LVN

vn bn k thut o lng vit nam

LVN 139 : 2004

nht k mao qun thy tinh

o nht ng hc
Quy trnh kim nh
Glass capillary viscosimeters for the measurement of kinematic viscosity
Methods and means of verification

Li ni u :
LVN 139 : 2004 do Ban k thut o lng TC 17 Phng tin o ho l bin son.
Trung tm o lng ngh, Tng cc Tiu chun o lng Cht lng ban hnh.

h ni - 2004

Li ni u :
LVN 139 : 2004 do Ban k thut o lng TC 17 Phng tin o ho l bin son.
Trung tm o lng ngh, Tng cc Tiu chun o lng Cht lng ban hnh.

vn bn k thut o lng vit nam

2

lvn 139 : 2004

Nht k mao qun thy tinh o nht ng hc

Quy trnh kim nh
Glass capillary viscosimeters for the measurement of kinematic viscosity
Methods and means of verification

1 Phm vi p dng
Vn bn k thut ny quy nh quy trnh kim nh nht k mao qun thy tinh o nht
ng hc c hng s nht k (0,01 10) mm2/s2, chnh xc n 0,2 %.

2 Cc php kim nh
Phi ln lt tin hnh cc php kim nh ghi trong bng sau:

STT

Tn php kim nh

Theo iu mc ca QTK

Kim tra bn ngoi

5.1

Kim tra o lng

5.2

2.1

Tin hnh xc nh hng s nht k

5.2.1

2.2

Tnh hng s nht k C

5.2.2

3 Phng tin kim nh

- Mu chun nht c chng nhn: c gi tr danh ngha nht ph hp, chnh xc
0,1 % (bng 1).

lvn 139 : 2004

Bng 1
Cc mu chun nht dng kim nh cc nht k mao qun thy tinh
Gi tr danh ngha nht ng hc (mm2/s) ti nhit

K hiu
mu
chun -53,89oC - 40oC
3

300

20

20 oC

80

25 oC

37,78oC

40 oC

50 oC 98,89oC

100o
C

4,6

4,0

3,0

2,9

1,2

1,2

11

8,9

6,0

5,7

1,8

1,8

44

34

20

18

4,0

3,9

60

170

120

60

54

7,4

7,2

200

640

450

200

180

17,5

17

600

2 400

1 600

600

520

280

33

32

2 000

8 700

5 600

2 000

1 700

78

75

8 000

37 000 23 000

8 000

6 700

30 000

81 000

27 000

23 000 11 000

- Bnh iu nhit
+ Phm vi iu nhit (0 100) oC;
+ n nh 0,01 oC;
- Phng tin o thi gian, gi tr chia: 0,01 giy.
3.2 Phng tin ph
- Bm tia nc hoc loi bm ht khc;
- Bnh ht m;
- Cc dng c thy tinh phng th nghim (cc, chai, phu, tm lc v. v...);
- Cc cht lng ra nht k: nc ct, sunfuacromic (ph lc 2), xng trng, cn telic
chng ct, axeton, tluen hay cc dung mi khc;
- Cc ng cao su hay ng nha nh;
- Cc g;
- Ngun sng lnh;
- Phng tin o nhit v m mi trng:
+ Phm vi o nhit : (0 50) oC, gi tr chia 1 oC;
+ Phm vi o m: (0 100) %RH, gi tr chia 2 %RH.

lvn 139 : 2004

4

4 iu kin kim nh v chun b kim nh

4.1 iu kin kim nh
Khi tin hnh kim nh phi m bo cc iu kin sau y:
- Nhit : (25 2) o C;
- m tng i: (40 70) %RH;
- Phi c h thng ht khng kh;
- Khng c cc cht d gy chy n.
4.2 Chun b kim nh
Trc khi tin hnh kim nh phi thc hin cc cng vic chun b sau y:
4.2.1 Lm sch v sy kh nht k cn kim nh
- i vi nht k khng b thm nhim cc sn phm xng du: ra bng nc nng,
hn hp sunfuacromic vo ngm t nht 2 gi. Sau phi ra nht k bng nc ct v sy
kh nhit khng vt qu 120 oC.
- i vi nht k b thm nhim cc sn phm xng du: ra bng xng trng, ri ra bng
nc nng cho ti khi ht mi xng v sau hn hp sunfuacromic vo ngm t nht 2
gi. Sau phi ra nht k bng nc ct v sy kh nhit khng vt qu 120 oC.
- i vi nht k b thm nhim cc sn phm khc: ra lin tip bng dung mi ph hp.
Sau phi ra nht k cn kim bng nc ct v sau hn hp sunfuacromic vo
ngm t nht 2 gi. Sau phi ra nht k bng nc ct v sy kh nhit khng vt
qu 120 oC.
4.2.2 Chn mu chun nht
Cc mu chun nht phi c chn sao cho t s gi tr nht t 2 n 5. Thi gian
chy ca cht lng i vi mi loi nht k cn kim nh khng c nh hn 200 giy.
i vi nht k c C 0,05 mm2/s2 thi gian chy ti thiu phi ln hn 200 giy.
4.2.3 Trc khi tin hnh kim nh, nht k cn kim sau khi c lm sch v mu
chun nht phi c t trong phng kim nh t nht 4 gi.

5 Tin hnh kim nh

5.1 Kim tra bn ngoi
Phi kim tra bn ngoi theo cc yu cu sau y:

lvn 139 : 2004

Kim tra bng mt xc nh s ph hp ca nht k vi cc yu cu quy nh trong ti

liu k thut v hnh dng, kch thc, nhn hiu, s hiu sn xut. Cc k hiu phi khng
b hng khi s dng.
Nht k b loi b nu khng tha mn tt c cc yu cu ny.
5.2 Kim tra o lng
Nht k mao qun thu tinh c kim tra o lng theo trnh t ni dung, phng php v
yu cu sau y:
5.2.1 Tin hnh xc nh hng s nht k C
xc nh hng s C i vi mi nht k dng 2 mu chun nht. Trc mi ln np
mu chun nht, phi ra sch v sy kh nht k nh nn mc 4.2.1.
5.2.1.1 Np mu chun nht th nht vo nht k cn kim nh, t nht k vo bnh
iu nhit c nhit theo yu cu ca php o. Sau 60 pht tin hnh o thi gian chy ca
cht lng.
Qu trnh o c thc hin nh sau:
o thi gian chy ca mu chun nht trong nht k t nht 5 ln lin tip, mi ln cch
nhau 10 pht. i vi nht k dng o nht cc cht lng c s php o thi gian
chy khng c t hn 3 ln. Ghi kt qu vo bin bn kim nh.
Thi gian chy ca mu chun nht phi c o vi chnh xc 0,2 giy, chnh lch
thi gian chy gia gi tr ln nht v nh nht khng c vt qu 0,2 % thi gian chy
trung bnh (khng c vt qu 0,3 % thi gian chy trung bnh i vi nht k dng o
nht ca cht lng c).
Nu cc gi tr o t yu cu nu trn th ra v sy kh li nht k v thc hin php kim
tng t i vi mu chun th hai.
Nu cc gi tr o khng t yu cu nu trn th phi ra v sy kh li nht k v kim
nh li i vi mu chun th nht.
Nu kim ln th hai i vi mu chun th nht vn khng t yu cu nu trn th phi
loi b nht k khng tin hnh cc bc kim nh tip theo.
5.2.1.2 i vi mu chun th hai: Tin hnh o thi gian chy i vi mu chun th hai
nh mc 5.2.1.1

lvn 139 : 2004

6

5.2.2 Tnh hng s nht k C

- Hng s nht k C c xc nh bng gi tr trung bnh cng ca gi tr C1 v C2 vi s
ch s c ngha khng t hn 4.
- Cc gi tr C1 v C2 tnh theo cng thc sau:
C1 =

1 g n
.
t1 g

C2 =

2 gn
. .
t2 g

Trong :
C1 : gi tr hng s nht k xc nh bng mu chun nht th nht, (mm2/s2);
C2 : gi tr hng s nht k xc nh bng mu chun nht th hai, (mm2/s2);
1 : nht ca mu chun nht th nht, (mm2/s);
2 : nht ca mu chun nht th hai, (mm2/s);
t1 : thi gian chy trung bnh ca cht lng chun th nht trong nht k, (s);
t2 : thi gian chy trung bnh ca cht lng chun th hai trong nht k, (s);
gn : gia tc trng trng chun, (9,80665 m/s2);
g : gia tc trng trng ti a im xc nh hng s C1 v C2;, (m/s2);
Ti H Ni, g = 9,78669 m/s2;
Ti Nng, g = 9,78402 m/s2;
Ti Bin Ha, g = 9,78234 m/s2;
Ti cc a phng khc g c tnh theo cng thc sau:
g = 9,780 318. (1 + 0,005 302 4 sin2 - 0,000 005 9 sin22) 2.10-6 h, (m/s2);
Trong :
: v ti a phng cn tnh g, (o);
h : cao (so vi mt bin) ti ni cn tnh g, (m).
5.2.3 Chnh lch gia cc hng s nht k C1, C2 tnh c phi khng ln hn 0,2 % i
vi nht k o cht lng trong sut v phi khng ln hn 0,4 % i vi cc cht lng c.
- Nu gi tr hng s nht k C1, C2 t yu cu trn th thc hin tip bc tnh hng s nht
k C theo mc 5.2.4.
- Nu gi tr hng s nht k C1, C2 khng t yu cu trn th phi thc hin kim nh li
ln th hai. Nu ln th hai cng khng t th nht k b loi b.

lvn 139 : 2004

7

5.2.4 Gi tr hng s nht k C c tnh bng trung bnh cng ca C1 v C2.

C=

C1 + C 2
,
2

(mm2/s2)

6 X l chung
6.1 Nht k mao qun thy tinh o nht ng hc t cc yu cu quy nh trong mc
tin hnh kim nh c ng du v cp giy chng nhn kim nh.
6.2 Nht k mao qun thy tinh o nht ng hc khng t mt trong cc yu cu quy
nh trong mc tin hnh kim nh th khng cp giy chng nhn kim nh v xo du
kim nh c (nu c).
6.3 Chu k kim nh: 01 nm.

Ph lc

Bin bn kim nh

Tn c quan kim nh:

............................

Tn phng tin o: ..............................................................................................................

Kiu: ......................................................................... S: ................................................
C s sn xut: .......................................................... Nm sn xut: ..............................
c trng k thut: ...............................................................................................................
- Hng s nht k
chnh xc: ...............................
Ni s dng: .................................................... .....................................................................
Phng php thc hin: .........................................................................................................
Chun, thit b chnh c s dng: .....................................................................................
iu kin mi trng: ...........................................................................................................
Ngi thc hin: ........................................................ Ngy thc hin: ............................
Kt qu
1 Kim tra bn ngoi:
2 Kim tra o lng
t = ......oC

Mu chun nht th nht

TT

Thi gian chy

t1

Gi tr chun
1

(s)

(mm2/s)

gn
g

Hng s nht k
C1
(mm2/s2)

Hng s nht k
C + C2
C= 1
2
2 2
(mm /s )

1
2
3
4
5
TB
Mu chun nht th hai
Thi gian chy
t2
(s)

Gi tr chun
2
(mm2/s)

gn
g

Hng s nht k
C2
(mm2/s2)

1
2
3
4
5
TB
Kt lun :
Ngi sot li

Ngi thc hin

9

LVN 139 : 2004

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10