, BR
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Food
Sample Preparation with Molecularly Imprinted Polymers (MIP) SPE for Phenolic Compounds (Paraben, Guaiacol and Carsonic Acid) Sami Bayoudh, Delphine Derrien, Kaynoush Naraghi Polyintell, Val De Reuil, FR Evaluation of Herb and Fruit Juice Adulteration and Authenticity by Coulometric Array Detection and Pattern Recognition Analysis Bruce Bailey, Qi Zhang, Marc Plante, David Thomas, Ian Acworth Thermo Fisher Scientific, Chelmsford, US Fast, Simple, and Reproducible SPE Cleanup of Corn, Wheat, and Peanut Extracts Prior to HPLC Analysis for Mycotoxins 1 2 1 1 1 1 Dave Bell , Frank Michel , Emily Barrey , Ken Espenschied , Matilal Sarker , Michael Ye , Olga 1 Shimelis 1 2 Sigma-Aldrich/Supelco, Bellefonte, PA, US; Sigma-Aldrich/Supelco, Taufkirchen, DE HPLC/MS Analysis of Phenolic Compounds in Green Tea and Correlation with their Antioxidant Capacity Lenka Ceslova, Petr Cesla, Petra Dinisova, Iva Nedopilova, Jan Fischer University of Pardubice, Department of Analytical Chemistry, Pardubice, CZ Determination of Phytochemical Compounds in Litchi (Litchi chinensis Sonn)-flowerwater-extract by HPLC and its Anti-obesity Effect 1 1 2 1 2 Chih-Hsien Chiu , Yi-Chen Chen , Deng-Jye Yang , Yi-Sheng Wu , Yi-Ling Lin 1 2 National Taiwan University, Taipei, TW; Chung Shan Medical University, Taichung, TW Determinations of Inorganic Anions and Organic Acids in Beverages Using Suppressed Conductivity and Charge Detection Terri Christison, Linda Lopez Thermo Fisher Scientific, Sunnyvale, CA, US Determination of Aflatoxins in Spina Date Seed by High Performance Liquid Chromatographywith Post-Column Derivatization Xiongxiong Qiu, Hui Gao, Chao Ma, Caiyong Lin, Yin Huo, Song Zhan, Taohong Huang, Yuki Hashi Shimadzu (China) Co.,Ltd., Beijing, CN Analysis of Black Tea by High-Resolution UPLC-MS Boudewijn Hollebrands, Christian Grn Unilever R&D Vlaardingen, Vlaardingen, NL Antioxidant Activity and Anticancer Effect of Ethanolic and Aqueous Extracts of the Roots of Ficus Beecheyana and their Active Components 1 2 3 1 Chin-Lin Hsu , Yu-Shan Yu , Gow-Chin Yen , Wei-Tang Chang 1 2 School of Nutrition, Chung Shan Medical University, Taichung, TW; Health Bureau, Taichung 3 City Government, Taichung, TW; Department of Food Science and Biotechnology, National Chung, Taichung, TW 84
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Evaluation of Dispersive and Cartridge SPE Clean-up Procedures Using the Modified QuEChERS Method for Determination of Pesticide Residues in Strawberries by UHPLC-DAD Isabel Jardim, Daniele Oshita Institute of Chemistry/UNICAMP, Campinas, BR Variability of Matrix Effects in Multi-Residue Analysis of Pesticides in Lettuce Using QuEChERS with Different Extraction Solvents and Salts Isabel Jardim, Fernanda Begnini Institute of Chemistry/ UNICAMP, Campinas, BR Validation of a Method for Pesticide Residues Screening in Food Using UPLC-QTOF MS and Automated Data Processing Software 1 2 2 2 2 Jean-Marc Joumier , Sara Stead , Dominic Roberts , Michael McCullagh , Ramesh Rao , Monica 3 4 Garcia Lopez , Richard Fussell 1 2 3 Waters EHQ, St Quentin en Yvelines, FR; Waters Corp, Manchester, GB; Food and 4 Environment research agency, York, GB; Food and Environment research agency, St Quentin en Yvelines, GB Determination of Prenylflavonoid and Hop Bitter Acid in Brewer's Yeast Biomass by HPLC-DAD-MS Tsai Hua Kao, G. Y. Wu Fu Jen Catholic University, New Taipei City, TW On-Line SPE-UHPLC-UV/VIS Method for Determination of 11 Illegal Dyes in ChiliContaining Spices Maria Khalikova, Dalibor Satinsky, Tereza Smidrkalova, Hana Sklenarova, Petr Solich Charles University in Prague, Hradec Kralove, CZ Isolation and Identification of Major Antioxidant Components of Litchi Flower Chao-Tian Lin, Deng-Jye Yang, Yan-Zin Chang, Chuan-Hsiang Hsu Chung Shan Medical University, Taichung, TW Analysis of B Vitamins from Feed with Liquid Chromatography Tandem Mass Spectrometry 1 1 1 Marja Lahti , Pertti Koivisto , Kimmo Peltonen 1 Finnish Food Safety Authority Evira, Helsinki, FI A Sensitive Online Enrichment System Based on Fractionized Sampling and Stacking Strategy Coupled with Ultra-High Performance Liquid Chromatography for Ultratrace Analysis of 24-Epibrassinolide in Plant Samples 1 1 1 Jialiang Pan , Yuling Hu , Gongke Li 1 Department of Chemistry, Sun Yat-sen University, Guangzhou, CN Determination of Perchlorate Levels in Food and Soil Samples Using Accelerated Solvent Extraction and Ion Chromatography 1 1 1 1 Linda Lopez , Carl Fisher , Bruce Richter , Brett Murphy 1 Thermo Fisher Scientific, Sunnyvale, US Selective Online SPE via Dynamic Covalent Hydrazine Chemistry for Determination of Zearalenone in Edible Oils 1 1 2 Silvia Marten , Stefan Risch , Julia Heinze 1 2 Wissenschaftlicher Gertebau Dr. KNAUER GmbH, Berlin, DE; Beuth University of Applied Science, Berlin, DE Carotenoid Composition of Different Kinds of Raw and Processed Pumpkins (Cucurbitaceae) Krisztina Marton, Erika Turcsi, Ferenc Kilr, Jzsef Deli University of Pcs, Pcs, HU 85
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A Confirmatory Method for the Determination of Histamine Levels in Fishery Products by HPLC/FLD with Post-Column Derivatization 1 1 2 1 Marilena Muscarella , Sonia Lo Magro , Carmen Palermo , Antonio Armentano 1 2 IZS della Puglia e della Basilicata, Foggia, IT; Dipartimento di scienze Agro-Ambientali, Chimica e Difesa vegetale Universit degli Studi Foggia, Foggia, IT Highly Sensitive LC-MS/MS Analysis of Imidazole Compounds Derived from Caramel Colorants in Drinks 1 1 1 1 1 Yasushi Nagatomi , Rinako Hagino , Tomonori Inoue , Atsuo Uyama , Naoki Mochizuki 1 Asahi Group Holdings, Ltd, Moriya, JP Development of Method for Extraction and Chromatographic Determining of Free Sugars in Green Coffee Beans 1 1 1 1 Leonel V. Constantino , Tiago B. Madeira , Cyntia H. G. Alves , Brbara S. Caldas , Elisa Y. 1 1 Hirooka , Suzana Lucy Nixdorf 1 Universidade Estadual de Londrina, Londrina, BR Determination of Macrolide Antibiotics in Sheeps Milk by Molecularly Imprinted Solid Phase Extraction Coupled with High-Performance Liquid Chromatography- UV Diode-Array Detection 1 1 1 Gema Paniagua Gonzlez , Asuncin Garca Mayor , Rosa Mara Garcinuo Martnez , Pilar 1 1 Fernndez Hernando , Jess Senn Durand Alegra 1 National University of Distance, Madrid (Spain), ES Determination of Silicate in Foods by High Performance Liquid Chromatography 1 1 1 1 1 Se Jong Park , Jae Chon Choi , Ho Soo Lim , Su Jin Jang , Meehye Kim 1 Ministry of Food and Drug Safety, Chungcheongbuk-do, KR Determination of Heterocyclic Aromatic Amines in Beefburguers by Using Microwave-Assisted Extraction (MASE) and Dispersive Liquid-Ionic Liquid Microextraction (DLILME). Optimization of the DLILME by Using a Central Composite Design Procedure 1 1 1 1 Mario Reta , Leidy Bibiana Agudelo Mesa , Juan Manuel Padr , Alicia Califano 1 Fac. de Ciencias Exactas, Universidad Nacional de La Plata, La Plata, AR Determination of Bisphenol A(BPA) in Drinking Water by HPLC-FLD 1 1 1 1 1 Hande Ozbay , Hande Sarman , Deniz Sarica , Serpil Tasdelen , Ustun Ezer 1 Losev Food Research Lab, Ankara, TR Authenticity and Quality Analysis of Virgin Olive Oils Thermal Treatment Analysis Sonja Schneider Agilent Technologies, Waldbronn, DE Identification and Quantification of 1,3-dimethylamylamine (DMAA) in Food Supplements by Liquid Chromatography Tandem Mass Spectrometry Eva Stejskalov, Radim tpn, Petr Cuhra, Martin Kubk Czech Agriculture and Food Inspection Authority, Prague, CZ Investigation of the Occurrence of Vitamin E Isomers, Based on an Innovative Quechers Extraction Procedure Combined with Ultra Pressure Liquid Chromatography and Fluorescence Detection 1 2 2 1 2 Babette Vanberghen , Catarina L. Silva , Jorge Pereira , Karel Dekoninck , Jos S. Cmara 1 2 Katholieke Hogeschool Kempen, Geel, BE; CQM, UMa, Funchal, PT a
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HPLC Separation of Flavanols and Methylxanthines on two C18 Core-Shell Columns 1 2 1 Vesna Glavnik , Breda Simonovska , Irena Vovk 1 2 National Institute of Chemistry, EN-FIST Centre of Excellenc, Ljubljana, SI; National Institute of Chemistry, Ljubljana, SI
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A New Method for the Separation of the Protein Fractions Prolamin and Glutelin in Cereal Grain by Modified SE-HPLC and SDS-PAGE 1 1 2 1 Stefanie Wroblewitz , Liane Hther , Hermann Wtzig , Sven Dnicke 1 2 Fredrich-Loeffler-Institute, Institute of Animal Nutrition, Braunschweig, DE; Technische Universitt Braunschweig, Institute of Medicinal and Pharmaceutical Chemistry, Braunschweig, DE Determination of Quality Indicators and Antioxidant Content in Various Fruit Juices 1 Blanka vecov , Kateina Andrlov University of Pardubice, Pardubice, CZ Development of a Dispersive LiquidIonic Liquid Microextraction Method for the Determination of Nifurtimox and Benznidazole in Human Breast Milk 1 1 1 1 Mario Reta , Juan Manual Padr , Roco Pellegrino Vidal , Leidy Bibiana Agudelo Mesa , Alicia Califano, Mara Elena Marsn, Guido Mastrantonio Fac. de Ciencias Exactas, Universidad Nacional de La Plata, La Plata, AR The Use of Microflow UHPLC in Mycotoxin Analysis Stephen Lock AB SCIEX, Pudsey, GB
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Forensic
Multiclass Detection and Quantification of Drugs of Abuse in Biological Samples Based on the Combination UHPLC-MS/MS with Microextraction Techniques Diego Airado-Rodrguez, Manuel Lombardo-Ag, Carmen Cruces-Blanco, Ana Mara GarcaCampaa University of Granada, Granada, ES Determination of the Nitrogen Content of Nitrocellulose by Capillary Electrophoresis after Alkaline Denitration 1 2 3 3 2 Elodie Alinat , Nathalie Delaunay , Christine Costanza , Xavier Archer , Pierre Gareil 1 2 PECSA/Central Laboratory of the Prfecture De Police of Pari, Paris (France), FR; Laboratory of Physicochemistry of Electrolytes, Colloids, and Analytical Sciences (PECSA), Paris (France), FR; 3 Central Laboratory of the Prfecture De Police of Paris, Paris (France), FR Microwave-Assisted Extraction Followed by the Chromatographic Determination of Antidepressants in Plasma Antonia M Carro, Rosa A. Lorenzo, Mara Regenjo, Ana Bermejo, Purificacin Fernndez University of Santiago De Compostela, Santiago De Compostela, ES Capillary Electrophoresis in Combination with Laser Induced Fluorescence Detection for the Sensitive Analysis of LSD and ISO-LSD in Human Hair Samples Diego Airado-Rodrguez, Maykel Hernndez-Mesa, Carmen Cruces-Blanco, Ana Mara GarcaCampaa University of Granada, Granada, ES Highly Sensitive Capillary Electrophoresis-Mass Spectrometry for Rapid Screening and Accurate Quantitation of Drugs of Abuse in Urine 1 1 2 1 Isabelle Kohler , Julie Schappler , Martin Greiner , Serge Rudaz 2 University of Geneva, Geneva 4, CH; Agilent Technologies, Waldbronn, DE Determination of Nimetazepam and 7-Amino Nimetazepam in Human Urine Using LCMS/MS 1 2 2 Kuang-Chuan Wang , Jen-Der Wu , Ching-Kuo Lee 1 2 Forensic Science Division, Criminal Investigation Bureau, Taipei, TW; School of Pharmacy,Taipei Medical University, Taipei, TW 87
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UPLC-PDA and Dispersive Liquid-Liquid Microextraction for Determination of Drugs of Abuse in Human Plasma 1 1 1 2 1 Rosa A Lorenzo , Antonia M Carro , Mara Regenjo , Ana M. Fernndez , Purificacin Fernndez 1 2 University of Santiago De Compostela, Santiago De Compostela, ES; 2Drug Addiction Health Care Unit, Monforte De Lemos, ES Exploring Low and High pH Eluents Using a New Silica-Based Extended pH Range C18 Column for Analysis of Amphetamines & Opiates from Urine by LC-MS 1 2 Alan Mckeown , Carl Zimmerman 1 2 Advanced Chromatography Technologies Ltd, Aberdeen, Scotland, GB; macmod Analytical Inc., Chadds Ford, Pa 19317, US LC-MS/MS Method for the Determination of 21 Opiates and Opiate Derivatives in Urine Luisa Pereira, Joanne Jones, Steve Westwood, Tim Liddicoat, Tony Edge Thermo Fisher Scientific, Runcorn, GB Confirmation of the Presence of Gunshot Residue by Means of Organic Compounds Using Time of Flight Mass Spectrometry Alicia Sanchez, Sandra Benito, Zurie Abrego, Nora Unceta, Maria Aranzazu Goicolea, Ramon J. Barrio University of the Basque Country, Vitoria-Gasteiz, ES Novel UPLC Columns for the Analysis of Synthetic Cannabinoids and Metabolites in Whole Blood for Forensic Toxicology Mia Summers, Jonathan Danaceau, Erin Chambers, Kenneth Fountain Waters, Milford, Ma, US Cation-Selective Exhaustive Injection and Sweeping MEKC for Analysis of Methadone and its Metabolites in Serum of Heroin Addicts Shou-Mei Wu Kaohsiung Medical University, Kaohsiung, TW
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FUND01_MO
Fundamentals
Predicting Chromatographic Gradient Elution of Acid-Base Compounds with Simplified Models Axel Andrs, Mart Ross, Elisabeth Bosch Departament de Qumica Analtica, Universitat de Barcelona, Barcelona, ES Influence of Wide Pore Size Distribution in Size-Exclusion Chromatography Ivett Bacskay, Annamria Sepsey, Attila Felinger University of Pcs, Pcs, HU Microstructural Characterization of Random Hard-Sphere Packings Using Pore-Size Entropy Vasili Baranau, Dzmitry Hlushkou, Siarhei Khirevich, Ulrich Tallarek Philipps-Universitt Marburg, Marburg, DE Monodisperse Particles in HPLC Columns 1 1 1 1 1 David Bell , Richard Henry , William Cambell , William Betz , Carmen Santasania , Anders 2 1 1 1 Fridstrom , Frank Michel , Gaurang Parmar , Roy Eksteen 1 2 Sigma-Aldrich/Supelco, Bellefonte, PA, US; Sigma-Aldrich/Supelco, St. Gallen, CH The Scientist Is No Longer in the Laboratory, but Integrated in the Overall Quality Process Peter Boogaard Industrial Lab Automation, Moordrecht, NL 88
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Multiresidue Determination of Pesticides in High Water Content Vegetable and Fruits by LC-MS/MS and GC-MS/MS Hande Ozbay, Hande Sarman, Deniz Sarica, Serpil Tasdelen, Ustun Ezer LOSEV Food Research Lab, Ankara, TR Transfer Prediction from HPLC to UHPLC by Using Modelling Software 1 1 2 Frdric Goldschmidt , Barbara Channer , Imre Molnr 1 2 Actelion Pharmaceuticals Ltd., Allschwil, CH; Molnr-Institute, Berlin, DE Validated Gradient Stability Indicating HPLC Method for Determining Diltiazem Hydrochloride and Related Substances in Bulk Drug and Novel Tablet Formulation Vivekanand Chatpalliwar, Pawan Porwal, Santosh Chajjed SNJB's SSDJ College of Pharmacy, Chandwad, IN Determination and Comparison of Geniposide Content Following Oral Administration of Geniposide, Gardenia Jasminoides Ellis, and Gardenia Herbal Formulation in Rats by High Performance Liquid Chromatography 1 2 1 1 Sharleen Cheng , Lie-Chwen Lin , Chi-Hung Lin , Tung-Hu Tsai 1 2 National Yang-Ming University, Taipei, TW; National Research Institute of Chinese Medicine, Taipei, TW Computer Organized Screening and Method Optimization System Phase 2 (COSMOS 2) 1 2 2 2 3 Gabriela Cimpan , Rudy Sneyers , Jeroen Peeters , Vivienne Malanchin , Andrey Vazhentsev 1 2 Advanced Chemistry Development (ACD/Labs), Bracknell, GB; Janssen Pharmaceutical 3 Companies of J&J, Beerse, BE; Advanced Chemistry Development (ACD/Labs), Moscow, RU A Fundamental Study of Peak Enhancement in Liquid Chromatography Jelle De Vos, Gert Desmet, Sebastiaan Eeltink Vrije Universiteit Brussel, Brussels, BE An Operation Platform for the Automation of Biopolymer Separation by Liquid Chromatography 1 1 1 2 Xindu Geng , Fei Wang , Peng Liu , Huiqiang Zhang 1 2 Northwest University, Xi'an, CN; Northwest, Xi"an, CN Analysis of the Random-Close Packing Limit of Polydisperse Hard-Sphere Packings Vasili Baranau, Ulrich Tallarek Philipps-Universitt Marburg, Marburg, DE A Mathematical Relationship between the Freundlich and the Bilangmuir Isotherms George Horvai Budapest University of Technology and Economics, Hungary, HU Determination of Bioactive Components in Chinese Herbal Formulae and Pharmacokinetics of Rhein in Normal and Constipated Rats by UPLC-MS/MS and Gene Expression Profiling in Drug Metabolizing Genes 1 1 2 3 1 Mei-Ling Hou , Li-Wen Chang , Lie-Chwen Lin , Chi-Hung Lin , Tung-Hu Tsai 1 2 Institute of Traditional Medicine, NYMU, Taipei, TW; National Research Institute of Chinese 3 Medicine, Taipei, TW; Institute of Microbiology and Immunology, NYMU, Taipei, TW Fast Reversed Phase HPLC Method for Content Determination of Insulin Analogues 1 1 1 1 2 Aage Hvass , Karin Juul Jensen , Gillian Danielsen , Jette Christensen , Marianne Nielsen , Rikke 2 Pedersen 1 2 Novo Nordisk A/S, Mlv, DK; Novo Nordisk A/S, Bagsvrd, DK Improving Productivity in Natural Product Compound Isolation Using Isocratic Preparative Liquid Chromatography Jo-Ann Jablonski, Rui Chen Waters Corporation, Milford, MA, US 89
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High Temperature Liquid ChromatographyAerosol Detector Analysis: Effect of Elution Bandwidth on Detection Response Manish Khandagale, Joseph Hutchinson, Gregory Dicinoski, Paul Haddad University of Tasmania - ACROSS, Hobart (Tasmania), AU Screening of Multiple Oxidative Hair Dyes by High Performance Liquid Chromatography Jia Yi Kwang, Kin Har Kiang, Nuan Ping Cheah Health Sciences Authority, Singapore, SG Analysis of Transverse Dispersion in Bulk Structures: Sphere Packings, Regular Pillar Arrays, and Silica Monolith. Anton Daneyko, Dzmitry Hlushkou, Siarhei Khirevich, Ulrich Tallarek Philipps Universitaet Marburg, Marburg, DE Determination of Diuretics in Urine Using Multi-Walled Carbon Nanotubes as Sorbent in Dispersive Solid Phase Extraction Combined with Liquid Chromatography Tandem Mass Spectrometry Maw-Rong Lee, Tse-Tsung Ho National Chung Hsing University, Taichung, TW Spider Diagram: A Universal and Versatile Approach for Chromatographic System Comparison and Classification. Part 1: Solvent Classification Eric Lesellier, Caroline West ICOA, Universit Orlans, Orlans, FR Determination of Molar Mass and Size Distributions of Polymeric and Colloidal Samples by Taylor Dispersion Analysis 1 1 1 2 Herv Cottet , Jean-Philippe Biron , Luca Cipelletti , Michel Martin 1 2 University of Montpellier, Montpellier, FR; ESPCI, Paris, FR Retention Prediction of Ionizable Analytes in RP-HPLC by Organic Modifier Gradients in Different Eluent PHs Chrysostomi Zisi, Stella Fasoula, Ahmed Mansour, Panagiotis Nikitas, Adriani Pappa-Louisi Aristotle University of Thessaloniki, Thessaloniki, GR Comparison between Refractometry, Spectrophotometry and Liquid Chromatography in Determination of Total Free Sugars in Commercial Juices and Nectars of Grape and Orange Leonel Constantino, Cyntia Alves, Brbara Caldas, Elisa Hirooka, Suzana Nixdorf Universidade Estadual de Londrina, Londrina, BR Validated Stability Indicating HPLC Method for Determining Acitretin in Bulk Drug and Pharmaceutical Preparation Pawan Porwal, Vivekanand Chatpalliwar, Jayesh Patil SNJB's SSDJ College of Pharmacy, Nasik (Maharashtra), IN High Through-Put and High Sensitivity Analyses Using Active Flow Technology Chromatography with Mass Spectral Detection. 1 1 2 2 3 2 Andrew Shalliker , Danijela Kocic , Luisa Pereira , Tony Edge , Jackie Mosely , Harald Ritchie , 2 4 Dominique Foley , Xavier Conlan 1 2 University of Western Sydney, North Parramatta, AU; ThermoFisher Scientific, Runcorn, GB; 3 4 Durham University, Durham, GB; Deakin University, Geelong, AU On-Line Determination of Arsenic Species in Rice by High Performance Liquid Chromatography Inductively Coupled Plasma Spectrometry (HPLC-ICP-MS) Pinar Nas, Hande Sarman, Deniz Sarica, Serpil Tasdelen, Ustun Ezer LOSEV Food Research Lab, Ankara, TR 90
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Optimization of Concentration Gradient Analyses for Highly Reproducible Results in VHPLC Joseph Stankovich, Fabrice Gritti, Paul Stevenson, Georges Guiochon University of Tennessee, Knoxville, US SAXS (Small Angle X-Ray Scattering) Investigation of Mesoporous Chromatographic Adsorbents and Correlation with Physisorption Experiments 1 2 3 4 1 Daniela Stoeckel , Dirk Wallacher , Gerald Zickler , Ulrich Tallarek , Bernd Smarsly 1 2 3 Justus-Liebig-University, Giessen, DE; Helmholtz Center, Berlin, DE; Montan-University, 4 Leoben, AT; Philipps-University, Marburg, DE A Rapid HPLC/PDA Method for the Evaluation of Labeling Accuracy of Soy Dietary Supplements Commercially Available in Romania Alina Uifalean, Cristina Iuga University of Medicine and Pharmacy, Cluj-Napoca, RO Imaging of Non-Uniform Motion of Single DNA Molecules Reveals the Kinetics of Varying-Field Isotachophoresis Hailin Wang, Shengquan Liu, Bailin Zhao, Dapeng Zhang, Cuiping Li Research Center for Eco-Environmental Sciences, Beijing, CN Spider Diagram: A Universal and Versatile Approach for Chromatographic System Comparison and Classification. Part 2: Stationary Phases Eric Lesellier, Caroline West ICOA, Universit Orlans, Orlans, FR UHPLC Getting it Right! Considerations for Optimal Performance! Mark Woodruff, Ken Butchart Fortis Technologies Ltd, Neston, GB Screening and Evaluation of Adulterants in 247 Illegal Sexual Performance Enhancement Products Using HPLC-DAD and GC-MS Yimin Xu, Min Yong Low, Yun Zeng Health Sciences Authority of Singapore, Singapore, SG Multilinear Gradient Elution Optimization in Combined pH/Organic Solvent Gradient RP-HPLC Chrysostomi Zisi, Stella Fasoula, Ahmed Mansour, Panagiotis Nikitas, Adriani Pappa-Louisi Aristotle University of Thessaloniki, Thessaloniki, GR Novel Methods for Detection and Quantitation of Impurities Using a New High Sensitivity Photodiode Array Detector Daisuke Nakayama, Yusuke Osaka, Masatoshi Takahashi, Toshinobu Yanagisawa, Junichi Masuda, Okiyuki Kunihiro Shimadzu Corporation, Kyoto, JP
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GLYC01_MO
Glycans
Characterization of Glycans by Capillary-Scale Anion Exchange Chromatography Hyphenated to Ion Trap Mass Spectrometry 1 2 3 1 1 Cees Bruggink , Franck van Veen , Remco Swart , Andr M. Deelder , Manfred Wuhrer 1 2 3 LUMC, Leiden, NL; Thermo Fisher Scientific, Breda, NL; Thermo Fisher Scientific, Amsterdam, NL Comparison of Released N-Glycans between the Innovator and a Candidate Biosimilar: A Case Study on Etanercept. Stephane Houel, Ying Qing Yu, Eoin Cosgrave, Weibin Chen Waters Corp., Milford, US 91
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Oriented Immobilization of PNGase F on a Monolithic Support for Glycoprotein Analysis 1 2 3 1 2 Jana Krenkova , Akos Szekrenyes , Zsolt Keresztessy , Frantisek Foret , Andras Guttman 1 2 Institute of Analytical Chemistry, v.v.i., Brno, CZ; Horvath Laboratory of Bioseparation Sciences, 3 University of Debrecen, Debrecen, HU; Debrecen Clinical Genomics Center, University of Debrecen, Debrecen, HU Development of New Bioaffinity Phases for Glycoprotein Separation and Analysis 1 2 3 4 4 Ruth Larragy , Brendan OConnor , Michael OConnell , Paul Clarke , Roisin Thompson , Damien 3 2 2 2 1 Keogh , Amy Harrington , Norah Cassidy , Colm Cooke , Triona OConnell 1 2 Irish Separation Science Cluster, Dublin, IE; Irish Separation Science Cluster, School of 3 Biotechnology, Dublin, IE; Irish Separation Science Cluster, School of Biotechnology, Dublin, IE 4 ProLegere, Dublin, IE Site-Specific N-Glycosylation Analysis of Human Immunoglobulin E Rosina Plomp, Gerhild Zauner, Paul Hensbergen, Andr Deelder, Manfred Wuhrer Leiden University Medical Centre, Leiden, NL Capillary Electrophoresis with Contactless Conductivity Detector for Myrosinase Activity Assays Reine Nehme, Gregory Roux, Hala Nehme, Patrick Rollin, Arnaud Tatibouet, Philippe Morin Institute of Organic and Analytical Chemistry, Orlans cedex 2, FR Separation of Labeled and Native N-Glycans on a Novel Mixed-Mode Stationary Phase Xiaodong Liu, Udayanath Aich, Christopher Pohl Thermo Fisher Scientific, Sunnyvale, California, US Unambiguous Characterization of Glycosylation Patterns of Monoclonal Antibodies Integrated Use of LC-MS/MS and NMR Techniques Alena Wiegandt, Bernd Meyer Insitute of Organic Chemistry - University of Hamburg, Hamburg, DE Workflow for High-Throughput Negative Ion Mode MALDI-TOF-MS Analysis of Complex N-Glycan Samples Karli Reiding, Dennis Blank, Andr Deelder, Manfred Wuhrer Leiden University Medical Center, Leiden, NL
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HILC01_MO
HILIC
Analysis of Highly Hydrophilic Compounds by Using Inorganic/Organic Hybrid Based Reversed-Phase and HILIC Columns 1 2 2 2 2 Friederike Becker , Noriko Shoji , Takashi Sato , Takatomo Takai , Naohiro Kuriyama 1 2 YMC Europe GmbH, Dinslaken, DE; YMC Co., Ltd., Komatsu, JP Fundamental Investigation Regarding Robustness and Repeatability in HILIC Chromatography David Bell, Craig Aurand, Hugh Cramer, Gaurang Parmar Sigma-Aldrich/Supelco, Belleofnte, PA, US A Comparative Study of Two HPLC Columns in the Determination of Phenoxy Acid Pesticides Sagrario Torres-Cartas, Susana Meseguer-Lloret, Carmen Gmez-Benito, Mnica Catal-Icardo IGIC-Universitat Politnica de Valncia, Gandia (Valncia), ES Determination of Carbamate Pesticides by HPLC-Photoinduced Chemiluminescence Mnica Catal-Icardo, Susana Meseguer-Lloret, Sagrario Torres-Cartas, Carmen Gmez-Benito IGIC-Universidad Politcnica de Valencia, Ganda-Valencia, ES
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Polyanionic Monosized Particles as a Stationary Phase for Hydrophilic Interaction Chromatography Gunes Kibar, Bekir Celebi, Ali Tuncel Hacettepe Uni, Ankara, TR Determination of Paraquat and Diquat in Environmental Samples Using a New High Efficiency Ultraperformance LC Column for HILIC Kenneth Fountain, Jeremy Shia, Michael Young, Mia Summers Waters Corporation, Milford, MA, US Determination of Tartaric Acid in Human Plasma by Hydrophilic Interaction Liquid Chromatography Coupled to Mass Spectrometry Evgueni Fedorov, Michel Coutu, Jean-Franois Larocque, Michael Mancini Biotrial Bioanalytical Services, Laval, QC, CA Development of a Quantitative LC-MS/MS Assay for the Simultaneous Quantitation of Acetylcholine, Histamine, and their Metabolites in Human Cerebrospinal Fluid (CSF) Using Sub 2m HILIC UPLC Kenneth Fountain, Mary Lame, Erin Chambers Waters, Milford, US Do Electronic Cigarettes Help in Quitting Nicotine and Smoking Addiction? Evaluation of Nicotine Content in Zero-Level E-Liquids with the Approach Dilute and Shoot by RPLC-MS/MS and HILIC-MS/MS Pawe Kubica, Kamila Wilczewska, Andrzej Wasik, Agata Kot-Wasik, Jacek Namienik Gdansk University of Technology, Gdansk, PL Comparative Study of Retention Behavior for Water-Soluble Vitamins on Diol-, Triazole- and Sulfobetaine- Modified Silica Columns in HILIC Mode Alexey Lapin Euroscreen SA, Gosselies, BE Using Chromatographic Information to Validate Molecular Docking Estimations. A Case Study 1 2 2 2 Njabulo J. Gumede , Parvesh Singh , Myalowenkosy I Sabela , Khirsna Bisetty , Yolanda Martin3 3 3 4 Biosca , Laura Escuder-Gilabert , Maria Jos Medina-Hernndez , Salvador Sagrado , Sagrario 5 Torres-Cartas 1 2 Departament of Chemistry. Mangosuthu University of Technology, Jacobs, ZA; Departament of 3 Chemistry. Durban University of Technology, Durban, ZA; Departamento de Qumica Analtica, 4 Facultad de Farmacia, Universitat de Valncia, Burjassot, ES; Centro de Reconocimiento Molecular y Desarrollo Tecnol gico (IDM), Unidad mixta Universitat Politcnica de 5 ValnciaUniversitad de Valncia), Valencia, ES; IGIC-Universitat Politcnica de Valncia, Gandia, ES Separation of Polar Compounds in Hydrophilic Interaction Chromatography Mode Using a New, Polymer Based Zwitterionic Stationary Phase Gunes Kibar, Ali Tuncel Hacettepe Uni, Ankara, TR Cyclofructan and Amide Based Stationary Phases for Hydrophilic Interaction Liquid Chromatography 1 1 2 3 1 Kveta Kalikova , Petr Kozlik , Martin Gilar , Daniel Armstrong , Eva Tesarova 1 2 3 Charles Universtiy in Prague, Prague, CZ; Waters Corporation, Milford, US; The University of Texas at Arlington, Arlington, US Evaluation of Different Column Chemistries for Fast Urinary Metabolic Profiling 1 1 1 2 2 Dick-Paul Kloos , Henk Lingeman , Wilfried Niessen , Andr Deelder , Oleg Mayboroda , Martin 2 Giera 1 2 Free University Amsterdam, Amsterdam, NL; Leiden University Medical Center, Leiden, NL 93
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HILC15_WE
Method Development Approaches in HILIC Anthony Edge, Monica Dolci, Luisa Pereira Thermo Fisher Scientific, Runcorn, GB Polar Basic Drugs in Environmental Samples; Improved Analysis Using a New High Efficiency Ultraperformance LC Column for HILIC Kenneth Fountain, Michael Young, Mia Summers Waters Corporation, Milford, MA, US Acetone Based HILIC SPE As an Alternative Approach for Eliminating Matrix Effects in LC-MS. 1 1 1 2 1 Thomas Van Damme , Miroslava Lachov , Frederic Lynen , Roman Szucs , Pat Sandra 1 2 University of Ghent, Ghent, BE; Pfizer Global R&D, Sandwich, GB HPLC-Chemiluminesce for the Determination of Organothiophosphorus Pesticides 1 2 1 1 Mnica Catal-Icardo , Luis Lahuerta-Zamora , Sagrario Torres-Cartas , Susana Meseguer-Lloret 1 2 IGIC-Universidad Politcnica de Valencia, Ganda-Valencia, ES; Universidad CEU-Cardenal Herrera, Moncada-Valencia, ES Evaluation of Amide and C28 Phases for Separation of Hydrophilic Compounds 1 1 1 2 2 Tsukamoto Tomoyasu , Norikazu Nagae , Vinay Gaitonde , Anders Grahn , Ralf Jutvik 1 2 ChromaNik Technologies Inc., Osaka, JP; Biotech AB, Onsala, SE Sample Preparation and Analysis of Pteridines in Urine by Means of UHPLC-FD with Emphasis on their Stability Helena Tomkov, Lucie Novkov Faculty of Pharmacy in HK, Charles University in Prague, Hradec Krlov, CZ Systematic Comparison of Sensitivity between HILIC-MS and RPLC-MS for Analysis of Pharmaceutical Compounds Aurlie Priat, Jean-Luc Veuthey, Serge Rudaz, Davy Guillarme University of Geneva, Geneva, CH A New HPLC-Chemiluminescence Method for the Analysis of MCPB in Water Samples Sagrario Torres-Cartas, Susana Meseguer-Lloret, Mnica Catal-Icardo, Carmen Gmez-Benito IGIC-Universitat Politnica de Valncia, Gandia (Valncia), ES Fit-For-Purpose HPLC Method for Determining the Antibiotic Amikacin in Human Plasma from Patients Using O-Phthalaldehyde - N-Acetyl-L-Cysteine (OPA-NAC) as a Fluorogenic Pre-Column Reagent 1 1 1 Carlos Ezquer-Garin , Yolanda Martn-Biosca , Laura Escuder-Gilabert , Mara Jos Medina1 2 3 Hernndez , Salvador Sagrado , Mnica Catal-Icardo 1 Departamento de Qumica Analtica. Facultad de Farmacia. Universitat de Valncia., Burjassot, 2 ES; Centro Interuniversitario de Reconocimiento Molecular y Desarrollo Tecnolgico. Unidad 3 Mixta Universidad Politcnica de Valencia-Universitat de Valncia., Burjassot, ES; IGICUniversidad Politcnica de Valencia, Ganda, ES
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HRMS01_MO
High-Resolution MS
Determination of Pristine Fullerenes and Surface Functionalized Fullerenes in Environmental Samples by UHPLC-APPI-MS(/MS) Alina Astefanei, Oscar Nez, Encarnacion Moyano, Maria Teresa Galceran University of Barcelona, Barcelona, ES Photodegradation of Tetracycline Antibiotics in Natural Water Samples Anna Jakimska, Kamila Wilczewska, Weronika Hewelt-Belka, Agata Kot-Wasik, Andrzej Wasik, Jacek Namienik Gdask University of Technology, Faculty of Chemistry, Gdask, PL 94
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A Novel High Resolution Fractionation Technique Combined with High Resolution Mass Spectrometry to Identify Toxic Compounds in Estuarine and Marine Waters 1 1 2 2 1 3 Petra Booij , Pim Leonards , Sascha Sjollema , Pim de Voogt , Dick Vethaak , Jeroen Kool , Marja 1 Lamoree 1 2 Institute for Environmental Studies, Amsterdam, NL; University of Amsterdam, Amsterdam, 3 NL; Vrije Universiteit Amsterdam, Amsterdam, NL Gradient Transfer for a Rapid and Efficient Large Scale Isolation of Natural Products on MPLC-UV-ELSD Platform with Enhanced Pressure and Temperature Control Soura Challal, Emerson Ferreira Queiroz, Werner Kloeti, Davy Guillarme, Jean-Luc Wolfender University of Geneva, Geneva 4 (Switzerland), CH A Highly Sensitive Method for the Quantification of Key Oxysterols in Plasma Using Liquid Chromatography with High Resolution Mass Spectrometry Stefania Della Gatta, Daniel Arndt, Mark Bentley Philip Morris International R&D, Neuchtel, CH Development of Qualitative Method for Marker Compounds of Bang-Poong-TongSung-San by Iontrap-Time of Flight (IT-TOF) Mass Spectrometry Han Young Eom, Unyong Kim, Joon Hyuk Suh, Junghyun Kim, Hyun-Deok Cho, Juhee Jung, Yura Jung, Jeong-Rok Youm, Sang Beom Han Chung-Ang University, Seoul, KR Environmentally Friendly Method to Determine Polar Benzotriazoles, Benzothiazoles and Benzenesulfonamides Derivates in Sewage Sludge by Pressurised Hot Water Extraction and Liquid Chromatography-High Resolution Mass Spectrometry Pol Herrero, Francesc Borrull, Eva Pocurull, Rosa Maria Marc Universitat Rovira i Virgili, Tarragona, ES Qualitative and Semi-Quantitative Analysis of Intact Chicken Ovalbumin by HighResolution Native Mass Spectrometry Reveals 59 Proteoforms Arjan Barendregt, Yang Yang, Albert J.R. Heck Utrecht University, Utrecht, NL Elucidation of Degradation Pathway of Ketoprofen and Ibuprofen by UPLC-QTOF-MS Anna Jakimska, Pawe Kubica, Agata Kot-Wasik, Andrzej Wasik, Jacek Namienik Gdask University of Technology, Faculty of Chemistry, Gdask, PL Characterization of Selected Drug Metabolites in Rat Tissues Using Combined Information from UHPLC/ESI-MS/MS and MALDI-MS imaging 1 1 2 1 Robert Jirsko , Michal Holapek , Ivan Vokl , Vitaliy Chagovets 1 2 University of Pardubice, Pardubice, CZ; Faculty of Pharmacy, Charles University, Hradec Krlov, CZ LC-LC-MS/MS Heart-cut Approach for Software assisted Pharmaceutical Impurity Identification from a non-ms compatible LC method 1 2 Siji Joseph , Yuqin Dai 1 2 Agilent Technologies, Bangalore, IN; Agilent Technologies, Santa Clara, US Separation, Identification and Characterization of Stress Degradants and Related Impurities of Bortezomib Using LC and LC-MS/MS M V N Kumar Talluri, Divya Chundi, Srinivas Ragampeta National Instutute of Pharmaceutical Education and Research, Hyderabad/India, IN Use of Liquid Chromatography-High Resolution Mass Spectrometry (LC-HR/MS) in Bioanalytical Assays in Combination with Micro-Sampling of Biological Fluids Monica P. Cala Molina, Juan P. Rincon Pabon, Roland J.W. Meesters Universidad de los Andes, Bogota D.C., CO 95
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HRMS14_TU
Effect-Directed Isolation and Identification of Antibacterial Chelidonium Majus L. Components 1 2 3 4 3 gnes M. Mricz , Emilia Fornal , Wioleta Jesionek , Barbara Majer-Dziedzic , Irena M. Choma 1 2 Plant Protection Institute CAR HAS, Budapest, HU; Chemistry Department and Laboratory of Separation and Spectroscopic Method Applications, Center for Interdisciplinary Research, The 3 John Paul II Catholic University of Lublin, Lublin, PL; Department of Chromatographic Methods, 4 University of Maria Curie-Skodowska, Lublin, PL; Department of Veterinary Microbiology, University of Life Sciences, Lublin, PL Structural Characterization of Biosimilar Therapeutic Monoclonal Antibody by LCMS Marcell Olajos, Zsolt Gengeliczki, Krisztin Lenkey, Katalin Ganzler Gedeon Richter Plc., Budapest, HU Frontal Affinity Chromatography Method for Quick Determination and Characterization of the Inhibitors of Tyrosinase in Complex Mixtures. The Comparison of Capillary-Format Miniaturized Approach and Modified 'Staircase' Frontal Affinity Chromatography. Aleksander Salwiski, Raphal Delpe, David Da Silva, Benot Maunit Institut de Chimie Organique et Analytique, UMR 73, Orlans, FR Bio-Oil Oxygenated Compounds Analysis Using HPLC-MS Methods 1 2 1 2 Martin Sta , Josef Chudoba , David Kubika , Milan Pospil 1 2 Vzkumn stav anorganick chemie, a.s., st nad Labem, CZ; ICT Prague, Prague, CZ Comparison between LC-Full Scan (Orbitrap) MS and Triple Quadrupole MS For Residue and Contaminant Screening in Fruits and Vegetables Pieter Dekker, Paul Zomer, Hans Mol RIKILT, Wageningen, NL Profiling of N-Acylhomoserines and N-Acylhomoserine Lactones Using Automated Sample Preparation and UPLC-UHR-Tof-MS Michael Witting, Jenny Westphal, Juliano Fonseca, Philippe Schmitt-Kopplin Analytical BioGeoChemistry, Helmholtz Zentrum Mnchen, Neuherberg, DE Ultra-Sensitive Determination of 5-Methylcytosine and 5-Hydroxymethylcytosine in Genomic DNA from Hepatocellular Carcinoma Tissues by Capillary HydrophilicInteraction Liquid Chromatography Coupled with Quadrupole Time-Of-Flight Mass Spectrometry Bi-Feng Yuan, Ming-Luan Chen, Fan Shen, Wei Huang, Jia-Hui Qi, Yu-Qi Feng, Song-Mei Liu Wuhan University, Wuhan, CN QTOF Performance Improvements for Qualitative and Quantitative Multi-Target Pesticide Screening in Food 1 1 1 1 2 Petra Decker , Carsten Baessmann , Oliver Raether , Ilmari Krebs , Ellen Scheerbaum , Rebekka 2 3 Loetterle , Robert van der Heijden 1 2 Bruker Daltonik GmbH, Bremen, DE; Chemisches Veterinruntersuchungsamt Stuttgart, 3 Stuttgart, DE; Bruker Daltonics BV, Wormer, NL
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INST01_MO
Instrumentation
Extending the Linear Dynamic Range of Absorbance Detectors Richard Andrews, Peyton Beals Waters Corp., Milford, MA, US
96
INST02_TU
Quantitation of Surfactants in Samples by High Performance Liquid Chromatography and Corona Charged Aerosol Detection Bruce Bailey, Marc Plante, Ian Acworth Thermo Fisher Scientific, Chelmsford, US Determination of Polyacrylic Acid in Boiler Water Using Size-Exclusion Chromatography with Charged-Aerosol Detection 1 2 3 Bruce Bailey , Xiaodong Liu , Mark Tracy 1 2 3 Thermo Fisher Scientific, Chelmsford, US; Thermo Fisher Scientific, Sunnyvale, US; Thermo Fisher Scientific, Sunnvale, US Extending the Limits of Operating Pressure of Normal and Narrow Bore Column Liquid Chromatography Instrumentation 1 1 1 2 1 Ruben De Pauw , Sebastiaan Eeltink , Bart Degreef , Harald Ritchie , Gert Desmet , Ken 1 Broeckhoven 1 2 Vrije Universiteit Brussel, Brussels, BE; Thermo Fisher Scientic, Runcorn, GB Automating pH Manipulation in Reversed-phase Method Development Aparna Chavali, Thomas E. Wheat, Patricia R. Mcconville Waters Corporation, Milford, Us How to Control and Optimize Gradient Elution in Capillary Liquid Chromatography 1 2 1 Enrique Javier Carrasco-Correa , Agustn Acquaviva , Jos Manuel Herrero-Martnez , Guillermo 1 Ramis-Ramos 1 2 Dept. de Qumica Analtica, Universidad de Valencia, Burjassot, Valencia, ES; Facultad de Ciencias Exactas, Universidad Nacional de La Plata, La Plata, AR Trace Determinations of Hexavalent Chromium in Soil Using Automated Extractions and Ion Chromatography 1 1 2 1 1 Terri Christison , Richard Jack , Jinshui Che , Lipika Basumallick , Linda Lopez 1 2 Thermo Fisher Scientific, Sunnyvale, CA, US; Thermo Fisher Scientific, Shanghai, CN Hyphenated HPLC-DAD-MS-SPE-NMR Interface for Identification of Phytochemicals: Application to an Orchid Extract 1 1 1 1 2 Cyril Antheaume , Veronika Cakova , Nicole Rimlinger , Patrick Wehrung , Patrice Andr , 2 1 Frdric Bont Bont , Annelise Lobstein 1 2 Universit de Strasbourg, Illkirch, FR; LVMH-Recherche, Saint-Jean de Braye, FR HPLC NETWORK in Elucidation of Drug Metabolites Matthias Schiell, Markus Kohlmann Sanofi Deutschland GmbH, Frankfurt / Main, DE Use of Variable Pixel Read Time to Improve Performance of Photodiode Array Detectors Joseph DiCesare PerkinElmer Corporation, Shelton, CT, US Development of a Multidimensional Method for Screening Acetylcholinesterase Inhibitors in Crude Plant Extracts 1 2 1 Luciana Freitas , Alexandre Cruz , Cardoso Carmen Lucia 1 2 University of Sao Paulo, Ribeiro Preto, BR; Sinc do Brasil, Ribeiro Preto, BR Analysis of High- and Low-Dosed Vitamins in a Single Run Using the Agilent 1200 Infinity Series High Dynamic Range Diode Array Detector Solution Angelika Gratzfeld-Huesgen Agilent Technologies, Waldbronn, DE
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Highly Sensitive Electrochemical Detector for a Miniaturized Liquid Chromatography System with a Microfluidic Chip Akihiko Ishida, Satoshi Yokogawa, Tatsuya Tanaka, Hirofumi Tani, Manabu Tokeshi Hokkaido University, Sapporo, JP CHROM-COMMANDER, A Software Application for Combining Multiple HPLC Time Bases Sharing one HPLC Autosampler Unit under Dionex Chromeleon Integration Software 1 1 2 Rainer Schmid , Anton Luf , Wolfhardt Freinbichler 1 2 Medical University of Vienna, Vienna, AT; MAYLAB Corp., Vienna, AT Novel, Universal Approach for the Measurement of Natural Products in a Variety of Botanicals and Supplements Bruce Bailey, Marc Plante, Qi Zhang, David Thomas, Ian Acworth Thermo Fisher Scientific, Chelmsford, US HPLC-DAD-SPE-NMR Methodology for Structure Elucidation of Secondary Organic Aerosol (SOA) Products Formed Through Aqueous Phase Photooxidation of Guaiacol 1 1 2 3 Zoran Kitanovski , Irena Grgi , Alen usak , Magda Claeys 1 2 National Institute of Chemistry, Ljubljana, SI; EN-FIST Center of Excellence, Ljubljana, SI; 3 University of Antwerp, Antwerp, BE Relative Response Factor Determination for an HPLC-UV Method Using Nuclear Magnetic Resonance Spectroscopy Lakshmy Nair, Christina Szabo, Catherine Quinn, Michael Koberda, Christopher Cullen, Yakov Genchanok, Karalyn Havel, Xiaohui Yang Baxter Healthcare, Round Lake, US HPLC with Hyphenated Diode Array, Charged Aerosol and Electrochemical Detection Targeting Antioxidants in Apples 1 2 1 Merichel Plaza , Janes Kariuki , Charlotta Turner 1 Lund University, Lund, SE 2 University of Alberta, Camrose, CA Recent Advances in Electrochemical Detection for UHPLC Nico Reinhoud, Hendrik-Jan Brouwer, Jean-Pierre Chervet Antec, Zoeterwoude, NL In-Cell and External Hydrolysis of Biomass for Carbohydrate Determinations Using Automated Solvent Extraction Terri Christison, Richard Carlson, Lipika Basumallick, Linda Lopez Thermo Fisher Scientific, Sunnyvale, CA, US Development and Evaluation of a Microscale UPLC System Thomas Wheat, Daniel Root, Patricia McConville Waters Corporation, Milford, MA, US Computational Flow Study of the Optimal Design and Operating Conditions of the Flow Split Ring Used in Parallel Segmented Flow Columns Wim Smits, Gert Desmet Vrije Universiteit Brussel, Brussels, BE Development of UHPLC Fingerprint Chromatographic Method for Phyllanthus Niruri Employing Quality by Design Approach 1 2 3 1 Ricardo Sprenger , Tiago Loureno , Fernando de Paula , Quezia Cass 1 2 Federal University of So Carlos, So Carlos - So Paulo, BR; Waters Technologies of Brasil, 3 Barueri - So Paulo, BR; Waters Technologies of Brasil, So Carlos - So Paulo, BR
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Quantitation of Trace Level Antibiotics in Minnesota River Water and Wastewater Effluent Using an Automated, Integrated Online-SPE LC-MS/MS System 1 1 2 Dwight Stoll , David Harmes , Klaus Witt 1 2 Gustavus Adolphus College, St. Peter, US; Agilent Technologies, Waldbronn, DE Ensuring Data Quality and Facilitating Rapid LC System Troubleshooting Using a QC Reference Material Mia Summers, Kenneth Berthelette, Kenneth Fountain, Euan Ross Waters Corp, Milford, MA, US Intelligent System Emulation (ISET): New Possibilities in the Field of Method Development and Further Applications Heike Waechtler, Monika Dittmann, Klaus Witt, Konstantin Choikhet, Gerhart Metzler Agilent Technologies, Waldbronn, DE Evaluation between UPLC and HPLC Analytical Methods for Characterizing Natural Dyestuffs 1 1 2 Ana Serrano , Maarten van Bommel , Jessica Hallett 1 2 Rijksdienst voor het Cultureel Erfgoed, Amsterdam, NL; CHAM (Centre for Overseas History), Faculdade de Cincias Sociais e Humanas, Universidade Nova de Lisboa and Universidade dos Aores, Lisbon, PT An Ion Mobility Detector for a High Pressure Liquid Chromatograph Hermann Wollnik, Gary Eiceman, Stephen Davila, Cheng-Hui Yuan New Mexico State University, Dept. Chem & Biochem., Las Cruces, NM, US Latest Improvements in Development of Simple Splitless Gradient Liquid Chromatographic System for Micro and Nano Columns 1 2 2 Jozef estk , Vladislav Kahle , Filip Dua 1 2 Faculty of Chemistry, Brno University of Technology, Brno, CZ; Institute of Analytical Chemistry of the ASCR, v.v.i., Brno, CZ Multiple Switching Device for Complex and Accelerated HPLC Systems 1 1 2 Rainer Schmid , Goran Mitulovic , Hans Mayrhofer 1 2 Dept. Laboratory Medicine, Medical University of Vienna, Vienna, AT; MAYLAB Corp., Vienna, AT
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LCLC
Solid-Phase-Assisted Modulation for Two-Dimensional Liquid Chromatography Anna Baglai, Michelle Camenzuli, Peter Schoenmakers University of Amsterdam, Amsterdam, NL Development and Application of 2D-LC-MS Analysis of Phospholipids 1 2 1 Rbert Berkecz , Viktor Szegedi , Tams Janky 1 2 Department of Medical Chemistry, University of Szeged, Szeged, HU; Institute of Biochemistry, Biological Research Centre, Szeged, HU 2D LC/MS Separation of Tryptic Peptides from Human Serum Proteins Using Reversed-Phase, Strong Cation Exchange, Weak Anion Exchange and Fused Core Fluorinated Stationary Phases 1 1 2 1 Alexander Boichenko , Natalia Govorukhina , Ate van der Zee , Rainer Bischoff 1 2 University of Groningen, Groningen, NL; University Medical Centre Groningen, Groningen, NL Evaluation of Different Polar Stationary Phases for Hydrophilic Interaction Liquid Chromatography for in-depth Proteome Analysis Nhat Bui, Serena Di Palma, Albert J.R. Heck, Shabaz Mohammed Chemistry Department, Utrecht, NL 99
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Optimization of Gradient Conditions in Two-dimensional Liquid ChromatographyMicellar Electrokinetic Capillary Chromatography Separations Petr esla, Jana Vov, Jan Fischer, Pavel Jandera University of Pardubice, Department of Analytical Chemistry, Pardubice, CZ Advances in Hardware for Reliable and Informative 2D-LC Konstantin Choikhet, Herbert Anderer, Uwe Freisler, Klaus Witt Agilent Technologies Germany, Waldbronn, DE LAM: Light-Induced Modulation for One- and Two-Dimensional Liquid Chromatography Henrik Cornelisson-van-de-Ven, Rudy J. Vonk, D.L.J. Broer, Peter J. Schoenmakers University of Amsterdam, Van 't Hoff Institute for Molecular Sciences, Amsterdam, NL Two-Dimensional Liquid Chromatography (RP X HILIC) of Herbal Extracts 1 2 1 1 1 Petra Dinisov , Peter Schoenmakers , Petr esla , Lenka eslov , Jan Fischer 1 2 University of Pardubice, Department of Analytical Chemistry, Pardubice, CZ; University of Amsterdam, Vant Hoff Institute for Molecular Sciences, Amsterdam, NL RPLCRPLC of Dietary Supplements Using an 8-Port Valve Interface 1 2 1 1 Mari Egeness , Hernan Cortes , Emily Hilder , Robert Shellie 1 2 ACROSS, University of Tasmania, Hobart, AU; HJ Consulting LLC, Hobart, US Comprehensive Two-Dimensional Liquid Chromatography (Lcxlc) Coupled with Mass Spectrometry for the Analysis of Fatty Alcohol Derivatives 1 2 2 3 Victoria Elsner , Michaela Wirtz , David Melchior , Oliver J. Schmitz 1 2 University of Wuppertal, Analytical Chemistry, Wuppertal, DE; BASF Personal Care and 3 Nutrition GmbH, Dsseldorf, DE; University of Duisburg-Essen, Applied Analytical Chemistry, Essen, DE Validation of a Rapid Lc-Ms/Ms Method for Determination of Mad Honey Toxins in Rhododendron Ponticum Muammer Kaplan, znur Karaolu, Elmas ktem Olgun Tubitak Mrc Food Institute, Kocaeli, TR Optimization of Gradients in Online Comprehensive Two-Dimensional Liquid Chromatography: Linear Solvent Strength Modeling of Peak-Capacity 1 1 1 2 Rune Grsbll , Jan H. Christensen , Nikoline J. Nielsen , Hans-Gerd Janssen 1 2 University of Copenhagen, Frederiksberg C, DK; University of Amsterdam, Amsterdam, NL Development of a Novel Two-Dimensional HPLC Method in Order to Analyze the Change of Topoisomer Pattern of Supercoiled Plasmid DNA during Fermentation Process 1 1 1 2 Elisabeth Haller , Marek Mahut , Wolfgang Lindner , Michael Laemmerhofer 1 2 University of Vienna, Vienna, AT; University of Tuebingen, Tuebingen, DE Development of a Comprehensive Heart-cut 2D-LC-MS Method for the Analysis and Identification of New Steviol Glycosides in Stevia Rebaudiana 1 1 1 1 2 Stijn Hendrickx , Jari Rubbens , Laura Van Den Bossche , Wesley Vermaelen , Etienne Jooken , 2 1 1 1 Amery Ruis , Erwin Adams , Sebastien Carpentier , Deirdre Cabooter 1 2 KU Leuven, Leuven, BE; KHBO, Oostende, BE HILICRP and RPRP Comprehensive Two-Dimensional Liquid Chromatography Coupling 0.5 mm I.D. Monolithic Microcolumn and Core-Shell Column Tom Hjek, Magda Stakov, Pavel Jandera University of Pardubice, Pardubice, CZ
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100
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Separation Improvements with Orthogonal Chemistries and 2D LC Using Superficially Porous Columns 1 1 1 2 Maureen Joseph , William Long , Jason Link , Andrew Coffey 1 2 Agilent Technologies Inc, Wilmington, US; Agilent Technologies UK Ltd, Church Stretton, GB New Method for the Determination of Pesticides and Insecticides in Water Samples by Large Volume Injection in 2-Dimensional HPLC Carolina Fernndez-Ramos, Dalibor atnsk, Petr Solich Faculty of Pharmacy, Charles University, Hradec Krlov, CZ Validation of Triphenylmethane Dyes and their Metabolites in Fish by Lc-Ms/Ms znur Karaoglu, Elmas ktem Olgun, Muammer Kaplan tubitak Mrc Food Institute, Kocaeli, TR Using of Shift Gradient in Second Dimension to Improve The Separation Space in Comprehensive Two-Dimensional Liquid Chromatography Duxin Li, Oliver J. Schmitz University of Duisburg-Essen, Essen, DE The Qualification of Bi-Dimensional Chromatograms Based on Nearest Neighbors Distances Approach 1 2 2 2 Witold Nowik , Myriam Bonose , Sylvie Heron , Alain Tchapla 1 2 C2RMF, Paris, FR; Univ. Paris-Sud, LETIAM, Orsay, FR Comprehensive Multi-Dimensional Liquid Chromatography Approaches for Application in Effect-Directed Analysis Xiyu Ouyang, Marja Lamoree, Pim Leonards Institute for Environmental Studies, VU University Amsterdam, Amsterdam, NL Two-Dimensional LC and GC-MS: A Combination towards the Evaluation of Potential Geotracers in Saudi Arabian Oil Fields Saroj Panda, Khaled Arouri, Adnan Al-Hajji Saudi Aramco, Dhahran, SA Comparison of Commercial Software Approaches for Quantitation in TwoDimensional Liquid Chromatography Melissa Phillips, Mallory Morris, Benjamin Place, Catherine Rimmer, Lane Sander NIST, Gaithersburg, US Single-Pumped Heart-Cut Bi-Dimensional Liquid Chromatography Applied to the Determination of Surfactants and Block Copolymers Containing Ethylene Oxide Aaron Escrig-Domenech, Miriam Beneito-Cambra, Ernesto F. Simo-Alfonso, Guillermo RamisRamos University of Valencia, Fac. of Chemistry, 4600 Burjassot, ES Data Analysis Workflow for Comprehensive Two-Dimensional Liquid Chromatography (LCxLC) 1 1 2 3 Stephen Reichenbach , Satya Vijay Devarakonda , Edgar Naegele , Qingping Tao , Gerd 4 Vanhoenacker 1 2 3 University of Nebraska, Lincoln, US; Agilent Technologies, Waldbronn, DE; GC Image, LLC, 4 Lincoln, US; Research Institute for Chromatography, Kortrijk, BE Improving Resolution and Sensitivity in Multidimensional Chromatography Daniel Root, Aparna Chavali, Thomas Wheat Waters Corporation, Milford, US On-Line Lcxlc Hyphenation by a Machine Vision Controlled Solvent Evaporation Interface Jan-Willem Schoonen, Paul Vulto, Heiko van der Linden, Thomas Hankemeier Netherlands Metabolomics Centre, Leiden, NL 101
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Data Pre-Processing Technique for Fast Multidimensional High Performance Liquid Chromatography Paul Stevenson, Danielle Bassanese, Xavier Conlan, Neil Barnett Deakin University, Geelong, Victoria, AU Drug Target Deconvolution in Cancer Cells Using Liquid Chromatography, Fluorescence Polarization and Mass Spectrometry 1 1 1 1 2 Tore Vehus , Steven Ray Wilson , Elsa Lundanes , Tyge Greibrokk , Stefan Krauss 1 2 University of Oslo, Oslo, NO; Oslo University Hospital, Oslo, NO HPLC Online SPE Method Analysis Morphine in Compound Glycyrrhiza Preparation Yao Xiao, Lang Li Agilent Technologies (China) Co.,Ltd., Beijing, CN Highly Orthogonal Off-Line Hsax Fractionation for the Analysis of Alternatively Activated Macrophages 1 2 2 2 3 Robert van Ling , Maria Stella Ritorto , Manman Guo , Matthias Trost , Ken Cook 1 2 Thermo Scientific, Breda, NL; MRC Phosphorylation Unit, University of Dundee, Dundee, GB; 3 Thermo Scientific, Hemel Hempstead, GB
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LC-MS Principles
Analysis of Cavitand Derivatives with High Performance Liquid Chromatography Mass Spectrometry Endre Bart, Ibolya Prauda, Viktor Sndor, Ferenc Kilr, Attila Felinger, Ibolya Kiss University of Pcs, Pcs, HU Influence of Column Internal Diameter Upon Chromatographic Performance and Detection Sensitivity in Ultra High Performance LC/MS Analysis Stephan Buckenmaier, Monika Dittmann Agilent Technologies, Waldbronn, DE Experimental Evidence and Characterization of Cobalt(I) Complexes Relevant in Regioselective Diels-Alder Reactions. A Gas Phase Study 1 2 2 2 2 Lukas Fiebig , Julian Kuttner , Gerhard Hilt , Martin C. Schwarzer , Gernot Frenking , Hans1 1 Gnther Schmalz , Mathias Schfer 1 2 Department of Chemistry, Institute of Organic Chemistry, Kln, DE; Fachbereich Chemie, Philipps-University of Marburg, Marburg, DE Fluorous Derivatization Technique for Matrix Effect-Free LC-MS/MS Analysis: Application to Biogenic Amine Analysis 1 1 1 2 1 Tadashi Hayama , Yohei Sakaguchi , Erina Tamashima , Kenichiro Todoroki , Hideyuki Yoshida , 1 1 Hitoshi Nohta , Masatoshi Yamaguchi 1 2 Fukuoka University, Fukuoka, JP; University of Shizuoka, Shizuoka, JP Negative Electrospray Ionisation of Fluorotelomer Alcohols (FTOH) and FTOHDerived Fluoroacrylate Surfactants Using Liquid Chromatography Coupled to Accurate (Tandem) Mass Spectrometry 1 2 3 Xenia Trier , Jan H. Christensen , Wilfried M. A. Niessen 1 2 National Food Institute, Technical University of Denmark, Sborg, Copenhagen, DK; Analytical Chemistry group, Department of Plant and Environmental Sciences, University of Copenhagen, 3 Frederiksberg, DK; Hyphen MassSpec, Leiden and AIMMS Division of BioMolecular Analysis, VU University Amsterdam, Amsterdam, NL
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102
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Novel Methylated Ornithine Lipids in Russian Wetland Planctomycetes 1 1 1 1 2 Ellen Hopmans , Elisha Moore , Irene Rijpstra , Laura Villanueva , Svetlana Dedysh , Hans 3 4 1 Wienk , Frans Schoutsen , Jaap Sinninghe Damst 1 2 NIOZ Royal Netherlands Institute for Sea Research, Den Burg, NL; S. N. Winogradsky Institute 3 of Microbiology, Russian Academy of Sciences, Moscow, RU; Bijvoet Center for Biomolecular 4 Research, Utrecht University, Utrecht, NL; Thermo Fisher Scientific, Breda, NL Analysis of Steroidal Compounds in Wastewater by Liquid Chromatography Mass Spectrometry: Comparison of Different Ionization Techniques Matias Kopperi, Raymundo Lizcano, Kari Hartonen, Marja-Liisa Riekkola University of Helsinki, Helsinki, FI Reduction of Matrix Effects and Improvement of Sensitivity during Determination of Two Polar Pesticide Metabolites by Using LC-MS 1 1 1 2 Sebastian Kowal , Friedrich Werres , Peter Balsaa , Torsten Schmidt 1 2 IWW Water Centre, Mlheim an der Ruhr, DE; university duisburg essen, Essen, DE Permanent Post-Column Infusion as a Challenge of Matrix Effect Compensation in Quantitative LC -MS/MS Analysis of Pharmaceuticals in Sewage of Dresden Julia Rossmann, Robert Gurke, Sara Schubert, Reinhard Oertel, Wilhelm Kirch Institut for Clinical Pharmacology, Technical University, Dresden, DE Identification of Imidacloprid Metabolites in Onion (Allium Wakegi) Using High Resolution Mass Spectrometry and Accurate Mass Tools 1 1 2 2 Michael Thurman , Imma Ferrer , Paul Zavitsanos , Jerry Zweigenbaum 1 2 University of Colorado, Boulder, Colorado, US; Agilent Technologies, Inc., Wilmington, DE, US Fluorous Derivatization Technique for Matrix Effect-Free LC-MS/MS Analysis: Application to Biogenic Amine Analysis 1 1 1 2 1 Tadashi Hayama , Yohei Sakaguchi , Erina Tamashima , Kenichiro Todoroki , Hideyuki Yoshida , 1 1 Hitoshi Nohta , Masatoshi Yamaguchi 1 2 Fukuoka University, Fukuoka, JP; University of Shizuoka, Shizuoka, JP Mass Spectrometric Analysis of the Interaction between Transferrin and Gadolinium Kristina Wentker, Olga Reifschneider, Christoph A. Wehe, Uwe Karst University of Mnster, Mnster, DE Determination of Trace Amounts of Bisphenol A in Human Serum by Liquid Chromatography Coupled with Tandem Mass Spectrometry 1 1 2 1 1 Kamila Wilczewska , Andrzej Wasik , Aleksandra Rutkowska , Pawe Kubica , Agata Kot-Wasik , 1 Jacek Namienik 1 2 Gdask University of Technology, Faculty of Chemistry, Gdask, PL; Medical University of Gdask, Department of Clinical and Exp, Gdynia, PL Quantitative, Antibody-Free LC-MS/MS Analysis of Recombinant Tumor Necrosis Factor-Related Apoptosis-Inducing Ligand (TRAIL) in Serum 1 1 1 1 Daniel Wilffert , Carlos R. Rodrigues dos Reis , Jos Hermans , Natalia Govorukhina , Tushar 2 2 1 1 1 Tomar , Steven de Jong , Wim J. Quax , Nico C. van de Merbel , Rainer Bischoff 1 2 University of Groningen (RUG), Groningen, NL; Universitair Medisch Centrum Groningen (UMCG), Groningen, NL
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103
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Anthocyanin Constituents of Blue and Purple Wheat and their Thermal Stability during Baking 1 1 2 3 4 Alen Albreht , Irena Vovk , Mihaela Skrt , Nataa Poklar Ulrih , Pavel Bartl , Bohuslava 4 Tremlova 1 2 National Institute of Chemistry;EN-FIST Centre of Excellence, Ljubljana, SI; University of 3 Ljubljana, Biotechnical Faculty, Ljubljana, SI; University of Ljubljana, Biotechnical Faculty; Centre of Excellence for Integrated Approaches in Chemistry and Biology of Proteins, Ljubljana, 4 SI; University of Veterinary and Pharmaceutical Sciences Brno, Faculty of Veterinary Hygiene and Ecology, Brno, CZ LC-MS/MS Method Development for the Determination of Triazines and Triazoles Migrating from Food Packaging Materials Zsolt Bodai, Mrton Novk, Zsuzsanna Eke Etvs Lornd University - EKOL, Budapest, HU How to Use Column Characterization Databases to Select Similar/Dissimilar Reversed Phase Columns for Liquid Chromatography? 1 2 Endler Borges , Melvin Euerby 1 2 Universidade Estadual de Campinas, Campinas, BR; Strathclyde Institute of Pharmacy and Biomedical Sciences, Glasgow, GB LC/MS/MS Measurement of Kynurenine Metabolites from Tissue Samples in the Study of Neurological Disorders Associated with Neuroinflammation David Budac, Cayla Vila, Danielle LaBarbiera, Manuel Cajina, Guiying Li, Stephanie Bisulco, Anna Lee, Brian Campbell Lundbeck Research USA, Paramus, NJ, US Determination of 74 Pesticides in Vegetables by Ultra High Performance Liquid Chromatography/Triple Quadrupole Mass Spectrometry 1 1 1 1 1 2 Gao Hui , Yueqi Li , Chao Ma , Hongyuan Hao , Guixiang Yang , Taohong Huang , Shin-ichi 2 2 Kawano , Yuki Hashi 1 2 Shimadzu (China) Co.,Ltd., Beijing, CN; Shimadzu (China) Co.,Ltd., Shanghai, CN Semi-Preparative LC-UV Method for Purification of Compounds by Stacked Injections 1 1 2 Josiane de Oliveira Cardoso , Tiago Venncio , Rosngela Gonalves Peccinini , Ivan da Rocha 3 4 1 Pitta , Maria C. A. Lima , Regina Vincenzi de Oliveira 1 2 Federal University of So Carlos, So Carlos, BR; State University of So Paulo, Araraquara, BR; 3 4 Federal University of Pernambuco, Recife, BR; Federal University of Pernambuco, Brazil, Recife, BR Development of a Novel Method for the Extraction of Norbixin from Whey and its Subsequent Quantification via High Performance Liquid Chromatography 1 2 1 Rachel Campbell , Ilco Boogers , Mary Anne Drake 1 2 NC State University, Raleigh, US; DSM Biotechnology Centre, Delft, NL High-Through-Put LCMS Using Active Flow Technology Chromatography Columns Tony Edge, Dominic Foley, Luisa Pereira Thermo Fisher Scientific, Runcorn, GB Water Soluble Biopolymers as Sampling Medium for Dried Matrix Spot. Lars Erik Eng Eibak, Astrid Gjelstad, Knut Einar Rasmussen, Stig Pedersen-Bjergaard University of Oslo, Oslo, NO Development of a SPE-HPLC-ESI+-Scheduled-MS/MS -Method for the Qualification and Quantification of Pharmaceuticals in an Urban Sewage System in Germany Robert Gurke, Julia Rossmann, Sara Schubert, Reinhard Oertel, Wilhelm Kirch Institute of Clinical Pharmacology, TU Dresden, Dresden, DE
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104
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Development of a Liquid Chromatography Ion Trap Mass Spectrometry (LC-ITMS) Method for the Analysis of Nimbolide in Rat Liver Microsomes Josiane de Oliveira Cardoso, Bianca Ferreira da Silva, Tiago Venncio, Regina Vincenzi de Oliveira Federal University of So Carlos, Anapolis, BR Analysis of Calix[4]resorcinarene Cavitand with High Performance Liquid Chromatography Mass Spectrometry Ibolya Prauda, Endre Bart, Viktor Sndor, Ferenc Kilr, Ibolya Kiss, Attila Felinger University of Pcs, Pcs, HU LC-MS/MS Method for Determination of Anti-Cancer Agent Bp4eT and its Main Phase I Metabolites in Rat Plasma 1 1 1 1 2 Petra Kovarikova , Jan Stariat , Vlasta Suprunova , Vit Sestak , Des R. Richardson 1 2 Faculty of Pharmacy, Charles University in Prague, Hradec Kralove, CZ; Department of Pathology and Bosch Institute, University of Sydney, Sydney, AU Comparison of LC and LC-MS Methods for the Determination of Hydroxylated Polycyclic Aromatic Hydrocarbons in Different Matrices 1 1 2 1 Jutta Lintelmann , Evelyn Huebner , Juergen Wendt , Ralf Zimmermann 1 2 Helmholtz Zentrum Muenchen, Neuherberg, DE; Leco Instrumente GmbH, Moenchengladbach, DE Determination of Illicit Drug Compounds from Biological Samples with BioCompatible SPME Fibers and HPLC/MS 1 2 2 2 2 Frank Michel , Craig R. Aurand , Robert E. Shirey , Yong Chen , Leonard M. Sidisky 1 2 Sigma-Aldrich, Taufkirchen, DE; Supelco/Sigma-Aldrich, Bellefonte, US Identification of Mauveine in Victoria Postage Stamps by HPLC-DAD-MS/MS 1 1 2 M. Conceio Oliveira , Ana Dias , Srgio Seixas Melo 1 2 Centro Qumica Estrutural, Instituto Superior Tcnico, UTL, Lisboa, PT; Department of Chemistry, University of Coimbra, Coimbra, PT A Novel Derivatization Method for the Determination of Fosfomycin Trometamol in Human Plasma by LC-ESI-MS Via Phase Transfer Catalyzed Derivatization Theodora Papakondyli, Aikaterini Gremilogianni, Nikolaos Megoulas, Michael Koupparis University of Athens, Athens, Gr Method Development Strategy for Derivatization LC/ESI/MS Riin Rebane, Koit Herodes, Maarja-Liisa Oldekop University of Tartu, Tartu, EE Optimization of a LC-MS2 Method for Analysis of Iminosugars from Natural Sources Sonia Rodrguez-Snchez, Jess Eduardo Quintanilla-Lpez, Ana Cristina Soria, Maria Luz Sanz IQOG (CSIC), Madrid, ES Evaluation of Recent Analytical Development in Bioanalysis in the Latest Decade. A Case Study: The Assay of the Budesonide Epimers in Human Plasma Bruno Streel, Cahay Bernard, Klinkenberg Rgis, Traina Karl Galephar, Marche en Famenne, BE The Development of Fast, Sensitive and Selective Multistatin Method for the Determination of Statins, their Metabolites and Interconvesion Products in Human Serum 1 2 1 1 1 Hana Vlckova , Ondrej Novak , Pavel Svoboda , Petr Solich , Lucie Novakova 1 2 Charles university in Prague, Faculty of Pharmacy, Hradec Kralove, CZ; Palacky University and Institute of Experimental Botany, Academy of Sciences of the Czech Republic, Olomouc, CZ
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Sample Preparation and HPLC/MS Determination of Veterinary Drugs in Milk and Animal Tissue 1 2 2 2 2 Frank Michel , Emily Barrey , Katherine K. Stenerson , Olga Shimelis , Michael Ye 1 2 Sigma-Aldrich, Taufkirchen, DE; Supelco/Sigma-Aldrich, Bellefonte, US The Use of Microflow UHPLC as a Way to Solvent Usage in Pesticide Screening of Food Samples by LC-MS/MS Stephen Lock AB SCIEX, Pudsey, GB Screening of 25-OH Vitamin D2,D3 Using Shimadzu LCMS-8040 1 2 3 Giancarlo La Marca , Sabrina Malvagia , Stefano Zaza 1 2 Mass Spectrometry and Pharmacology Laboratory, A. Meyer Chil, Florence, IT; Mass Spectrometry and Pharmacology Laboratory, A. Meyer Childrens Hospital Pediatric Neurology 3 Unit and Laboratories, University of Florence, Florence, IT; Shimadzu Italia, Milan, IT
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Lipids
Detection and Structural Elucidation of Esterified Oxy-Lipids in Human Synovial Fluid by ESI-FTICRMS and LC-IT-MS3: Detection of Esterified Hydroxylated Docosapentaenoic Acid Containing Phospholipids Hulda Jnasdttir, Simone Nicolardi, Rico Derks, Magnus Palmblad, Andreea Ioan-Facsinay, Rene Toes, Yuri van der Burgt, Andre Deelder, Oleg Mayboroda, Martin Giera LUMC, Leiden, NL A Global Method for the Quantitation and Characterization of Lipids by High Performance Liquid Chromatography and Corona Charged Aerosol Detection Bruce Bailey, Marc Plante, Ian Acworth Thermo Fisher Scientific, Chelmsford, US Mass Spectrometric Investigation of Rhamnolipids Beate Behrens, Jeannine Engelen, Heiko Hayen University of Wuppertal, Department of Food Chemistry, Wuppertal, DE Employment of a Stop-Flow Technique in Comprehensive Two-Dimensional Liquid Chromatography for Fish Oil Analysis Marco Beccaria, Giuseppe Sullini, Paola Donato, Francesco Cacciola, Ivana Bonaccorsi, Antonella Cotroneo, Paola Dugo, Luigi Mondello University of Messina, Messina, IT Method Development for Complex Samples in Achiral SFC: Vegetable Oils as A Case Study 1 2 1 Eric Lesellier , Alessandra Lopes de Oliveira , Anna Latos 1 2 ICOA, Orlans, FR; FZEA/UPS, Sao Paulo, BR Investigating the Presence of Specialized Pro-Resolving Lipid Mediators in Rheumatoid Arthritis Patients Using an Advanced LC-MS/MS Platform Hulda Jnasdttir, Andreea Ioan-Facsinay, Oleg Mayboroda, Rene Toes, Andre Deelder, Martin Giera LUMC, Leiden, NL Nontargeted Quantitation of Non-Polar Lipids Blanka erven, Eva Cfkov, Miroslav Lsa, Michal Holapek University of Pardubice, Pardubice, CZ Separation of Hydrocarbons by Silver Ion High-Performance Liquid Chromatography 1 1 2 1 Petra Hork , Vladimr Vrkoslav , Karolina Peckov , Josef Cvaka 1 2 Institute of Organic Chemistry and Biochemistry AS CR, v.v.i, Prague, CZ; Department of Analytical Chemistry, Faculty of Science, Charles University in Prague, Prague, CZ 106
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Application of Sub-2m particle CO2-based Chromatography Coupled to Mass Spectrometry for Comprehensive and Targeted Analysis of Lipids in Cottonseed Extracts 1 2 3 3 Michael Jones , Giorgis Isaac , Vladimir Shuleav , Carolina Salazar 1 2 3 King's College, London, London, GB; Waters, Milford, MA, US; University of Northern Texas, Denton, TX, US Comprehensive GC-MS Analysis of Fatty Acids and Sterols Using Sequential One-Pot Silylation 1 2 1 2 1 Dick-Paul Kloos , Emmanuel Gay , Henk Lingeman , Oleg Mayboroda , Wilfried Niessen , Andr 2 1 Deelder , Martin Giera 1 2 Free University Amsterdam, Amsterdam, NL; LUMC, Leiden, NL Lipidomic Characterization of Vital Porcine Organs Using HILIC-HPLC/ESI-MS Eva Cfkov, Michal Holapek, Miroslav Lsa University of Pardubice, Pardubice, CZ Development of an Analytical Strategy for the Analysis of Different Classes of Solutes in Reversed Phase Liquid Chromatography. Fast Determination of Isoeluotropic Conditions by Changing the Stationary Phase in Aqueous and Non-Aqueous Liquid Chromatography. 1 2 3 4 Alain Tchapla , Tamba Sompila Arnaud , Didier Charbonneau , Marie Genevive Maloumbi , 1 Sylvie Heron 1 2 Univ.Paris Sud/Groupe de Chimie Analytique de Paris-Sud, Orsay, FR; Univ. Paris-Sud/Groupe 3 4 de Chimie Analytique de Paris-Sud, Orsay, FR; Interchim R & D, Montluon, FR; Univ.M. Ngouabi/ UC2V, Brazzaville, CG Glycerophospholipids Analysis by Two-Dimensional Liquid Chromatography Coupled with a Triple Quadrupole Mass Spectrometer Daisuke Nakayama, Jing Dong, Keiko Yamabe, Takashi Suzuki, Yoshihiro Hayakawa, Junichi Masuda, Okiyuki Kunihiro Shimadzu Corporation, Kyoto, JP Detection and Identification of Natural Anti-Oxidants in Edible Oils Using Liquid Chromatographic Fractionation with Off-Line Effect-Based Detection Ruud Poort, Herrald Steenbergen, Hans-Gerd Janssen Unilever Research and Development Vlaardingen, Vlaardingen, NL Identification and Quantification of Triglycerides by UHPSFC-UV-ELSD: Classification of Vegetable Oils with Cluster Analysis Eric Lesellier, Anna Latos, Caroline West ICOA, UMR 7311, Universit Orlans, Orlans, FR Microdetermination of Labile Estrogen-O-Quinones and their Cysteine/Glutathione Conjugates by High Performace Liquid Chromatography-Electrospray Ionization Tandem Mass Spectrometry Kouwa Yamashita, Miki Shiratori, Emi Kondo, Sachiko Komatsu, Hajime Kato, Ken-ichi Ohno Tohoku Pharmaceutical University, Sendai, JP
LPDS10_MO
LPDS11_TU
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MASS01_MO
Mass Spectrometry
Separation of Steroid Isomers by Ion Mobility Mass Spectrometry 1 2 1 1 2 Linda Ahonen , Mara Fasciotti , Gustav Boije af Genns , Tapio Kotiaho , Marcos Eberlin , Risto 1 Kostiainen 1 2 University of Helsinki, Helsinki, FI; University of Campinas, Campinas, BR
107
MASS02_TU
Combining Mass and UV Online Detection in Flash Chromatography 1 2 2 2 Mark Allen , Lawrence Klecha , Nigel Sousou , Ben Trumbore 1 2 Advion Ltd., Harlow, GB; Advion Inc,, Ithaca, US MISPE-LC-Tof Sorbent Selective Determination of Triazine Compounds in Corn Felipe Andrade, Carlos Nazario, lvaro Santos Neto, Fernando Lanas Institute of Chemistry So Carlos/University of So Paulo, So Carlos-SP, BR Rapid and Sensitive Liquid Chromatography Triple Quadrupole Mass Spectrometry (LC-QQQ) Method for the Determination of Gemifloxacin in Human Urine and its Pharmacokinetic Application Adnan Kadi, Mohamed Attwa, Ali Abdelhameed Department of Pharmaceutical Chemistry, King Saud University, Riyadh, SA Electrospray Ionization Mass Spectrometry of Didodecylpolysulfides Using Silver(1) Complexation Christie Bowden, Sriraj Srinivasan, Gary Smith Arkema Inc., King of Prussia, PA, US Micro-Scaled HPLC-SPE/MS for Isolation of Metabolites Obtained by Micro-Batch Synthesis Using Recombinant Human CYP450-1A1 and their Structure Elucidation by NMR 1 1 1 1 1 Thierry Dlmont , Reiner Aichholz , Joachim Blanz , Jrme Dayer , Werner Gertsch , David 1 1 2 2 3 3 Pearson , Philippe Ramstein , Alexandre Luneau , Lukas Oberer , Dirk Behnke , David Carcache , 3 3 3 3 Fabian Kurt Eggimann , Matthias Kittelmann , Stephan Ltz , Alexandra Vargas 1-3 Novartis Pharma AG, Novartis Institutes for Biomedical Research, CH-4053 Basel, Switzerland 1 2 3 ( Metabolism and Pharmacokinetics, Analytical Sciences, Global Discovery Chemistry) Determination of 23 Synthetic Cannabinoids in Human Hair by Ultra-High Performance Liquid Cromatography Tandem Mass Spectrometry Daniele Di Corcia, Alberto Salomone, Clemente Luciano, Enrico Gerace, Marco Vincenti Centro Regionale Antidoping, Orbassano (TO), IT Different Approaches for the Online Determination of Endocrine Disruptors and Related Compounds in Water Samples by Equantm and Turbulent-Flowtm Chromatography-LC-MS/MS 1 2 3 Marina Gorga , Mira Petrovic , Dami Barcel 1 2 3 CSIC-IDAEA, Barcelona, ES; ICRA and ICREA, Girona, ES; CSIC and ICRA, Barcelona, ES Ultra Fast UHPLC-LCMSMS Method Development in Clinical Drug Monitoring 1 1 2 1 1 Anja Gruening , Brigitte Dr. Richrath , Klaus Dr. Bollig , Sven Vedder , Robert Ludwig 1 2 Shimadzu Europa GmbH, Duisburg, DE; Shimadzu Deutschland GmbH, Duisburg, DE Supercritical Carbon Dioxide Extraction and Fourier Transform Ion Cyclotron Resonance Mass Spectrometry Analysis of Pyrolysis Bio-oil Yehua Han State Key Laboratory of Heavy Oil Processing, Beijing, CN Challenges and Opportunities of Developing Ultra-Low Dose Inhalation Products. Combination of Ultraviolet (UV) and Mass Spectrometry (MS) Detection. Viktoria Hartung, Phillip Krger Almirall Sofotec GmbH, Bad Homburg, DE Determination of 25-hydroxy Vitamin D in Human Breast Milk 1 2 2 2 3 1 Eva Kasalov , Ji Plek , Jana Aufartov , Lenka Krmov , Dagmar Solichov , Petr Solich 1 2 Fac. of Pharmacy, Charles University, Dept. Anal. Chem., Hradec Krlov, CZ; Fac. of Pharmacy, Charles University, Dept. Anal. Chem. and III.Internal Gerontometabolic Clinic, University 3 Hospital, Hradec Krlov, CZ; III.Internal Gerontometabolic Clinic, University Hospital, Hradec Krlov, CZ 108
MASS03_WE
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MASS05_TU
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MASS13_MO
Detection and Quantification of Electrochemically Generated Metabolites of Thyroxine (T4) by means of LC-ESI-MS and LC-ICP-MS 1 2 2 2 Chun Kong Mak , Christoph A. Wehe , Michael Sperling , Uwe Karst 1 2 NRW Graduate School of Chemistry, University of Muenster, Muenster, DE; University of Muenster, Muenster, DE Determination of 11 Coccidiostats in Feeds by UPLC-MS/MS 1 1 2 1 Cinzia Civitareale , Paolo Stacchini , Marilena Muscarella , Maurizio Fiori 1 2 Istituto Superiore di Sanit, Roma, IT; Istituto Zooprofilattico Sper. Puglia e Basilicata, Foggia, IT High-Throughput Bioanalytical LC-MS/MS Methods Applied to Snapshot PK and Full PK Studies in Anti-Trypanosomal Drug Development 1 2 3 1 3 Mouhssin OUFIR , Kirsten Gillingwater , Tanja Wenzler , Daniela Eigenmann , Reto Brun , 1 Matthias Hamburger 1 2 Division of Pharmaceutical Biology, University of Basel, Basel, CH; Parasite Chemotherapy, 3 Swiss TPH, University of Basel, Basel, CH; Parasite Chemotherapy, Swiss TPH, University of Base, Basel, CH Multivariate Analysis of a Herbal Medicinal Product Using UPLC-QTOF-MS 1 2 2 2 2 Mark Powell , Margaret Maziarz , Michael D. Jones , Warren Potts , Kate Yu 1 2 Quay Pharmaceuticals, Deeside, Flintshire, GB; Waters Corporation, Milford, MA, US UHPLC Coupled to Mass Spectrometry Applied on the Phenolic Fraction Characterization of Eucalyptus Grandis, E. Urograndis (E.Grandis X E. Urophylla) and E. Maidenii Woods 1 Snia Santos , Carla Vilela, Carmen Freire, Carlos Pascoal Neto, Armando Silvestre University of Aveiro/CICECO, Aveiro, PT Quantification of the Endogenous Peptide Ghrelin in Human Plasma by LC-SRM/MS and LC-SRM3/MS Jonathan Sidib, Emmanuel Varesio, Grard Hopfgartner University of Geneva, Geneva, CH LC/MS/MS Study on Bioactivation of a Cardioprotective Drug Dexrazoxane in Vivo 1 1 1 2 2 Jan Stariat , Petra Kovarikova , Jan Bures , Eduard Jirkovsky , Olga Popelova-Lencova , Martin 2 Sterba 1 2 Faculty of Pharmacy in Hradec Kralove, Charles University, Hradec Kralove, CZ; Faculty of Medicine in Hradec Kralove, Charles University, Hradec Kralove, CZ Development of a Validated LC-MS/MS Method to Monitor a Traditional Chinese Medical Formulation of Ling-Gui-Zhu-Gan Decoction 1 2 1 Chang Yang Tan , Lie-Chwen Lin , Tung-Hu Tsai 1 2 National Yang-Ming University, Taipei, TW; National Research Institute of Chinese Medicine, Taipei, TW Development and Validation of a Gas Chromatography Mass Spectrometry Method for Analysis of Phytoestrogens and Mycotoxins in Estuarine Water Samples 1 2 3 Cludia Ribeiro , Ana R Ribeiro , Maria E Tiritan 1 2 CICS-ISCSN-CESPU, Gandra - Paredes, PT; CICS-ISCSN-CESPU, CBQF-ESB-UCP, CEQUIMED-UP, 3 Gandra - Paredes, PT; CICS-ISCSN-CESPU, CEQUIMED-UP, Gandra - Paredes, PT Comparison of Two Multi-Residue Methods Using Solid-Phase Extraction (SPE) and Direct-Injection (DI) for the Determination of Pesticide Residues in Wines by LCMS/MS 1 1 1 2 Despina Tsipi-Stefanitsis , Helen Botitsi , Spyros Antoniou , Sotirios Katsikis , Anastasios 2 Economou 1 2 General Chemical State Laboratory, Athens, GR; University of Athens, Athens, GR 109
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Online ESI-MS Analysis of HPTLC-Separated Compounds with a New Compact Single Quadrupole Mass Spectrometer 1 1 2 2 Kees Vlak , Frank Porbeck , Ines Klingelhoefer , Gerda Morlock 1 2 Advion Ltd., Harlow, GB; Justus-Liebig-University, Giessen, DE Combining Mass and UV Spectral Information with Systematic Mobile Phase Screening for Chromatographic Method Development Thomas Wheat, Patricia McConville Waters Corporation, Milford, MA, US A Simple and Rapid Method for Simultaneous Determination of Food Additives in Beverages and Soft Drinks Kamila Wilczewska, Anna Jakimska, Weronika Hewelt-Belka, Andrzej Wasik, Agata Kot-Wasik, Jacek Namienik Gdask University of Technology, Faculty of Chemistry, Gdask, PL Molecularly Imprinted Polymer Sorbent for Analysis of Triazines by MEPS-LC-ESIToF Felipe Andrade, lvaro Santos Neto, Fernando Lanas Institute of Chemistry So Carlos, University of So Paulo, So Carlos-SP, BR Determination of Four Immunosuppressive Drugs in Whole Blood Using MEPS and LC-MS/MS Allowing Automated Sample Work-Up and Analysis Rana Said, Olof Beck Karolinska institute, Huddinge, SE
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META01_MO
Metabolomics
Search for Markers of Bladder Cancer with a Metabolomic Approach 1 2 3 3 1 Antonia Garca-Fernndez , Juliana Alberice , Alberto Amaral , Nuria Malats , Coral Barbas 1 2 CEMBIO Facultad de Farmacia, Universidad CEU San Pablo, Boadilla del Monte, ES; IQSC, 3 Instituto de Qumica de So Carlos, Universidade de So Paulo, So Carlos, BR; CNIO Centro Nacional de Investigaciones Oncolgicas, Madrid, ES Metabolic Profiling by Hydrophilic Interaction Ultra-Performance Liquid Chromatography Time-Of-Flight Mass Spectrometry in the Study of Chronic Kidney Disease 1 2 2 2 2 Jente Boelaert , Griet Glorieux , Eva Schepers , Nathalie Neirynck , Raymond Vanholder , 1 Frdric Lynen 1 2 Separation Science Group, Ghent University, Gent, BE; Renal Division, Ghent University, Gent, BE Identification of Metabolites of Davidiin, a Potential Antitumor Ellagitannin, Transformed by Rat Intestinal Bacteria in Vitro, Based on Liquid Chromatography/Quadrupole Ion Trap/Time-Of-Flight Mass Spectrometry Analysis 1 2 2 2 2 Ma Chao , Fu Jie , Ma Jingyi , Wang Yan , Gao Hui 1 2 Shimadzu Global COE, Shimadzu (China) Co., Ltd., Beijing, CN; Institute of Materia Medica, Chinese Academy of Medical Sciences & Peking Union Medical College, China, Beijing, CN High Volume Injections of Biological Samples for Sensitive Metabolite Profiling Russell Jones, Marc Bockx, Filip Cuyckens Janssen R&D, Beerse, BE The Pitfall of Cytokinin Nucleotide Determination by LC/MS Petre I. Dobrev, Vclav Motyka, Radomra Vakov Institute of Experimental Botany AS CR, Prague, CZ
META02_TU
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110
META06_WE
Comparison of an Optimized LC-MS Method with Direct Infusion MS for Metabolomic Analysis in Human Cell Cultures Ines C. Forstenlehner, Volker Neu, Christian G. Huber University of Salzburg, Salzburg, AT LC- and GC-MS Based Non-Targeted Metabolomics in the Study of Chronic Kidney Disease 1 2 2 3 3 3 Jente Boelaert , Ruben t' Kindt , Lucie Jorge , Griet Glorieux , Eva Schepers , Nathalie Neirynck , 3 1 2 2 Raymond Vanholder , Frdric Lynen , Pat Sandra , Koen Sandra 1 2 Separation Science Group, Ghent University, Gent, BE; Metablys, Research Institute for 3 Chromatography, Kortrijk, BE; Renal Division, Ghent University, Gent, BE Multidimensional HPLC+GC-MS: A Powerful, Novel, Analytical Tool for Universal Quali/Quanti of Volatiles, Semivolatiles and Polar Compounds. Example of Application in Metabolomics. Josep M Gibert, NIeves Sarrin, Roger Gibert, David Alonso KONIK-Tech S.A., Sant Cugat del Valls, ES Towards a LC-MS Library Compatible with Metabolomic Profiling Oskar Gonzalez Mendia, Eric Tijssen, Carola Damen, Rob Vreeken, Thomas Hankemeier Division of Analytical Biosciences, Leiden University, Leiden, NL Molecularly Imprinted Polymers Separation Combined with UHPLC-MS/MS: A Tool for Experimental and Clinical Diagnostics Petr Kacer, Michaela Gajdosova, Kamila Syslova, Marek Kuzma ICT - Prague, Prague 6, CZ Ion Pair Chromatography vs. HILIC - Survey of Different Separation Techniques for Highly Polar Metabolites Rudolf Khling, Roland Wohlgemuth, Bernhard Schnenberger Sigma-Aldrich, Buchs SG, CH Rapid Screening for Detection and Differentiation of Adulterated Infant Milk Formula by LC-MS Sam Li NUS, Singapore, SG Metabolite Analysis by LC-Q-TOF-MS to Investigate the Molecular Basis of Storage Disorders in Apple Fruit 1 1 2 Tony McGhie , Daryl Rowan , Jason Johnston 1 2 Plant & Food Research, Palmerston North, NZ; Plant & Food Research, Havelock North, NZ HPLC-UV Determination of Nonspecific Binding of the Casearin X to Rat Liver Microsomes 1 1 2 1 Rodrigo Moreira Silva , Anderson R. M. Oliveira , Alberto J. Cavalheiro , Norberto P. Lopes , 1 Cristiane M. Gaitani 1 2 USP, Ribeiro Preto / SP, BR; UNESP, Araraquara / SP, BR Micro Flow LC/MS/MS Applications in Drug Metabolism and Bioanalysis Khaled Mriziq, Remco Van Soest, Tina Settineri Eksigent, part of AB SCIEX, Dublin, CA, US Beer Metabolomics of Light and Dark Beers Robert Murphy Kroungold Analytical, Encinitas, US
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META08_TU
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111
META17_TU
Simultaneous Analysis of Organic and Inorganic Anions in Saliva Using AnionExchange ChromatographySuppressed Conductivity Detector 1 1 1 1 1 2 Yoon Jong Oh , Ji Eun Kim , Seung Jin Kim , Ji Hyun Kim , Yong Duk Park , Kyung Suk Hwang 1 2 Department of Preventive Social Dentistry, Kyung Hee Univ, Seoul, KR; Department of Dental Technology, Shinheung Univ., Uijeongbu, Kyunggido, KR Improving Cancer Diagnostics through Assembly of the Cancer Metabolome 1 2 3 4 1 Jorge Pereira , Srikanth Rapole , Hampapathalu Nagarajaram , David Wishart , Jos S. Cmara 1 2 CQM, UMa, Funchal, PT; Scientist Proteomics Lab, National Center for Cell Science (NCCS), 3 Ganeshkhind, IN; Laboratory of Computational Biology (LCB), Centre for DNA Fingerprinting 4 and Diagnostics (CDFD), Hyderabad, IN; University of Alberta, Department of Computing Science, Edmonton, CA Metabolic Effects of ZnO Nano Particle Exposure on A459 Alveolar Carcinoma Cells Determinded by Reversed Phase LC, HILIC and Gas Chromatography with Mass Spectrometric Detection 1 1 2 2 1 Roland Reischl , Christina Ranninger , Mark Rurik , Oliver Kohlbacher , Christian G. Huber 1 2 University of Salzburg, Salzburg, AT; University of Tbingen, Tbingen, DE UHPLC-MS/MS Method for Monitoring of Neurotransmitters and their Metabolites in Brain Microdialysates 1 1 2 1 Kamila Syslova , Michaela Gajdosova , Marek Kuzma , Petr Kacer 1 2 ICT Prague, Prague, CZ; Institute of Microbiology, Prague, CZ Profiling of Plant Hormones Cytokinins by Hyphenated Techniques Petr Tarkowski, Tibor Bres Palacky University, Olomouc, CZ Hydrophilic Interaction Liquid Chromatography (HILIC) Coupled to Mass Spectrometry (MS) A Powerful Analytical Platform to Obtain a Broad Metabolites Coverage in Metabolic Profiling Sara Tufi, Marja Lamoree, Pim Leonards Vrije Universiteit, Amsterdam, NL HPLC-MS/MS Flux Measurements for Study of Metabolism in Hsp90 inhibited Cancer Cells 1 2 1 2 2 Christian Wachsmuth , Maria Mycielska , Katja Dettmer , Sven Lang , Edward Geissler , Peter 1 Oefner 1 2 Institute of Functional Genomics, University of Regensburg, Regensburg, DE; Department of Surgery, University Hospital Regensburg, Regensburg, DE Comparison of Pharmacokinetics of Buspirone in Rats At Low Altitude and Acute Exposure High Altitude (Corresponding to an Altitude of 4,100 M) Rong Wang, Juanhong Zhang, Hua Xie, Zhengping Jia, Xiandong meng, Liting Xu, Qiang Zhang, Xiaohui Zhang, Dengfeng Guo Key Laboratory of the plateau of the environmental damage, Lanzhou, CN A Novel LC-MS Approach for Urine Modified Metabolome Profiling Peiyuan Yin, Weidong Dai, Zhongda Zeng, Hongwei Kong, Xin Lu, Guowang Xu Dalian institute of chemical physics, Dalian, CN Development and Optimization of an HPLC-UV Assay for Measurement of Indoleamine2.3-Dioxygenase (IDO) Activity 1 2 2 2 Randa Ghedira Chkir , Mohamed Hachem Saadaoui , Wahiba Douki , Mohamed Fadhel Najjar , 1 1 1 1 Sallouha Gabbouj , Abdelfatteh Zakhama , Lotfi Chouchane , Elham Hassen 1 2 Molecular Immuno-Oncology Laboratory, Faculty of Medicin, Monastir, TN; Biochemistry and Toxicology Laboratory, University Hospital Fattouma Bourguiba, Monastir, TN
META18_WE
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112
META27_WE
Metabolic Profiling of Yeast Arginine Biosynthesis Deletion Mutants 1 2 1 3 4 Aiko Barsch , Sandy Yates , Gabriela Zurek , Manhong Wu , Rob van der Heijden 1 2 3 Bruker Daltonik GmbH, Bremen, DE; Bruker Daltonics, Billerica, MA, US; Stanford University, 4 Stanford, CA, US; Bruker Daltonics B.V., Wormer, NL
MONO01_MO
Monoliths
Selective Monolithic Microemulsion Liquid Chromatographic Method for Simultaneous Quantification of Rosiglitazone and Glimepiride in Wistar Rats Serum and its Application in Pharmacokinetic Studies 1 1 1 2 Mohamed Hefnawy , Mohammed Al-Omar , Nasser ALGRAIN , Sabry Attia 1 2 Pharmaceutical Chemistry Department,College of Pharmacy, KSU, Riyadh, SA; Pharmacology Department,College of Pharmacy, KSU, Riyadh, SA Preparation, Characterization and Application of Methacrylate Monolithic Columns for Capillary Liquid Chromatography Ahmad Aqel, Kareem Yusuf, Zeid ALOthman, Yacine Badjah-Hadj-Ahmed King Saud University, Riyadh, SA Preparation of Highly Ordered Monolithic Structures by Unidirectional Freezing and Radical Polymerisation R. Dario Arrua, Paul R. Haddad, Emily F. Hilder School of Chemistry, University of Tasmania, Hobart, AU Poly(3-Chloro-2-Hydroxypropyl Methacrylate) Based Reactive Monolith with Derivatization Flexibility as a New Separation Medium for Capillary Electrochromatography. Part II: Taurine Functionalized Zwitterionic Stationary Phase 1 2 1 2 Cemil Aydoan , Bekir elebi , Adil Denizli , Ali Tuncel 1 2 Hacettepe University, Department of Chemistry, Ankara, TR; Hacettepe University, Department of Chemical Engineering, Ankara, TR Synthesis, Chromatography, and Morphological Analysis of a New TMOS/PTMS Hybrid Capillary Monolith 1 2 2 1 Kristof Hormann , Romana Hakim , Bernd Smarsly , Ulrich Tallarek 1 2 Philipps-Universitt Marburg, Marburg, DE; Justus-Liebig-Universitt Giessen, Giessen, DE Vinyl Phenyl Boronic Acid Functionalized Lauryl Methacrylate Based Monolith for Nano Liquid Chromatography of Small Molecules and Proteins 1 2 1 Cemil Aydoan , Fatma Ylmaz , Adil Denizli 1 2 Hacettepe University, Department of Chemistry, Ankara, TR; Abant Izzet Baysal University, Gerede Vocational School, Bolu, TR Monolithic Stationary Phases for Capillary Liquid Chromatography Based on Silica and Zirconium Oxides Carla Grazieli Azevedo da Silva, Raquel Costa Silva, Carol Collins, Carla Beatriz Grespan Bottoli University of Campinas (UNICAMP), Campinas/SP, BR Miniaturized Immunosorbents Coupled On-Line with Nanolc : Synthesis, Characterization and Applications to Environmental Samples Fabien Brothier, Valrie Pichon LSABM - UMR PECSA 7195 ESPCI ParisTech, PARIS, FR Silica-based Monoliths and Particulate Beds: A Morphological Comparison Stefan Bruns, Alexandra Hltzel, Ulrich Tallarek Philipps-Universitt Marburg, Marburg, DE
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Detailed Characterization of the Kinetic Performance of First and Second Generation Monolithic Silica Columns 1 1 1 2 2 Deirdre Cabooter , Roman Sterken , Alison Vanmessen , Sander Deridder , Gert Desmet 1 2 K.U.Leuven, Leuven, BE; V.U.B., Brussel, BE Determination of Parabens in Human Urine and Serum by Capillary Liquid Chromatography Using Methacrylate Monolithic Columns 1 2 2 Enrique Javier Carrasco Correa , Fernando Vela-Soria , Oscar Ballesteros , Jos Manuel Herrero1 Martnez 1 2 Dept. de Qumica Analtica, Universidad de Valencia, Burjassot, Valencia, ES; Dept. de Qumica Analtica, Universidad de Granada, Granada, ES Agilent Bio-Monolith Protein A column Monitoring of monoclonal antibody titer and yield from supernatants 1 2 2 Andrew Coffey , Phu Duong , Maureen Joseph 1 2 Agilent Technologies UK Ltd, Church Stretton, GB; Agilent Technologies Inc, Wilmington, US Morphological Similarity and Radial Homogeneity of Silica Monoliths Kristof Hormann, Dzmitry Hlushkou, Ulrich Tallarek Philipps-Universitt Marburg, Marburg, DE Performance Characterization of Polymer Monolithic Columns for Small-Molecule Separations Using Total-Pore-Blocking Conditions Catherine Stassen, Gert Desmet, Sebastiaan Eeltink Vrije Universiteit Brussel, Brussels, BE Photografting as a Simple and Versatile Functionalization Route of Silica-Based Monoliths Racha El Debs, Claire Demesmay, Vincent Dugas Institute of Analytical Sciences, Villeurbanne, FR New Polar Coatings for Stir Bar Sorptive Extraction of Emerging Pollutants 1 1 1 2 1 Nria Fontanals , Nria Gilart , Nria Miralles , Peter A. G. Cormack , Francesc Borrull , Rosa M. 1 Marc 1 2 Universitat Rovira i Virgili, Tarragona, ES; University of Strathclyde, Glasgow, GB Polymer Monolith Microextraction with UPLC-UV for the Determination of Phenylurea Herbicides in River Water Ming-Ren Fuh, Yu-Ru Wu, Shu-Ling Lin Soochow University, Taipei, TW Comparison of First and Second Generation Analytical Silica Monoliths by Pore-Scale Simulations of Eddy Dispersion in the Bulk Region 1 1 1 1 Dzmitry Hlushkou , Kristof Hormann , Alexandra Hltzel , Siarhei Khirevich , Andreas Seidel2 1 Morgenstern , Ulrich Tallarek 1 2 Philipps-Universitt Marburg, Marburg, DE; Max-Planck-Institut fr Dynamik Komplexer Technischer Systeme, Marburg, DE Fast Analysis of Phthalates and Degradation Products in Waters Using In-Tube Solid Phase Microextraction Coupled On-Line to Capillary Liquid Chromatography Neus Jornet-Martinez, Maria Muoz-Ortuo, Yolanda Moliner-Martinez, Rosa HerrezHernndez, Jorge Verd-Andrs, Pilar Campns-Falc Universidad Valencia, Burjassot, ES
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114
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Poly(3-Chloro-2-Hydroxypropyl Methacrylate) Based Reactive Monolith with Derivatization Flexibility as a New Separation Medium for Capillary Electrochromatography. Part III: Polyethylenimine Functionalized Strong Anion Exchange Stationary Phase 1 2 2 1 2 Cemil Aydoan , Bekir elebi , Aslhan Gkaltun , Adil Denizli , Ali Tuncel 1 2 Hacettepe University, Department of Chemistry, Ankara, TR; Hacettepe University, Department of Chemical Engineering, Ankara, TR Monolithic Poly (N-vinlycarbazole-co-1,4-divinylbenzene) Stationary Phases Optimized for the Separation of Biomolecules or Small Molecules 1 1 1 2 1 Rainer Koeck , Martin Fischnaller , Rania Bakry , Richard Tessadri , Guenther K. Bonn 1 2 Analytical Chemistry and Radiochemistry, Innsbruck, AT; Mineralogy and Petrography, Innsbruck, AT Modelling the B-Term Band Broadening in Monolithic Silica Columns 1 2 2 1 Sander Deridder , Deirdre Cabooter , Alison Vanmessen , Gert Desmet 1 2 Vrije Universiteit Brussel, Elsene, BE; K.U. Leuven, Leuven, BE Incorporation of Sporopollenin Particles Into Polymethacrylate Based Monolithic Capillary Columns to Be Use as Templates for HPLC Separations 1 1 2 1 1 Kareem Yusuf , Ahmad Aqel , Amro Dyab , Zeid ALOthman , Yacine Badjah-Hadj-Ahmed 1 2 Advanced Materials Research Chair- King Saud University, Riyadh, SA; Collage of Science- King Saud University, Riyadh, SA Comparison of Performance of Monolithic Silica Columns Clad by Glass or Stainless Steel 1 2 2 2 1 Riichi Miyamoto , Yukiko Ando , Chie Kurusu , Hong-zhi Bai , Kazuki Nakanishi , Masamichi 2 Ippommatsu 1 2 Graduate School of Science, Kyoto University, Kyoto, JP; Renaissance Energy Investment, Co., Ltd., Kyoto, JP Reconstruction and Characterization of Polymeric Monolithic Stationary Phases Using Serial Block Face Scanning Electron Microscopy 1 2 2 1 Tibor Muellner , Armin Zankel , Herbert Reingruber , Ulrich Tallarek 1 2 Philipps-Universitt Marburg, Marburg, DE; Institute for Electron Microscopy, Technische Universitt Graz, and Center for Electron Microscopy Graz, Graz, AT Development of Hypercrosslinked Monolithic Stationary Phases for Chiral Capillary Liquid Chromatography Veronika Skerikova, Kristyna Dedova, Jiri Urban University of Pardubice, Pardubice, CZ 3D Reconstruction of a Mesoporous Monolithic Silica Structure Using Scanning Transmission Electron Microscopy (STEM) Tomography 1 2 3 1 Daniela Stoeckel , Christian Kbel , Ulrich Tallarek , Bernd Smarsly 1 2 Justus-Liebig-University, Giessen, DE; Karlsruhe Institute of Technology, Karlsruhe, DE; 3 Philipps-Universita, Marburg, DE Comparison of Chromolith Performance RP-18e, 1.8m Zorbax Eclipse XDB-C18 and XTerra MS C18 Columns in the Analysis of Phenols and -Adrenolytic Drugs 1 2 1 Jos Ramn Torres-Lapasi , Sandra Pous-Torres , Mara Celia Garca-lvarez-Coque 1 2 University of Valencia, Burjassot (Valencia), ES; University of Amsterdam, Amsterdam, NL Hypercrosslinked Monolithic Capillary Columns for Reversed-Phase and Hydrophilic Interaction Liquid Chromatography of Small Molecules Jiri Urban, Veronika Skerikova, Pavel Jandera University of Pardubice, Pardubice, CZ
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115
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Comparison of Various Silica-Based Monoliths for the Analysis of Large Biomolecules Karine Vuignier, Szabolcs Fekete, Pierre-Alain Carrupt, Jean-Luc Veuthey, Davy Guillarme University of Geneva, Switzerland, Geneva 4, CH Titanium-Reinforced Polymer-Based Monolithic Stationary Phases for Application in Liquid Chromatography 1 2 1 R.J. Vonk , S. Eeltink , P.J. Schoenmakers 1 2 Univeristeit van Amsterdam, Amsterdam, NL; Vrije Univeristeit Brussel, Brussel, BE Thermally Polymerized Organo-Silica Monoliths: Optimization of Preparation Conditions and Pore Surface Functionalization 1 1 1 1 2 Zuzana Zajickova , Anna-Marie Weed , Deepa Gharbharan , Gabriela Soto , Frantisek Svec 1 2 Barry University, Miami Shores, FL, US; The Molecular Foundry, Berkeley, CA, US Characterization of Polymer Monolithic Stationary Phases Using Differential Scanning Calorimetric Techniques Sam Wouters, Bert Wouters, Axel Vaast, Guy Van Assche, Sebastiaan Eeltink Vrije Universiteit Brussel, Brussel, BE Effect of Crosslinking Monomers on the Efficiency of Monolithic Capillary Columns for Hydrophilic Interaction Chromatography Magda Stakov, Pavel Jandera, Ji Urban, Veronika kekov University of Pardubice, Pardubice, CZ Nanoscale Characterization of Polymer Monoliths Using Atomic Force Microscopy and Confocal Raman Imaging 1 2 2 1 3 Martin Laher , Tim J. Causon , Wolfgang Buchberger , Sabine Hild , Ivo Nischang 1 2 Institute of Polymer Science/JKU Linz, Linz, AT; Institute of Analytical Chemistry/JKU Linz, Linz, 3 AT; Institute of Polymer Chemistry/JKU Linz, Linz, AT
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MS Data Analysis
Determination of Emerging Illicit Drugs in Waste Water Mara Jess Andrs-Costa, Ana Masi, Yolanda Pic University of Valencia, Valencia, ES Meeting CODEX Guidelines: Utilisation of Complete Workflow Procedures for Pesticide Residue Analysis 1 1 1 1 2 Antonietta Gledhill , Sara Stead , Mike McCullagh , Dominic Roberts , Richard Fussell 1 2 Waters Corporation, Manchester, GB; FERA, York, GB LC-QTOFMS Analysis of Polyethylene Glycol (PEG) and Pegylated Lysozyme 1 1 2 3 Ravindra Gudihal , Sundaram M Palaniswamy , Lakshmi NS , Ning Tang 1 2 Agilent Technologies India Pvt. Ltd, Bangalore, Karnataka, IN; Amrita University, Kollam, 3 Kerala, IN; Agilent Technologies Inc, Santa Clara, CA, US Suitable Gradient Conditions for the Separation of Bio-Oils Samples in RPLC X RPLC 1 2 2 2 2 Sabine Heinisch , Ccile Gouin , Agns LeMasle , Jrmie Ponthus , Alain Quignard 1 2 Institut des Sciences Analytiques, Villeurbanne, FR; IFPEN, Solaize, FR Feature Detection in LC-MS Fingerprints Using the Combined Matched Gaussian Filter and Two-Fold Differentiation with Median Measures for Threshold Determination (Comfidimed) 1 2 1 Nikoline J. Nielsen , Rolf Danielsson , Jan H. Christensen 1 2 University of Copenhagen, Frederiksberg C, DK; Uppsala University, Uppsala, SE
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116
MSDA06_WE
Comprehensive Chemical Fingerprinting of Chamomile SFE Extracts Using UPC2/MS 1 2 3 3 4 3 Michael Jones , Giorgis Isaac , Bharathi Avula , Yan-Hong Wang , Kate Yu , Troy Smillie , Iklas 5 1 Khan , Norman Smith 1 2 3 King's College, London, London, GB; Waters Corp., Milford, MA, US; NCNPR, University, MS, 4 5 US; Waters Corp, Milford, US; University of Mississippi, University, MS, US Quality of Ultrapure Water for Environmental Analyses of Hormones and Pesticides in Water Samples at Ng/L Levels 1 2 2 2 Anastasia Khvataeva-Domanov , Mikael Tilli , Jevgeni Parshintsev , Matias Kopperi , Marja-Liisa 2 1 3 1 Riekkola , Cecilia Devaux , Patrik Appelblad , Stephane Mabic 1 2 3 Merck Millipore, Guyancourt, FR; University of Helsinki, Helsinki, FI; Merck Millipore, Umea, SE Data Processing Method Development for HPLC-MS-Based Metabonomics Xiaohui Lin, Hai Wei, Jiuchong Gao, Xiangfei Ding Dalian University of Technology, Dalian, CN Evaluation of Photodegradation Profile of Lercanidipine Enantiomers by HPLC-UV and Characterization of Degradation Products by LC-ESI/MS-MS Luciana Loureno, Cristiane Gaitani, Luiz Moraes University of So Paulo, Ribeiro Preto - SP, BR LCxLC-MS Separations of Protein Tryptic Digests Sabine Heinisch, Amlie D Attoma, Marion Iguiniz Institut des Sciences Analytiques, Villeurbanne, FR Matching Features across Chromatographic Platforms to Assess Orthogonality for Liquid Chromatography Mass Spectrometry Fingerprinting 1 2 1 Nikoline J. Nielsen , Giorgio Tomasi , Jan H. Christensen 1 2 University of Copenhagen, Frederiksberg C, DK; European Commission Joint Research Centre, Ispra, IT Development, Optimization and Validation of a Fingerprinting Method for Simultaneously Determining Guaianolide and Parthenolide in Tanacetum Parthenium (L.) Schultz-Bip Using Quality-By-Design Approach and Liquid Chromatography 1 2 3 1 Mirela F. Rabito , Mariana B. Almeida , Amadeu H. Iglesias , Amanda L. Moreira , Fernando De 3 1 2 Paula , Izabel C. P. Ferreira , Suzana Lucy Nixdorf 1 2 Universidade Estadual de Maring, Maring, BR; Universidade Estadual de Londrina, Londrina, 3 BR; Waters Technology do Brasil, Sao Paulo, BR Metabolomics of Urinary Tract Infection Tiziana Pacchiarotta, Rico Derks, Katja Nevedomskaya, Paul Hensbergen, Manfred Wuhrer, Willize van der Starre, Bart Schoenmaker, Jaap van Dissel, Andr Deelder, Oleg Mayboroda LUMC, Leiden, NL Identification of Unknowns Using High Resolution Liquid Chromatography/Mass Spectrometry (LC/MS), LC/MS/MS, Liquid Chromatography/Infrared Spectroscopy (LC/IR), and Gas Chromatography/Mass Spectroscopy (GC/MS) 1 1 1 2 3 Teresa Peterson , Rick Borders , Wade Thompson , Fred Stroebel , Tracy Phillpott 1 2 Kimberly-Clark Corporation, Roswell, Georgia, US; Emory University, Atlanta, Georgia, US; 3 Spectra Analysis, Greenville, South Carolina, US Pesticides in Source and Drinking Waters in the State of So Paulo (Brazil) by SPE-LCESI-MS/MS 1 2 1 1 2 Cassiana Raimundo , Cristiane Vidal , Raphael Acayaba , Gisela Umbuzeiro , Isabel Jardim 1 2 University of Campinas, Limeira, BR; University of Campinas, Campinas, BR
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117
MSDA17_TU
In Vitro Metabolism of Monensin A: Identification of Metabolites by LC-MS/MS Spectrometry Bruno Rocha, Marilda Assis, Ana Peti, Luiz Moraes, Norberto Lopes, Anderson de Oliveira University of So Paulo, Ribeiro Preto, SP, BR Integrity Assessment of Thymopentin under Conditions for Production of Hydrogels by LCMSn Mehrnoosh Shirangi, Javier Sastre Torao, Wim E Hennink, Govert W Somsen, Cornelus F van Nostrum Utrecht University, Utrecht, NL Fast Multi-Residue Method for Determination of Nineteen Benzimidazoles in Meat by Liquid Chromatography and Tandem Mass Spectrometry Georgi Stoev, Milena Peicheva, Alexander Stoyanov CLVCE, Sofia, BG HPLC and LC-MS/MS for the Detection of Early Biomarkers of Neonatal Growth in Human Amniotic Fluid Christina Virgiliou, Maria Fotiou, Alexandra Michailidou, George Theodoridis, Apostolos Athanasiadis, George Menexes, Vasiliki Koulourida, Costas Biliaderis, Vasilios Tarlatzis Aristotle University of Thesaloniki, Thesaloniki, Gr Batch Effects in Liquid Chromatography: Setting the Data Straight Franziska Vogl, Jochen Hochrein, Wolfram Gronwald, Katja Dettmer-Wilde, Peter Oefner Institute of Functional Genomics, Regensburg, DE Characterization of Commercially Available Stevia-Derived Sweeteners Using Liquid Chromatography-High Resolution Time of Flight Mass Spectrometry and Advanced Data Processing 1 2 Juergen Wendt , Jutta Lintelmann 1 2 LECO European LSCA Centre, Moenchengladbach, DE; Helmholtz Zentrum Mnchen, Neuherberg, DE Urinary Biomarker for Behce'ts Disease Using LC/ MS-MS and HPLC-DAD 1 2 1 Saied Jaradat , Khaldoon Alawneh , Mohammad Dwairi 1 2 Jordan university of Science and Technology, Irbid, JO; King Abdullah University Hospital, Irbid, JO Validation of a Method for the Determination of Thyreostatic Drugs in Urine by LCMS/MS Elmas ktem Olgun, znur Karaolu, Muammer Kaplan Tubitak Mrc Food Institute, Kocaeli, TR
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NANO01_MO
Nanomaterials
Measurement of Quercetin by High-Performance Liquid Chromatography Coupled to Photodiode Array Detection for Pharmacokinetic Application of UltrasoundTriggered Micro-Formulation Li-Wen Chang, Mei-Ling Hou, Tung-Hu Tsai Institute of Traditional Medicine, NYMU, Taipei, TW Preparation and Evaluation of Methacrylate Monoliths Functionalized with Silver Nanoparticles Marta Mon-Conejero, Mara Navarro-Pascual-Ahuir, Ernesto Sim-Alfonso, Guillermo RamisRamos, Jos Manuel Herrero-Martnez Dept. Analytical Chemistry, University of Valencia, Burjassot (Valencia), ES
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118
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Immobilization of PNGASE F onto Gold Nanoparticles via Linker SH-PEG7-COOH. Markus Hldrich, Michael Lmmerhofer University of Tbingen, Institute of Pharmaceutical Science, Tbingen, DE Application of Miniaturized Sample Preparation Technique: -Hydroxyprene Case Study 1 1 2 Okechukwu Ifegwu , Chimezie Anyakora , Nelson Torto 1 2 University of Lagos, Akoka, Lagos, Nigeria, Lagos, Ng; rhodes University, Grahamstown, Za The Use of Nanometer-Scale Chemicals to Make New Separation Media Showing Unique Selectivity and Stability Xiaodong Liu, Christopher Pohl Thermo Fisher Scientific, Sunnyvale, California, US Optical Isomer Separation of Flavanones and Flavanone Glycosides by Nano-Liquid Chromatography Using a Phenyl-Carbamate-Propyl-B-Cyclodextrin Chiral Stationary Phase 1 1 1 2 Fairouz Tazerouti , Kahina Si-Ahmed , Ahmed Yacine , Badjah-Hadj-Ahmed , Zeineb Aturki , 2 2 2 Giovanni DOrazio , Anna Rocco , Salvatore Fanali 1 2 University of Science and Technology Houari Boumedien, USTHB, Algiers, DZ, Institute of Chemical Methodologies, Italian National Council of Research, Area della Ricerca di Roma, Rome, IT Electrospun Nanofiber Based Sorbents for Sample Clean-Up of Environmental Or Biological Samples Nelson Torto, Samuel Chigome, Boitumelo Mudabuka, Bellah Pule, Dezzline Ondigo, Zenixole Tshentu Rhodes University, Grahamstown, ZA High-Speed Gradient Separations of Peptides and Proteins Using Polymer-Monolithic Poly(Styrene-Co-Divinylbenzene) Capillary Columns at Ultra-High Pressure 1 1 2 2 1 Axel Vaast , Lucie Novkov , Bjorn de Haan , Remco Swart , Sebastiaan Eeltink 1 2 Vrije Universiteit Brussel, Brussels, BE; Thermo Fisher Scientific, Amsterdam, NL Magnetic Nanoparticles Coated with Immobilized Alkaline Phosphatase for Enzyme Inhibition Assays by HPLC Siming Wang, Ping Su, Jun Huang, Jingwei Wu, Yi Yang Beijing University of Chemical Technology, Beijing, CN Highly Efficient Extraction of the Cellular Nucleic Acid Associated Protein in Vitro with Magnetic Oxidized Carbon Nanotube Yi Zhang, Zhengyan Hu, Hongqiang Qin, Xiaoluan Wei, Kai Cheng, Fangjie Liu, Ren'an Wu, Hanfa Zou Dalian Institute of Chemical Physics, CAS, Dalian, CN Highly Sensitive Determination of Phenylarsonic Acids Based on Sorptive Extraction of Carboxymethyl A- Cyclodextrin Immobilized Fe3O4 Magnetic Nanoparticles by High Performance Liquid Chromatography-Mass/Mass Spectrometry 1 2 1 Ruohua Zhu , Peilong Wang , JIng Jia 1 2 Capital Normal University, Beijing, CN; Institute of Quality Standards and Testing Technology for Agriculture Products, Beijing, CN Synthesis of Silver Nanoparticles Confined in Hierarchically Porous Monolithic Silica: A New Function in Aromatic Hydrocarbon Separations 1 2 3 1 1 Yang Zhu , Kei Morisato , Wenyan Li , Kazuyoshi Kanamori , Kazuki Nakanishi 1 2 3 Kyoto University, Kyoto, JP; GL Science, Inc., Tokyo, JP; Zhejiang University, Hangzhou, CN
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119
PHAR01_MO
Pharmaceutical
Assay Develoment and Method Validation of Colchicine Tablets by RP-HPLC Arman Abrahamyan Arpimed LLC, Abovyan, AM HPLC Method for Analysis of Prochelator Boronyl Salicylaldehyde Isonicotinoyl Hydrazone and its Application to in Vitro Activation Study Jan Bures, Hana Jansova, Petra Kovarikova Faculty of Pharmacy, Charles University, Hradec Kralove, CZ Response Surface Methodology in Optimization of HPLC Analysis of Fluoxetine and Olanzapine Fatih Karademir, Mehmet Gokhan Caglayan, smail Murat Palabiyik, Feyyaz Onur Ankara University, Ankara, TR Development of an HPLC Method for Determination of Related Impurities in Iodixanol Drug Substance 1 2 1 Neila Cassiano , Bruno Rondon , Quezia Cass 1 2 Federal University of So Carlos, So Carlos - So Paulo, BR; U.S. Pharmacopeia of Brazil, Barueri - So Paulo, BR Predicting Drug Penetration Across the Blood-Brain Barrier: Comparison of Micellar Liquid Chromatography and Immobilized Artificial Membrane Liquid Chromatography 1 1 1 2 1 Mike De Vrieze , Frdric Lynen , Kai Chen , Roman Szucs , Pat Sandra 1 2 Ghent University, Ghent, BE; Pfizer, Sandwich, GB Pharmacokinetic Studies of Loosening the Isoniazid Ale Eisner, Adam Martin, Bajerov Petra, Bajer Tom, Ribrov Pavla, Ventura Karel Univerzity of Pardubice, Pardubice, CZ Stability-Indicating UPLC Assay Method for Moxonidine Active Pharmaceutical Ingredient and Pharmaceutical Dosage Form 1 2 1 1 1 Jelena Golubovic , Svetlana Milovanovic , Biljana Otasevic , Mira Zecevic , Ana Protic 1 2 University of Belgrade-Faculty of Pharmacy, Belgrade, RS; Medicines and Medical Devices Agency of Serbia, Belgrade, RS Simultaneous Analysis of Gadolinium Chelates as Ionic MRI Contrast Agents and Anions by High Performance Ion Chromatography Peter Hajos, Diana Lukacs, Flora Geczo, Krisztian Horvath University of Pannonia, Veszprem, HU Head and Neck Irradiation Modulated Both Pharmacokinetics of 5-Fluorouracil and Cisplatin in Rats 1 2 3 1 4 3 Chen-Hsi Hsieh , May-Ling Hou , Hung-Chi Tai , Hui-Ju Tien , Li-Ying Wang , Yu-Jen Chen , 2 Tung-Hu Tsai 1 2 Far Eastern Memorial Hospital, New Taipei City, TW; National Yang-Ming University, Taipei, 3 4 TW; Mackay Memorial Hospital, Taipei, TW; National Taiwan University, Taipei, TW Research of Pyridinium Compounds in Plants with Therapeutic Properties UPLC/MS Studies Malgorzata Jakubowska, Malgorzata Urbaniak, Andrzej Marcinek, Jerzy Gebicki Lodz University of Technology, Lodz, PL Determination of Amlodipine Besylate in Pharmaceutical Preparations by Green Chromatographic Method Juhee Jung, Junghyun Kim, Unyong Kim, Joon Hyuk Suh, Han Young Eom, Hyun-Deok Cho, Yura Jung, Jeong-Rok Youm, Sang Beom Han Chung-Ang University, Seoul, KR 120
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Sphingosine 1-Phosphate Lyase Activity Measurement by HPLC-Fluorescence Detection Yong-Moon Lee, Kyong-Oh Shin, Cho-Hee Seo, Shin-Hee Lee College of Pharmacy, Chungbuk National University, Chongju, KR Streamlining Analysis of Desogestrel and Ethinyl Estradiol Oral Contraceptives with UPLC Margaret Maziarz, Sean M. McCarthy, Micheal D. Jones, Warren B. Potts Waters Corporation, Milford, MA, US Development and Validation of Rapid UHPLC Method for Determination of Risperidone and its Impurities in Bulk Powder and Tablets. Tomas Nejedly, Pavla Pilarova, Petr Kastner, Jiri Klimes Charles University in Prague, Faculty of Pharmacy, Hradec Kralove, CZ HPLC Method for Quantifying Tenofovir Disoproxil Fumarate in Raw Material, Tablet and their Degradation Products Mariana B. Almeida, Mirela F. Rabito, Erieldes S. Silva, Vinicius Acquaro Junior, Tiago B. Madeira, Marlene M. F. Nery, Suzana Lucy Nixdorf Universidade Estadual de Londrina, Londrina, BR The HPLC Method for Simultaneous Determination of Meropenem and Clavulanate Potassium Magdalena Paczkowska, Przemyslaw Zalewski, Judyta Cielecka-Piontek Dep. of Pharm. Chemistry, Poznan University of Medical Sciences, Poznan, PL Antiarrhytmics Determination by Liquid Chromatography 1 1 1 Juan Peris-Vicente , Samuel Carda-Broch , Beatriz Beltran-Martinavarro , Maria Rambla1 2 1 Alegre , Enrique Ochoa-Aranda , Josep Esteve-Romero 1 2 University Jaume I, Castell, ES; Hospital Provincial, Castell, ES Determination of Flavones in Passiflorae Herba (Passiflora Incarnata L., Passifloraceae) by UHPLC 1 2 2 1 Klaus Reif , Silvia Sponza , Johannes Novak , Hartwig Sievers 1 2 PhytoLab GmbH & Co. KG, Vestenbergsgreuth, DE; University of Veterinary Medicine Vienna, Vienna, AT Ion Chromatography: An Important Technique for Assay and Analysis of Drug Substances and Drug Products 1 1 2 Jeffrey Rohrer , Lipika Basumallick , Suparerk Tukkeeree 1 2 Thermo Fisher Scientific, Sunnyvale, CA, US; Thermo Fisher Scientific, Bangkok, TH Stability Indicating LC Method and LC-Qtofms Studies for the Separation and Identification of Degradation Products of Darunavir 1 2 3 3 3 Josilene Corra , Cristina Serra , Guilherme Titato , Fernando Lanas , Alvaro Santos-Neto , 1 Hrida Salgado 1 2 School of Pharmaceutical Sciences / UNESP, Araraquara, SP, BR; School of Pharmaceutical 3 Sciences / University of So Paulo, So Paulo, SP, BR; Institute of Chemistry of So Carlos / University of So Paulo, So Carlos, SP, BR A Risk- and Science-Based Quality-By-Design Approach in UPLC Method Development Case Study Ebastine Alexander H. Schmidt, Mijo Stanic Steiner Pharmaceuticals, Berlin, DE Highres MS Screening of Known and Unknown Impurities and Related Substances in Stability Study of Selected Pharmaceuticals. Ludovit Schreiber, Radoslav Halko, Milan Hutta Faculty of Natural Sciences Comenius University in Bratisl, Bratislava, SK 121
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The HPLC-DAD Method for Stability Studies of Tebipenem Pivoxyl Magdalena Paczkowska, Judyta Cielecka-Piontek, Przemyslaw Zalewski Dep.of Pharm.Chemistry,Poznan University of Medical Sciences, Poznan, PL HPLC-MS Methods for Detection of Pt(II) and Pt(IV) Complexes with Large Lipophilic Ligands Kamila Syslova, Petra Rehackova, Jan Svoboda, Milos Mikoska, Petr Kacer ICT Prague, Prague, CZ An Alternative Approach for the Estimation of Variance Components of Analytical Results in the Pharmaceutical Industry 1 1 2 Zsolt Szemk , Katalin Ganzler , Sndor Kemny 1 2 Gedeon Richter Plc., Budapest, HU; Budapest University of Technology and Economics, Budapest, HU Development of a Novel and Rapid Isocratic Rp-HPLC Method for the Analysis of Peptide Drug (Salmon Calcitonin)in Pharmaceutical Formulations 1 2 3 4 Cetin Tas , Saffar Mansoor , Ajay K. Banga , Mark R. Prausnitz 1 2 Gulhane Military Medical Academy Dept. of Pharm. Sci., Ankara, TR; School of Chemical and 3 Biomolecular Engineering, Georgia Institute of Technology, Atlanta, US; Department of Pharmaceutical Sciences College of Pharmacy and Health Sciences Mercer University, Atlanta, 4 US; School of Chemical and Biomolecular Engineering Georgia Institute of Technology, Atlanta, US UPLC-FLR Study for Determination of Nitric Oxide Production from Potential Nitric Oxide Donors Malgorzata Urbaniak, Adam Sikora, Andrzej Marcinek, Jerzy Gebicki Lodz University of Technology, Lodz, PL A High Resolution MS, MS/MS and UV Database of Fungal Secondary Metabolites as a Dereplication Protocol for Bioactive Natural Products 1 2 2 2 2 Albert Van Wyk , Tamam El-Elimat , Mario Figueroa , Brandie Ehrmann , Nadja Cech , Cedric 2 2 Pearce , Nicholas Oberlies 1 2 Advanced Chemistry Development (ACD/Labs), Bracknell, GB; Dept. of Chemistry and Biochemistry, University of North Carolina, Greensboro, US Development of Gradient HPLC Method for Simultaneous Determination of Sotalol Hydrochloride and Potassium Sorbate in Oral Liquid Paediatric Preparations 1 1 1 2 1 Lukas Zahalka , Oxana Zahalkova , Ludmila Matysova , Sylva Klovrzova , Zdenka Sklubalova , 1 Petr Solich 1 2 Charles University in Prague, Faculty of Pharmacy, Hradec Kralove, CZ; General Hospital in Motol, Hospital Pharmacy, Prague, CZ Stability-Indicating HPLC Method for the Determination of Cefozopran Hydrochloride 1 1 1 2 Magdalena Paczkowska , Przemyslaw Zalewski , Judyta Cielecka-Piontek , Anna Krause 1 2 Dep.of Pharm.Chemistry,Poznan University of Medical Sciences, Poznan, PL; PozLab, Contract Research Organization, Poznan, PL Use of a Multidimensional Design Space for in Silico Robustness Testing of a Compendial LC Purity Method Alexander H. Schmidt, Mijo Stanic Steiner Pharmaceuticals, Berlin, DE
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Determination of Trioxsalen in Capsules by High Performance Liquid Chromatography 1 1 1 Naiana Gondim Pereira Barros Lima , Igor Prado Barros Lima , Denise Michele Costa Barros , 1 1 1 Thays Santos Oliveira , Karla Danielle Gomes dos Santos , Lilian Grace Silva Solon , Cicero 1 2 Flavio Soares Aragao , Ana Claudia Dantas de Medeiros 1 2 UFRN, Natal, BR; UFCG, Campina Grande, BR Transfer of USP Methods for Impurities Analysis of Ziprasidone Hcl between HPLC Systems and to UPLC Margaret Maziarz, Michael D. Jones, Frederic Forini, Warren B. Potts, Sean M. McCarthy Waters Corporation, Milford, MA, US
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Polymers
Advances in Size-Based Separations of Synthetic Polymers Bonnie Alden, Ed Bouvier, Ken Glose, Pamela Iraneta, Gary Izzo, Nicole Lawrence, Mike Savaria, Jeremy Shia, Mia Summers, Tom Walter, Jessica Wilson, Kevin Wyndham Waters Corporation, Milford MA, US A Novel Selective Molecularly Imprinted Polymer for Application in Solid Phase Extraction for the Determination of Hydrochlorothiazide in Urine Using HPLC Leonardo Barros, Susanne Rath University of Campinas, Campinas/SP, BR Monitoring the Degradation of Stabilizers for Polypropylene after Exposure to Heat by HPLC-MS/MS 1 1 2 Susanne Beimann , Wolfgang Buchberger , Gernot Wallner 1 2 JKU - Institute of Analytical Chemistry (JKU-IAC), Linz, AT; JKU - Institute of Polymeric Materials and Testing (JKU-IPMT), Linz, AT Size Exclusion Chromatography as an Alternative Technique for the True Boiling Point (TBP) and Final Boiling Point (FBP) Determination of High Boiling Petroleum Fractions and Products Boczkaj Grzegorz, Marian Kamiski Gdansk University of Technology, Gdansk, PL Using the Hydrophobic Subtraction Model to Choose Orthogonal Columns for Online Comprehensive Two-Dimensional Liquid Chromatography Rune Grsbll, Nikoline Nielsen, Jan Christensen University of Copenhagen, Frederiksberg C, DK High Temperature Gradient Liquid Chromatography of Bimodal High Density Polyethylene 1 1 1 2 2 Kavimani Nagar Prabhu , Tibor Macko , Robert Brll , Priya Garg , Linda Havermans , Klaas 2 Remerie 1 2 Fraunhofer Institute, LBF, Darmstadt, DE; SABIC, Geelen, NL Preparation and Characterization of Mesoporous Organosilica Adsorbents Xue Min, Xu Zhong, Tai Yang, Zihui Meng Beijing Insititute of Technology, Beijing, CN Analysis of Purified Terephthalic Acid (PTA) by Capillary Zone Electrophoresis 1 1 1 2 John C. Hudson , Jim Thorn , Hans Dewald , Zhen-lei Peng 1 2 Beckman Coulter Inc., Brea, CA, US; Sinopec SRIPT, Shanghai, CN A Screen for Eleven Electrospun Nanofiber Sorbents for their Sorption Capacity towards a Carcinogenic Biomarker: 1-Hydroxypyrene 1 2 1 2 Okechukwu Ifegwu , Samuel Chigome , Chimezie Anyakora , Nelson Torto 1 2 University of Lagos, Akoka, Lagos, NG; Rhodes University, Grahamstown, ZA 123
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Application of Electrophoretically Mediated Microanalysis to the In-Capillary Digestion of Poly-L-Lysine Amal Ibrahim, Andrea Megret, Galle Coussot, Catherine Perrin Institute of Biomolecules Max Mousseron, UMR 5247 CNRS, UM, Montpellier, FR Using CE-MS for the Identification of Polyimide Materials Christian Klampfl, Timothy Causon, Markus Himmelsbach, Wolfgang Buchberger Johannes Kepler University Linz, Linz, AT Preparation and Characterization of Ethinyloestradiol Molecular Imprinted Membrane Xue Min, Xiaofeng Wu, Xiangrong Mu, Zihui Meng Beijing Institute of Technology, Beijing, CN Analysis of Stabilisers in Plastic Materials Used for Photovoltaic Modules by HPLC and MS Techniques 1 1 2 Ingrid Hintersteiner , Wolfgang Buchberger , Gernot Wallner 1 2 Institut of Analytical chemistry, JKU Linz, Linz, AT; Institut of Polymer and Material Testing, JKU Linz, Linz, AT Advances in SEC for Polymer Engineering Applications Michael OLeary, Bonnie Alden, Edouard Bouvier, Peter Hancock, Jeremy Shai, Mia; ummers, Marian Twohig Waters Corp, Milford, MA, US Evaluation of Electrospun/Electrospray Polysulfone Fibers and Particles as SPE Sorbent for Pesticides Analysis Noor Gulamussen, Nelson Torto Rhodes University, Grahamstown, ZA Gradient Liquid Chromatography of Ethylene/1-Alkene Copolymers 1 1 1 1 2 Rajesh Chitta , Tibor Macko , Robert Brll , Prabhu Kavimani Nagar , Christophe Boisson , 2 Olivier Boyron 1 2 Fraunhofer Institute, LBF, Darmstadt, DE; University of Lyon, Lyon, DE Electrospun Poly(Co-Styrene) Solid Phase Extraction Sorbents for Alkylphenols Yolanda Tancu, Nelson Torto Rhodes University, Grahamstown, ZA Molecularly Imprinted Polymer (MIP) Dedicated to the Extraction of Glyphosate and its Metabolite, AMPA, in Water 1 1 2 2 2 Kinga Puzio , Berengere Claude , Catherine Berho , Emeline Grellet , Laurence Amalric , Sami 3 1 Bayoudh , Philippe Morin 1 2 ICOA UMR 7311, Universit dOrlans, Orlans, FR; BRGM Direction des laboratoires, 3 Orlans, FR; POLYINTELL, Val de Reuil, FR Application of the General Theory of Gradient Elution to Characterization of Functionalized Polymers Christopher Rasmussen, Brian McCauley, Yefim Brun DuPont, Wilmington, US Quantitative Evaluation of the Evaporative Light Scattering Detector Response for Linear Polyethylene Jan-Hendrik Arndt, Tibor Macko, Robert Brll, Kavimani Nagar Prabhu Fraunhofer Institute, LBF, Darmstadt, DE
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124
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Multivariate Curve Resolution Alternating Least Squares for Improved SEC-DAD Deconvolution of Complex Polymer Samples Tim Van Hoeylandt, Kai Chen, Filip Du Prez, Frdric Lynen Ghent University, Ghent, BE Comprehensive Characterization of Copolymers and Polymer Mixtures Containing Polymers of Different Polarities Elena Uliyanchenko, Christian Wold, Jan Henk Kamps, Tanzeela Raja SABIC, Bergen op Zoom, NL
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PROT01_MO
Proteomics
Intact Protein LC-MS, How to Overcome the Challenges? 1 1 1 2 3 Mauro De Pra , Evert-Jan Sneekes , Laurent Rieux , Christian Ravnsborg , Dafydd Milton , 1 Remco Swart 1 2 3 Thermo Fisher Scientific, Amsterdam, NL; Thermo Fisher Scientific, Odense, DK; Thermo Fisher Scientific, Runcorn, GB Simple Two-Dimensional Separation Platform for Peptide Analysis Filip Dua, Josef estk, Dana Moravcov, Josef Planeta, Vladislav Kahle Institute of Analytical Chemistry of the ASCR, v. v. i., Brno, CZ High Performance Thin Layer Chromatography Nanospray Mass Spectrometry Using the Advion Nanomate System Hans Griesinger, Susanne Minarik, Bernhard Schubach, Katerina Matheis, Michael Schulz Merck KGaA, Darmstadt, DE Solid-Phase Based Technologies and Methods for Glycoproteome and Phosphoproteome Analysis Zou Hanfa, Fangjun Wang, Mingliang Ye, Jun Zhu, Zhen Sun, Hongqiang Qin, Junfeng Huang Dalian Institute of Chemical Physics, Dalian, CN Charged Surface Hybrid C18 for High Resolution Peptide Analyses and Lab Scale Peptide Purifications Matthew Lauber, Stephan Koza, Pamela Iraneta, Kenneth Fountain Waters Corporation, Milford, US Electrochemically Assisted Reduction of Disulfide Bonds in Peptides and Proteins with On-Line Mass Spectrometric Detection Agnieszka Kraj, Martin Eysberg, Hendrik-Jan Brouwer, Jean-Pierre Chervet Antec, Zoeterwoude, NL Quantitative Proteomic Profiling with HPLC-MS/MS: Comparison of Various Labelling Strategies Using Itraq and TMT 1 2 1 1 2 Theresa Kristl , Marc Rurik , Angela Schmiedlechner , Albert Duschl , Oliver Kohlbacher , 1 Christian Huber 1 2 University of Salzburg, Salzburg, AT; University of Tbingen, Tbingen, DE Characterization of an Immobilized Trypsin PLOT Column Used in an On-Line LC-MS System Hanne Kolsrud Hustoft, Ole Kristian Brandtzg, Steven Ray Wilson, Tyge Greibrokk, Elsa Lundanes Department of Chemistry, Oslo, NO A Proteomics Screening Method for the Identification of Antimicrobial Active Molecules in Colombian Snake Venom Andres M. Tibabuzo, Jackson Ocampo, Barbara H. Zimmermann, Chad Leidy, Roland J.W. Meesters Universidad de los Andes, Bogota D.C., CO 125
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PROT03_WE
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PROT09_WE
PROT10_MO PROT11_TU
Peptide Separation on a Normal Phase Column Under HILIC Separation Conditions Goran Mitulovi, Andreas Fichtenbaum, Rainer Schmid Medizinische Universitt Wien, KILM, Wien, AT High-Resolution Peptide Separations Using Nano-Liquid Chromatography At UltraHigh Pressure 1 2 2 2 3 Lucie Novakova , Axel Vaast , Catherine Stassen , Ken Broeckhoven , Mauro De Pa , Remco 3 2 Swart , Sebastiaan Eeltink 1 2 Charles University in Prague, Hradec Krlov, CZ; Vrije Universiteit Brussel, Brussel, BE; 3 Thermo Fisher Scientific, Amsterdam, NL A Natural Point Mutation Changes Both Target Selectivity and Mechanism of Action of Sea Anemone Toxins. 1 2 3 3 4 Steve Peigneur , Lszl Bress , Carolina Mller , Frank Mar , Wolf-Georg Forssmann , Jan 1 Tytgat 1 2 3 University of Leuven, Leuven, BE; Hannover Medical University, Hannover, DE; Florida 4 Atlantic University, Boca Raton, US; Pharis Biotec GmbH, Hannover, DE Robust Phosphoproteome Enrichment Using Titanium (IV) Affinity Chromatography 1 1 2 1 1 Houijang Zhou , Harm Post , Hanfa Zou , Shabaz Mohammed , Albert J.R. Heck 1 2 Utrecht University, Utrecht, NL; Chinese Academy of Sciences, Dalian, CN The Effects of HPLC-Analysis to Proteins and How to Affect These Effects for Precise and Reproducible Protein Analytic Tobias Rakow, Hermann Wtzig Technische Universitt Braunschweig, Braunschweig, DE Specific Recognition of Tyrosine-Phosphorylated Peptides by Epitope-Imprinting Strategy Xueqin Ren, Yufeng Hu, Feng Shen, Qiushui Li, Lin Xu China Agricultural University, Beijing, CN Molecular Imprinted Polymers as New Tools in Small Cell Lung Cancer Diagnosis. 1 1 2 2 1 Cecilia Rossetti , Trine Halvorsen , Abed Qader , Brje Sellergren , Lon Reubsaet 1 2 University of Oslo, Oslo, NO; Technical University of Dortmund, Dortmund, DE Optimized Superficially Porous Particles for Peptide and Protein Analysis Stephanie A. Schuster, Joseph J. Kirkland, Brian M. Wagner, Barry E. Boyes, Joseph J. DeStefano Advanced Materials Technology, Inc., Wilmington, DE, US High Performance Thin Layer Chromatography Mass Spectrometry Using the Camag TLC-MS Interface Axel-Walter Thomasberger, Hans Griesinger, Susanne Minarik, Katerina Matheis, Michael Schulz Merck KGaA, Darmstadt, DE Parameters Affecting the Gradient Reversed-Phase Separation of Peptides and Intact Proteins Axel Vaast, Eva Tyteca, Gert Desmet, Sebastiaan Eeltink Vrije Universiteit Brussel, Brussel, BE Proteomic Analysis of N- and O-Linked Glycosylation Based on Hydrophilic Interaction Chromatography Jun Zhu, Fangjun Wang, Kai Cheng, Mingliang Ye, Hanfa Zou Dalian Institute of Chemical Physics, CAS, Dalian, CN
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126
PROT21_WE
The Kinetic Study of Petide Digestion by Trypsin 1 1 2 1 Tereza lechtov , Kvta Kalkov , Martin Gilar , Eva Tesaov 1 2 Charles University in Prague, Prague, CZ; Waters Corporation, Milford, US Contichrom: A Versatile Purification Platform with All-In-One Process Capabilities Guido Stroehlein, Thomas Mueller-Spaeth, Lars Aumann, Michael Bavand ChromaCon AG, Zuerich, CH
PROT23_TU
QTMS01_MO
Quantitative MS
Development and Validation of Reverse Phase Liquid Chromatography Time-OfFlight / Mass Spectrometry Method for Simultaneous Analysis of Four Antiinflammatory Pharmaceuticals in Water. 1 1 1 2 1 Fouad Al-Qaim , Pauzi Mohamed , Mohamed Othman , Zuriati Zakaria , Jalifa Latip 1 2 National University of Malaysia (UKM), Bangi, MY; Malaysian-Japan International Institute of Technology(MJIIT), Kuala Lumpur, MY Optimization of a Transglycosylation Assay for S. Aureus PBP2 Bart Blanchaert, Erwin Adams, Ann Van Schepdael KU Leuven, Leuven, BE Determination of Asymmetric and Symmetric Dimethylarginine in Serum from Patients with Chronic Kidney Disease: UPLC-MS/MS Versus ELISA 1 2 2 2 1 Jente Boelaert , Eva Schepers , Griet Glorieux , Raymond Vanholder , Frdric Lynen 1 2 Separation Science Group, Ghent University, Gent, BE; Renal Division, Ghent University, Gent, BE High Performance Liquid Chromatography Mass Spectrometry for Simultaneous Determination of Polar Pollutants in Zebrafish Embryos Stephan Brox, Axel P. Ritter, Eberhard Kster, Thorsten Reemtsma Helmholtz- Centre for Environmental Research UFZ, Leipzig, DE Determination of Residual Amounts of Aminoglycosides in Food Products of Animal Origin by Ultra High Performance Liquid Chromatography Coupled with High Resolution Mass Spectrometry Serguei Calugaru, Evgeny Khvatov, Pavel Metalnikov, Alexander Komarov VGNKI, Moscow, RU Rapid Determination of Selected Artificial Sweeteners in Beverage Samples by Ultra Performance Liquid Chromatography with Photodiode Array and Tandem Mass Spectrometry Detection Antonia M Carro, Teresa Pena, Purificacin Fernandez, Maria Regenjo, Paula Gonzalez, Rosa A. Lorenzo University of Santiago de Compostela, Santiago De Compostela, ES Development, Validation and Application of a Method for the Analysis of Quaternary Ammonium Compounds (Qacs) in Dairy Products by LC-MS/MS Christoph Czerwenka, Eveline Dorn Austrian Agency for Health and Food Safety, Wien, AT Analysis of Perfluorinated Surfactants in Electroplating Industries by HPLC-MS/MS 1 1 2 Ina Ebersbach , Oliver J. Schmitz , Joachim M. Marzinkowski 1 2 University Duisburg-Essen, Applied Analytical Chemistry, Essen, DE; University of Wuppertal, Wuppertal, DE
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QTMS03_WE
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QTMS05_TU
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QTMS08_TU
127
QTMS09_WE
Fast UHPLC-MS/MS Method for Simultaneous Quantification of Erlotinib, OSI-420, Sunitinib, SU-12662, and Pazopanib in Dried Blood Spots (DBS) 1 1 1 2 Massimiliano Donzelli , Daria Winogradova , Benjamin Berger , Bjrn-Thoralf Erxleben , Udo 3 4 5 1 1 Burger , Magdalena Swiderska , Markus Joerger , Stephan Krhenbhl , Manuel Haschke 1 2 3 University Hospital Basel, Basel, CH; Shimadzu Europe, Duisburg, DE; Shimadzu Schweiz 4 5 GmbH, Reinach, CH; Camag, Muttenz, CH; Kantonsspital St. Gallen, St. Gallen, CH A Survey of the Occurrence of Ochratoxin A in Madeira Wines Based on a Modified Quechers Extraction Procedure Combined with Liquid ChromatographyTriple Quadrupole Tandem Mass Spectrometry 1 1 2 2 Paulo Fernandes , Nlson Barros , Jorge Pereira , Jos S. Cmara 1 2 Laboratrio Regional de Veterinria e Segurana Alimentar, Funchal, PT; CQM, UMa, Funchal, PT Rhpda Probe for Nitric Oxide- UPLC/MS Analysis Ewa Gapys, Malgorzata Urbaniak, Jan Adamus, Adam Sikora, Andrzej Marcinek Lodz University of Technology, Lodz, PL Analysis of Carnitine Precursors in Biological Matrices by Ultra Performance Liquid Chromatography Tandem Mass Spectrometry (UPLC/MS/MS) Solveiga Grinberga, Eduards Sevostjanovs, Osvalds Pugovics, Edgars Liepins Latvian Institute of Organic Synthesis, Riga, LV Validated LC-MS/MS Method for the Determination of Tranquilizers and -Blocker Residues in Animal Kidney Dominique Hurtaud-Pessel, Pierrick Couedor, Eric Verdon Anses, Laboratoire De Fougres, Fougeres, FR Determination of Antifungal Drugs Illegally Added in Cosmetics by Ultra High Performance Liquid Chromatography/Triple Quadrupole Mass Spectrometry Yin Huo, Chao Ma, Hui Gao, Qisheng Zhong, Lingling Zhong, Song Zhan, Shinichi Kawano, Taohong Huang, Yuki Hashi Shimadzu (China) Co.,Ltd., Beijing, CN Validation of an LC-MS/MS Method in Line with EU Decision 2002/657/EC for Triphenyl Methane Dyes in Fish Muammer Kaplan, Elmas ktem Olgun, znur Karaolu Tubitak MRC Food Institute, Kocaeli, TR Development of a Rapid LC-MS/MS Method for the Determination of Thyreostatic Drugs in Urine and Gland Tissue Muammer Kaplan, Elmas Oktem Olgun, Oznur Karaoglu Bar Mah. Dr. Zeki Acar Cad. No: P.K. 2, Kocaeli, TR Ultra Performance Liquid Chromatography Coupled to Mass Spectrometry Determination of Salmeterol and its Main Degradation Product in a Pharmaceutical Dry Powder Inhaler Reginald Klinkenberg Galephar M/F, Marche-en-Famenne, BE Comparison of Direct Large Volume Injection and Online-Solid Phase Extraction LCMS for the Determination of Hormones in Different Water Bodies 1 1 1 2 2 Sebastian Kowal , Friedrich Werres , Peter Balsaa , Torsten Schmidt , Kristina Lang 1 2 IWW Water Centre, Mlheim an der Ruhr, DE; university duisburg essen, Essen, DE
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128
QTMS19_MO
Development of Chemical and Physical Methods to Examine a Multiple Traditional Chinese Herbal Prescription by LC-MS/MS, Electron Microscope and Congo Red Stained 1 1 2 1 Chia-Ming Lu , Mei-Ling Hou , Lie-Chwen Lin , Tung-Hu Tsai 1 2 National Yang-Ming University, Taipei, TW; National Research Institute of Chinese Medicine, Taipei, TW Nano UPLC-ESI-MS/MS for the in Vivo Monitoring of Neuropeptides During Epileptic Seizures 1 2 1 1 Katrien Maes , Guillaume Bchade , Jolien Van Schoors , Yvan Vander Heyden , Yvette 1 1 1 Michotte , Ilse Smolders , Ann Van Eeckhaut 1 2 Vrije Universiteit Brussel, Brussels, BE; Waters, Zellik, BE Ultraperformance Lc and Dried Blood Spot Sampling as Novel Tools in the Rapid Determination of Pharmacokinetic Parameters of Drug Substances. Krishna Mahabir, Hans-Gerd Janssen, Boudewijn Hollebrands, Pieter vd Pijl, Guus Duchateau Unilever R&D, Vlaadingen, NL Identification and Quantification of Lignans in Wine By-Products in Marc and Grape Seeds Using Lc-Ms 1 2 2 2 1 Iveta Maresova , Jan Triska , Martin Moos , Nadezda Vrchotova , Dana Jirotkova 1 2 University of South Bohemia, Faculty of Agriculture, Ceske Budejovice, CZ; Global Change Research Centre AS CR, Ceske Budejovice, CZ LC-MS/MS Determination of Ibuprofen Enantiomers in Human Serum Using Automated SPE Extraction Natalija Nakov, Liljana Bogdanovska, Ljiljana Ugrinova, Zoran Kavrakovski, Aneta Dimitrovska, Rumenka Petkovska Faculty of Pharmacy, University "Ss Cyril and Methodius", Skopje, MK Validation and Application of an UPLC-MS/MS Method for a PK Study of an AntiAllergic Indolinone Derivative in Rat Plasma 1 2 3 1 Mouhssin OUFIR , Veronika Butterweck , Chethan Sampath , Daniela Eigenmann , Matthias 1 Hamburger 1 2 Division of Pharmaceutical Biology, University of Basel, Basel, CH; Institute of Pharma; Technology, University of Applied Sciences Northwestern Switzerland, Muttenz, CH; 3 Department of Pharmaceutics, University of Florida, Gainesville FL, US LC-MS and LC-MS/MS for Determination of Water-Soluble Vitamins in Foods Melissa Phillips, Catherine Rimmer, Lane Sander NIST, Gaithersburg, US Rapid and Robust Analysis Method for Quantifying Antidepressants and Major Metabolites in Human Serum by UHPLC-MS/MS 1 2 1 1 Christ Pijnenburg , Vincent Goudriaan , Jacob Diepenbroek , Jan Giesbertsen , Annemieke 1 Vermeulen Windsant-v.d. Tweel 1 2 ZANOB BV, 's-Hertogenbosch, NL; Shimadzu Benelux BV, 's-Hertogenbosch, NL Quantitation of Central Carbon Metabolites in Human Blood Spots by Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) 1 2 1 1 Estitxu Rico , Oskar Gonzlez , Mara Encarnacin Blanco , Rosa Mara Alonso 1 2 University of the Basque Country, Leioa, ES; Leiden University, Leiden, NL Quantitative Determination of Fentanyl in Newborn Pig Plasma and Cerebrospinal Fluid by HPLC-MS/MS 1 2 1 1 1 M. Encarnacin Blanco , Oskar Gonzlez , Estitxu Rico , Rosa Mara Alonso , Esther Encinas , 1 Elena Surez 1 2 Universidad del Pas Vasco/EHU, Leioa, ES; Leiden University, Leiden, NL 129
QTMS20_TU
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Quantification of Dabigatran in Human Plasma by LC-MS/MS 1 1 2 1 Yuko Rnquist-Nii , Anton Pohanka , Rickard E. Malmstrm , Olof Beck 1 2 Karolinska University Hospital, Huddinge, Stockholm, SE; Karolinska Institutet & Karolinska University Hospital, Stockholm, SE A Bioanalytical Study on Two Thiosemicarbazone Antineoplastic Agents, DPC and DP44MT, in Rats Using LC-MS 1 1 1 2 3 Vit Sestak , Jan Stariat , Vlasta Suprunova , Stanislav Micuda , Des Richardson , Petra 1 Kovarikova 1 2 Faculty of Pharmacy, Charles University, Hradec Kralove, CZ; Faculty of Medicine in HK, 3 Charles University, Hradec Kralove, CZ; Department of Pathology and Bosch Institute, University of Sydney, Sydney, AU Micro Ultra High Pressure Liquid Chromatography - Mass Spectrometry for the Quantification of Pharmaceuticals Using Dried Blood Spot Sample Collection Format 1 2 1 1 Kyoko Watanabe , Neil Loftus , Emmanuel Varesio , Grard Hopfgartner 1 2 University of Geneva, Geneva, CH; Shimadzu Corporation, Manchester, GB Determination of Proanthocyanidins in Litchi (Litchi Chinensis Sonn.) Flower by HPLC-DAD-ESI/MS 1 1 1 2 1 Deng-Jye Yang , Jau-Tien Lin , Yan-Zin Chang , Yi-Chen Chen , Shih-Chuan Liu , Chuan-Hsiang 1 Hsu 1 2 Chung Shan Medical University, Taichung, TW; National Taiwan University, Taipei, TW Specific Enrichment of 3-NitrotyrosineContaining Peptides for Biomarker Discovery Yun Yang, Sara Ongay, Ido Kema, Rainer Bischoff University of Groningen, Groningen, NL Analysis of Gluconate in Radioactive Wastes Prior to their Disposal 1 1 1 2 Laurence du Bois de Maquill , Laetitia Renaudin , Florence Goutelard , Alain Jardy , Jrome 2 2 Vial , Didier Thibaut 1 2 CEA Saclay, France, FR; ESPCI-LSABM, France, FR
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RMEC01_MO
Retention Mechanisms
Adamantyl-Group Containing Mixed-Mode Acrylamide-Based Continuous Beds for Capillary Electrochromatography Ayat Allah Al-Massaedh, Ute Pyell University of Marburg, Marburg, DE Preparation and Characterization of Stationary Phases for HPLC Using Mixture of PDMS and PMODS Carla Grazieli Azevedo da Silva, Elias Silva Jnior, Carol Collins Institute of Chemistry/University of Campinas (UNICAMP), Campinas/SP, BR Analysis of Glyphosate and AMPA in Environmental Water Samples by Ion Chromatography and on Line Mass Spectrometry Without Derivatization. Cees Bruggink, Frans Schoutsen Thermo Fisher Scientific, Breda, NL Investigation of the Retention Mechanisms on Grafted Monolithic Columns Based on Adsorption Isotherms 1 1 1 2 2 Ekaterina Davydova , Rudy Vonk , Muzi Li , Patrik Forssn , Torgny Fornstedt , Peter 1 Schoenmakers 1 2 University of Amsterdam, Amsterdam, NL; Karlstad University, Karlstad, SE
RMEC02_TU
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130
RMEC05_TU
Influence of Pressure and Temperature on Molar Volume and Retention Properties of Peptides in Ultra-High Pressure Liquid Chromatography 1 2 1 Szabolcs Fekete , Krisztian Horvath , Davy Guillarme 1 2 University of Geneva, Geneva, CH; University of Pannonia, Veszprem, HU Hydrophilic Interaction Liquid Chromatography as an Alternative Method for the Determination of Iodinated X-Ray Contrast Media Nuria Fontanals, Daniela Salas, Francesc Borrull, Rosa Maria Marc Universitat Rovira i Virgili, Tarragona, ES Poly(3-Chloro-2-Hydroxypropyl Methacrylate) Based Reactive Monolith with Derivatization Flexibility as a New Separation Medium for Capillary Electrochromatography. Part I: Sulfonic Acid Functionalized Strong Cation Exchance Stationary Phase Aslihan Gokaltun, Cemil Aydogan, Bekir Celebi, Adil Denizli, Ali Tuncel hacettepe University, Ankara, TR A New Approach to Increase Volume Loading for Analytical and Semi-Preparative RP Gradient Separations of Small Molecules Wolfgang Goetzinger, Shawn Ayube, Grace Bi, Larry Miller Amgen, Cambridge, US Practical Observations on the Dynamic Performance of Bare Silica in HILIC Compared to RPLC 1 2 2 3 1 James Heaton , Xiaoli Wang , William Barber , Stephan Buckenmaier , David McCalley 1 2 3 University of the West of England, Bristol, GB; Agilent Technologies, Delaware, US; Agilent Technologies, Waldbronn, DE Polymethacrylate Monoliths Functionalized with Cysteine for Capillary Electrochromatography Applications Isabel Ten-Domnech, Ernesto Sim-Alfonso, Guillermo Ramis-Ramos, Jos Manuel HerreroMartnez Dept. Analytical Chemistry, University of Valencia, Burjassot (Valencia), ES Molecular Shape Recognition of Self-Assembled Molecular Gel-Grafted Silica Particles in RP-HPLC Noguchi Hiroki, Thiraporn Charoenraks, Makoto Takafuji, Hirotaka Ihara Kumamoto University, Kumamoto, JP Combined Pore-Scale Modeling of Mass-Transport and Stochastic Simulation of Sorption in Chromatographic Packings Dzmitry Hlushkou, Anton Daneyko, Ulrich Tallarek Philipps-Universitt-Marburg, Marburg, DE Analysis of Marine Biotoxins, Paralytic Shellfish Poisoning (PSP) and Diarrheic Shellfish Poisoning Toxins (DSP) in Mussels, (Mytilus Galloprovincialis) Along the Namibian Central Coast. Dijerenge Kahe Johanna University of Namibia, Swakopmund, NA Analysis of Anti-Oxidant Phenolic Compounds in Dentifrices by RP-HPLC in Different Column Temerature 1 2 3 3 3 JungHyun Kim , Jungin Kim , Jeehyun Hwang , Hyo Kwang Ahn , Joo Young Lee , Chang woog 4 Kim 1 2 KAIST, Chemical and biomolecular engineering, Daejeon, KR; Kwandong University College of 3 Medicine, Gangneung, KR; Department of Preventive Social Dentistry School of Dentistry, 4 Kyung Hee University, Seoul, KR; Gabriel Dental Clinic, Seoul, KR
RMEC06_WE
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RMEC08_TU
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RMEC11_TU
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131
RMEC15_WE
Simultaneous Analysis of Carbapenems in Human Bodily Liquids Using HFIP as Buffer Additive in LC/ESI/MS/MS 1 1 2 2 1 Karin Kipper , Kristi Hdma , Kadri Tamme , Joel Starkopf , Koit Herodes 1 2 Institute of Chemistry, University of Tartu, Tartu, EE; Clinic of Anaesthesiology and Intensive Care, University of Tartu, Tartu, EE Comparison of the Mass-Transfer Properties of Insulin on Stationary Phases of Different Geometry in HPLC Ibolya Kiss, Nndor Lambert, Ferenc Kilr, Attila Felinger University Pcs, Pcs, HU Development of a Hydrophilic Interaction Liquid Chromatography Method with Tandem Mass Spectrometric Detection for the Analysis of Pteridines in Two Graphosoma Species (Insecta: Heteroptera) 1 1 2 2 1 Petr Kozlik , Jan Krajicek , Kveta Kalikova , Eva Tesarova , Zuzana Bosakova 1 2 Charles University, Department of Analytical Chemistry, Prague, CZ; Charles University, Department of Physical and Macromolecular Chemistry, Prague, CZ Comparison of Three HILIC Approaches for the Determination of Pharmaceutical Residues by Electrospray Ionization Tandem Mass Spectrometry (HILIC ESIMS/MS) Pawe Kubica, Anna Jakimska, Agata Kot-Wasik, Andrzej Wasik, Jacek Namienik Gdansk University of Technology, Gdansk, PL Large Volume Injection of Aqueous Samples in Nano Liquid Chromatography Using Serially Coupled Columns. 1 1 1 2 Juri Leonhardt , Thorsten Teutenberg , Terence Hetzel , Torsten C. Schmidt 1 2 Institute of Energy and Environmental Technology e.V. (IUTA), Duisburg, DE; University Duisburg-Essen, Instrumental Analytical Chemistry, Essen, DE Substitution of Water by Methanol in Aqueous Normal Phase Liquid Chromatography Jan Soukup, Pavel Jandera University of Pardubice, Pardubice, CZ Hydrophilic Liquid Chromatography with Ternary Mobile Phases: A Molecular Dynamics Study Versus Experimental Observations 1 1 2 1 Sergey Melnikov , Alexandra Hoeltzel , Andreas Seidel-Morgenstern , Ulrich Tallarek 1 2 Philipps-Universitt, Marburg, DE; Max-Planck-Institut fr Dynamik komplexer technischer Systeme, Magdeburg, DE Computer-Assisted Modeling of Separation and Investigation of Dominant Retention Mechanism for Naturally Occurring Triterpenoids and Phytosterols 1 1 2 Katerina Naumoska , Zoran Kitanovski , Irena Vovk 1 2 National Institute of Chemistry, Ljubljana, SI; National Institute of Chemistry; EN-FIST Centre of Excellence, Ljubljana, SI Investigation of Stability and Determination of Contents for Catecins in Camellia Sinensis Containing Dentifrices 1 1 2 3 4 Yong Duk Park , Jung Eun Park , Su Min Yoo , Ji-Hwan Kim , Ha-Jeong Kwon 1 2 Department of Preventive Social Dentistry, Kyung Hee Univ., Seoul, KR; Department of 3 Dental Hygiene, Dong-Woo College, Sokcho, KR; College of Health Science, Korea University, 4 Seoul, KR; Department of Preventive Social Dentistry, Kyung Hee Univ.,, Seoul, KR A Comparison of the HPLC Retention Mechanisms on Silica Gel and Silica C 1 1 1 2 Eman Santali , Darren Edwards , David Watson , Oliver Sutcliffe 1 2 University of Strathclyde, Glasgow, GB; Manchester Metropolitan University, Manchester, GB
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Molecular Theory of Size Exclusion Chromatography for Wide Pore Size Distributions Annamria Sepsey, Ivett Bacskay, Attila Felinger University of Pcs, Pcs, HU Adsorption of WaterAcetonitrile Mixtures to Model Silica Surfaces 1 1 2 1 Sergey Melnikov , Alexandra Hoeltzel , Andreas Seidel-Morgenstern , Ulrich Tallarek 1 2 Philipps-Universitt, Marburg, DE; Max-Planck-Institut fr Dynamik komplexer technischer Systeme, Magdeburg, DE Comparison of Fundamental Equations for Gradient Elution Chromatography Jos Ramn Torres-Lapasi, Juan Jos Baeza-Baeza, Mara Celia Garca-lvarez-Coque University of Valencia, Burjassot (Valencia), ES Education in Liquid Chromatography in the Lab. Poster Presentation 1,2 Wim Staal 1 2 Hogeschool van Arnhem en Nijmegen, Hoogerheide, NL; HAN University of Applied Sciences, Nijmegen, NL Ion-Pair UHPLC Analysis of Monoamines: Peak-Splitting At High Flow Rates 1 2 1 1 Jolien Van Schoors , Hendrik-Jan Brouwer , Katrien Maes , Yvette Michotte , Ann Van 1 Eeckhaut 1 2 Vrije Universiteit Brussel, Jette, Brussels, BE; Antec BV, Zoeterwoude, NL Adapting the Surface Chemistry of Organic Monolithic Stationary Phases Using a Central Composite Design for the Optimization of an 2-Step Photografting Approach 1 1 2 1 1 R.J. Vonk , M. Li , S. Eeltink , G. Viv-Truyols , P.J. Schoenmakers 1 2 Universiteit van Amsterdam, Amsterdam, NL; Vrije Universiteit Brussel, Brussel, BE Effect of Buffer Salt Concentration in Hydrophilic Interaction Chromatography on a Zwitterionic Stationary Phase Caroline West, Emeline Auroux ICOA, CNRS UMR 7311, University of Orlans, Orlans, FR Application of Amino Stationary Phases for the Analysis of Carbohydrates Mark Woodruff, Neil McGrath Fortis Technologies Ltd, Neston, GB Prediction of Overloaded Profiles in Gradient Elution Chromatography 1 2 1 1 1 Dennis sberg , Marek Lesko , Martin Enmark , Jrgen Samuelsson , Patrik Forssn , Krzysztof 2 1 Kaczmarski , Torgny Fornstedt 1 2 Department of Engineering and Chemical Sciences, Karlstad, SE; Rzeszow University of Technology, Rzeszow, PL
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SAMP01_MO
Sample Preparation
Development and Evaluation of Quechers-Based Extraction and HPLC Method for Quantifying of Synthetic Food Dyes in Confectionery Samples Martin Adam, Petr esla, Ale Eisner, Andrea kov, Karel Ventura University of Pardubice, Department of Analytical Chemistry, Pardubice, CZ Determination of Enzimatic Degradation Products of N-Homocysteinylated Proteins in Plasma by High Performance Liquid Chromatography Kamila Borowczyk, Edward Bald, Rafa Gowacki University of Lodz, Faculty of Chemistry, Dep. Env. Chem., Lodz, PL
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Surfactant-Modified Sorbents and their Applications for Extraction of Carbamate Insecticides Prior to Analysis by HPLC Rodjana Burakham, Prapha Arnnok Khon Kaen University, Khon Kaen, TH Analysis of Various Matrix Containing Food Samples Utilizing Robust Monolithic Silica Column Technology and LC-MS Karin Cabrera, Stephan Altmaier Merck KGaA, Darmstadt, DE Automated Determination of Urinary Folate Metabolites PAcetamidobenzoylglutamate and P-Aminobenzoylglutamate in Urine by HPLCMS/MS Through in Situ Propyl Chloroformate Mediated Derivatization Liquid Liquid Extraction 1 2 3 1 Jana Cimlova , Gry Kvalheim , Per Magne Ueland , Petr Simek 1 2 Biology Centre, AS CR, Ceske Budejovice, CZ; Institute of Medicine, University of Bergen, 3 Bergen, NO; Haukeland University Hospital, Bergen, NO Stir Bar Sorptive Extraction-Liquid Chromatography Tandem Mass Spectrometry Method for the Determination of Tributyltin Species in Seawater 1 1 1 Noem Dorival-Garca , Francisco Javier Camino-Snchez , Alberto Zafra-Gmez , Bartolom 1 2 2 1 Oliver-Rodrguez , I Ruz-Naranjo , I Ruz-Garca , Jos Luis Vlchez 1 2 University of Granada, Granada, ES; Certio Environment S.L.TM, Granada, ES Method Optimisation in Bottom-Up Analysis of Proteins Anthony Edge, Luisa Pereira Thermo Fisher Scientific, Runcorn, GB Miniaturized Solid Phase Extraction Coupled to Capillary Liquid Chromatography for Online and Efficient Determination of Hormones At Low Levels in Water Supplies Rodrigo Padovan, Marassa Franco, Lucas Carvalho, lvaro Santos-Neto, Fernando Lanas, Eduardo Azevedo University of So Paulo/Institute of Chemistry of So Carlos, SAO CARLOS, BR Comparison of the Efficiency of Different MEPS Sorbents for the Extraction of the Fungal Metabolites Deoxynivalenol and Zearalenone 1 2 1 1 Priscila Figueira , Paulo Fernandes , Jorge Pereira , Jos S. Cmara 1 2 CQM, UMa, Funchal, PT; Laboratrio Regional de Veterinria e Segurana Alimentar, Funchal, PT Boron Nitride, a Novel Material for the Enrichment and Desalting of Tryptic Digest and the Depletion of Proteins Martin Fischnaller, Rainer Koeck, Rania Bakry, Guenther K. Bonn Analytical Chemistry and Radiochemistry, Innsbruck, AT Magnetic Bead Based Novel Sample Preparation Method for Automated NGlycosylation Analysis of Biotherapeutics by Capillary Electrophoresis 1 2 2 2 1 Csaba Varadi , Clarence Lew , Hans Dewald , James Thorn , Andras Guttman 1 2 Horvath Laboratory of Bioseparation Sciences, Debrecen, HU; Beckman Coulter, Brea, US Selective Determination of Illicit Drugs and Pharmaceuticals in Wastewaters by a Novel Strong Cationic Exchange Solid-Phase Extraction Coupled to Liquid Chromatography and Tandem Mass 1 2 1 1 1 Nria Gilart , P.A.G. Cormack , Rosa Maria Marc , Nria Fontanals , Francesc Borrull 1 2 Universitat Rovira i Virgili, Tarragona, ES; University of Strathclyde, Glasgow, GB
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134
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A New Stationary Phase for Solid-Phase Extraction with Marshmallow-Like Silicone Monoliths 1 2 1 1 Gen Hayase , Kei Morisato , Kazuyoshi Kanamori , Kazuki Nakanishi 1 2 Kyoto University, Kyoto, JP; GL Sciences Inc., Saitama, JP Towards Unbiased Dried Blood Spot Analysis Using Temperature-Enhanced FlowThrough Desorption Coupled Online to Solid Phase Extraction and Mass Spectrometry Christel Hempen, Lena Knegt, Bert Ooms Spark Holland, Emmen, NL Enzyme-Assisted Extraction of Proteins from Olive Fruit and Leaves Mara Vergara-Barbern, Cecilia Bataller-Fayos, Vicente Sez-Montaner, Ernesto Francisco Sim-Alfonso, Jos Manuel Herrero-Martnez Dept. Analytical Chemistry, University of Valencia, Burjassot (Valencia), ES Novel New Pseudo-Solvent Cloud-Point Microextraction for the Rapid Determination of Alkylphenols in Waters by High-Performance Liquid Chromatography and Ultraviolet Detection Jen-Fon Jen, Hou-Kung Shih, Ting-Yun Shu National Chung Hsing University, Taichung, TW Development of an Analytical Method for Determination of Pesticides Used in the Cultivation of Cucumbers, Using Ultra High Performance Liquid Chromatography Luana C. Macedo, Elisa C. Morais, Isabel C. S. F. Jardim UNICAMP, Campinas, So Paulo, BR Miniaturized Salting-Out Liquid-Liquid Extraction in Coupled-Syringes Combined with HPLC-UV for Extraction and Determination of Sulfanilamide Marzieh Khosraviani, Hassan Sereshti University of Tehran, Tehran, IR Application of Lewis Acid/Base Interactions of Zirconia Based Sorbents for Sample Extraction Michal Klivicky, Radim Kucera, Jiri Klimes Charles University in Prague, Phaculty of pharmacy, Hradec Kralove, CZ Automated Liquid-Liquid Extraction (LLE) of Drugs from Plasma Syed Lateef, Sundaram Palaniswamy, Siji Joseph, Vinayak AK Agilent Technologies, Bangalore, IN Target 2D UHPLC-MS/MS Quantification of Rifampicin and 25-Desacetylrifampicin in Rat Liver Microsomes Bianca Lopes, Josiane Cardoso, Bianca Silva, Quezia Cass, Regina Vincenzi UFSCar, Sao Carlos, BR Dispersive LiquidLiquid Microextraction Applied to Extraction of Benzodiazepines in Urine Followed by Ultra Performance Liquid Chromatography with Photo Array Detector (UPLC-PAD) 1 1 1 1 2 Rosa A. Lorenzo , Mara Regenjo , Mara Teresa Pena , Antonia M Carro , Ana M Fernandez , 1 Purificacin Fernndez 1 2 University of Santiago de Compostela, Santiago de Compostela, ES; Unidade Asistencial de Drogodepencias, Monforte de Lemos (LUGO), ES
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135
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Simultaneous PAH and PCB Extraction from Soil and Tissues with Accelerated Solvent Extraction Aaron Kettle, Linda Lopez, Frank Hoefler Thermo Fisher Scientific, Sunnyvale, CA, US Solid Phase Extraction of Fluoroquinolone Antibiotics from Wastewaters Assessment of Different Commercial Sorbents 1 2 3 4 Alexandra S Maia , Ana R Ribeiro , Paula ML Castro , Maria Elizabeth Tiritan 1 2 CICS-ISCSN-CESPU, CBQF-ESB-UCP, Gandra - Paredes, PT; CICS-ISCSN-CESPU, CBQF-ESB-UCP, 3 4 CEQUIMED-UP, Gandra - Paredes, PT; CBQF-ESB-UCP, Porto, PT; CICS-ISCSN-CESPU, CEQUIMED-UP, Gandra - Paredes, PT Validation and Application of a Method for Determination of Pesticide Residues in Samples of Green Pepper Using Quechers and HPLC-MS/MS Elisa Morais, Luana Macedo, Isabel Jardim Unicamp, Campinas, BR Novel Double-Confined Polymeric Ionic Liquids as Sorbents for Solid-Phase Microextraction with Enhanced Stability in High-Ionic-Strength Solution Juanjuan Feng, Hongdeng Qiu, Shuai Wang, Xia Liu, Shengxiang Jiang Lanzhou Institute of Chemical Physics, Lanzhou, CN Determination of Light Alcohols, Cellosolves, Alcoholic Components of Fragrances and Non-Ionic and Anionic Surfactants in Cleaners by Ion-Exchange Separation, Derivatization and Liquid Chromatography Laura Ripoll-Seguer, Miriam Beneito-Cambra, Jos Manuel Herrero-Martnez, Ernesto F. SimoAlfonso, Guillermo Ramis-Ramos University of Valencia, Fac. of Chemistry, Burjassot, ES Obtaining Partition Coefficients of Biological Compounds between Ionic Liquids and Water by Using the Solvation Parameter Model Mario Reta, Juan Manuel Padr, Leidy Bibiana Agudelo Mesa, Roco Pellegrino Vidal Fac. de Ciencias Exactas, Universidad Nacional de La Plata, La Plata, AR Improved Recoveries of Planar Pesticides from Quechers Extracts of Fruits and Vegetables When Using an Engineered Carbon Material for Pigment Removal 1 2 2 2 Dwight Stoll , Conor Smith , Doug Fryer , Jonathan Thompson 1 2 Gustavus Adolphus College, St. Peter, US; United Science LLC, Center City, US Detection of Trace Level Herbicides from Drinking Water, Surface Water and Ground Water by Automated Online SPE-LC Triple Quadruple MS/MS Analysis
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Variables Influencing the Injection Solvent Effect in Reverse Phase Liquid Chromatography Bradley VanMiddlesworth, John Dorsey Dublin City University, Dublin, IE Surfactant-Assisted Emulsification Dispersive Liquid-Liquid Microextraction Combined with HPLC for Analysis of Cabamate Residues Jitlada Vichapong, Rodjana Burakham Faculty of Science,Khon Kaen university, Khon Kaen, TH
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136
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HPLC Method for Determination of Different Forms of Cysteine and Glutathione in Cucumber Leaves 1 1 2 2 Monika Wyszczelska-Rokiel , Grayna Chwatko , Elbieta Kuniak , Ewa Gajewska , Marzena 2 1 Wielanek , Rafa Gowacki 1 2 University of d, Faculty of Chemistry, Dep. Env. Chem., Lodz, PL; University of d, Faculty of Biology and Environmental Protection, Department of Plant Physiology and Biochemistry, Lodz, PL Determination of 1,3-Thiazolidine Derivative of Cysteine and Pyridoxal 5Phosphate by HPLC with UV Detection 1 2 1 Monika Wyszczelska-Rokiel , Hieronim Jakubowski , Rafa Gowacki 1 2 University of d, Faculty of Chemistry, Dep. Env. Chem., Lodz, PL; Department of Microbiology and Molecular Genetics, University of Medicine and Dentistry of New Jersey, Newark, New Jersey and Institute of Bioorganic Chemistry, Polish Academy of Sciences, Pozna, PL Automated Solid-Phase Extraction of Phthalates for Drinking Water Samples 1 2 2 Alex Zhang , Pranathi Pareti , Linda Lopez 1 2 Thermo Fisher Scientific, Sunnyvale, US; Thermo FIsher Scientific, Sunnyvale, US Solid-Phase Extraction Enrichment of Pahs in Water Using Tetraazacalix[2]Arene[2]Triazine Modified Silica Gel (N-Calix-Tmsg) Zhang Shusheng Zhengzhou University, Zhengzhou, CN Evaluation of Direct Sample-Inlet Mass Spectrometry (ASAP) of Vanilla Flavourings Baudien te Nijenhuis, Wilma du Chatinier, Boudewijn Hollebrands, Hans-Gerd Janssen Unilever R&D Vlaardingen B.V., Vlaardingen, NL Screening of Pesticides in Water Using SPE On Line Stefano Zaza, Stefano Lucini Shimadzu Italia, Milan (Italy), IT
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Selectivity
Comparative Evaluation of Reversed-Phase HPLC Columns for the Analysis of Darifenacin in the Presence of its Related Compounds 1 2 3 Mufarreh Asmari , Mohamed Hefnawy , Mohamed Attwa 1 2 3 King Khalid University, Asir, SA; King Saud University, Ryiadh, SA; King Saud University, Riyadh, SA Investigating Retention Characteristics of a Mixed Mode Stationary Phase and the Enhancement of Monolith Selectivity for HPLC 1 2 1 2 1 Danielle N. Bassanese , Arianne Soliven , Paul G. Stevenson , Gary R. Dennis , Neil W. Barnett , 1 2 Xavier Conlan , R. Andrew Shalliker 1 2 Deakin University, Geelong, VIC, AU; University of Western Sydney, Parramatta, NSW, AU Efficient and Rapid Method Development with Hybrid Silica Based Material by Utilizing Particle Size, Temperature and Bonded Chemistry 1 2 2 2 2 Friederike Becker , Noriko Shoji , Takashi Sato , Takatomo Takai , Naohiro Kuriyama 1 2 YMC Europe GmbH, Dinslaken, DE; YMC Co., Ltd., Komatsu, JP Development of Highly Selective LC/MS Assay for Vitamin D Metabolites 1 1 1 2 1 David Bell , Craig Aurand , Hugh Cramer , Anders Fridstrom , Frank Michel 1 2 Sigma-Aldrich/Supelco, Bellefonte, PA, US; Sigma-Aldrich/Supelco, St. Gallen, CH
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137
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Design of Surface Selectivities for Special Applications with Silica Monoliths Karin Cabrera, Peter Knoell, Gisela Jung, Anita Piper, Benjamin Peters, Klaus Kreher Merck KGaA, Darmstadt, DE Size Exclusion Chromatography of Biomolecules Detector Combinations to Obtain Maximum Information with Minimum Effort Andrew Coffey Agilent Technologies UK Ltd, Church Stretton, GB Transferring Multiple Methods Into a Single Analytical Solution Using Biocides in Consumer Products as a Model 1 2 Jane A. Cooper , Marian Twohig 1 2 Waters Corporation, Manchester, GB; Waters Corporation, Milford, US HILIC, Mixed-Mode, and Reversed-Phase: A Study in Retention Mechanisms Chris Denicola, Ty Kahler, Sharon Lupo, Rick Lajke Restek Corporation, Bellefonte, PA, US HILIC and Mixed-Mode Retention of the Pentafluorophenyl Propyl (PFPP) Stationary Phase Ty Kahler, Sharon Lupo, Jason Thomas, Chris Denicola, Rick Lake Restek Corporation, Bellefonte, PA, US An HPLC-UV Method Supporting the Reactivity Assessment of IVA Acyl-Glucuronide Derivative 1 1 2 2 Emmanuel Hardillier , Batrice Cautain , Delphine Chevillon , Colette Prevost , Olivier 1 Lacombe 1 2 Inventiva, Daix, FR; Laboratoires Fournier, Daix, FR Evaluation of Performance in Reversed-Phase, and Ion-Exchange Modes of the Flare C18/Amino Polymer/Nanodiamond Mixed-Mode Column 1 2 2 2 3 Chuan-Hsi Hung , Tom Kazarian , Brett Paull , Pavel Nesterenko , Andrew Miles , David 3 3 1 Jensen , Andrew Dadson , Matthew Linford 1 2 3 Brigham Young University, Provo, US; University of Tasmania, Hobart, AU; Diamond Analytics, Orem, US HILIC-Phase Selectivity Chart for Characterization of HILIC Stationary Phases Mohammed E. A. Ibrahim, Yang Liu, Charles A. Lucy University of Alberta, Edmonton, Alberta, CA Phenylpiracetam Diastereomers Separation on Normal Phase Achiral Phases Helena Kazoka, Agrita Sproge, Grigorij Veinberg, Maksim Vorona Latvian Institute of Organic Synthesis, Riga, LV HILIC and Mixed-Mode Retention of an Embedded-Polar Stationary Phase Ty Kahler, Sharon Lupo, Jason Thomas, Chris Denicola, Rick Lake Restek Corporation, Bellefonte, PA, US Green Chromatographic Fingerprinting: A Trade Off between Separation and Sustainability 1 2 3 1 Cristiano Funari , Renato Carneiro , Alberto Cavalheiro , Emily Hilder 1 2 Australian Centre for Research on Separation Sciences/UTAS, Hobart, AU; Department of 3 Chemistry, Federal University of So Carlos So Carlos, Sao Carlos, BR; Chemistry Institute, So Paulo State University, Araraquara, BR Quality by Design in UHPLC Method Development 1 2 2 Rbert Kormny , Imre Molnr , Hans-Juergen Rieger 1 2 Egis Pharmaceutical, Budapest, HU; Molnr-Institute, Berlin, DE
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138
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Selective Preconcentration and Determination of a PPCP, Sulpiride in River Water by an Online SPE-LC-MS Using a Molecularly Imprinted Adsorbent 1 1 2 1 Takuya Kubo , Kenta Kuroda , Ken Hosoya , Koji Otsuka 1 2 Kyoto University, Kyoto, JP; Kyoto Prefectural University, Kyoto, JP Complementary Selectivity in Hydrophilic Interaction Liquid Chromatography (HILIC) on Columns with Densely Bonded Zwitterionic Phosphorylcholine and Sulfobetaine Functional Groups 1 2 2 2 2 2 Petra Lewits , Tobias Jonsson , Wen Jiang , Petrus Hemstrm , Patrik Appelblad , Lena Westin 1 2 Merck Millipore, Merck KGaA, Darmstadt, DE; Merck Millipore, Merck SeQuant AB, Ume, SE Retention Indices of Some Monoaromatics Using a Multiparametric Method in Binary, Ternary and Quaternary Solvent RP-LC Systems Didaoui Linda, Hassina Larbi USTHB University, Alger, Algeria, Alger, DZ Analyze Pharmaceuticals by Mixed-Mode Chromatography Xiaodong Liu, Mark Tracy, Udayanath Aich, Christopher Pohl Thermo Fisher Scientific, Sunnyvale, US Use of High Liquid Performance Chromatography (HPLC) for Determination of Folic Acid in Tablets Lilian Grace Silva Solon, Eliane Goncalves Araujo, Janiele Mayara Ferreira de Almeida, Cicero Flavio Soares Aragao, Carlos Alberto Martinez-Huitle, Nedja Suely Fernandes UFRN, Natal - RN, BR Column Comparison and Method Development for the Analysis of Short-Chain Carboxylic Acids by Zwitterionic HILIC with UV Detection 1 1 1 2 2 Gabriella Massolini , Alice Pedrali , Giorgio Marrubini , Petrus Hemstrm , Tobias Jonsson , 2 Patrik Appelblad 1 2 Department of Drug Sciences, University of Pavia, Pavia, IT; Merck SeQuant AB, Ume, SE Development of Guidelines for HPLC Method Transfer to New 5m Fused-Core Particles 1 2 2 2 2 Frank Michel , Richard A. Henry , David S. Bell , Carmen T. Santasania , Hugh M. Cramer 1 2 Sigma-Aldrich, Taufkirchen, DE; Supelco/Sigma-Aldrich, Bellefonte, US Rapid HPLC Method Development with C18 and Phenyl Columns 1 1 2 2 Toshi Ono , Ken Tseng , Tsunehisa Hirose , Kazuhiro Kimata 1 2 Nacalai USA, Inc., San Diego, US; Nacalai Tesque, Inc., Kyoto, JP Development of a Mip-Mspd-Meck Method for Analysis of Natural and Synthetic Steroids in Goat Milk 1 2 3 3 3 Judith Gan , Sonia Morante , Alejandrina Gallego , Rosa Mara Garcinuo , Pilar Fernndez , 2 Isabel Sierra 1 2 Rey Juan Carlos University, Madrid, ES; School of Experimental and Technologies Sciences, 3 Rey Juan Carlos University, Madrid, ES; Department of Analytical Sciences, Faculty of Sciences, National University of Distance, Madrid, ES Adsorption Thermodynamics of Phenylcarboxylic Acids Enantiomers on a Chiral Adsorbent with Grafted Eremomycin Antibiotic Elena Reshetova, Arseny Blinov Institute of Technical Chemistry, Ural Branch of RAS, Perm, RU Exploring HPLC / UHPLC Chromatographic Selectivity with Low and High Ph Eluents on a New Extended Ph Range Stable Silica-Based Stationary Phase 1 2 Alan Mckeown , Carl Zimmerman 1 2 Advanced Chromatography Technologies Ltd, Aberdeen, Scotland, Gb; Macmod Analytical Inc., Chadds Ford, Pa, US 139
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An Ultra Fast Liquid Chromatography Method Development Using Surface Response Techniques to Determine Betamethasone and Dexamethasone in Topical Dermatologic Creams Lilian Grace Silva Solon, Marcelo Vitor Paiva Amorim, Larissa Marina Pereira Silva, Rhadames Menezes Costa Rocha, Jose Renato Lima Costa, Cicero Flavio Soares Aragao UFRN, Natal, BR Generic Method Approach for Pharmaceutical Drug Discovery and Development Using Reversed-Phase Hydrophilic Interaction Liquid Chromatography with Universal Charged Aerosol Detection Frank Steiner, Michael Heidorn, Markus Martin Thermo Fisher Scientific, Germering, DE Exploring the Possibilities of One-Segment-Per-Component Strategies to Enhance the Selectivity of Multi-Segment Gradient LC Eva Tyteca, Kim Vanderlinden, Gert Desmet Vrije Universiteit Brussel, Elsene, BE Efficiency of Solvatic Sorbtion Model for Prediction of Multi-Step Gradient Elution in Reversed-Phase Liquid Chromatography 1 2 2 1 Svetlana Vorslova , Jelena Golushko , Sergey Galushko , Arturs Viksna 1 2 Department of Analytical Chemistry, University of Latvia, Riga, LV; Institute of Chromatography, Riga, LV Transfer of Methods in LC and UHPLC, What Calculations Do I Need? Mark Woodruff, Helen Lomax Fortis Technologies Ltd, Neston, GB Applications of Venusil AQ C18 in the Study of Pharmacokinetics and Bioavailability Zhu Xudong, Jack Liu Bonna-Agela, Tianjin, CN
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Implementation of Ultraperformance Supercritical Fluid Chromatography (UPSFC) for Chiral Separations Katrijn De Klerck, Debby Mangelings, Yvan Vander Heyden Vrije Universiteit Brussel, Brussels, BE Supercritical-Fluid Chromatography for the Separation of Complex Bio-Oils 1 1 2 3 Henrik Cornelisson-van-de-Ven , B.W.J. Pirok , Pieter Kooijman , Andre van der Doel , Noortje 2 1 4 1 de Haan , Dennis Drost , Wim Genuit , P.J. Schoenmakers 1 2 Van 't Hoff Institute for Molecular Sciences, Amsterdam, NL; VU University Amsterdam, 3 4 Amsterdam, NL; Radboud University Nijmegen, Nijmegen, NL; Shell Research and Technology Centre, Amsterdam, NL The Kinetic Plot Method in Supercritical Fluid Chromatography: Theoretical Validation and Evaluation of Constant Pressure Gradient Elution. Ruben De Pauw, Gert Desmet, Ken Broeckhoven Vrije Universiteit Brussel, Brussel, BE Stationary Phase Optimized Selectivity Supercritical Fluid Chromatography (SOSSFC) Sander Delahaye, Frdric Lynen Ghent University, Gent, BE
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Enantioselective Ultrahigh-Pressure Liquid Chromatography and UltrahighPerformance Supercritical Fluid Chromatography in the Chiral Science Separation Scenario: Ultra-Fast Separations on a New Sub-2-m Whelk-O 1 Stationary Phase. 1 1 1 2 3 4 Dorina Kotoni , Alessia Ciogli , Marco Pierini , Jelena Kocergin , Ted Szczerba , Harald Ritchie , 1 1 Claudio Villani , Francesco Gasparrini 1 2 Sapienza University of Rome, Rome, IT; Regis Technologies, Morton Grove (Illinois), US; 3 4 Regis Technologies, Morton Grove (Illinoiso, US; Thermo Fisher Scientific, Runcorn, GB Way to Extending SFC Application Scopes Chuping Luo, Ziqiang Wang Waters, New Castle, DE, US Method Transfer of the United States Pharmacopeias Normal Phase Methods to Supercritical Fluid Chromatography Methods. Syed Lateef, Sundaram Palaniswamy, Siji Joseph, Vinayak AK Agilent Technologies, Bangalore, IN Optimal Column Geometry for High Kinetic Performance Supercritical Fluid Chromatography Using State-Of-The-Art Instruments. Alexandre Grand-Guillaume Perrenoud, Davy Guillarme, Jean-Luc Veuthey, Szabolcs Fekete School of Pharmacy, University of Geneva, Geneva, CH UHPSFC-MS/MS : From Hyphenation Optimisation to High Sensitivity Analysis. Alexandre Grand-Guillaume Perrenoud, Jean-Luc Veuthey, Davy Guillarme School of Pharmacy, University of Geneva, Geneva, CH Chromatographic Method Development Strategies for Convergence Chromatography Paula Hong, Michael Jones, Patricia McConville Waters Corporation, Milford, US Application of the Isopycnic Kinetic Plot Method for Elucidating the Potential of Sub2 Micron and Core/Shell Particles in SFC 1 2 2 1 Sander Delahaye , Ken Broeckhoven , Gert Desmet , Frdric Lynen 1 2 Ghent University, Gent, BE; Vrije Universiteit Brussel, Brussel, BE Stochastic Analysis of Mass-Transfer Properties in Supercritical Fluid Chromatography and in Liquid Chromatography Nndor Lambert, Felinger Attila University of Pcs, Pcs, HU Ultraperformance Convergence Chromatography and State-Of-The-Art Stationary Phases Jacob Fairchild, Jason Hill, Pamela Iraneta, Darryl Brousmiche, Kevin Wyndham, Thomas Walter Waters Corporation, Milford, US Ultra High Performance Supercritical Chromatography (UHPSFC) for Triglycerides Separation: Method Development. Eric Lesellier, Anna Latos ICOA, UMR 7311, Universit Orlans, Orlans, FR Development of a Strategy for Scaling SFC Methods: Applications for Preparative Chromatography Christopher Hudalla, Abhijit Tarafder, Kenneth Fountain Waters Corporation, Milford, MA, US
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C18 Bonded Phases with Small Molecule Spacers: Supercritical Fluid Chromatography (SFC) Characterization and Carotenoid Test. 1 2 2 Eric Lesellier , Catherine Rimmer , Lane Sander 1 2 ICOA, UMR 7311, Orlans, FR; NIST, Gaithersburg, US Separation of Clenbuterol Enantiomers A Comparison between HPLC and SFCMS/MS 1 1 2 1 3 Franz Liebetrau , Maria Kristina Parr , Alexander Schmidt , Peter Witte , Saskia Sterk , Marco 3 Blokland 1 2 Institute of Pharmacy, Freie Universitt Berlin, Berlin, DE; Steiner & Co. Deutsche 3 Arzneimittelgesellschaft mbH & Co. KG, Berlin, DE; RIKILT Institute for Food Safety, Wageningen, NL Evaluation of Core Shell Columns for Improved Separation of Pharmaceutical Compounds by SFC 1 2 2 3 Toshi Ono , William Farrell , Nicole Aurigemma , Norikazu Nagae 1 2 3 Nacalai USA, Inc., San Diego, US; Pfizer, Inc., San Diego, US; ChromaNik Technologies, Inc., Osak, JP Method Development for the Separation of Sulfated Estrogens by Ultraperformance Convergence Chromatography (UPC2) 1 1 2 2 2 Christopher Hudalla , Kenneth Fountain , Manisha Patel , Mark Hardink , Frank Riley 1 2 Waters Corporation, Milford, MA, US; Pfizer Inc., Groton, CT, US Application of Ultraperformance Convergence Chromatography - UPC2 - in Pharmaceutical Development Mijo Stanic, Alexander H. Schmidt Steiner Pharmaceuticals, Berlin, DE Rapid Analysis of Endogenous Steroids Using UPC2 MS/MS for Clinical Research 1 1 1 2 2 Christopher Hudalla , Andrew Peck , Kenneth Fountain , Stuart Chadwick , Fiona Liddicoat 1 2 Waters Corporation, Milford, MA, US; Waters Corporation, Manchester, GB Purification Using HPLC-MS and SFC-MS in a medicinal chemistry environment Johan Sderlund, Pernilla Korsgren, Annika Langborg Weinmann AstraZeneca R&D, RIA iMed, Mlndal, SE Rapid Enantiomeric and Diastereomeric Resolutions of Chiral Pesticides Using Ultra Performance Convergence Chromatography with UV Detection 1 1 2 3 3 Marian Twohig , Michael O Leary , Jane A. Cooper , Sherry C. Perine , David R. Stubbs 1 2 3 Waters Corporation, Milford, US; Waters Corporation, Manchester, GB; Syngenta Crop Protection LLC, Greensboro, US Rapid SFC Method for Separation of Chlorthalidone Enantiomers Ji Vozka, Kvta Kalkov, Eva Tesaov Faculty of Science, Charles University in Prague, Prague, CZ Analysis of Metoclopramide and Related Impurities Using UPC2/MS Michael Jones Waters Corporation, Milford, MA, US The Use of an Ionic Liquid Stationary Phase for the Separation of Ionic Liquids with Supercritical Fluid Chromatography Guor-Tzo Wei, Yu-Siou Hung, Po-Hseuh Chen National Chung Cheng Universit, Ming-Hsiung, TW Comparison of Pentafluorophenyl Stationary Phases in Supercritical Fluid Chromatography Caroline West, Syame Khater, Eric Lesellier ICOA, CNRS UMR 7311, University of Orlans, Orlans, FR 142
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Chiral and Achiral Reaction Monitoring with Sub 2 Particle Columns with CO2 Chromatography Sean McCarthy, Michael Jones, Andy Aubin, Margaret Maziarz Waters, Milford, US Comparison of Chlorinated Polysaccharide Chiral Stationary Phases in Supercritical Fluid Chromatography Syame Khater, Caroline West ICOA, CNRS UMR 7311, University of Orlans, Orlans, FR Efficiency Study on Overloaded Columns Using SFC and Using Chiral Compounds and Stationary Phases John Whelan, Ziqiang Wang Waters Corp, New Castle, US Consequences of the Transfer from SFC to HPLC Conditions on the Overall Performance of a Chiral Zwitterionic Ion Exchange Type CSP Denise Wolrab, Michal Kohout, Wolfgang Lindner University of Vienna-Department of Analytical Chemistry, Vienna, AT Chiral HPLC-to-Chiral SFC: An Easy Transfer? 1 2 2 2 1 Syame Khater , Anne-Marie Lozach , Isabelle Adam , Eric Francotte , Caroline West 1 2 ICOA, CNRS UMR 7311, Universit d'Orlans, Orlans, FR; Novartis Institutes for BioMedical Research, Basel, CH CO2 Recycling Study from a Efficiency and CFD Persperctive John Whelan, John Baugher, Ziqiang Wang Waters Corp, New Castle, DE, US On the Reproducibility between Different Modern Supercritcal Fluid Chromatographic Systems Martin Enmark, Jrgen Samuelsson, Torgny Fornstedt Department of Engineering and Chemical Sciences, Karlstad, SE
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Stationary phases
Characterization of a Mixed-Mode Reversed Phase/Cation-Exchange Stationary Phase Prepared by Thermal Immobilization of Poly(Dimethylsiloxane) Onto the Surface of Silica. 1 2 Endler Borges , Melvin Euerby 1 2 Universidade Estadual de Campinas, Campinas, BR; Hichrom Ltd.,, Berkshire, GB Mucin-Based Stationary Phases as Potential Tool for the Characterization of Drug Mucus Interaction 1 2 3 Andrea Gargano , Michael Laemmerhofer , Tomas Leek 1 2 3 University of Vienna, Vienna, AT; University of Tuebingen, Tuebingen, DE; R&D Astra Zeneca, Mondal, SE Evaluation of HPLC Stationary Phases for Environmental Analysis Ken Butchart, Sandra Hanson Fortis Technologies Ltd, Neston, GB Zwitterionic Monosized-Porous Beads for Ion Chromatography 1 2 1 Gunes Kibar , Saba Samatya , Ali Tuncel 1 2 Hacettepe Uni, Ankara, TR; SIIRT UNI, SIIRT, TR
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Kinetic Performance Comparison of Fully and Superficially Porous Particles with a Particle Size of 5 m: Intrinsic Evaluation and Application to the Impurity Analysis of Griseofulvin 1 2 3 1 1 Getu Kahsay , Ken Broeckhoven , Gert Desmet , Erwin Adams , Deirdre Cabooter 1 2 3 KU Leuven, Leuven, BE; Vrije Universiteit Brussels, Brussels, BE; Vrije Universiteit Brussel, Brussels, BE Separation and Determination of Organic Acids in Energy Drinks Using Polar Endcapped Reversed-Phase Column Ha Jeong Kwon, Yoon Jong Oh, Yu mi Jung, Jung Eun Park Department of Preventive Social Dentistry, Kyung Hee Univ., Seoul, KR Simple, Fast and Accurate Quantitation of Human Plasma Vitamins and their Metabolites by Rapid Protein Precipitation Combined with Columns Using HPLC-UV, HPLC-FLD Or LC-MS/MS Shuguang Li, Jason Anspach, Sky Countryman, Erica Pike Phenomenex, Torrance, CA, US Varying the Porosity of PS/DVB Beads and its Influence on RP-HPLC Performance Kristian Lungfiel, Andreas Seubert Philipps Universitt Marburg, Marburg, DE A Novel Fluorous Solid Phase Extraction Method for the Determination of Environmentally Relevant Perfluoro-Alkyl Acids in Waters 1 1 1 1 2 Nicola Marchetti , Alberto Cavazzini , Luisa Pasti , Francesco Dondi , Aldo Lagana` 1 2 University of Ferrara, Ferrara, IT; University of Rome "La Sapienza", ROME (ITALY), IT Improved Sample Preparation and HPLC/MS Determination of Pesticides in FatRich Vegetables 1 2 2 2 2 Frank Michel , Emily Barrey , Katherine K. Stenerson , Olga Shimelis , Michael Ye 1 2 Sigma-Aldrich, Taufkirchen, DE; Supelco/Sigma-Aldrich, Bellefonte, US Application of On-Column Polymerization Method of Acrylic Acid on Silica Monolith to the Preparation of Particle Type HILIC Stationary Phases 1 1 2 1 Tomoyuki Okada , Haruyuki Tanigawa , Nobuo Tanaka , Tohru Ikegami 1 2 Kyoto Institute of Technology, Kyoto, JP; GL Science, Saitama, JP Poly(Ionic Liquid)-Grafted Silica as Multi-Mode Stationary Phases for HighPerformance Liquid Chromatography 1 1 2 2 Hongdeng Qiu , Shengxiang Jiang , Makoto Takafuji , Hirotaka Ihara 1 2 Lanzhou Institute of Chemical Physics, Lanzhou, CN; Department of Applied Chemistry and Biochemistry, Kumamoto University, Kumamoto, JP Enantioselective Adsorption of Ibuprofen Enantiomers on a Chiral Adsorbent with Grafted Eremomycin Antibiotic Elena Reshetova Institute of Technical Chemistry of Ural Branch of the Russi, Perm, RU Development of a Novel Stationary Phase for HPLC: Polymeric Ionic Liquids Kevin Roeleveld, Frank David, Frdric Lynen Ghent University, Ghent, BE How to Determine the Experimental Isoeluotropic Conditions by Change of the RPLC Stationary Phase in Carrying Out Only Two Manipulations 1 2 2 2 1 Alain Tchapla , Didier Charbonneau , Guillaume Estievenart , Pauline Albisson , Sihem Groni , 1 Sylvie Heron 1 2 Univ.Paris Sud/Groupe de Chimie Analytique de Paris-Sud, Orsay, FR; Interchim R & D, Montluon, FR 144
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Chiral Chromatography on Solid Supported Ice Stationary Phase Satsuki Takahashi, Tetsuo Okada Tokyo Institute of Technology, Tokyo, JP A Simple Method for Resolution of 22 Amino Acids in LC Ken Butchart, Sandra Hanson Fortis Technologies Ltd, Neston, GB The Development of a New Hydrolytically Stable Stationary Phase for U(H)PLC: Column Development 1 2 3 2 Matthias Ide , Frdric Lynen , Pat Sandra , Pascal Van Der Voort 1 2 3 University Ghent/Mesosol, Ghent, BE; University Ghent, Ghent, BE; University Ghent/RIC, Ghent/Kortrijk, BE
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Method development software with optional instrument control for LC/MS and LC/UV systems*
ACD/AutoChrom
Intelligent parameter screening for a better starting point following QbD principles Automatic peak tracking between runs Assistance with data interpretation Databasing of experimental knowledge at the click of a button
*Available for Agilent ChemStation and Waters Empower software
Vendor seminars
Monday, June 17, 2013
13:00 14:00
13:00 14:00
Auditorium
Waters Corporation
Ultimate Efficiency Unleashed: A New UltraPerformance Column Technology for Maximizing Resolution and Throughput Speaker: Nicole M. Cotta, Waters Corporation Milford, MA , US 13:00 14:00
Sigma-Aldrich
Emerald
Improving UHPLC Performance: Views from Industrial and Academic perspectives Trends in HPLC Column Technology and their Application: From Small Particles and Long Columns Speaker: Dr. Stefan Lamotte, Competence Center Analytics, BASF SE, DE Achieving the Highest Efficiency by Reduction of the Extra-Column Volume in a UHPLC Instrument: A Case Study of the New Titan C18 Columns Speaker: Dorina Kotoni, PhD,Dept. of Drug Chemistry and Technologies, Sapienza University of Rome, IT Impact of Particle Designs for Achieving Performance in Liquid Separations Speaker: David S. Bell, PhD, Manager Pharmaceutical and Bioanalytical Research, Supelco, US 13:00 14:00
Thermo Scientific
G102-103
New Developments in Chromatography and Mass Spectrometry for Better and Faster Analytics of Biopharmaceuticals Speakers: Wim Decrop, Senior Research Scientist, Thermo Fisher Scientific Amsterdam, NL and Prof. Mag. Dr. Christian Huber, Head of Research Group Huber, Department of Molecular Biology, University of Salzburg, AT Moderator: Dr. Remco Swart, Manager Biomolecule Solutions HPLC Business Unit, Thermo Fisher Scientific Amsterdam, NL 13:00 13:30
G104-105
13:30 14:00
G104-105
Advantages of Using LC/MS Solvent Packaged in Schott Bottles in LC/MS Applications Speaker: Ivana Ivanovic, Marketing Manager Laboratory Products, Avantor Performance Materials, Deventer, NL
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General UHPLC Method Development and Separation Modelling within the QbDFramework Speakers: Imre Molnr, Hans-Jrgen Rieger, Institute for Applied Chromatography, Berlin, DE Robert Kormny, EGIS Pharmaceutical, Budapest, HU 13:00 14:00
Thermo Scientific
Auditorium
Increased Throughput Pharma R&D and QA Workflows with Maximum Versatility How Generic Can a UHPLC Method for Polar Analytes be? Speakers: Dr. Frank Steiner, Thermo Fisher Scientific, Germering, DE Stephen Luke, Thermo Fisher Scientific, Runcorn, UK 13:00 14:00
Shimadzu Europe
Emerald
Excellence in Science - Solutions and Innovations Speakers: Dr. Gesa Schad, Dr. Bjrn-Thoralf Erxleben, Dr. Francesco Cacciola, Mikal Levi 13:00 14:00
AB SCIEX
G102-103
The use of Microflow UHPLC in Food and Environmental analysis Speakers: Dr. Thorsten Teutenberg, Institut fr Energie- und Umwelttechnik e.V. Bereich Forschungsanalytik, Duisburg, DE Dr. Stephen Lock, AB SCIEX, Warrington, Cheshire, UK 13:00 14:00
Phenomenex
G104-105
Importance of Instrumentation in Fast Liquid Chromatography Speakers: Szabolcs Fekete, Davy Guillarme School of Pharmaceutical Sciences, University of Geneva, University of Lausanne, Geneva, CH Improved Separations of Large and Small Bio Molecules Using Core-Shell Particles Jason A. Anspach, Jeff Layne, Michael McGinley, Lawrence Loo, and Tivadar Farkas
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Evaluation of Method Robustness Speakers: Imre Molnr, Hans-Jrgen Rieger, Institute for Applied Chromatography, Berlin, DE Robert Kormny, EGIS Pharmaceutical, Budapest, HU 13:00 14:00
Merck Millipore
Latest Advances in Fast HPLC' and 'Separations of Polar Compounds' Monolithic Technologies superior to Core Shell Materials New complementary Selectivities in HILIC Speaker: To be announced
Auditorium
13:00 14:00
Waters Corporation
Emerald
Novel Applications of Ultraperformance Convergence Chromatography (UPC2) Speaker: Kenneth J. Fountain, Waters Corporation Milford, MA, US 13:00 14:00
G102-103
3A review of Columns Used in Chiral Chromatography and their Application in HPLC and SFC Which Column Type and Selector to Choose? Speaker: Pilar Franco - Manager Technical Operations 13:00 14:00
Agilent Technologies
G104-105
Orthogonality, Efficiency, Selectivity and Detection Tools for Profiling, Detection and Identification of Unknown Compounds Speakers: Dr. Michael Frank, Marketing Manager, Dr. Udo Huber, LC Solutions Manager, Agilent Technologies, Waldbronn, DE
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Agilent Technologies
The Agilent 1290 Infinity 2D-LC Solution Get Your Most-Complex Samples Separated Speaker: Dr. Jens Trafkowski, Product Manager, Agilent Technologies, Waldbronn, DE Application of Heart-Cut and Comprehensive 2D LC Separation for Advanced Chemical Analysis Matthias Pursch, Technology Associate, Analytical Technology Center, Dow Deutschland, Rheinmuenster, DE Optimizing Two-Dimensional Liquid Chromatography Systems: Can We Have it All? Gabriel Vivo-Truyols, Peter Schoenmakers, Sjoerd van der Wal, University of Amsterdam, NL 12:50 13:30
Restek Corporation
G102-103
A Simple and Directed Approach to Faster Separations Development Utilizing the Selectivity of Modern LC Phases Speakers: Ty Kahler, Chris Denicola, Ed Franklin Restek Corporation, Bellefonte, PA, US 12:50 13:30
Agilent Technologies
G104-105
Increase Your Sensitivity - The Agilent 1200 Infinity Series Online SPE Solution Speaker: Dr. Anneke Mhlebach, Product Manager, Agilent Technologies, Waldbronn, DE Quantitation of Trace Level Antibiotics in Minnesota River Water and Waste Water Effluent Using an Automated, Integrated Online-SPE LC-MS/MS System Speakers: Prof. Dwight Stoll*, Dr. David C. Harmes and Prof. Kristine Wammer *Gustavus-Adolphus College, St. Peter, Minnesota, US
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UNCOMPROMISING PERFORMANCE
www.avantormaterials.com
Symposium proceedings
It has been a tradition to publish the proceedings of the HPLC symposia in the Journal of Chromatography A. The organizers of HPLC 2013 therefore strongly encourage participants presenting lectures or posters at HPLC 2013 to submit a full-length manuscript for potential inclusion in a regular issue of the journal followed by a virtual special issue devoted to HPLC 2013. This is a totally new concept which essentially rules out possible delays in publication for contributors to a special issue and includes options for videos and additional (colour) photos which would not be included in a printed issue. Thus making a Conference special issue more complete and accessible than in the past. Papers are published individually in regular issues as soon as they are accepted. Footnotes indicate at which Conference they were presented, and are the source for selection and linking to the virtual special issue. Virtual special issue is prepared and placed on Journal homepage with links to papers on Science Direct. Preface and possible photos with the added possibility of videos e.g. from poster sessions, available via virtual special issue.
Points to note: The deadline to submit your manuscript to the HPLC 2013 virtual conference issue of Journal of st Chromatography A is 1 September 2013. When preparing your manuscript please carefully follow the journals Guide to Authors, which you can find on the online submission site: http://ees.elsevier.com/chroma. In your cover letter please mention that your manuscript is intended for the HPLC 2013 virtual issue. All manuscripts will be subject to the usual selection process including the strict peer review procedure, therefore acceptance for presentation at the meeting is not a guarantee for publication in the journal. A separate dedicated video website will also contain videos comprised of a PowerPoint presentation or graphics presented along with an audio commentary given by you, the presenter, or one of your colleagues. This is intended as part of the expanded virtual issue, and will not be included in the regular issue of the journal. If you wish to submit your poster presentation via this method, please contact the undersigned for a template and further instructions.
In order to deal with the manuscripts as fast and efficiently as possible, you are invited to submit your article via the journals online submission and reviewing system which is accessible at: http://ees.elsevier.com/chroma. Below please see instructions for submitting your manuscript: To submit: Go to: http://ees.elsevier.com/chroma Click on the Submit Paper option from the top menu Enter your user name and password (first time users will have to register) After entering the title of your manuscript, please select HPLC 2013 as the Article Type Follow the remaining step-by-step instructions to submit your paper
If you experience any technical problems or have any technical questions during the submission process, please contact Elsevier Authors Support: authorsupport@elsevier.com. If you have any questions on the submission and reviewing process, please contact the Editorial Office: chrom-eo@elsevier.com. We sincerely hope you will wish to contribute to this exciting project, and would wish you every success with the submission and eventual publication of your paper(s).
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Please note that all oral presentations, including the technical (vendor) seminars, will be handled by the RAI Speakers Centre. This means that you will have to hand in your (power point) presentation at the Speakers Centre, preferably on the day before the time of your presentation. It will not be possible to run your presentation from your own laptop.
Poster mounting time for all posters: Monday 8:00 11:00. Poster removal time for all posters: Thursday 13:30 15:00. Poster boards are 98 cm (32) wide and 2 m (66) high. Poster that exceed the size of the boards will not be permitted. You will be referred to the poster-printing service (see below). Each poster board will be labelled with the poster number. Make sure this number remains visible after mounting your poster. Posters have to be removed on Thursday, 20 June before 15:00. All remaining posters will be discarded after 16:00. Poster sessions Poster authors will be required to be present on the designated poster day from 16:00 17:00. Poster sessions are scheduled during the breaks from 11:00 11:30, 12:30 14:00 and from 16:00 17:00 on Monday, Tuesday and Wednesday and from 11:00 11:30 and 12:30 13:30 on Thursday. Poster printing services In case you did not carry your poster with you (or lost it) on your trip to Amsterdam, the RAI Bussiness Centre offers the possibility to have your poster printed on-site Size: A0 (84x119 cm, portrait) Full color Original: as pdf, prepared on A0 size Price: 35 Euro
You can hand your PDF-file on USB for printing, at the RAI Business Centre (entrance Elicium floor -1). Opening hours 9:00 17:00 on Sunday. Payment: in cash or by credit card, when collecting your poster.
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Exhibition
List of Exhibitors AB SCIEX Advanced Chromatography Technologies Ltd. (ACE) Advanced Chemistry Development Inc. (ACD/Labs) Advion Agilent Technologies Akzo Nobel PPC Analytical Sales and Services, Inc. Antec BV Avantor Performance Materials Biosolve Bonna Agela Technologies Inc. C&EN Cecil Instruments Ltd. Chiral Technologies Europe ChromSword CI Informatics Ltd. DIKMA Technologies Elsevier F-DGS Future Conferences GE Healthcare GL Science Hamilton Bonaduz AG JSB Group Knauer - Wissenschaftliche Geraetebau Dr. Ing. H. Knauer GmbH LCGC Macherey Nagel Merck Millipore Molnr Institute (for applied chromatography) MS Vision Nacalai Tesque Peak Scientific Instruments Phenomenex Polyintell Publishers/Media Restek RPD TOOL AG SCAT Europe GmbH Scharlab SL SelectScience LSI Schmidlin Screening Devices BV Sedere SAS Shimadzu Europe GmbH Showa Denko Europe Shodex
Booth number A8 E15 A19 U16 A9 U7 E2 E25 E3 D3 E5 U1 E7 A7 A2 E4 E10 E24 U4 U0ab, D0 A11 U18 E6 U9 A15 E17 U19 A12 E18 U2 A20 U10 U20 A6 U00 E13 A14 E22 E11 E12 U11 U3 E16 A1 E9
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List of Exhibitors Sigma Aldrich International GmbH Spark Holland BV The Analytical Scientist Thermo Scientific Inc. Tosoh Bioscience GmbH VICI AG International VWR International GmbH Waters Corporation Wyatt Technology Europe GmbH YMC Europe GmbH
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Exhibitors
Advanced Chromatography Technologies Ltd. (ACE) ACE ultra-inert HPLC/UHPLC columns from Advanced Chromatography Technologies Limited are designed to meet the most challenging of chromatographic applications. A wide range of particles /pore sizes, bonding chemistries and column dimensions are available providing excellent reproducibility and robustness with acidic, basic and neutral molecules. NEW additions include the ACE Excel Ultra Robust UHPLC column product family and the ACE SuperC18 extended pH range phase. ACE Excel is available throughout the world in 2 m particles and a wide range of phases including the ACE C18-AR, ACE C18-PFP and ACE SuperC18. Advanced Chemistry Development Inc. (ACD/Labs)
Advion is a leader in ultra-high performance, small footprint mass spectroscopy & synthesis solutions for life science, which deliver speed, flexibility, ease-of use, reliability and exceptional data quality. The expression CMS is a high performance mass spec, yet half the size and half the price of conventional single quadrupole systems. Its compact size allows it to be placed in a fume hood or on the bench for direct access and immediate results for chemists engaged in drug discovery requiring mass confirmation, reaction monitoring, QC and purity analysis. The expression CMS puts the power of performance where chemists need it. AkzoNobel offers Kromasil, high performance chromatographic media based on state-of-theart spherical silica for analytical and industrial HPLC applications. Products are available in slurrypacked columns for lab analysis and small scale purification plus bulk material for pharmaceuticals' manufacturing. The new range of UHPLC columns completes Kromasil's line; scientists can now use the same quality products with unmatched ratio of resolution per analysis time as their counterparts in production. Kromasil is the premium choice for API purification for its outstanding mechanical and chemical stability and is available for a wide range of NP, RP, SCF and chiral applications. Analytical Sales and Services, Inc. Akzo Nobel PPC
Advion
Antec BV
Antec is the worlds leading supplier of Electrochemical Detectors for (U)HPLC and Potentiostats for use in Electrochemistry (EC) as a reaction technique upfront MS.
The Decade II electrochemical detectors (ECD) are known for their superior sensitivity and versatility. They fit with any (U)HPLC to perform LC/ECD. The ROXY EC systems is the ultimate Electrochemistry system that complements any MS to conduct on-line EC/(LC)/MS. All these instruments will be on display at the exhibition together with new accessories such as the SenCell, ChipCell, or dedicated new electrodes for specific chemical reactions in EC/MS.
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Avantor Performance Materials Avantor Performance Materials manufactures and markets high-performance chemistries and materials around the world under several respected brand names, including the J.T.Baker and Macron Fine Chemicals brands. Avantor is an established global supplier of high-purity laboratory chemicals, including solvents, acids, solutions, salts, minerals and sugars. Avantor products are at work in research and production laboratories, pharmaceutical and environmental testing, industrial manufacturing and many other areas around the world, delivering the high quality and purity needed for demanding applications. For over three decades, we produce and distribute selected high purity solvents, reagents and formulations for the research, pharmaceutical and biotechnology industries, and are now a major supplier in this field. Bio-Lab, Biosolve and more recently Biosolve Chimie, our new plant established in Lorraine France, meet the latest quality and environmental ISO standards, manufacturing under stringent quality control processes and serving you with the highest quality products on the market. As our customer, you deserve excellent service, starting from the right packaging for your application through to swift and reliable delivery. We welcome you to contact us whenever you need our sound advice for quality, safety or product design, or to discuss the grade that best accommodates your special needs Bonna-Agela Technologies Inc. is a separation technology company that serves chemists and biochemists in the field of drug discovery, food analysis, drug testing, environmental analysis and chemical research. We offer a full line of products designed to meet your separation and purification needs from bulk separation media to chromatography columns, purification system, SPE cartridges and automated SPE workstation. C&EN, the weekly newsmagazine of the chemical & life sciences worlds, reaches the largest group of scientists in the world-over 128,000 worldwide. More than 75,000 readers work in life sciences and 85% have purchasing and specifying authority with 80% reading only C&EN in their professional role. C&EN brings breakthrough R&D, technology and industry news to the life sciences, pharmaceutical and instrumentation industries. C&EN is the best way to reach your target audience with 20 instrumentation-specific editorial issues, an award winning mobile app, 13 ACS online journals, along with C&EN Online (cen-online.org). Cecil Instruments Ltd. Cecil Instruments are leading designers and manufacturers of HPLC systems, Ion Chromatography systems and UV /Visible Spectrophotometers. Cecil Instruments' Adept and Q-Adept ranges of modular HPLC and IonQuest Ion Chromatography instrumentation may be configured to individual requirements. There is a wide range of low noise and low drift detectors, including the ultra-fast scanning UV/Visible WaveQuest, electrochemical and conductivity detectors. Other LC modules include the astoundingly reliable AutoQuest autosamplers, various pumps and column heater/chillers. These may all be used with third party LC systems. PC control is by Windows based PowerStream and/or DataStream software. C&EN Bonna Agela Technologies Inc. Biosolve
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Chiral Technologies Europe Chiral Technologies is the global leader in enantioselective chromatography, offering the largest portfolio of chiral stationary phases, analytical and preparative chiral columns, and custom separation services. Chiral Technologies serves the North and Latin American markets through Chiral Technologies Inc. (CTI) and the European market through Chiral Technologies Europe SAS (GTE), wholly-owned subsidiaries of Daicel Chemicals Industries Ltd. The ChromSword group is a leading provider of HPLC method development solutions for customers in the Life Science Research, Pharmaceutical and Chemical Industry. The ChromSword group provides analytical scientists worldwide with a range of software packages for computer assisted and fully automatic HPLC method development and support services. ChromSwordAuto is powerful, method development software capable of developing new methods or improving existing method fully automatically with HPLC instruments from different vendors including Agilent, Hitachi, Knauer, Thermo and Waters. CI Informatics Ltd. CI Informatics are European distributors for S-Matrix Corporation. We supply and support their Fusion AE platform, comprising of tools to support pharmaceutical development. These include: LC Method Development LC Method Validation Fusion Product Development Fusion Inhaler Testing (FIT) ChromSword
We are also UK distributers for iCD supplying the Validat product to the UK market as well as iCD's Laboratory Information Management system, LABS/Q. In addition to these activities CI Informatics sell and support Galaxie CDS software and offer a wide range of related consultancy services. We are also Bruker re-sellers for the closely related Compass CDS platform. DIKMA Technologies We are a company dedicated to developing innovative chromatography products including HPLC/UHPLC and GC columns, sample preparation products, bulk chromatographic media, reference chemicals, and chromatographic accessories and equipment. Our products are designed to meet the most challenging of chromatographic applications. A wide range of particle size, pore size, bonding chemistries and column dimensions are available. Excellent column performance and reproducible chromatography with acidic, basic and neutral molecules is ensured by the most stringent of validation protocols. Strong relationships with customers are a key component of our culture.
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F-DGSi proposes innovating solutions in gas equipment. Dont buy your gas, make it! The gas generators offer comfort, reliability, economy and safety. Hydrogen generators, without maintenance, pressure max. 16 bars, purity 99.99999%, ideal tool for carrier gas / FID applications. Nitrogen generator, with/without integrated compressor, of technology PSA and membrane enable us to match applications such as GC, ICP, COT, DEDL, SAMPLE EVAPORATION, LCMS. Zero air generators with/without integrated compressor produce a dry, clean air, without hydrocarbons for GC-FID. Ultra zero air generators, unique system, combine an air dryer and zero air generator to obtain purities of air even higher. Air dryers with/without CO2 are designed to match applications such as FT-IR, NMR, AA, TOC, rheometer etc. All of our laboratory gas generators offer superb technical performance and end user benefits in the lab, and, of course, our world- class service and support come as Standard. We feel confident that we offer the best gas generators on the market GE Healthcare Life Sciences provides tools for drug discovery, biopharmaceutical manufacturing and cellular technologies, so research scientists can be more productive, effective and creative. Our vision is to be the start-to-finish bioprocessing solution provider, the partner of choice in cell and protein research and the leader in life sciences services. Building on our broad expertise across life sciences, we are committed to helping researchers understand life at a molecular level and develop solutions that can prevent, diagnose, treat, and cure disease. GE Healthcare Life Sciences delivers breakthroughs in drug discovery, biopharmaceutical manufacturing and the latest in cellular technologies, so scientists and specialists discover new ways to predict, diagnose and treat disease. GL Science GL Science is one of the leading suppliers of products for HPLC, LC/MS, Ultra HPLC, samples preparation, and proteomics consumables throughout the world. Visit GL Sciences to see and learn the latest developments in column and separation technology for your critical separation. Hamilton Bonaduz AG Hamilton is a manufacturer of products designed for the measurement and handling of liquids. Microliter syringes are outstanding in all areas of precision liquid handling. GE Healthcare
F-DGS
In the field of analysis Hamilton is renowned for its innovative laboratory and process electrodes such as pH, Redox, oxygen and conductivity sensors plus a superior selection of armatures, pH buffer and conductivity standards. Hamilton supplies HPLC columns and polymer- and silica-based bulk material. Completing the range are semi-automatic diluter/dispensers and SoftGrip TM pipettes. Hamilton also manufactures innovative robotic pipetting systems and OEM products for laboratories in the fields of biotechnology, analytical and pharmaceutical chemistry. JSB Group
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LSI Schmidlin
LNI Schmidlin SA, based in Geneva, Switzerland, create products for Air Pollution Monitoring, Emission & Process, Automotive, Laboratory and Medical Applications: Ozone Generators for low and high concentrations,
High precision components for Gas flow and pressure regulation, No maintenance Laboratory Hydrogen Generators, Hydrogen and Zero air 19" rack mounted systems for industrial application, Nitrogen Generators for GC and LCMS application, Zero Air and Ultra Zero Air Generators. To insure the highest quality, we has got ISO 9001-2008 and ISO 13458-2003 certifications, our Gas Flow Standard laboratory is ISO 17025 certified and our medical gas mixers are CE certified. Macherey Nagel Since 1911 MACHEREY-NAGEL represents high quality, innovation and reliability in biomolecular and chemical analysis. Friendly expert advice as well as outstanding product quality have been the cornerstones of our corporate success for over 100 years. Our comprehensive line of laboratory supplies includes products for filtration, testing, water analysis, chromatography and bioanalysis.
MACHEREY-NAGELs expertise in R & D and manufacturing of separation media is based on many years of experience in silica technology, thereby playing a pioneering role in separation science. Our research and manufacturing capabilities are the core competency enabling us to make your daily laboratory work easier. MS Vision
Nacalai Tesque
COSMOSIL chromatography product line includes analytical and preparative HPLC or UHPLC columns for low-molecular compounds, hydrophilic compounds, Saccharides, Proteins, Fullerenes.
Peak Scientific Instruments Ltd are a manufacturer of laboratory Gas Generators including nitrogen, hydrogen and zero air suitable to operate most laboratory analytical applications such as LCMS (liquid chromatography mass spectroscopy) and GC (Gas chromatography).
With varying flow rates, purities & pressures of gas generators, available with or without internal air compressors, Peak are confident to offer the complete solution to your total Gas requirements. Our Gas Generators provide a safe & economical alternative to combustible bottled Gas cylinders offering a constant purity resulting in accurate analysis.
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Leader in development of molecularly imprinted polymers, POLYINTELL develops and manufactures from the commonly polymeric SPE products for a crude sample cleanup to the most innovative SPE for very specific extractions. POLYINTELL provides innovative extraction ready-to-use kits from complex media (food, biologic fluids,) for various compounds such as Mycotoxins, Endocrine disruptors like Bisphenol A, Estogens, Antibiotics, Phenolics compounds, under different formats. Visit and discover our latest innovations based on Molecularly Imprinted Polymers! RPD TOOL AG
Polyintell
Scharlab SL
Scharlab S.L. aim to be a global supplier of scientific solutions for chemical and microbiological laboratories and to improve and facilitate the work carried out by our customers.
Scharlab is an internationally recognised company, manufacturing its own "Scharlau" brand of more than 2.000 laboratory chemicals and 400 culture media of microbiology. Headquarter in Barcelona (Spain) with subsidiaries in Poland, Hungary, Indonesia, Philippines and China, and network of distributors in more than 90 countries worldwide. Our investment in technology means we can offer high quality at competitive prices. Innovation and quality are a must in all of our activities. Screening Devices BV
Sedere SAS
SEDERE develops, manufactures, distributes and supports SEDEX detectors, the most complete and versatile product line dedicated to Low-Temperature Evaporative Light-Scattering Detection (LT-ELSD). As one of the originators of this detection mode, SEDERE remains exclusively focused on this technology as a core competency.
As the industry leader, SEDERE leverages decades of experience and customer knowledge to continually raise the bar for High Sensitivity, High Flexibility and High Fidelity detector performance for chromatography laboratories. The unparalleled selection of three LT-ELSD models can match both very high performance requirements and budget for all chromatography applications from basic research to quality control. Showa Denko Europe Shodex Shodex is the brand name of the HPLC columns manufactured by Showa Denko KK in Japan. Our European headquarters with Sales and Customer Support are located in Munich, Germany. We have the largest market share in Japan with our advanced polymer-based columns. Experts in polymer, sugar and protein analysis Polymer-based and silica-based LC columns Product portfolio: IC, IEX, RP, HILIC, SEC (GPC-GFC), IEC and ligand exchange chromatography Dimensions: micro, analytical and preparative columns CD and RI-detectors Manufacturer of polymer standards like Pullulan, PMMA and PS Huge application database 163
We are a leading supplier of front-end HPLC and UHPLC instruments such as autosamplers, column ovens and pumps. Our autosamplers have become a benchmark for the industry and we have a reputation as dependable, no-worry OEM partner. Combined with our advanced technology for online Solid Phase Extraction, our instruments enable unsurpassed performance and reliability for automated HPLC and UHPLC based assays. Tosoh Bioscience is a leading manufacturer in the field of bio chromatography. The portfolio encompasses SEC/GPC instruments and a comprehensive line of media and HPLC columns for all common modes of liquid chromatography, including IEX, HIC, mixed-mode, reversed phase, HILIC, SEC and affinity. TOYOPEARL and TSKgel resins and columns are renowned for their quality and reliability. Latest product innovations include size exclusion columns tailored to monoclonal antibody analysis and multimodal media for preparative chromatography. We offer solutions for research, drug discovery, clinical chemistry, environmental analysis, manufacturing and other industrial applications. Our technical support team offers application development, on-site training and workshops. VICI AG International VICI (Valco Instruments Co. Inc. and VICI AG International) is one of the leading sources for top quality components for HPLC, UHPLC, LC, GC, FIA, SFE, SFC and Lab Safety. The Valco, Cheminert, Jour, and Precision Sampling product lines include injectors, selection valves for low pressure, HPLC and UHPLC, valve actuators, polymeric and metal fittings, inline and solvent filters, polymeric tubing (PEEK, PTFE, ETFE, FEP, PFA), metal tubing (Stainless Steel, Titanium, Nickel, Hastelloy C), sample loops, syringes, tools, dilutor/dispensers, liquid handling pumps, safety filters and safety caps for bottles and other canisters, CO2 and humidity filters. VWR enables the advancement of the world's most critical research through the distribution of a highly diversified product line to most of the world's top pharmaceutical and biotech companies, as well as industrial, educational and governmental organizations. With over 150 years of industry experience, VWR offers a well-established distribution network that reaches thousands of specialized labs and facilities spanning the globe. VWR offers a Chromatography portfolio of leading manufacturers plus the VWR Collection brand. You get a choice of quality and price as well as advice from Chromatography specialists, application laboratoratories and Chromatography service technicians. Wyatt Technology Europe GmbH VWR International GmbH Tosoh Bioscience GmbH
Spark Holland BV
YMC Europe GmbH YMC Europe offers a wide range of UHPLC and HPLC columns, bulk silica media for preparative chromatography and lab- and pilot-scale glass columns for customer packing. In addition we provide an on demand service for application support and method development. As a new field of business YMC has strongly invested in the sector of micro reaction technology and continuous synthesis. This new range of products, developed and engineered in YMC facilities, is available worldwide supported by dedicated YMC product specialists. Our extensive distribution network guarantees availability of all YMC products in countries all over the world.
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Exhibition Area
General Floor Plans
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Social Events
Welcome Reception
Sponsored by Shimadzu Free of charge
19:10 21:00 Sunday, 16 June, 2013 Location: Auditorium Lounge and Upper Lounge
Reception
Sponsored by Elsevier 18:00 19:30 Monday, 17 June, 2013 Location: Caf Amsterdam and Europe Foyer Free of charge
Farewell Reception
17:00 18:00 Thursday, 20 June, 2013 Location: First Floor restaurant All attendees are invited for an informal farewell meeting. We are looking forward to meet you next HPLC2013 symposium to be held in Hobart, Tasmania, Australia
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General Information
Date and Venue
The HPLC2013 Symposium is held from 16-20 June, 2013. Symposium and Exhibition Venue Amsterdam RAI Address: Europaplein, 1078 GZ, Amsterdam, The Netherlands Phone: +31 (0) 20 549 12 12 Fax: +31 (0) 20 646 44 69 Website: http://www.rai.nl/en/
The registration desk is located close to the entrance. Opening hours 8:30 10:00 Sunday, 16 June, 2013 (short-course participants only) 14:30 20:30 Sunday, 16 June, 2013 8:00 18:00 from Monday, 17 June to Wednesday, 19 June, 2013 8:00 15:00 Thursday, 20 June, 2013 Symposium delegates and their companions will receive their badges, symposium materials and social event tickets at the registration desk.
Badges
You are required to wear your name badge visibly when participating in the conference.
Catering Services
Coffee and lunch breaks Coffee, tea, refreshments and lunch (included in the registration fee) will be served in the exhibition and poster area (locations designated with a red-coloured C on the exhibition maps).
The internet corner is located in the back of area E (Europe Foyer). Please switch off your mobile phones during the lecture sessions. Smoking is not allowed in the congress centre. There will be free Wi-Fi for all participants and exhibitors in the RAI Conference Centre.
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Public Transportation
Travelling within Amsterdam is straight-forward and convenient. There is an extensive transport network connecting the city's many districts, and commuters can choose a variety of methods to reach their destination as efficiently as possible. This includes the train, tram, metro, bus and ferry. The I Amsterdam City Card gives you unlimited use of the GVB public transport system for 24, 48 or 72 hours. Metro Amsterdam's metro runs underneath the centre, from Central Station to the outer districts. This can be a fast and efficient way to travel, though the trains only run above ground away from the centre, so you lose out on the picturesque view. You'll need a PT Smart Card (OV-chipkaart) to ride the metro. All tickets must be purchased in advance at the GVB Tickets & Info office or GVB Ticket Vending Machines. From Amsterdam Central Station to the RAI Congress Centre: Metro line 51, stop Station Amsterdam RAI. Tram Trams are common in Amsterdam, with routes heading out from the centre in all directions. Trams are ideal for short journeys around the city centre, as well as for travelling to other districts. You'll need a PT Smart Card (OVchipkaart) to ride the tram. Only single-use disposable tickets can be purchased from the conductor. Tickets valid for multiple journeys can be purchased at the GVB Tickets & Info office or GVB Ticket Vending Machines. Bus Amsterdam operates a full bus network, which will take you anywhere you have to go. Just like the tram, only single-journey tickets can be purchased on board. Tickets valid for multiple journeys can be purchased at the GVB Tickets & Info office or GVB Ticket Vending Machines. Taxi Taxis can be handy when travelling to and from the airport, late at night when the trams have stopped running or when you're running late. Depending on the traffic during peak times, however, public transport may get you there even quicker. All licensed taxi drivers in Amsterdam must adhere to a defined fare structure. Below is an overview of the three components that are used to calculate the total price paid per journey. Maximum start price: 2.83 euros Maximum price per kilometre: 2.08 euros Maximum price per minute: 0.34 euros
Amsterdam city centre is a myriad of roads, lanes and footpaths. Because space in the city centre is limited, taxis cannot stop anywhere they like. To keep traffic flowing in the city at peak efficiency, stopping is not allowed at various places. Planning your journey Before seeing the sights, you may wish to consult the 9292 route planner or GVB website to help you find the quickest and most convenient way to get from A to B. In addition, there are a number of excellent apps available to help you find your way around the city.
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