This document describes the gravimetric method for determining nickel using dimethylglyoxime. Nickel salts are precipitated as nickel dimethylglyoximate by adding an ethanolic solution of dimethylglyoxime to an acidic nickel solution. The precipitate is filtered, washed, dried and weighed to determine the amount of nickel. The precipitate is soluble in mineral acids, hot water, and concentrated solutions of cobalt salts but insoluble in dilute ammonia solutions.
Original Description:
Original Title
Experiments on Gramimetry and Precipitation Titration
This document describes the gravimetric method for determining nickel using dimethylglyoxime. Nickel salts are precipitated as nickel dimethylglyoximate by adding an ethanolic solution of dimethylglyoxime to an acidic nickel solution. The precipitate is filtered, washed, dried and weighed to determine the amount of nickel. The precipitate is soluble in mineral acids, hot water, and concentrated solutions of cobalt salts but insoluble in dilute ammonia solutions.
This document describes the gravimetric method for determining nickel using dimethylglyoxime. Nickel salts are precipitated as nickel dimethylglyoximate by adding an ethanolic solution of dimethylglyoxime to an acidic nickel solution. The precipitate is filtered, washed, dried and weighed to determine the amount of nickel. The precipitate is soluble in mineral acids, hot water, and concentrated solutions of cobalt salts but insoluble in dilute ammonia solutions.