Two TGA models are analyzed in this study: TGA Q5000 IR from TA Instruments and TGA 4000 from Perkin Elmer. The old TGA requires frequent repair and gives less accurate data than what most of the modern TGAs are capable of providing. The purpose of this study is to determine which TGA model would best suit the needs of Goodyear Tire and Rubber Company.
Two TGA models are analyzed in this study: TGA Q5000 IR from TA Instruments and TGA 4000 from Perkin Elmer. The old TGA requires frequent repair and gives less accurate data than what most of the modern TGAs are capable of providing. The purpose of this study is to determine which TGA model would best suit the needs of Goodyear Tire and Rubber Company.
Two TGA models are analyzed in this study: TGA Q5000 IR from TA Instruments and TGA 4000 from Perkin Elmer. The old TGA requires frequent repair and gives less accurate data than what most of the modern TGAs are capable of providing. The purpose of this study is to determine which TGA model would best suit the needs of Goodyear Tire and Rubber Company.
Samant Khanna November 7, 2013 ENGL 311 Dr. A. Kantar
Abstract Goodyear Tire and Rubber Company has commissioned a feasibility study to determine which TGA model should be purchased to replace the old and unreliable TGA, to get more accurate data. Two TGA models are analyzed in this study: TGA Q5000 IR from TA Instruments and TGA 4000 from Perkin Elmer. The instruments will be evaluated according to the following criteria: Capabilities, Value and Operational Costs. Following are an Introduction, Factual Summary, Conclusions, Recommendation and Annexes.
FEASIBILITY STUDY FOR THE SELECTION OF NEW TGA FOR GOODYEAR TIRE AND RUBBER COMPANY Introduction Jennifer Banks, a senior research analyst at Goodyear Tire and Rubber Company plans to replace the old TGA (Thermogravimetric analyzer) in the R&D department with a modern and more reliable version. The old TGA requires frequent repair and gives less accurate data than what most of the modern TGAs are capable of providing. The evaluation of TGA models requires a feasibility study due to the expensive nature of such an investment along with a wide range of TGA models available. The purpose of this study is to determine which TGA model would best suit the needs of Goodyear Tire and Rubber Company. Some of the minimum requirements established by Goodyear are as follows: must be able to reach temperature of 1000 C, must have a heating rate of up to 180 C/min, and must cost less than $80,000. The two TGA models which meet all the minimum requirements are: TGA Q5000 IR from TA Instruments and TGA 4000 from Perkin Elmer. The instruments will be evaluated according to the following criteria: Capabilities, Value and Operational Costs. Capabilities is divided into two subparts: Weight Balance and Furnace. Weight Balance evaluates the specifications of weight balance used in TGA such as capacity and accuracy. Furnace compares the specifications of furnace used in TGA such as temperature range and heating rate. Value is divided into three subparts: Initial Investment, Training and Features. Initial investment analyzes prices of the base models, shipping cost and warranty. Training evaluates training opportunities provided by the instrument manufacturers based on cost and effectiveness. Features compares the standard features that come with each TGA and their
significance. Operational Costs is divided into two subparts: Energy Costs and Service. Energy costs evaluates cost of resources required to keep the TGA running. Service analyzes both TGAs in terms of the cost of their replacement parts for repair. The following types of references were used to gather information for this study: email interviews, product brochures, specifications, websites and product manuals. The recommendation in this study is tailored specifically to fit the needs of Goodyear Tire and Rubber Company to meet their requirements and uses data current as of November 2013. Following are Factual Summary, Conclusions, Recommendation and Annexes. Factual Summary Goodyear Tire and Rubber Company is committed to being the world leader in tire industry with its wide range of high performance and long lasting tires. To accomplish this goal, they need access to state-of-the-art research instruments to generate accurate and reliable data. TGA is one of the most important instrument used in tire and rubber industry for reverse engineering analysis. It can decrypt the rubber compound of a competitor's product or for quality control purposes. The Capabilities of the TGA are most important for Goodyear as they determine the detail and accuracy of data that can be gathered from TGA. The Value of the TGA is important for Goodyear as they want the best suitable features and training support with TGA at a reasonable price. The Operational Costs are important for Goodyear to determine which TGA would cost more to operate and repair in the long run. The following table summarizes the findings of this feasibility study, organized based on the three criteria.
TGA Q5000 IR TGA 4000 A. Capabilities 1. Weight Balance Capacity 100 mg (Good) 1500 mg (Good) Sensitivity <0.1 g (Good) 1 g (Good) Signal resolution 0.01 g (Good) 0.2 g (Acceptable) Accuracy 0.1 % (Acceptable) 0.02 % (Good) Precision 0.01 % (Good) 0.01 % (Good) Scanning baseline dynamic drift <10 g (Good) <50 mg (Acceptable) 2. Furnace Temperature range Ambient - 1200 C (Good) Ambient - 1000 C (Good) Maximum heating rate 500 C/min (Good) 200 C/min (Good) Minimum heating rate 0.1 C/min (Good) 0.1 C/min (Good) Cooling rate 1200 C to 35 C in 10 min 1000 C to 100 C in 8 min 1000 C to 50 C in 11 min Scan temperature accuracy 1 % (Good) 1 % (Good) Scan temperature precision 0.1 % (Good) 0.8 % (Acceptable)
B. Value 1. Initial Investment Base price with shipping and insurance $68,000 (Acceptable) $42,100 (Good) Warranty One year (Good) One year (Good) 2. Training * See commentary below table Courses Theory and Applications- $850 Hands-on Training - $2250 Total- $3100 Introduction to TGA - $1325
TGA Q5000 IR TGA 4000 3. Features Hangdown pan 3 0 Top-loading pan 0 5 Digital display screen 3 0 Autosampler - 45 samples 0 5 Autosampler - 25 samples 3 0 Hi-Res TGA TM
C. Operational Costs 1. Energy costs (Electricity and Nitrogen gas) $2.38 /hour (Good) $9.15/hour (Acceptable) 2. Service (Total cost of replacement parts) $21,810 (Acceptable) $16,498 (Good)
Q5000 IR is capable of detecting very minute weight changes in comparison to TGA 4000 due to its lower signal resolution as well as sensitivity. This can assist Goodyear in determining the amount of additives or volatiles present in rubber compound in small quantities especially in reverse engineering of competitor's product. The specifications indicate that TGA 4000 has a better accuracy than Q5000 IR, but sensitivity and resolution specifications ensure that Q5000 IR will have more accurate weight measurements. Q5000 IR has a very low baseline drift which will ensure better repeatability and aid with detection of sub microgram weight changes.
Q5000 IR has the capability to cool down from 1200 C to 35 C in 10 minutes, which is a wider range of temperature with lower time when compared to cooling rates of TGA 4000. Faster cooling rates help in productivity by reaching the ambient temperature quickly, so the next test can be started. Q5000 IR has a better precision value than TGA 4000 ensuring more consistent temperature control and experiment results. TGA 4000 is $25,900 cheaper than Q5000 IR making it an attractive investment for Goodyear. Both instrument manufacturers offer training courses with similar content but TA Instruments offers a hands-on lab training session which is 2 days long. Perkin Elmer also offers customized training solutions at the customer's facility if required. Although TA Instruments does not offer on-site customized training and its two-course package is expensive than the course offered by Perkin Elmer, the courses offered by TA Instruments are better in terms of time taken for delivery and effectiveness making it worth the extra money. Q5000 IR clearly offers more features than TGA 4000 which lead to Q5000 IR getting a good rating. The Hi-Res TGA TM feature can help detect very small weight changes and increases the sensitivity to detect presence of additives present in small quantities. The Modulated TGA feature allows Q5000 IR to calculate activation energy in relation to time and temperature all throughout the experiment and can be useful for Goodyear in determining activation energy to calculate tire cure times. TGA 4000 uses a top-loading pan which is easier for manual loading of samples and offers a more robust design with no moving parts. This saves on repair cost but the TGA capabilities matter more than repair cost. Q5000 IR costs about 70% lower than TGA 4000 to operate, mainly due to higher volume of nitrogen gas used in TGA 4000. Q5000 IR has more expensive replacement parts as
the furnace is quite expensive compared to the one for TGA 4000; the furnace of Q5000 IR has a complex construction and uses IR technology.
Conclusions 1. Q5000 IR's excellent capabilities in both weight balance and furnace technology make it overall best choice in the area of Capabilities. (1-5)
2. Though TGA 4000 requires remarkably low initial investment, Q5000 IR's superior features and advantages in training options make it the overall best choice in the area of Value. (5-11)
3. Though TGA 4000 requires less expensive Service, Q5000 IR's significantly low energy costs make it the overall best choice in the area of Operational Costs. (11-14)
4. Clearly, Q5000 IR outperforms TGA 4000 in all the three criteria, making it the best choice for Goodyear Tire and Rubber Company.
Recommendation It is the recommendation of this study that Goodyear Tire and Rubber Company purchase the TA Instruments TGA Q5000 IR.