EDX-700HS 800HS 900HS SM Rev0ocr

Shimadzu Energy Dispersion
Fluorescence X-ray Spectrometer

Ray ny E DX-700HS/800HS/900HS
SERVICE MANUAL
Installation of this unit may be dangerous task. Only qualified Shirnadzu service
engineers may install this unit; the user is prohibited fiom attempting
installation. This manual is intended solely for the use of Shirnadzu service
SHIMADZU CORPORATI0N
ANALYTICAL & MEASURING INSTRUMENTS DIVISION
KYOTO, JAPAN
Contents
Chapter l Installation
1 . lnstallation Requirements
..................................................................................................... . 1.1 An example of layout 1 3
. 1.2 Installation conditions .................................................................................................... 1 4
......................................................................................................... 1.3 Power requirement 1 . 5
.................................................................. . 1.4 Refrigerant for a detector (Liquid nitrogen) 1 5
..................................................................................................................... . 1.5 Helium gas 1 6
................................................................................ . 1.6 Check list of Installation condition 1 8
2 . Installation Procedure
................................................. 2.1 Installation (Wiring. piping. replenishment included)
...................................................................... 2.1.1 Checking installation environment
............................................................................... 2.1.2 Installing the EDX main unit
......................................................... 2.1.3 Checking the appearance of the instrument
.................................................................. 2.1.4 Checking the contents of the packing
......................................................................................... 2.1 . 5 Installing the SDT unit
................ 2.1.6 Installing the personal computer (PC, Display. keyboard) and printer
.................................................................................. 2.1.7 Connecting the SCSI cable
2.1 . 8 Adding liquid nitrogen .........................................................................................
..................... 2.1.9 Adjusting the positions of cover closing-part's inclination sensors
(One at each of the right and left sides)
.......................................................................... . 2.1 10 Installing the evacuation system
(Regarding other options, refer to the corresponding Instruction Manual.)
2.2 Energizing (Starting the instrument) ............................................................................
..................................................................................................... 2.2.1 EDX main unit
....................................................................................... 2.2.2 Starting the workstation
............................... 2.3 Checking the EDX main unit operation (On the operation panel)
............................................... 2.3.1 Checking the cover open/close-part for operation
2.4 Installing the System Sheet ..........................................................................................
2.4.1 Installing the Device Information sheet ...............................................................
............................................................................. 2.5 Setting the instrument environment
....................................... 2.5.1 Change to EDX-900 environment (EDX-9OOHS only)
........................................................................ 2.5.2 Environment utility "eu3" setting
..................................................... 2.5.3 Setting and checking instrument environment
(All instruments Including EDX-900HS)
2.6 Checking the EDX main unit for operation (by the EDX software) ............................
2.6.1 Starting the EDX software ...................................................................................
2.6.2 Initializing the instrument ....................................................................................
............................................................... 2.6.3 Checking each drive unit for operation
............................................................ 2.6.4 Checking the position of the detector cap
........... 2.6.5 Checking functions of the standard accessory (Liquid sample adapter)
................................................................................................................... 2.7 Adjustment
....... 2.7.1 Starting the instrument (Turning ON the X-ray and detector high voltage.)
................................................ 2.7.2 Changing to the adjustrnent/inspection directory
.............................................................................. 2.7.3 Checking the energy position
(Carry out the calibration and data check at least one hour after energization.)
.................................................................... 2.7.4 Carrying out the Energy Calibration
.......................................................................................... 2.8 Inspection (Standard units)
2.8.1 Checking the position after the Energy Calibration .............................................
......................................................................................................... 2.8.2 Repeatability
........................................................................................... 2.8.3 FP Qual-Quantitative
..................................................................................... 2.8.4 Resolution Confirmation
.................................................................. 2.8.5 Carbon Analysis (EDX-800HS only)
2.9 Inspection (Option units) .............................................................................................
...................................................................... 2.9.1 Atmosphere Control: Vaccum Unit
................................................................... 2.9.2 Atmosphere Control: He Purge Unit
2.9.3 Turret ...................................................................................................................
2.9.4 Collimator ............................................................................................................
............................................................................................... 2.9.5 CCD Camera Unit
........................................................................................................... 2.9.6 Pilot Lamp
.................................................................................... 2.10 Checking option configuration
................................................................................................... 2.11 Checking traceability
2.12 Checking instrument information ................................................................................
2.13 Operational explanation ...............................................................................................
2.14 Reporting completion of installation ...........................................................................
Chapter 2 Maintenance* Adjustment
Maintenance . Adjustmant Procedure of Unit Replacement
............................ . 1 . 1 Adjustment Item and Check Item according to the unit replacement 2 3
. 1.2 Replacing the detector ................................................................................................... 2 5
. 1.2.1 Replacing the detector of EDX-700HS 1 800HS ................................................... 2 5
. 1.2.2 Replacing the detector of EDX-900HS ................................................................. 2 9
....................................................................................................... . Replacing the tube 2 13
. Replacing the belts (Shutterlfilter. collimator) ............................................................. 2 14
. Replacing the belt for operating the cover ................................................................... 2 15
.................................................................................................. . X-ray indicator lamp 2 16
. Adjusting the cover closing-part's inclination sensor ................................................. 2 17
. .
. Adjustmg the cover operation sensor ........................................................................... 2 17
. Adjusting the liquid mode proximity sensor ................................................................ 2 18
. Adjusting the liquid mode fiber sensor (for a turret) ................................................... 2 19
. ........................................................ Offset adjustment of shutterlfilter and collimator 2 20
. .
. Adjusting the turret stop pos~tion ................................................................................. 2 24
. .
. Adjusting the turret ongm ............................................................................................ 2 25
................................................................................... . Checking the degree of vacuum 2 26
MCA PCB .................................................................................................................... 2 . 27
........................................................................................ . 3 . 1. 1 Checking input voltage 2 27
........................ . 3 . 1 . 2 Adjusting the LLD level controller R2 (Only the PCB possible) 2 27
3.1.3 Checking adjustment of the offset level controller R1 (Only the PCB possible) 2 . 29
.................................. . . . 3 1 4 MCA PCB Check TerminalLED Display Function Table 2 30
........................................................................................... . 3.1.5 Replacing the ROM 2 31
................................................................................................................... 3.2 CTRL PCB 2 . 33
3.2.1 Checking input and output voltage ...................................................................... 2 . 33
3.2.2 Adjusting the M5 offset controller VR1 .............................................................. 2 . 34
. 3.2.3 CTRL PCB Display LED Function Table ............................................................ 2 34
. 3.2.4 CTRL PCB Check Terminal Function Table ....................................................... 2 36
........................................................................ 3.3 AMP PCB (only EDX.700HSlSOOHS) 2 . 37
3.3.1 Adjusting the gain of the amplifier ..................................................................... 2 . 37
............................................................. . 3.3.2 AMP PCB Display LED Function Table 2 39
. ......................................................... 3.3.3 AMP PCB Check Terminal Function Table 2 40
3.4 PSPCB ........................................................................................................................ 2- 41
. 3.4.1 Adjusting the detector bias .................................................................................. 2 41
. 3.4.2 PS PCB Check Terminal Function Table ............................................................. 2 41
. Stepping drive motor .................................................................................................... 2 42
Mounting the turret drive unit ...................................................................................... 2 . 43
. Installation orders of collimator ................................................................................... 2 44
. Mounting the X-ray indication lamp ............................................................................ 2 47
FP Sensitivity Coefficient Input Method ..................................................................... 2 . 48
Registering collimator standard intensity .................................................................... 2 . 57
. Checking the PV ratio .................................................................................................. 2 59
Procedure of installing the EDX software ................................................................... 2 . 61
Settings for Windows XP ............................................................................................. 2 . 64
.Instruction for settings ........................................................................................................ 2 - 66
..................... [Reference] Settings of Administrator (Normally you do not need to set.) 2 - 73
[Reference21 Comparison Window style (English) ......................................................... 2 - 74
About the identification of the instrument ....................................................................... 2 - 77
Chapter 3 Consumable and Maintenance Parts
. 1.1 EDX Assembling structure (EDX-700HS El800HS E) ................................................. 3 2
. 1.2 EDX Assembling structure (EDX-900HS E) ................................................................ 3 4
. 1.3 EDX Assembling structure (EDX-700HS CEl800HS CE) ..................................... 3 6
. 1.4 EDX Assembling structure (EDX-900HS CE) .............................................................. 3 8
. 2 . Consumables List ......................................................................................................... 3 10
. 3 . Maintenance Parts List ................................................................................................. 3 11
Chapter 4 Electronical Circuit Diagram
Chapter 5 Trouble Shooting
. 1 . Error message ................................................................................................................ 5 2
Chapter l Installation
1 . Installation Requirements
........................................................................................................ 1 . l An example of layout 1 - 3
....................................................................................................... 1.2 Installation conditions 1 - 4
............................................................................................................ 1.3 Power requirement 1 - 5
...................................................................... 1.4 Refrigerant for a detector (Liquid nitrogen) 1 - 5
........................................................................................................................
1.5 Helium gas 1 - 6
................................................................................... 1.6 Check list of Installation condition 1 - 8
2 . Installation Procedure
.................................................... 2.1 Installation (Wiring, piping, replenishment included) 1 - 10
Checking installation environment .......................................................................
................................................................................ Installing the EDX main unit
.......................................................... Checking the appearance of the instrument
Checking the contents of the packing ...................................................................
Installing the SDT unit ..........................................................................................
................. Installing the personal computer (PC. Display. keyboard) and printer
Connecting the SCSI cable ...................................................................................
. .
Addlng liquid nitrogen ..........................................................................................
...................... Adjusting the positions of cover closing-part's inclination sensors
Installing the evacuation system ...........................................................................
(Regarding other options. refer to the corresponding Instruction Manual.)
............................................................................. . 2.2 Energizing (Starting the instrument) 1 17
2.2.1 EDXmainunit ...................................................................................................... 1- 17
........................................................................................ . 2.2.2 Starting the workstation 1 17
.................................. . 2.3 Checking the EDX main unit operation (On the operation panel) 1 17
. ................................................ 2.3.1 Checking the cover open/close-part for operation 1 17
............................................................................................. 2.4 Installing the System Sheet 1 . 17
................................................................ 2.4.1 Installing the Device Information sheet 1 - 17
................................................................................ 2.5 Setting the instrument environment
........................................ 2.5.1 Change to EDX-900 environment (EDX-9OOHS only)
......................................................................... 2.5.2 Environment utility "eu3" setting
...................................................... 2.5.3 Setting and checking instrument environment
(All instruments Including EDX-900HS)
............................... 2.6 Checking the EDX main unit for operation (by the EDX software)
.................................................................................... 2.6.1 Starting the EDX software
. . .
..................................................................................... 2.6.2 Initializing the instrument
2.6.3 Checking each drive unit for operation ................................................................
2.6.4 Checking the position of the detector cap ...........................................................
............ 2.6.5 Checking functions of the standard accessory (Liquid sample adapter)
...................................................................................................................... 2.7 Adjustment
2.7.1 Starting the instrument (Turning ON the X-ray and detector high voltage.) ........
2.7.2 Changing to the adjustment/inspection directory .................................................
............................................................................... 2.7.3 Checking the energy position
(Carry out the calibration and data check at least one hour after energization.)
..................................................................... 2.7.4 Carrying out the Energy Calibration
.............................................................................................. 2.8 Inspection (Standard units)
.............................................. 2.8.1 Checking the position after the Energy Calibration
......................................................................................................... 2.8.2 Repeatability
............................................................................................ 2.8.3 FP Qual-Quantitative
...................................................................................... 2.8.4 Resolution Confirmation
................................................................... 2.8.5 Carbon Analysis (EDX-800HS only)
2.9 Inspection (Option units) .................................................................................................
....................................................................... 2.9.1 Atmosphere Control: Vaccum Unit
2.9.2 Atmosphere Control: He Purge Unit ....................................................................
.................................................................................................................... 2.9.3 Turret
............................................................................................................. 2.9.4 Collimator
................................................................................................ 2.9.5 CCD Camera Unit
2.9.6 Pilot Lamp ............................................................................................................
........................................................................................ 2.10 Checking option configuration
2.11 Checking traceability ......................................................................................................
................................................................................... 2.12 Checking instrument information
.................................................................................................. 2.13 Operational explanation
............................................................................... 2.14 Reporting completion of installation
1. Installation Requirements
1 .l An example of layout
Figure 1 shows an example of layout when the EDX-700HSl800HS is placed on a
table. In the figure, a PC, printer and EDX-700HSl800HS are placed on the table of
1,800 (W) X 800 (D) X 700 mm (H).
The EDX main unit weighs approximately 80 kg. Place a table sturdy enough to load
the EDX main unit, PC and printer (min. withstand load: 120 kg).
The EDX-700HSl800HS requires space around its main unit for maintenance. As
shown in the example, place a movable PC and printer around the main unit. Also, keep
at least a 80 cm distance between the EDX main unit and the wall and units difficult to
move.
*
In case that a rotary pump is attached as an option
Place the rotary pump on a stable floor. The piping attached to the rotary pump
has a length of 1,500 mm and therefore, you must set the rotary pump on the floor
behind the table. Keep a 30 cm distance between the table rear panel and the wall.
CE type only .
Fig. 1. Example of Layout
Humidity:
Installation site:
Others:
Installation conditions
Ambient temperature: 10 to 30C
Temperature fluctuation: & 5C at a temperature of 10 to 30C
Temperature change: 2"CIhour or less, a sudden change not
permissible
40 to 70% (No condensation allowed)
Sturdy table or testing bench of about 1,800 (W) X 800 (D) X
700 mm (H) (min. withstand load: 120 kg). If the instrument
is provided with a rotary pump as an optional feature, keep at
least 30 cm space behind the table.
To assure optimum performance of the instrument, the
installation room should have less interfering elements like
heavy dust particles, vibration, electric magnetic field noise,
corrosive gases.
To keep its optimum performance, choose an installation
site taking the following points into account.
Do not subject the instrument to;
A strong magnetic field, electric field, or radio
frequency. (They may deteriorate analysis accuracy.)
Vibration
Heavy dust particles, much humidity and corrosive
gases
Direct sunlight and also,
Keep fluctuation of supply voltage to the minimum.
Secure the instrument as a countermeasure against
earthquake.
Ground the main unit appropriately to prevent
electrical accidents. (Grounding Workpiece
Regulations, Solid grounding: 100Q or less )
1.3 Power requirement
The instrument must be powered by power supply protected by a leakage breaker.
The EDX main unit of standard type requires power supply of 100 VAC, 15 A and
50160Hz (single phase). The EDX main unit of CE type requires power supply of
1000VA, 22012301240VAC and 50160Hz (single phase). Do not use other type power
supply for the instrument.
To assure its performance, the following stability is required for power supply:
voltage fluctuation of k 10% and frequency off 5%.
If power supply of the above specification is not available, the power supply facility
must be changed.
l .4 Refrigerant for a detector (Liquid nitrogen)
You need liquid nitrogen to cool a detector during operation of the instrument. Also,
you need tools to feed liquid nitrogen to the detector (liquid nitrogen container, take-out
unit (CRY0 JET) ). Have at hand the following or the equivalent.
Table 1.2 Tools To Supply Liquid Nitrogen (Recommended Units)
The numbers with * are Part Nos. from Shimadm.
Liquid nitrogen container
038-00909-02*
038-00909-03*
*
Liquid nitrogen is liquid of extremely low temperature (-196C). You may get a
burn if the skin is exposed to it. Special care must be taken to handling of liquid
nitrogen.
Liquid nitrogen take-out unit
If you use it in a small room, be sure to ventilate the room well. Otherwise, you
may be suffocated by vaporized liquid gas.
Refer to the Instruction Manual, "Precautions on Safety Use", "4. Liquid
Nitrogen".
Manu
facturer
Shievel- l 0
Shievel-20
Manu
facturer
Capacity Part No. Part No. Model Model
10L
20L
Touri
Touri
038-00920-02*
038-00920-03 *
Cryojetshievel-l0 10L
Cryojetshievel- l0 20L
Touri
Touri
1.5 Helium gas
If the instrument is provided with an optional unit, He replacement measurement unit
P/N 212-22495, you need helium gas as replacement gas.
The required gas type, its purity and gas pressure are as follows. Gas and a pressure
governor are attached as standard features.
Table 1.3 Gas Specification and Pressure Governor
The numbers with * are Part Nos. from Shimadzu.
A piping unit (vinyl hose) between the helium gas cylinder and the EDX-7001800 is
included in the He replacement measurement unit.
Pressure governor
YBR-2501CGA
Model : 040-72016-52
Gas
Table 1.4 Piping Unit
I Part No. I Part Name I Inner dia. X Thickness I
Gas pressure
15MPa
TY pe
He gas
He
Purity
99.995% or more
The number with * is Part No. from Shimadzu.
If you place the gas cylinder outside of the room, you must lay another piping to a
place within 2.5 m radius of the instrument.
If you lay piping above, be careful about points below.
(a)
Use a stainless pipe for piping.
(b)
Be careful not to use a helium gas piping unit too narrow to feed the gas.
Generally, the required inner diameter of the piping unit is 6 mm, min.
(c)
At the end of the gas piping unit, attach a hose nipple (outer dia.: 6.5 to 7.0 mm)
which can accept the attached gas supply hose (inner dia.: 6.0 mm).
016-31329* Vinyl hose, length: 3.0 m 6mm X 2mm
Precautions on handling a high pressure gas cylinder
To a gas cylinder you will use, the High-pressure Gas Control Law is applied. Be sure
to observe the Law for use.
General precautions
1. The gas cylinder should be placed in a well-ventilated place not subjected to direct
sunlight and the gas should be introduced indoors through piping.
2. Do not allow ambient temperature to be higher than 40C, nor fire to enter a 2 m
radius of the cylinder.
3. When you use a high pressure gas, be sure to ventilate the site well and check for gas
leakage using soap-and-water solution before starting daily work. Particularly when you
use a combustible gas, NEVER smoke or use fire in a 5 m radius of the unit to use the
gas.
Also, the site should be provided with an effective fire extinguisher.
4. Secure the cylinder with rope or the like to prevent it from turning over or falling.
5. A pressure regulator must be one for which oil is not allowed to use. The gas goes
through its pipe and therefore, never use one of which pipe inner face is stained with oil.
6. On completion of use of the gas, close the main cock of the cylinder.
7. You are required to get a permission by the Law if you store cylinders of 300 m 3 or
more.
Refer to the High-pressure Gas Control Law, the Regulations for General
High-pressure Gas Safety and the Fire Laws.
1.6 Check list of Installation condition
detector
(EDX-900HS
does not need
1 - 1 Temperature
1-2 Humidity
1-3 Installation space
Installation bench space
Strength
Rear space
Side space
Space for options
1-4 Installation site
2-1 Fluctuation
Voltage fluctuation (Performance
guarantee)
Frequency fluctuation
(Performance guarantee)
2-2 Power requirement
EDX
Grounding (Grounding resistance)
2-3 Position of power supply terminal
Length of EDX main unit cable: 2.0m
The following items are required.
3-1 Liquid nitrogen
3-2 Container
3-3 Take-out unit (CRY0 JET)
Prior registration at the Labor Standards
Bureau required.
Condition
Fluctuation : f SC at a temperature of 10 to
30C, Temperature change: 2OChour or less
40 to 70% (No condensation allowed)
Width Depth Height
1,800 X 800 X 700 - 800 mm
Min. withstand load: 120 kg
200 mm, min.
Space of min. 800 mm should be assured for
maintenance.
Refer to "4. Options".
No units which generate strong magnetic field,
electric field, or radio hquency should be placed
near the instrument.
No heavy vibration
No heavy dust particles, humidity, nor comsive gases
No direct sunlight
Fluctuation of power supply should be kept to
the minimum.
Secure the instrument as a countermeasure against
earthquake.
f 10% of the rated voltage
100VAC, 15A, 50160Hz (Standard type) or
1000VA, 220/230/240VAC, 50160Hz (CE type)
Within a 1 .S m radius of the instrument
3 liter. min.
One which can store liquid nitrogen. (5 1, min.)
One which can supply liquid nitrogen from the
container to EDX
Must be submitted at least 30 days before using
the unit.
C M
Mark
0
0
5. Options
6. Other options
7. Others
5-1 Vacuum measurement unit
PM 2 12-22460 (with RP)
2 12-22460-01 (without RP)
Installation place of the rotary pump
Length of the attached piping: 1.5 m
5-2 He replacement measurement unit
P/N 2 12-22495
(with He Gas Cylinder)
PM 2 12-22495-0 1
(without He Gas Cylinder)
Installation place of the helium gas
cylinder
Length of the attached piping: 3.0 m
Configurations of options required
by customers
7-1 Consumable and maintenance parts
required by customers
Between the table rear panel and the wall
At least a 300 mm distance from the instrument
Within a 2.5 m radius of the instrument
Consult us.
As required
2. Installation Procedure
2.1 Installation (Wiring, piping, replenishment included)
2.1 .l Checking installation environment
Check that the installation conditions are conformed to referring to the
Installation Manual.
2.1.2 Installing the EDX main unit
Open the transport box and install the main unit.
Unlatching
l. Opmthe cover;
2. Remove the intermediate
cushion.
3. Take out the instrument.
i
Intermediate cushion
is. < ,
? t
8 ,I* Insert your hands on the recessed parts
2 1""
4'
1 )-, , J- - - on the right and left. Lift the main unit
/G' '*
' l +
Counterclockwise %
rotate it 180'.
+A
*
- " v a - L - -
&'
i'
;,&/
, . ' S
+ P y * -&$$/"
,
\.**
hands here.
Unlatch.
Fig. 1.3 (a) Fig. 1.3 (b)
2.1.3 Checking the appearance of the instrument
Check for damage after installing the instrument.
If you complete checking, give a check to the "Check mark" (0).
2.1.4 Checking the contents of the packing
Check the contents of the packing against the Instruction Manual "1.3 Standard
accessory list".
If you finish checking, give a check to the "Check mark" (U).
Table 1.5 Standard Accessory List
- - -
No.
1
2
3
4
I @ standard sample AI 212-21650-17 1
I
Part Name
EDX device floppjr ASSY (1 sheet)
DXP-700 media ASSY (4sheets)
5
EDX instruction manual kit
SCSI cable (with ferrite core)
Part No.
212-22512-91
2 12-29232-91
Standard pack
standard sam~l e SUS
Philips type driver
@ Liquid sample adapter ASSY
@ Sample cell (3529, for general use, with cover)
@ Sample cell (3577, for small amount sample)
Sample cell (357 1, for general use, open type)
@ Mylar 6pm (1 001set)
W'
1 set
1 set
2 12-29709-91
212-22615-91
@l Molycote grease
@I Vacuum grease
I ($3 SDT unit 230V ASSY (CE type only) 212-23018-94 1 I
1
1
2 12-22490
212-21650-02
086-1 1002
2 12-22687-91
2 16-85000-02
219-85000-04
2 19-85000-05
212-86501-55
@ Oil pen
I @ Screws (CE type only) 020-46546 8 I
l set
1
1
1
5
5
5
1
0 17-270 14-05
017-30812-01
286-7 102 1
Nos. 1 and 2 are included in the FLOPPY DISK FILE case.
1
1
1 I
2.1.5 Installing the SDT unit
Install the SDT unit using 8 screws backside in table 1 S. See Fig 1.4 (a).
At first, insert the AC cord attached the SDT unit to the EDX Main unit. And then install the SDT
Unit using the 8 screws.
I LAC cord for IOOV
Fig.l.4 SDT Unit
2.1.6 Installing the personal computer (PC, Display, keyboard) and printer
After unpacking, install the personal computer and connect cables.
2.1.7 Connecting the SCSI cable
Connect the EDX main unit to the PC using the SCSI cable. (The end with a
ferrite core must come to the main unit side.)
2.1.8 Adding liquid nitrogen
Open the upper cover, remove the Dewar cap and replenish it with 3 liter of
liquid nitrogen. Liquid nitrogen should be procured by the user.
2.1.9 Adjusting the positions of cover closing-part's inclination sensors
The cover closing-part's inclination sensors are secured at displaced positions
before shipment to prevent damage due to vibration during transportation.
Fig. 1.5
Detach the right and left covers. After that, align the cover closing-part's
inclination sensors of the right and left lifts with the dog of the shaft and then
secure them.
After setting, check that the LED 11 (left) and LED 5 (right) of the CTRL
board turn ONIOFF simultaneously with inclination of the cover.
2.1.10 Installing the evacuation system
(Regarding other options, refer to the corresponding Instruction Manual.)
@
Fit a brass coupling into the air outlet port on the system rear panel. Mount a
vacuum hose to it and secure it with a hose band.
@
Change the RP set voltage from 200 to 110 V. (Refer to the setting change
procedures below.)
Attach a centering unit to the RP air inlet port. Place the valve ASSY on it
and then secure it with a clamp.
@
Connect a hose coming from the main unit to the opening of the upper part
of the valve ASSY. Then, secure it with a hose band.
@
Detach the KF flange at the RP air outlet port and secure the mist trap with
insulating tape. (Be sure to check the mist trap for mounting orientation.)
@
Connect the cable to the EDX main unit, RP and valve ASSY.
@l
Detach the right and left covers. Then, connect the Pirani gauge cable to the
CTRL Board J2 and the hermetic H3 under the casting of the sample chamber.
I
Centering unit + clamp
Fig. 1.6
Remove the oil filling plug and put RP oil into the RP.
Put the oil until it reaches just the MAX level indicated on the upper edge of
the sight glass frame.
If the oil level exceeds the MAX, detach the drain plug to discharge excessive oil.
In about a few minutes, check oil level again. If you find it is below the
MAX by checking, add oil again.
@
Through the "Extras" of the EDX software, set conditions for evacuation.
(Regarding the setting method, refer to the "2.5 Setting and checking
instrument environment".
<Changing set voltage>
a Find four screws which secure the cover plate (1) and remove them. Now,
you can detach the cover plate. Remove the cover plate and take out the
voltage display panel (4).
@
Press the voltage select switch (3) to change the set voltage.
@
Face the panel reversibly so that you can see the changed voltage on the
voltage display panel and place it back in the pump.
@
Mount back the cover plate and secure it with the four screws.
A Upper side of the motor
B Motor interior viewed from the top
1. Cover plate
2. Power connector
3. Voltage select switch
4. Voltage display panel
5. Power switch
6. "0" position (OFF)
7. " I " position (ON)
Fig. 1.7
<Names of RV pump components>
The names of the RV pump components are shown in the left-sided figure.
<Setting the mode selector>
Set the High Vacuum Mode, the condition set before shipment.
<Setting the gas ballasp
Set 0, the condition set before shipment.
1. Power connector 5. Gas ballast controller 11. Mode selector
2. Voltage display panel 6. Oil filling plug 12. Power switch
3. Handle for carrying 7. NW25 outlet (Single acting pump only)
(Fixture for lifting for RV8 8. Oil level sight glass 1 3. Motor fan cover
and RV 1 2 pumps) 9. Oil drain plug 14. Correct adjusting direction
4. NW25 inlet 10. Rubber leg (4)
Fig. 1.8
2.2 Energizing (Starting the instrument)
2.2.1 EDX main unit
Turn ON the power switch on the right side of the EDX main unit.
2.2.2 Starting the workstation
Turn ON the computer. After a short time, the Windows XP starts, displaying a
screen to input a password. Type exactly as displayed on the Display.
<When a message "Unknown device detected" appears at the start-up of Windows>
@ Select the "Next". (Select it several times until you are brought to the screen
for selecting the2Complete".)
@
Finally, select the "Complete" to exit the Wizard window.
If you select it, a message "No driver for this device found" appears, but it is
no problem.
The driver is already incorporated and therefore, you do not have to install it
on this window.
If you run all the steps up till the selection of this "Complete", no message
will be displayed at the next and subsequent start-up.
2.3 Checking the EDX main unit operation (On the operation panel)
2.3.1 Checking the cover openlclose-part for operation
Check the cover openlclose part's operation by pressing the "OPEN" and
"CLOSE" buttons of the main unit operation panel.
2.4 Installing the System Sheet
2.4.1 Installing the Device Information sheet
@
Insert the Device Information sheet into the floppy drive.
@
Click the "3 112 Floppy", and then the contents of FD are displayed.
@
Double click the "flpy2sys.bat", and then some files for device information
are copied.
2.5 Setting the instrument environment
2.5.1 Change to EDX-900 environment (EDX-QOOHS only)
(A) Change to Monitor, Qual-Quantitative and Quantitative of system groups
for 900HS environment.
Change the EDX-900's environment by opening the Auto* window.
And then below settings are changed.
a) The Monitor is changed to 900 Monitor.
b) Activating Correcting Impurity Lie. (The "inpurity.inf' are changed.)
c) The default setting of system groups are changed for 900.
Integral time: Real Time 100s -+ Live Time 40s
DT%: 25 + 10
I
DT%
Qual-Quantitative
Integration
Using the "Explorer", double-click the "autofp.exe" in the "(C:)Xedx%in".
@
The "AutofjY' dialog box opens.
Quantitative
System Group
10%
Time
Live Time 40s
User Group
The same setting as
1 default
default
The same setting as
I default
System Group
10%
User Group
The same setting as
Live Time 40s
default
The same setting as
@l
In the "l.Prepare", click the "EDX-900" if EDX-900 has no Sample
Observation Unit or click "900-CCD if EDX-900 has a Sample
Observation Unit.
@
Don't execute the "2/3/4/5". Then close the Autofp dialog box.
2.5.2 Environment utility "eu3" setting
In environment utility "eu3" window, we set the X-ray output and filter.
< Setting procedure >
a Open the "Explorer", and run eu3 in the "c:XedxXbinW by double clicking the
@l And then the eu3 window is displayed.
Fixed Collimator
Select 10. If installed the fixed collimator of special specifications, select
the diameter.
Xrav Max. Power
Select "50"
Filter
Click the "new" button. And then the Polymer filter is changed to the MO
filter and the Ni filter's thickness is changed from 20.0 to 100.0. Set the
thickness of Ni filter to 20.
2.5.3 Setting and checking instrument environment
(All instruments Including EDX-9OOHS)
Set instrument environment according to the optional configuration specified
by the user. Even if no option is attached, you must check it.
Model Name
EDX-700HS/800HS/900HS
<Steps>
a
To open the "Extras" of the "EDX-Main Menu", exit the EDX software
screen other than the "EDX-Main Menu" window.
@ Click on the "Extras" to display the "Environment Utility".
@
On the "Environment" panel, click on the "Instrument" to display the
The thickness of Ni filter
p
20
"Instrument Environment" window.
@
On this window, set a condition for optional configuration specified by the
user.
@
After setting, click the "Save" button to send the Instrument Environment.
<When a vaccum unit is attached as an optional feature>
Setting meth
Left click on
If you see a
the setting is
od:
the 0.
check mark
completed.
there,
Fig. 1.11
As options, the following features are available.
Option Configuration
OAtmosphere Control 1 0 Vacuum Unit OHe Redacement
0 Turret
OCollimator
CCD Camera Unit
U Indicator 1,amn
0 8-Sample 0 16-Sample(for liquid samples)
0 8-Sample with Spinner .U r- f3 Stage
0 16-Sample (for solid samples)
Auto selection unit of 4 type
0 l , 3, 5, lOmm 0 00. 3, 1,3, lOmm 0
Sample Observation Unit
X-rav Pilot 1 ,amn
2.6 Checking the EDX main unit for operation
(by the EDX software)
2.6.1 Starting the EDX software
Double click on the "EDX software" icon to start the EDX software. On an
initial screen, the "Main Menu" and "Analysis" window appear.
2.6.2 Initializing the instrument
a Click on the "Maintenance" of the "EDX-Main Menu" window to display
the "Maintenance" window.
@l
Click on the "Initialization" of the "Control" panel on the "Maintenance"
~ ~ ~ p ~ p ~ p - p-p p p- - pp p-p p-
window.
2.6.3 Checking each drive unit for operation
Check for operation of each of cover, cover opedclose-part's tilting sensors
and shutterlfilter. Also, check options for operation (collimator, turret, others) if
attached.
<Cover operation>
Check cover operation with the right and left cover removed.
a
Click on the "Maintenance" of the "EDX-Main Menu" window to display
@
On the "Control" panel of the "Maintenance" window, click on the "Manual
Control" to display the "Manual Control" window appears.
Click on the Cover: "OPEN" or "CLOSE" of the "Sample Chamber" panel
to operate the cover. Check that no noise is heard and no excessive load is
given to the wiring during the operation.
<Operation of the cover openlclose tilting sensors>
Click on the "OPEN button of the operation panel to open the cover to the
maximum. Place an object (book or box) at the cover-closing path, and then, click
the "CLOSE" button. The alarm should be given when the cover touches the
object and the cover closing operation should stop. Check that it correctly
functions.
<Shutterhilter operation>
Check for shutterlfilter operation without sample plate.
a
Click on the Shutter: "OPEN" or "CLOSE" of the "Sample Chamber" panel
to operate the shutter. Check that no noise is heard and no unit touches the
wiring and the sensors during the operation.
@
Click on each position given for the "Filter:" of the "Sample Chamber"
panel to move it. Check that no noise is heard and no unit touches the wiring
and the sensors during the operation.
2.6.4 Checking the position of the detector cap
Check that the detector cap is correctly touching the stopper without clearance.
a
Click on the Filter: "MO" of the "Sample Chamber" panel to move the filter
to the MO position.
If a collimator is attached as an option, click on the Collimator: "10 mm" to
move it to a - 10 mm position.
Detector cap
Fig. 1.12
@
Check that the detector cap is placed at the stopper. If not, manually push it
in until it touches the stopper.
CAUTION : Since the detector window is inside the detector cap, special care must be
taken to handling the cap. (Never touch the detector window. Even if it is
contaminated, never wipe it with chemical or the like.)
2.6.5 Checking functions of the standard accessory
(Liquid sample adapter)
Check that the "LIQUID MODE of the operation panel lights when the liquid
sample adapter is set.
Afier checking it, give a check to the "Check mark" (17) of the Installation Report.
2.7 Adjustment
2.7.1 Starting the instrument (Turning ON the X-ray and detector high voltage.)
a
the "Maintenance" window appears.
@
Through the "State of Instrument" panel of the "Maintenance" window,
check that all units functions normally.
@
After checking, click on the "Manual Control" of the "Control" panel to
display the "Manual Control" window appears.
@
Carry out aging through the "X-ray Power Supply" panel to boot the X-ray
to the level of 50 kV-500 pA.
- P P P P P P - - - -
<Tube aging>
If this is the first time to use the tube or the tube has not been used for a long
time, boot the tube carrying out aging in conformance with the tube aging
conditions.
a TurnONthetubeat 10kV-1OpA.
@
Increase current up to 15 kV-1000pA for three minutes and wait 10 minutes.
Then, decrease the current once.
@
Increase voltage up to 50 kV-100pA for five minutes.
@
Increase current up to 50 kV-500pA and wait 10 minutes.
<Tube aging conditions>
Step Tube voltage [ k y Tube current [p41 Waiting time [min.]
1 10 10 1.0
2.7.2 Changing to the adjustmentlinspection directory
Since the adjustrnent/inspection groups is in the (C:) BedxXusrXtest directory,
change the directory.
@ Click on the "Extras" of the "EDX-Main Menu" window to display the
"Extras" window.
@ Click on the "Data Process" of the "Environment" panel to open the "Data
Process Environment" window.
On the "Directory" panel, set the directory of Qual-Quantitative and
Quantitative conditions and data to (C:) BedxBusrXtest.
@
After setting, click on the "Save".
P P - P P P P P P P - P
The list for group name Ad measurement conditions used for EDX
adjustment/inspection are shown below.
EDX Series Adjustment and Inspection Group's Table
Qual-Quantitative
Confirmation of Energy Poin
FP Qual-Qnantitative
Quantitative
I
I
Item I GroupName
I I Simple-Repeatability
Repeatability
9-Simple-Repeat
Long-Time-Rept
Long time Repeatability
9-Long-Time-Rept
Registration of Turret Turret Pos Correct
standard intensity 9 Tnrret Pos Corn
Repeatability of option's He
replacement (m the case of
9-He-Replacement
Repeatability of option's He
replacement (in the case of
vac) 9-He-Replacement_Vac
Registration of Collimator
standard intensity
Auto Integration time
c mn 4 Real T i e
Intensity Analysis
controd Live T i e
F calculation range
60 25 0.99-1.99
Analysis
0-40
2.7.3 Checking the energy position (Carry out the calibration and data
check at least one hour after energization.)
Before the Energy Calibration, measure a standard sample A750 to get
reference data.
<Steps>
-Setting an analytical group-
a
Click on the "Analysis" of the "EDX-Main Menu". (Usually, the "Analysis"
window is booted.)
a
Click on the "Analytical Group" of the "Next sample" panel in the
"Analysis" window. Then, the "Select-Analytical Gi6ip"windowappears.
@
Click on the "Qual-Quantitative" of the "Select-Analytical Group" window.
Also, set the "User Group" for the "Owner of Analytical Group".
@ After checking the group name, in the case of EDX-700HS/800HS7 click on
the "Energy - Position", and in the case of EDX-900HS, click on the
"9 - Energy - Position". (If you click on it, the group name is highlighted in
blue.) After selecting it, click on the "OK".
@ You do not have to set a sample name. As a result, a measurement date is
automatically input as a sample name.
-Setting a sample and starting an analysis-
@ Place a standard sample A750 at the measurement position.
@l
Click on the "START" of the "Analysis" window.
-Printing data-
@
Click on the "View Data" of the "Current Sample" in the "Analysis"
window. Then, the "Profile [Qual-Quant.1 [Datel)' windows open.
Click on the Printer icon, or left click on the "File (F)" and left click on the
"Print a". Then, the "Print: [Qual-Quant.] [Multiple Profile]" appears.
@
On the "Print Items" panel, set four items: Meas. Cond., Profile, Qual.
Result and Peak List.
After completing setting, click on the "Print".
2.7.4 Carrying out the Energy Calibration
Using a standard sample A750, carry out the EnergyIFWHM Calibration.
<Steps>
a
Place a standard sample A750 at the measurement position.
Click on the "Maintenance" of the "EDX-Main Menu". Then, the
"Maintenance" window appears.
Click on the "Instrument Calibration" of the "Control" panel in the
"Maintenance" window. Then, the "Instrument Calibration" window appears.
@ On the "EnergyIFWHM Calibration" panel of the ''Instrument Calibration"
window, select the "Yes". On the "Intensity Calibratign" panel, select the "No".
Now, click on the "Start".
2.8 Inspection (Standard units)
2.8.1 Checking the position after the Energy Calibration
Following the Steps a to @ given in the section "Checking the energy
position", collect data of a standard sample A750 and check the following items.
<Standard and ResulB
Check the following items against the Peak List.
Check that the energy position of 40: , "z to the specification,
$. OY 2 0.0 eC 4S%++M@(keV). Enter the value on the Inspection Sheet.
@
Check that the spectra of SnKa (L line included), AlKa, CuKa and NiKa are
identified.
Identification Spectra List
I Channel name I Line I Channel name 1 Line
of the Inspection
Ti-U
Sheet. Also, attach data to the Inspection Sheet.
After checking, give a check at "Check mark" in (U)
SnKa
SnLa
-Fdch
CuKa
NiKa
Na-Sc SnLa
-FdCs
CuKa
NiKa
AlKa
2.8.2 Repeatability
Check for repeatability by repeating analyses of A1 and Sn 10 times using a
standard sample A750.
<Steps>
a Click on the "Analysis" of the "EDX-Main Menu". (Usually, the "Analysis"
window is booted.)
@ Click on the "Sample Schedule" of the "Next sample" panel in the
"Analysis" window to dispIay the "Sample Schedule" window.
@
CTick on thT"SfipleRegis5ation"~of~EpESchedule" window to
display the "Sample Registration" window.
@
Click on the "Analytical Group" of the "Sample Registration" window to
display the "Analytical Group" window.
@ Click on the "Quantitative" of the "Select Analytical Group" window. Set
the "User Group" for the "Owner of Analytical Group".
After checking the group name, click on the "Simple Repeatability". (If you
click on it, the group name is highlighted in blue.) After selecting it, click on
the "OK.
a
Click on the "Option" of the "Option" panel to display the "Sample
Registration Option" window.
On the "Repeat Measurement" of the "Sample Registration Option" window,
set as follows.
Repeat measurements. (Left click on the white box on the left.)
Times: 10
Print statistic data. (Left click on the white box on the left.)
After setting, click on the "OK".
@
On the "Sample Name" panel, input "A750" as a sample name.
@ After inputting it, click on the "Apply", and then, click on the "Close".
@ Place a standard sample A750 at the measurement position.
-Printing data-
@
Click on the "Report" of the "EDX-Main Menu" window to display the
"Report" window.
Click on the "Select Group" of the "Searching Condition" panel to display
the "Select Analytical Group" window.
@
In the case of EDX-700HS/800HS, left click on the "Simple-Rept" in the
"Group Name List", and in the case of EDX-900HS, left click on the
"9-Simple-Rept". (If you click on it, the group name is highlighted in blue.)
After selecting it, click on the "OK".
Q
Click on the "Search" of the "Report" window to display the data obtained
by the "Inspection: Simple Repeat".
@
Select A750 (1) to (10).
Click on the "Print".
- P P P - P P Pp-P P
<Standard and Result>
Check the following items against the Report data.
Check that the measured CV (coefficient of variation) is equal to three times
the theoretical CV or less.
After checking, give a check to the "Check mark" (0) of the Inspection
Sheet. Enter values of the theoretical CV, measured CV and ratio, (Measured
CVITheoretical CV) on the Inspection Sheet. Attach all data to the Inspection
Sheet.
<Reference>
Measured CV: Coefficient of variation (%) of the Report data.
Theoretical CV: Calculation formula,
1/@x 100 = (11~vera~e X Current X Integration Time) X 100
Ex.: Sn (In case of Average 117.588cps/pA, Current 15pA, Integration Time 90
sec.)
17.588 X 15 X 90) X 100
= 0.24899 = 0.25 (The third decimal place rounded)
2.8.3 FP Qual-Quantitative
Measure a standard sample SUS by the FP Qual-Quantitative method and
check the quantitative value.
<Steps>
a
Click on the "Analysis" of the "EDX-Main Menu" window. (Usually, the
"Analysis" window is booted.)
@
"Analysis" window to display the "Select Analytical Group" window.
Click on thFQual-Q=titative" of thPSeTEi tAnalyticalri%upTwindow.
@ After checking the group name in the case of EDX-700HS/800HS, click on
the "FP-Qual-Quant", and in the case of EDX-900HS, click on the
"9 - FP - Qual-Quant". (If you click on it, the group name is highlighted in blue.)
After selecting it, click on the "OK.
@ You do not have to set a sample name. As a result, a measurement date is
@
Place a standard sample SUS at the measurement position.
a
-Printing data - (After the analysis)
8 Click on the "View Data" of the "Current Sample" panel in the
"Analysis" window to display the "Profile [Qual-Quant.] [Datel)' window.
Click on the Printer icon, or left click on the "File (F)" and left click on
the "Print (P)" to display the "Print: [Qual-Quant.] [Multiple Profile]"
window.
On the "Print Item" panel, set five items: Meas. Cond., Profile, Qual.
Result, Peak List and Qual. Result.
@ After completing setting, click on the "Print". On completion of the Print
processing, click on the "Close" to end the "Print": [Qual-Quant.] [Single
Profile] window.
Check that the resulted quantitative values of Fe, Cr, Ni and Mn are within the
allowable range.
After checking it, give a check to the "Check mark" (0) of the Inspection
Sheet. Enter the values on the Inspection Sheet. Attach all data to the Inspection
Sheet.
Allowable Range of Quantitative Value of Standard Sample SUS
2.8.4 Resolution Confirmation
Confirm the energy resolution of "FeKa", using FP Qual-Quantitative data.
Quantitative element
- re---
-Reading SUS data-
@
Click the "Data" in the "EDX-Main Menu" window.
@ Double-click the name of which sample already has been measured. And
then the profile is displayed.
@ Change the "Multiple Profile" to the "Single Profile" pressing
button.
@
Click the "Intensity Calculation" in the "Process" menu. And then the
"Intensity Calculation- Qual-Quant" is displayed.
@ Move the frame of display items to the right. And then the "FWHM(eV)"
hiding in right hand is displayed.
@
Click the "Calculate", and the real FWHM is calculated.(The displayed
value at first is theoretical value.
Allowable range
- m - m m -
Quantitative element
- - m - --
Allowable range
--6m?&-m%
< Standard & Result >
Confirm that the calculated FeKa FWHM(eV) in @ is 170eV or less.
2.8.5 Carbon Analysis (EDX-800HS only)
Analyze C using 6p Mylar of a standard accessory and check that peak is
detectable.
-Setting conditions-
a
Click on the "Analysis" of the "EDX-Main Menu" window. (Usually, the
"Analysis" window is booted.)
@
"Analysis" window to display the "Select Analytical Group" window.
@l
Click on the "Qual-Quantitative" of the "Select Analytical Group" window.
@
After checking the group name, click on the "Carbon Measurement". (If you
the "OK".
@
You do not have to set a sample name. As a result, a measurement date is
@ Using a standard accessory (sample cell (3571 for general use, open), 6y
Mylar), set a piece of Mylar in the sample cell. Then, place the cell at the
measurement position.
-Printing data- (After the analysis)
@ Click on the "View Data" of the "Current Sample" of the "Analysis"
window to open the "Profile [Qual-Quant.] [Dater window.
pp -p-p p p p-p -P P
On this window, left click on the "View" and leftclick on the ''channel
Single (S)".
@ Left click on the "View" and then, left click on the "Display Region
Setting". On the "Display Region Setting" window, change setting for the
Horizontal from 0.0-1 .O. After that, click on the "OK". By this operation, The
value for the Width is changed.
Left click on the "View" and left click on the "Vertical Axis Unit" to set a
value for the "Counts".
@
Adjust the display scale by clicking icons and m until the peak of C
(0.277 keV) appears approximately at the half the full scale of the Vertical-axis.
Click on the Printer icon, or left click on the "File" and left click on the
"Print". Then, the "Print: [Qual-Quant.] [Single Profile]" window appears.
@ On the "Print Items" panel, set four items: Meas. Cond., Profile, Qual.
Result and Peak List.
@ After completing setting, click on the "Print". On completion of the Print,
click on the "Close". Exit the "Print: [Qual-Quant] [Single Profile]" window by
this operation.
Check that the peak of C is detected based on the obtained data.
After checking it, give a check to the "Check mark" (0) of the Inspection
Sheet. Attach all data to the Inspection Sheet.
2.9 Inspection (Option units)
2.9.1 Atmosphere Control: Vaccum Unit
Checking the voltage setting of the vacuum pump
The voltage display panel is provided on the motor cover. Check that it reads
l00 v.
Checking an evacuation time until the degree of vacuum reaches 30 Pa.
<Steps>
@ Cfick on the "ManualContrd" on the "Control" panel, Then, the "Manual
control" window appears.
@ Check that no sample is placed in the sample chamber.
@ Click on the "Cover: CLOSE on the "Sample Chamber" panel to close it.
@ To check the degree of vacuum in the analysis chamber, click on the
"Monitor" of the "EDX-Main Menu" window to display the "Instrument
Monitor" window.
In the "Instrument Monitor" window, you see the item "Pressure: D Pa".
See the value to check the degree of vacuum.
Select the "Vac." of the "Atmosphere" panel and click on the "Execute".
Note the time when you clicked on the "Execute".
Check that the time between when the "Pressure" of the "Monitor" window
reads 30 Pa and when you clicked on the "Execute2 is 2.5 minutes or less. After
checking it, give a check to the "Check mark" (U) of the Inspection Sheet. Enter
the values on the Inspection Sheet.
2. 5 mi n r l n 1 1 cwr @l CO //c
3,s l ( 11 l , 1, s o *
2.9.2 Atmosphere Control: He Purge Unit
Check for repeatability by repeating analyses of A1 10 times using a standard
sample A750.
<Steps>
a
Click on the "Analysis" of the "EDX-Main Menu". (Usually, the "Analysis"
window is booted.)
a
Click on the "Sample Schedule" of the "Next sample" panel in the
"Analysis" window to display the "Sample Schedule" window.
@l
Click on the "Sample Registration" of the "Sample Schedule" window to
display the "Sample Registration" window.
@
Click on the "Analytical Group" of the "Sample Registration" window to
display the "Select Analytical Group" window.
@
Click on the "Quantitative" of the "Select Analytical Group" window. Set
"User Group" for the "Owner of Analytical Group".
After checking the group name, click on the "He Replacement". (If you
- - - - - -
the "OK".
a
Click on the "Option" of the "Option" panel to display the "Sample
Registration Option" window.
On the "Repeat Measurement" of the "Sample Registration Option" window,
set as follows.
Repeat measurements. (Left click on the white box on the left.)
Times: 10
Print statistic data. (Left click on the white box on the left.)
@
After setting, click on the "OK.
@
On the "Sample Name" panel, input "A750" as a sample name.
After inputting it, click on the "Apply", and then, click on the "Close".
@
Place a standard sample A750 at the measurement position.
-Printing data-
@
Click on the "Report" of the "EDX-Main Menu" window to display the
"Report" window appears.
@
Click on the "Select Group" of the "Searching Condition" panel to display
the "Select Group" window.
@
Left click on the "He Replacement" in the "Group Name List
7
'. (If you click
on it, the group name is highlighted in blue.) After selecting it, click on the
"Load".
@l
Click on the "Search" of the "Report" window to display the data obtained
by the "He Replacement".
Select A750 (1) to (10).
@ Click on the "Print".
Check the following items against the Report data.
Check that the measured CV (coefficient of variation) is equal to three times
the theoretical CV or less.
After checking, give a check to the "Check mark" (0) of the Report. Enter
values of the theoretical CV, measured CV and ratio, (Measured CVITheoretical
CV) and average on the Inspection Sheet.
2.9.3 Turret
Check the turret for operation through the "Maintenance".
<Steps>
@ Click on the "Manual Control" of the "Control" panel to display the
"Manual control" window.
Click on the "Cover: OPEN" on the "Sample Chamber" panel to open the
cover of the Sample Chamber.
@ Detach the sample chamber stand. (The X-ray must be OFF.)
@ Move each turret to the corresponding position by specifying it for the
"Turret:" of the "Sample Chamber" panel.
Check the initialize position and also check that they stops at correct analysis
positions. Furthermore, check that no noise is heard during the operation and they
do not touch the wiring and sensors. After checking them, give a check to the
"Check mark" (0) of the Inspection sheet.
2.9.4 Collimator
Check the collimator for operation.
<Steps>
- Same as the Steps for Turret a to @.
@ Click on each position at the "Collimator:" of the "Sample Chamber" panel.
By this operation, the collimator moves. Check the operation.
Check that no noise is heard during the operation and they do not touch the
wiring and sensors. After checking them, give a check to the "Check mark" (0) of
the Inspection Sheet.
2.9.5 CCD Camera Unit
Check images and registration values using EyeXRF-E software.
<Steps>
a
Double click the icon of "EyeXRF" on the desktop and display the image.
@
Seta &h& name em! a & ~ p ~ a s ~ - ~ ~ e & h e
Shimadzu logo.
After click Display Settings in the View(V) menu, Display settings screen is
displayed. Then confirm that the X and Y values of this screen are same as the
X and Y values of X-ray irradiation position sheet.
@ Check that the quality of the displayed image is almost same as the quality
of the image file ( c:Xpcx&temp).
After checking, give a check to the "check mark" (0) of the Inspection Sheet.
2.9.6 Pilot Lamp
Check that the X-ray rotation beacon lights with the X-ray ON.
<Steps>
@ Click on the "Manual Control" on the "Control" panel to display the
"Manual control" windows.
@ On the "X-ray Power Supply" panel, set X-ray: ON, X-ray voltage: 50 kV
and X-ray current: 100 pA, and then, click on the "Execute".
After clicking the "Execute", check that the X-ray lamp lights. Then, give a
check to the "check mark" (0) of the Inspection Sheet.
2.10 Checking option configuration
The following shows option configuration. The option configuration includes
features below.
Option Configuration Table
Option Configuration 1
OAtmos~here Control
0 Collimator
0 CCD Camera Unit
Vacuum Unit He Redacement I
0 8-Sample 0 16-Sample(for liquid samples)
8-Sample with Spinner 0 r-Wage
0 16-Sample (for solid samples)
Auto selection unit of 4 type
01, 3, 5, lOmm4 00.3,-1, 3, 1Omm-c@ -
Sam~l e Observation Unit
X-rav Pilot lam^ I
If an option is provided, give a check to the corresponding 0.
If not, enter nothing.
2.11 Checking traceability
Traceable units includes the following.
Traceability Unit Table
I Unit I Model
Traceability Unit I
1 vacuum P U ~ D I RV3
I Data Processim Unit I
I Printer I
Ver Re1
Ver Re1
Regarding a vacuum pump (if provided as an option), data processing unit,
Display and printer, enter their models and S/N. Regarding software, enter its
version.
To check software version, click on the "Version Information" through the "Help"
of the "EDX-Main Menu
7
' window.
<Untraceable units>
Units not from our factory, for example, ones procured by users are not
guaranteed. Therefore, give a check to for them.
2.12 Checking instrument information
Enter a value for each of the following instrument information items and attach data.
Instrument Information Table
Detector
Offset
Collimator Standard
Intensitv
X-ray Irradiation
Center Position
Sensitivity coefficient Print out the Sensitivity Coefficient List through the Quantitative System Group,
Instrument Information
Sysmetal and attach the data to Inspection Sheet.
0-40 KeV Gain :
0-40 KeV Offset :
a
To open the "Extras" of the "EDX-Main Menu" window, exit all EDX
software windows other than the "EDX-Main Menu" window.
@
Click on the "Extras" to display the "Extras".
@
Click on the "Instrument" of the "Environment" panel to display the
"Instrument Environment" window.
@
Note the value given on the "Detector" panel of this "Instrument
Environment" window.
0-20 KeV Gain :
0-20 KeV Offset :
<Offset>
0-0
Same as the Steps a to @ for the Detector described above.
@
Click on the "Options" of the "Instrument Environment" window to display
the "Instrument Environment: More Options" window.
@
Note the value given on the "Offset" panel of this window.
Temperature "C
ShutterJFilter
Collimator
. - pp
Irnm
5mm
X
r-0 : r :
0 :
p - - P P p-- p
3mm
l Ornm
Y
<Collimator Standard Intensity>
a Run c:Yedx!&bin$eu-smz.bat using the explorer. Double-click on the file,
"en-smz.batn in the "c:Xedx%in" .
@
Click on the "Options" of the "Instrument Environment" of the "Extras"
window to display the "Instrument Environment : More Options" window.
@l
Click the "Intensity Calibration" button on the lower right of this window to
display the "Intensity Calibration Information" window.
@ Note the values given on the "Standard Intensity" column of each collimator.
(Values to be input for the Standard Intensity column are the same.)
- p -- - - - p- -p - p
<CCD Camera Unit>
Note registration values using EyeXRF-E software.
<Steps>
a Double click the icon of "EyeXRF" on the desktop and display the image.
@
After click Display Settings in the View(V) menu, Display settings screen is
displayed.
@l Note the X and Y values given on the "Adjustment of Center Position".
<Sensitivity coefficient>
<Steps>
@ Click on the "Condition" of the "EDX-Main Menu" window to display the
"Select Analytical Group" window.
@ Click on the "Quantitative" of the "Select Analytical Group" window. Set
"System Group" for the "Owner of Analytical Group".
@l Select the "sysmetal" for the "Group Name" and left click on it. Then, the
group name, sysmetal, is highlighted in blue.
@ Click on the "Edit" to display the "Group Condition:
[Quantitative] [sysmetal]" window.
@
On this window, click on the "Analysis Information" to display the
"Analysis Information [Quantitative] [sysmetal]" window.
@
On this window, click on the "Sensitivity Coefficient List" to display the
"Sensitivity Coefficient List" window.
a
On the appeared window, set the "Sensitivity Coefficient List".
Click on the "Print" to print out the "Sensitivity Coefficient List".
<Result>
Attach the printed-out sensitivity coefficient list to the Report.
2.1 3 Operational explanation
Based on the following operational explanation list, give an explanation of basic
operation and maintenance to users.
If you finish it, give a check to the "Check mark" (0) of the Inspection Sheet.
Basic operational explanation
kern
1. Startinglstopping the instrument
2. Simple Analysis
3. QualitativeIQuantitative Date
Processing
4. Setting a
QualitativeIQuantitative group
(Measurement of bulk and
dioxide)
5. Setting a quantitative group (FP
method with a standard sample)
Shut Down
p-pppp
Setting based on the Sample schedule
-
Details
From Power-ON to X-ray-ON
Maintenance-Manual Control-
Remarks
Starting (Reserve included)
Stopping
Gr ou~ measurement condition I Atmos~here. Vacuum
Explanation of the SystemGroup and User
Group
Displaying Multiple Profile
Displaying Single Profile
Displaying Result of Quantitative Analysis
Changing over Channels to display
Expanding and shrinking data
Adding, deleting, changing peaks
Page layout of display of Multiple Profile
Sam~l e form I Bulk. Film
Disposable, with collar, open, for small
amount samples
Comoound form I Metal. Oxide
Measurement channel I
Elements Included I
I Data collection ranee (0-20 keVlO-40 keW
Setting measurement conditions Selecting voltage level, 50, 15 or 5 kV
Current: Auto. Fixed
Saving groups
Group measurement condition
Sample form
Measurement channel
Setting element information
Setting a standard sample
Setting an analysis range
Setting a measurement time
About Real Time, Live Time and Dead Time
Atmosphere, Vacuum
Bulk, Film
Selecting elements included in a sample
Quantitative, Fixed, Balance
Calibration method, FP method
Registering standard sample names
Setting a standard value
Calculating theoretical intensity
ltem
6. Processing of quantitative data
P
7. Report
-
8. Environment setting
Details
Measuring a standard sample
Starting an analysis
Calculating sensitivity coefficient
Saving a group
Analyzing an unknown sample
Reprocessing based on the Single Profile
p - --
Disdavine KLM marker
Remarks
Setting by the Analysis Schedule
Selecting Standard Sample Measurement
- P -
Checking measurement intensity
Calculating sensitivity coefficient
Smoothing
Peak Catch
Identification
Intensity Calculation
Quantitative Calculation
p - P - P
Manual input of Display Region
Details of setting for print
Editing quantitative condition I Deleting an element from the calculation
1 Changing a comoound form
Explanation of Maintenance
Selecting a group
Displaying result of the Report
Printing result of the Report
Making Report in the CSV format
Changing directories
Saving data onto a floppy By the Extras and Explorer
Instrument Calibration
Item
General maintenance
Analysis Chamber
I the state of instrument is all normal.
Adding liquid nitrogen 1 Check the date of oil replenishment.
Details
Instrument configuration
Startinglstopping the instrument
Maintenance window
Monitor window
Initializing the instrument
Energy Calibration
Remarks
On the Maintenance window, check that
Check after calibration
Once a month (At least one hour after
instrument power-ON)
Carry out the simple analysis using
standard sample A750 to check that
energy positions of FeKa (should be
6.336-6.446), SnKa (La line included),
Cleaning of the sample stage
AlKa, CuKa and Nika are identified.
Anytime if contaminated
Cover operation unit
Shutterlfilter
Grease up of 0 rings
Grease up of the drive unit of the sample
Option (Evacuation system)
Option (4-type collimator unit)
Twice a year
chamber cover
Grease up of the drive unit of the
shutterlfilter
Twice a year
Oil level of the vacuum pump
Grease up of the drive unit of the collimator
For detail information, refer to the
Instruction Manual.
Twice a year
2.14 Reporting completion of installation
Submit the Installation Completion Report, Installation Report and Data (original) to
the user. Together with the user, confirm that all inspection items conform to the
specifications. After the confirmation, get the person's signature in presence for the
items, Name: , Unit/Dept.: and User: on the Reports.
Produce one copy of Installation Completion Report and Installation Report and send
it to the Technical Service.
Inspection Item Table
Item
3. Standard accessories and their functions
4. Energy Calibration
5. Repeatability
6. FP QualitativeIQuantitative
7. Confirmation of Resolution
8. Operational Explanation
Standard and Result
Installition conditions fokfi e m~n u n i t Tk u l d be conformed
to.
No defects which may imvair the functions should be found.
No missing units and no damage should be found.
The energy position of FeKa should be 6.336 to 6.464 (KeV).
The svecified svectra should be identified.
Should be three times the theoretical C.V or less.
Measurement values of the following elements should be
within the allowable range.
F3: 68.50 to 73.00%
Cr: 16.00 to 20.50%
Ni: 6.00% to 10.50%
Mn: 0.50 to 3.50%
Confirm the Energy Resolution is less than 170eV using the FP
Qual-Quantative data.
Give a basic operational explanation.
Judgement
1. Atmosphere Control
(Evacuation system)
Voltage setting
Evacuation speed
EDX-800LHS only
Accuracy at the time of He replacement
2. Turret operation
3. Collimator operation
4. CCD Camera Unit
9. Carbon Measurement
5. Indicator lamp operation
The peak of C should be detected.
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Within 3 minutes (60 Hz)
Should be three times the theoretical C.V or less. I
Should normally function.
Confirm that the X and Y of adjustment of center position in
EyeXRF software are same as those of the X-ray irradiation
I
position sheet.
,.,.,.,.,......-, ",.,~*.,.....,.,.,.,.....,.....,.,..~.~~....-~.,-~~~...~...,.,..~.,.,...........,.,.,.....,..-....,.,-,.,..-,-.-,..-,....-.,-,-.-.-.-
l
Confirm that the quality of the displayed image is almost same
as the aualitv of the image file (c:~ocxrf%temu). I
Chapter 2 Maintenance Adjustment
Maintenance Adjustmant Procedure of Unit Replacement
............................... 1 . 1 Adjustment Item and Check Item according to the unit replacement 2 . 3
1-2 r, .................................. ........-.... ...S...<......... i.i.i...<r<~...r.-.i..i . . . . . C. . ..+...... 2 . 5
.................................................... 1.2.1 Replacing the detector of EDX-700HS / 800HS 2 . 5
.................................................................. . 1.2.2 Replacing the detector of EDX-900HS 2 9
........................................................................................................... Replacing the tube 2 . 13
Replacing the belts (Shutterlfilter. collimator) ................................................................ 2 . 14
Replacing the belt for operating the cover ...................................................................... 2 . 15
....................................................................................................... X-ray indicator lamp 2 . 16
..................................................... Adjusting the cover closing-part's inclination sensor 2 - 17
Adjusting the cover operation sensor .............................................................................. 2 - 17
Adjusting the liquid mode proximity sensor ................................................................... 2 - 18
Adjusting the liquid mode fiber sensor (for a turret) ...................................................... 2 - 19
........................................................... Offset adjustment of shutterlfilter and collimator 2 - 20
Adjusting the turret stop position ................................................................................... 2 - 24
. .
Adjusting the turret orlgm ............................................................................................. 2 - 25
Checking the degree of vacuum ...................................................................................... 2 - 26
MCA PCB ....................................................................................................................... 2 . 27
3.1.1 Checking input voltage ......................................................................................... 2 . 27
3.1.2 Adjusting the LLD level controller R2 (Only the PCB possible) ......................... 2 . 27
3.1.3 Checking adjustment of the offset level controller R1 (Only the PCB possible) . 2 . 29
3.1.4 MCA PCB Check TerminaVLED Display Function Table ................................... 2 . 30
3.1.5 Replacing the ROM .............................................................................................. 2 . 31
3.2 CTRL PCB ...................................................................................................................... 2 . 33
3.2.1 Checking input and output voltage ....................................................................... 2 . 33
3.2.2 Adjusting the M5 offset controller VR1 ............................................................... 2 . 34
3.2.3 CTRL PCB Display LED Function Table ............................................................. 2 . 34
3.2.4 CTRL PCB Check Terminal Function Table ........................................................ 2 . 36
3.3 AMP PCB (only EDX-700HS/800HS) ........................................................................... 2 . 37
3.3.1 Adjusting the gain of the amplifier ....................................................................... 2 . 37
3.3.2 AMP PCB Display LED Function Table .............................................................. 2 . 39
3.3.3 AMP PCB Check Terminal Function Table .......................................................... 2 . 40
. . . . . . ....... . . . . . -ppp---pp-pp-p-- ..........
3.4 PS PCB ......................................................................................................................... 2 - 41
3.4.1 Adjusting the detector bias ................................................................................... 2 . 41
3 A.2 PS PCB Check Terminal Function Table .............................................................. 2 . 41
3.5 Stepping drive motor ....................................................................................................... 2 . 42
Mounting the turret drive unit ......................................................................................... 2 . 43
Installation orders of collimator ...................................................................................... 2 . 44
Mounting the X-ray indication lamp .............................................................................. 2 . 47
FP Sensitivity Coefficient Input Method ........................................................................ 2 . 48
Registering collimator standard intensity ..................................................................... 2 . 57
Checking the PV ratio ..................................................................................................... 2 . 59
Procedure of installing the EDX software ..................................................................... 2 . 61
Settings for Windows XP ................................................................................................ 2 . 64
Instruction for settings ..................................................................................................... 2 . 66 .
[Reference] Settings of Administrator (Normally you do not need to set.) ......................... 2 . 73
. [Reference21 Comparison Window style (English) ............................................................. 2 74
About the identification of the instrument ......................................................................... 2 . 77
1 .l Adjustment ltem and Check ltem according to the unit replacement
Adjustment item
OAdjusting the gain of the amplifier
(AMP PCB)
(For this procedure, refer to 3.3.1
Adjusting the gain of the amplifier of
Chapter 2 Maintenance and Adjustment
@Energy calibration (software)
~ L L D level setting (MCA PCB)
-7
volume of Chapter 2 Maintenance and
Adjustment.)
@Renewal of sensitivity coefficient
Check item
@Check the exhaust time until it reaches
30 Pa.
- - - - - - - - - - - m - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
@check the energy position
@Checking PV ratio
(For this procedure, refer to 5.3 Checking
nf PV
Maintenance and Adjustment.)
@C measurement
(For this procedure, refer to 2.8.4 Carbon
analysis of Chapter 1 Installation.)
---------..-------------.-------------------.
@Checking SUS quantitative
analisis ofA750
@Aging of tube
Starting the instrument of Chapter 1
Installation.)
.........................................
@Renewal of sensitivity coefficient
-
--
L! -
. - - - -
LP-
I
, m - - -
--
-
- - - - - - - - - - - - - - - - - - - - - - - - - m - - - - - - - - - - .
@Checking energy position
(For this procedure, refer to
Sensitivity Coefficient Input Method of
Chapter 2 Maintenance and Adjustment
(For this procedure, refer to 5.1 FP
@Check the evacuation time until it
reaches 30 Pa.
Atmosphere control : Vacuum unit of
Cha~ter 1 Installation.)
I
Atmosphere control : Vacuum unit of
Chapter 1 Installation.)
@Checking SUS determination
(For this procedure, refer to 2.8.3 FP
Qual-Quantitative of Chapter 1 Installation.)
@Checking repeat reproducibility accuracy
by A750
Repeatability of Chapter 1 Installation.)
Replacement
of MCA PCB
Replacement
of AMP PCB
l Replacement
of PS PCB
Replacement
of X-ray power
Adjustment item
OSetting offset level
@Setting LLD level
PCB
pp -p -
@Adjustment of detector bias
Adjusting the detector bias of Chapter
2 Maintenance and Adjustment.)
Check item
..*..*.....................-..-.......--.--.--.,
................................................
@Checking repeatability by repeating analisis
@checking energy position
procedure, refer to 2.6.3 Checking each drive
unit for operation of Chapter 1 Installation.)
-.- -.--.--.--..-.--.--.--.--..-..-...---.-----..
-..----.--------.--.--------.--.---.-.--.--.---.
-..-.--.--.....-.--.--.--.--.--..-..-.--.--.--..
@Checking repeat reproducibility accuracy
bv A750
ofA750 supply
................................................
-.--.--.--.-......-..-..-.-...-..-..-.--..-..-..
@Checking repeatability by repeating analisis
of A750 supply
l .2 Replacing the detector
1.2.1 Replacing the detector of EDX-700HS I 800HS
1. Open the cover of the analysis chamber and keep it open. The filter must be
a polymer filter.
2. Turn OFF the power, unplug the instrument and wait five minutes until the
detector high voltage is discharged.
3. Detach the right and left covers, rear panel, the cover of the upper part of the
Dewar.
Detach the detector connectors on the right face. (5 connectors)
Fig. 2.1
4. Detach a fixture of the Dewar receiver from the rear side.
5. Remove the PS Assy securing screws.
Fig. 2.2
6. Detach the PS Assy bracket (with a SW) and displace it together with the PS
Assy to the right. RA By doing this, the detector Assy becomes movable
backward.
7. Detach the liquid sample check proximity sensor together with the bracket.
8. Loosen the two detector securing bolts (M6) alternately.
Remove the bolts while supporting the detector to prevent it from falling.
(Keep the detector window cap in position, if possible. If the instrument is
provided with a He replacement unit, they are connected through piping each
other. Be sure to detach it.)
Fig. 2.3
9. Without giving a shock to the detector, slowly pull it out backward.
10. Detach the cover of a new detector and set it without giving damage to the
window (without touching it) as follows (use vacuum grease).
Be careful to prevent the pipe, wiring and other units from being caught.
Fig. 2.4
2 - 6
11. Set the new detector where the old detector was positioned.
As shown in the figure to the right, set each unit and lead in the detector
flange. Do not tighten the bolts excessively. Excessive tightening causes
abrasion of the 0 ring. Tighten the right and left bolts evenly.
/ Bushing
Fig. 2.5
12. Make the rear tank free and lead it in with the two bolts. Check that the
flange face is set in position stably. Secure the Dewar holding fixture at the rear
side so that it will support the Dewar without breaking it.
13. Secure the switch bracket and PS Assy.
14. Connect the detector and the connectors.
15. Mount the proximity sensor (with the window cap), sample plate and cover.
16. Check the degree of vacuum and put liquid nitrogen. After cooling is
complete, check for operation by carrying out an analysis.
2 - 7
Precautions on replacing the detector
If you replace the detector with the shutterlfilter, collimator and sample plate
removed, follow the steps below.
1. Do not remove the detector cap if possible.
Tape the hole at the center of the cap to prevent something from entering.
Fig. 2.7
2. If you must remove the cap to detach units, attach the cover to the detector
front face using corrugated board before starting the steps.
The cover must be at least 30 mm in dia. and 2 to 3 mm in thickness.
Attach the cover by aligning it with the center of the detector window.
Tape
Fig. 2.8
2 - 8
1.2.2 Replacing the detector of EDX-9OOHS
Detector and control unit is adjusted together in the factory. So even though
detector unit or control unit has some troubles, exchange both detector and control
unit.
Notes about detector exchange:
1)
Registration of the Sensitivity Coefficient
2)
Remaking Calibration Curve (in the case of quantitative analysis using
Calibration Curve)
~~~~~
Step 1 for detector exchange
Follow the orders below.
1. Remove the left and right covers of EDX main body.
2. Remove the upper cover of control unit's upper part.
3. Remove the rear panel. If the EDX main unit is CE type, remove the SDT
Unit at first.
4. Remove the power cable from the power supply of 24V.
Standard type: The red cable connects with No.2. The blue cable connects with
No.4. There is one switching-regulator only.
CE type: The red cable connects with No.12. The blue cable connects with
No. 14. There are two switching-regulators.
Fig. 2.9
5. Remove the 2 cables that connects with the detector. The is a cable for
temperature detection. The m is a cable for signal and power.
Fig. 2.10
6. Remove the cable connected with PCB ASSY S10 fiom the control unit.
(m)
Fig. 2.11
7. Remove the control unit fiom the EDX main body by removing the left and
right screws used for fixing.
Fig. 2.12
2 - 10
8. The base of control unit for fixing to the EDX main body is used for the
control unit for exchange again. Remove the base from the control unit.
Fig. 2.13
9. For removing the detector unit, remove the sample plate, the sensor for
liquid sample detection and the plate that samples prevent from dropping
down.
10. While you are supporting the detector unit by your hand, remove the 2
screws of irradiation room in below figure. The LED for CCD camera unit is
fixed with the detector cone using the insulok. So when removing the detector
unit, pull out the detector unit from the insulok.
Fig. 2.14
11. Remove the flange for fixing the detector unit in the irradiation room, the
detector cone (aperture) and the parts for vacuum seal. These parts are used for
the exchange detector
Fig. 2.15
0 Step 2 for detector exchange
Follow the orders below.
1. Install the flange and the detector cone. At first, remove the cover. The
detector cone is installed at the same place as the cover.
The inclination of flange: Fix the flange at 5 mm to the detector edge
The height of flange: When there is no CCD camera unit, fix the flange
so that the distance between the edge of detector body and the top of flange
is 19 mm. When there is a CCD camera unit, fix the flange so that the
distance is 24 mm. (A spacer is inserted between the flange and detector
body.)
Fig. 2.16
2. Install the base of control unit.
3. According to the contrary orders to the "Step 1 for detector exchange",
install the detector unit and the control unit to the EDX main body.
1.3 Replacing the tube
a Turn off the X-ray.
@
Open the lid of sample compartment.
Remove the 4 flat head screws and then remove the sample plate.
@
Remove the left and right side panels.
@
Remove the front panel with LEDs. This panel is connected with flat-cable. So
before removing the panel, take off the flat-cable from the panel.
Fig. 2.17
Remove the high-voltage cable, the earth wire and the filament cable from the
tube. If needed, remove the amplifier for the sensor to detect the liquid sample
adapter.
Fig. 2.18
*As the tip of high-voltage cable may be charged, discharge compulsorily the
high-voltage by contacting the tip with the cast metal of the EDX main unit.
a While supporting the tube by your hand, remove the 4 screws to fix and remove
the tube from the cast metal.
Fig. 2.19
The tube is assembled with the thermal switch. This thermal switch and the
copper tape are used for the exchange tube again. So remove the thermal switch and
the copper tape politely.
Install the thermal switch and the tube according to the contrary orders from a
to B.
1.4 Replacing the belts (Shutterlfilter, collimator)
1. Turn OFF the power. Detach the right or left cover of the instrument (left one for
the shutterlfilter, right one for the collimator).
2. Detach the motor cover (M3).
3. Loosen the motor securing bolts (M4) and reduce the shaft-to-shaft distance.
4. Replace the belt with new one. Attach a new belt and slightly stretch it to a level
that it will not come out. Too tight stretching may give an excessive load to the motor,
causing step out and excessive abrasion.
5. Secure the motor and mount back the motor cover.
6. Initialize the instrument and check for operation.
7. Mount back the cover.
1.5 Replacing the belt for operating the cover
1. Have space under the instrument.
For example, place the instrument on a spacer as shown below.
Fig. 2.20
2. Raise the cover of the instrument and turn OFF the power.
Detach each of the right, left and front covers.
3. Loosen the bolts which secure the base with the front right cover operation motor
(induction). (If you press in the motor, the pulleys also move in. Accordingly, the belt
is loosened.)
4. Replace the belt being careful not to allow the right and left pulleys to rotate. Pull
the motor toward you and attach a new belt and stretch it. After that, tighten the bolts.
Check that the right and left lifts are positioned at a same distance from the
bearing face of the base. If there is a difference of 1 mm or more in distance, loosen
the belt and rotate the both pulleys until they come in position. After that, stretch the
belt.
5. Mount back the cover and check for operation.
Fig. 2.21 Fig. 2.22
1.6 X-ray indicator lamp
1)
Outer dimensions and each unit's name
Lamp bracket -l
Pole 1
I Mounting hole Hole of 10 in dia. for
Bottom View
Fig. 2.23
2) Replacing the bulb
@
To attach and detach the lamp lens, be sure to hold the pole or lamp bracket
and then, turn the lamp lens. Do not give excessive force; otherwise, the case may
be damaged.
@ Do not wipe the lamp lens, lamp bracket and case using paint thinner, benzine,
gasoline, oil or the like.
@ UseaglassbulbT10withabaseE10for12V,O.11A.
It is a bulb for a small-size indicator lamp and available on the market.
@
Be sure to turn OFF the power before replacing the bulb.
2.1 Adjusting the cover closing-part's inclination sensor
1. Detach the right and left covers.
2. Raise the cover.
3. Adjust the sector angle so that the right and left sensors are turned OFF when the
cover comes to a 3 mm above or below the front edge in free condition.
(Sensor operation range: 6 mm)
Note : You can check ONIOFF of the sensors by the LEDs of the control
panel (5 for the right one, 11 for the left one).
Adjust the angle H
Fig. 2.24
2.2 Adjusting the cover operation sensor
1. Detach the right and left covers.
2. Close the cover and find a sensor with a larger pressing edge. (Generally, the right
one)
3. The sensor you found by the Step 2 above is a stop sensor. Move it up and down
and check that the vacuum production is done correctly in the cover-close and auto
mode.
4. If it is not correctly done, adjust timing when the right and left pressing plates
press the sensor.
5. The sensor with a smaller pressing edge is a cover-close check sensor. This sensor
must be ON only when the cover is tightly closed. Adjust the pressing plate so that it
will never be turned ON when the cover is raised even a little.
(Regarding the cover-open check sensor, check only that the pressing plate
certainly presses it.)
2.3 Adjusting the liquid mode proximity sensor
On the "Extras", set a turret for a liquid sample.
1. Check that protrusion of the liquid sample adapter's pin is 6 mm. (If not, adjust it
to 6 mm.)
2. The sensor is attached in the hole of 4 in dia. on the inner right of the
measurement position of the sample plate. Find it.
Check that the distance of the sensor from bolt edge is 6 . 4 mm- 6 . 8 ~.
If not, remove the sample plate and loosen the nut of the sensor bracket. Then,
adjust height of the sensor face and tighten the nut. Mount back the sample plate.
Fig. 2.26
3. Detach each of the right, left and front covers. A switch and controller are provided
on the amplifier upper face of the relay socket on the front left side. Adjust them.
The switch is a NO/NC selector switch. Set it at NC.
Fig. 2.27
2 - 18
4. Next, rotate the controller viewing the Liquid Mode lamp of the instrument. Stop
it when the lamp is OFF.
5. Place the adapter and check that the lamp is turned ON.
If not, adjust the controller to a position where the lamp is turned ON.
6. Detach the adapter and check that the lamp is tuned OFF.
If not, repeat the Steps 4 to 6 to set the controller where,
Lamp ON when placing the adapter
Lamp OFF when removing the adapter
(Note: If the above condition is not obtained, carry out the adjustment in 1.2 again.
If still not, the sensor or amplifier is suspected of being defective.)
2.4 Adjusting the liquid mode fiber sensor (for a turret)
1. Through the "Extras", set the Turret Mode.
2. Detach the turret or sample plate. Check that red light
is emitted from the detector window on the front left side
and no debris is attached to it.
Set a turret disk.
-@
3. Detach each of the right, left and front covers.
An amplifier is secured to the front left leg of the
analysis chamber.
4. A DARK ONILIGHT ON selector switch is attached
to the amplifier. Check that it is set at DARK ON.
If not, set it at DARK ON.
5-a) In case that the turret is not for a liquid sample (in
case that it is for a solid or large size sample)
Fig. 2.28
[
Adjust the amplifier controller so that,
The liquid mode lamp is turned OFF by initializing the turret.
The liquid mode lamp is turned ON by manually rotating the turret to
slightly displace it.
5-b) In case that the turret is for a liquid sample
Adjust the controller so that,
3.
The Liquid Mode lamp is turned ON by initializing the turret.
The Liquid Mode lamp is turned OFF by detaching the turret.
6. Mount back the cover and other units to their original positions. Now, the
adjustment is complete.
2.5 Offset adjustment of shutterlfilter and collimator
<Jigs for adjustment>
Jig A: for shutter and filter adjustment
SHUTTER ADJUSTER 776-02 174
Jig B: for collimator adjustment
NOB 776-02 175
SHAFT 776-02 176
Fig. 2.29
<Preparation>
1. Turn off the X-ray.
2. Open the sample compartment lid and then remove the sample plate.
Fig. 2.30
3. We execute the "ad.exem. Double-click the "ad.exeV file in "&edx$bin"
using the "Explorer".
4. And the "EDX-Adiust" widow is displayed.
Fig. 2.31
<Offset adjustment of shutter/filter>
We adjust offset values for shutterlfilter using the "Adjust Filter" panel.
cc
5. Click the Initialize collimator = [lmml " button. (After initialization, the
collimator is set as 10mm position.)
6. Click the "Set filter [OUT] position" button. And then the filter is set as
"OPEN" position.
7. Click the "Set collimator [lOmm]". (After initialization, the collimator is set
as 1 Omrn position. So the collimator doesn't move.)
8. Insert the Jig A into the "OUT" hole of shutterlfilter. It is the center position
that you can smoothly insert the Jig A to the end. The height of Jig A is lower
than the height of collimator plate.
Fig. 2.32
2- 21
-In the case that the hole of shutterlfilter is shifting to the right-
Move the shutterlfilter to the right.
In the "Adjust Filter Offset" panel, set movement width as 5. And then move by
clicking the '+' button. (1 pulse correspond to 4p.m.)
-In the case that the hole of shutterlfilter is shifting to the left-
Move the shutter or filter to the right.
In the "Adjust Filter Offset" panel, set movement width as 5. And then move by
clicking the '-' button. (1 pulse correspond to 4p.m.)
After moving, confirm if the Jig A is inserted smoothly trying to insert the Jig A into
"OUT" hole or pull out.
Repeating this movement and this confirmation, find out the best position.
-Note-
While the Jig A is been inserting into the "OUT" hole, do not move the shutterlfilter
absolutely.
9. After adjusting, register the offset value by clicking the "Save current
collimator-offset" button. If you continuously adjust the offset value of
collimator, leave the inserted state as it is.
<Offset adjustment of collimator>
We adjust offset values for collimator using the "Adjust Collimator" panel.
10. Click the "Set collimator [lmm]" button.
11. Insert the Jig B into the "lmm" hole of collimator and the hole of Jig A. It is
the center position that you can smoothly insert the Jig B to the end.
Fig. 2.33
-In the case that the hole of collimator is shifting to the right-
Move the collimator to the left.
In the "Adjust Collimator Offset" panel, set movement width as 5. And then move by
clicking the '+' button. (1 pulse correspond to 4pm.)
-In the case that the hole of collimator is shifting to the left-
Move the shutter or filter to the right.
In the "Adjust Collimator Offset" panel, set movement width as 5. And then move by
clicking the '-' button. (1 pulse correspond to 4w.)
After moving, confirm if the Jig B is inserted smoothly trying to insert the Jig B into
"OUT" hole or pull out.
Repeating this movement and this confirmation, find out the best position.
-Note-
While the Jig B is been inserting into the "OUT" hole, do not move the collimator
absolutely.
12. After adjusting, register the offset value by clicking the "Save current
collimator-offset" button. If you continuously adjust the offset value of
collimator, leave the inserted state as it is.
1 3. Pull out the Jig B.
14. Click the "Set collimator [IOrnrn]" button.
15. Pull out the Jig A. (If you cannot pull out the Jig A, pinch and pull out the
Jig A using a pliers and so on.
16. Install the sample plate.
17. Run the instrument initialization in the maintenance window.
<Registration of collimator standard intensity>
After adjusting offsets, you have to confirmation and registration of collimator
standard intensity. Refer the "5.2 Registering collimator standard intensity".
Below table displays the intensity of each collimator and the intensity ratio to the " 4 10".
(These values of standard intensity are references. These values are different each instrument.)
Diameter of collimator
Intensity (cps/uA)
Intensity ratio to 4 l Omm
4 lOmm
222.9395
1
4 5mm
132.1838
111.7
4 3mm
49.6530
114.5
4 lmm
6.0050
1/37
2.6 Adjusting the turret stop position
Adjust the turret stop position when the turret bottom hole does not align with the
analysis window.
Fig. 2.34
2. On the turret drive motor, two sensors are provided; the upper one is an
origin sensor and the lower one is a feed pitch sensor.
Here, the sector angle of the lower one should be adjusted.
Feed the turret through the "Manual Control" until the sector securing screw
comes to one pitch right to the sensor front face. (It should be next to the
origin.)
Fig. 2.35
3. Loosen the securing screw with the ball screwdriver. Displace the sector.
4. Feed it back one pitch, then feed it again and check the stop position.
5. Repeat the Steps 3 and 4 until the turret stops at the correct position. Secure
it at the correct position and secure the securing screw.
6. Initialize it and check that the it synchronizes the origin sensor. Mount back
the cover. If an origin error occurs, adjust the origin.
2.7 Adjusting the turret origin
If an origin error occurs at the time of initialization of the turret, adjust the origin
sensor.
On the turret drive motor, two sensors are provided; the upper one is an
origin sensor and the lower one is a feed pitch sensor.
Here, the sector angle of the upper one should be adjusted.
2. First, disconnect the connector of the origin sensor S23 and insert
the short-circuit connector (dummy origin).
3. Carry out initialization. When doing this, Table No.1 is not always set for it
and therefore, bring it to the analysis position. Remove the short-circuit
connector and connect the cable connector CH1 1 to it to S23.
4. A disk is attached to the upper position. Immediately under it, the disk
securing screw (setscrew) is provided.
Two setscrews are accessible at positions of 30" to the right and 60" to the
left when the notch is positioned at the front.
Loosen them using the ball screwdriver and secure them at positions where
the LED 1 of the control PCB is turned ON.
Fig. 2.36
5. Check that the sensor is placed in position by the initialization. If an error
occurs, repeat the Steps 2 to 4 until the sensor comes to the correct position.
2.8 Checking the degree of vacuum
1. Click on the "Manual Control" of the "Maintenance" window.
2. After closing the cover, carry out evacuation.
3. If the analysis chamber is seasoned, the degree of vacuum will be recovered to 30
Pa or less within three minutes.
4. If it is not recovered, you must suspect that vacuum sealing of the recently
assembled or replaced units are not good enough. Disassemble and clean such units
and apply vacuum grease to them.
5. Also, if it has been exposed to the air for a long time, the degree
recovered easily. If it is not recovered to 30 Pal3 min. or
of vacuum is not
less even after
disassembling, cleaning and applying vacuum grease to the units above, carry out
continuous evacuation for about one hour and then try measurement again.
6. If the poor degree of vacuum is still resulted, turn OFF high voltage of the X-ray
detector and pour petroleum ether to locate a leaking position. Then, take a
corrective action.
3.1 MCAPCB
3.1.1 Checking input voltage
@
Turn ON the power of the MCA.
@ Check that voltage of 5 V, + 15 V are correctly supplied.
Table 2.1
- - p-
CPll + 15
3.1.2 Adjusting the LLD level controller R2 (Only the PCB possible)
vhi s is not necessary in the case of EDX-SOOHS]
@
Connect the GND of the tester to the CP5 [AG] and + of the tester to the
CP4 [LLD]. Measure a range with DC.
a
Connect the power supply of + 15 V and 5 V.
@
Turn ON the power of the MCA.
@
Control the controller R2 until the LLD reads the following.
EDX-700: 50 f 2 mV
EDX-800: 15 f 5 mV
Function
Analog grounding
Digital power (5 V)
--pp----
+ 15 V analog power supply
- 15 V analog power supply
<Adjusting the LLD on the EDX-800HS>
On the EDX-800HS, you should adjust the value of the LLD within 15 mV + 5
mV. Depending on the spectrum waveform of the carbon peak, decide a value to
set.
1. Measuring the PV ratio
Set the LLD at 10 mV and then, measure the PV ratio using styrene.
(Refer to "MaintenanceIAdjustment 5, Others 5.3 Checking the PV ratio".)
2. Calculating the LLD set voltage
Calculate the LLD set voltage depending on the energy position of the
valley of the obtained spectrum waveform.
For example, if the energy position of the valley is 200 eV, set LLD set
voltage at 20 mV, namely, LLD set voltage [mV] = Energy position of the
valley [eV]/10.
Standard value
-
+ 5V
+ 15V
- 15V
Tolerance
-
f 0.25V
f 0.75V
f 0.75V
Base potentia
-
CP l 0 (DG)
pp--
CPO5 (AG)
CPO5 (AG)
~
3. Setting the LLD
By adjusting the trimmer R2 of the MCA PCB, adjust a LLD set value to the
calculated value.
4. Checking the carbon peak
Checking the carbon peak using styrene.
5. Setting the LLD again
The adjustment is complete if a single peak is obtained just at the carbon
position (around 270 eV) of the obtained spectrum waveform and also
identified by the CKa marker.
If it is not a single peak or the peak form is not symmetric, adjust the LLD
p-
set value in increments/decrements of 2 mV until a single peak is obtained and
also identified by the CKa marker.
6. Printing and recording results
Print out the spectrum waveform of the carbon peak with the identified CKa
marker and record it with the waveform of which a PV ratio was measured.
7. Example of adjustment defect
7.1 The following causes should be suspected if the LLD set value is below
10 mV or over 20 mV.
7.1.1 The offset adjustment of the MCA PCB may have not been completed.
Readjust it and carry out energy calibration.
7.1.2 The energy calibration of the instrument may not have been completed.
Recalibrate it.
7.2 The following causes should be suspected if the PV ratio of the carbon
spectrum is poor.
7.2.1 The wiring inside the main unit is not correctly laid; particularly, the
wiring from 24 V and 5 V power supply units is sometimes laid under the
aluminurn housing of the detector or liquid nitrogen Dewar; or it may
touch the detector. In this case, the detector may be affected by power
noise, producing an abnormal carbon spectrum or poor PV ratio. Be sure
to secure the wiring away from the detector.
7.2.2 The instrument may be affected by external noise. Check that its cover
is correctly secured, it is appropriately grounded, and the computer is
powered from the service receptacle of the main unit. (A big grounding
wire loop makes the instrument be easily affected by noise.)
7.2.3 The detector is secured by a hexagon bolt. Its head may contact the
proximity sensor for liquid adaptor detection. Particularly, if the detector
is absorbed into the analysis chamber at the time of measurement in
vacuum, its head, which does not contact the sensor in atmosphere, may
contact it in vacuum. If it happens, the detector may be easily affected by
noise, resulting in an abnormal carbon spectrum. Slightly screw in the
bolt, displace the sensor, or wrap insulation tape around the sensor to
prevent it from contacting.
7.2.4 The high voltage connector (HV) fixing screw of the detector
preamplifier may be loosened.
7.2.5 The instrument becomes easily affected by noise sometimes, producing
an abnormal carbon spectrum. Tighten the fixing screw.
3.1.3 Checking adjustment of the offset level controller RI
(Only the PCB possible) phis is not necessary in the case of EDX-SOOHS]
a Connect the GND of the tester to the CP5 [AG] and + of the tester to the
CP8 [SH]. Measure a range with DC.
@l
Take out the connecter from J1 "SIG.
@
Adjust the controller R1 until votage of the [PHI reaches 0 f 3 mV while
checking a value indicated by the tester with the MCA PCB in stable condition
(at least 15 minutes after power-ON).
(The setting voltage of both EDX-700 and EDX-800 is common.)
3.1.4 MCA PCB Check TerminalILED Display Function Table
CPO 1 I SIG 1 I n ~u t signal monitor 1 I I CPO5 (AG)
Reference No. Display
CP02
CP03
CP07
C'OS -r
CP09
CPlO
Function
I Input signal level buffer output
CP04 I LLD I Low level discriminator setting
CPl l I + l 5
I CPO5 (AG)
I Input signal differential buffer output I
( CPO5 (AG)
Standard
value
I CPO5 (AG)
CP13 ( PD I Peak detection signal output ( TTL level ( ( CPlO @G)
Analog grounding
Peak detection gate signal
Peak hold circuit output
Sample ho1-
Digital power supply (5V)
Digital grounding
+ 15V analog power supply
- 15V analog power supply
CP14 I REJ I Rejection signal input I TTL level I ( CPlO (DG)
Tolerance
CP15 I BSY I Busy signal input I TTL level I I CPlO(DG)
Base
potential
v
TTL level
+ 5V
-
+ 15V
- 15V
-
TTL level
rt 0.25V
-
+ 0.75V
* 0.75V
CP16
CP17
LED0 1
-
CP05 (AG)
CPO5 (AG)
05 (AGJ-
CPlO (DG)
-
CP05 (AG)
CP05 (AG)
CRM
DG
Count rate meter input
Digital grounding
Lights up when 5V power supply is
i n~ut .
TTL level
- -
CPlO (DG)
-
3.1.5 Replacing the ROM
<Steps>
a Stop the instrument following the Steps below. Then, turn ON the power of
the EDX main unit.
Carry out the Stopping the instrument (Ending analyses), Stopping the X-ray,
Ending the EDX software and Ending the Windows.
Upper
Right
. cover
: cover
Left cover
SCSI cable
Rear panel
Fig. 2.37
Disconnect the power plug of the main unit.
Disconnect the power plugs of the PC and printer.
@ Disconnect the SCSI cable from the main unit.
Chassis B
AMP PCB
CTRL PCB
Connector CN9 -
MCA PCB
Fig. 2.38
2 - 31
@
Detach each of the right, left and front covers.
Loosen the four securing screws (truss screw, M4 X 8) and detach the right
and left covers.
Loosen the four securing screws (SUS sems with a hexagon socket head,
M4 X 16) and detach the upper cover.
@ Detach the rear panel.
Detach the rear panel by loosening the five securing screws (SUS sems, M4
X 8) and disconnecting the fan cable connector CN9. Since the fan is secured to
the rear panel, be careful about the cables when detaching the panel.
@l
Detach the chassis A of the controller.
- - P -P - - -
View the instrument main unit from behind. Find the chassis A which is
secured by three screws (SUS sems with a hexagon socket head, M4 X 6) and
remove them.
@
Detach the chassis B of the controller.
View the instrument main unit from behind. Find three securing screws of
the chassis B which secures the amplifier PCB. Remove two of them at the
front. Loosen one at the furthest position and incline the chassis B to facilitate
replacement of the ROM on the MCA PCB.
Fig. 2.39
@ Replace the ROM M23.
Detach the ROM of the old version and detach one of a new version.
@
To reassemble the ROM after the replacement, reversibly follow the Steps
Q to 8.
3.2 CTRLPCB
3.2.1 Checking input and output voltage
a
Turn ON the power of the CTRL PCB.
@ Check each voltage.
Input: 5 V, 24 V (CP08, CP15)
Output: 5 V (CP09, insulation power for the sensors, from 5 V)
f 12 V (CP1 l, CP12, insulation power for the Pirani gauge, fiom 5 V)
f 15 V (CP13, CP14, insulation power for X-ray control, from 5 V)
8 V (CP20, for the pressure sensor, from + 15 V)
f 5 V (CP25, CP26, for ADC, starting at 15 V)
8 V (CP18, for the spinner, starting at 24 V)
Standard voltage: - 10 V (CP04, standard voltage DAC)
+ 5 V (CP24, standard voltage ADC)
CP04 I RF I DAC standard voltage I -1OV I +O.lV I CPOl(AG) I
Reference
No.
CPO l
Display
AG
CP07 I DG I Digital ground
CP25 1 + 5 ] + 5V analog power supply I +5V I k 0.25V I CPOl (AG)
I l I I
CPO8
CP09
CPlO
CPl l
CP12
CP13
CP14
CP15
CP16
CP18
CP20
CP24
CP26 1 - 5 1 - 5V analog power supply I -5V I f0. 25V I CPO1 (AG) (
Function
Analog ground
- -
5V
I5
IG
+ 12
- 12
+ 15
- 15
24
PG
SPN
+ 8
R5
Standard
value
-
Digital power supply (5V)
Insulation digital power supply (5V)
Insulation digital grounding
+ 24V control power supply
+ 24V control power supply grounding
Spinner drive power supply
Tolerance
-
Base
potential
-
+ 5V
+ 5V
-
+ 12V
- 12V
+ 15V
- 15V
+ 24V
-
- . + 8V
f 0.25V
f 0.25V
-
f 0.6V
+ 0.6V
f 0.75V
f 0.75V
f 1.2V
-
f 0.8V
ADC standard voltage
CP07 (DG)
CPlO (IG)
-
CPOl (AG)
CPOl (AG)
CPOl (AG)
CPOl (AG)
CP 16 (PG)
-
CP16 (PG) -
+ 0.4V
f 0.05V
+ 8V
+ 5V
CPOl (AG)
CPOl (AG)
3.2.2 Adjusting the M5 offset controller VR1
a
Connect the GND of the tester to the CP1 [AG] and + of the tester to the
CP28 [AD]. Measure a range with DC.
@
Adjust the controller VR1 until output voltage reaches 0 to 1 mV while
checking a value indicated by the tester with the CTRL PCB in stable condition
(at least 15 minutes after power-ON).
(The setting voltage of both EDX-700 and EDX-800 is common.)
3.2.3 CTRL PCB Display LED Function Table
LED02 I I Detects liauid disk I OFF if detected
Reference No.
LED0 l
LED03 I I Detects liauid ada~t er I OFF if detected
LED04 I I Detects shutter is closed 1 ON if detected
Display
LED 14 I I Detects collimator limit (l 0 mm) I OFF if detected
Function
Detects X-ray Dower ON
LED05
LED06
LED07
LED08
LED09
LED l 0
LED l l
LED 12
LED 1 3
LED 15 I I Detects collimator origin (1 mm) I OFF if detected
Lighting condition
ON if detected
LED 16 I I Detects shutterlfilter limit ( o~en) I OFF if detected
Detects right cover tilting
Detects left cover is closed
(Detection of cover tilting is invalid)
Detects cover is opened
Detects right cover is closed
(AUX-IN2)
Detects left cover tilting
Detects turret pitch
Detects turret origin
OFF if detected
ON if detected
(ON at short-circuit)
OFF if detected
ON if detected
(ON at short-circuit)
OFF if detected
ON if detected
ON if detected
LED17 I Detects shutterhilter origin (close) I ON if detected
LED 1 8
LED25 I I START SW input I set SW to ON
I X-ray tube thermal switch input ( OFF if detected
LED1 9
LED20
LED2 1
LED22
LED23
LED24
LED26 I I STOP SW i n~ut I set SW to ON
Detects 9 origin
Detects R limit
Detects R origin
AUX-SW input
CLOSE-S W input
OPEN-S W input
LED28 I I S~i nner drive I ON at drive
OFF if detected
OFF if detected
OFF if detected
Set SW to ON
Set SW to ON
Set SW to ON
LED27 I X-ray power supply ON command I ON when command is output
LED3 1 I I Vacuum leak valve drive I ON at drive I
Reference No.
LED29
LED30
LED32 I I Vacuum D U ~ D drive I ON at drive I
LED33 I I Turret CW drive I ON at drive I
Display
LED34 I I Turret CCW drive I ON at drive I
LED35 I Cover drive brake I (ON at drive) I
Function
He replacement drive
(He high flash)
Lighting condition
ON at drive
(ON at drive) -
LED44 I I Detects X-rav over current I On if detected I
LED36
LED37
LED38
Cover open drive
Cover close drive
(AUX-OUT2)
LED40
LED4 1
LED42
LED43
ON at drive
ON at drive
(ON at drive)
/ A T T V N T T l \ pp
-
(Lock solenoid open)
(Lock solenoid close)
Detects X-ray tube over heating
Detects X-ray over voltage
I
(ON at drive)
(ON at drive)
On if detected
On if detected
3.2.4 CTRL PCB Check Terminal Function Table
Reference No. Display
I I
Function Standard Tolerance Base
I value I I ~otential
CPO l
CP02
CP03
CP04
CP05
I
AG
VM
KV
RF
IM
CP06 I MA I X-ray tube current command
I
I
CP18 1 SPN I Spinner drive power supply I + 8V I f 0.4V I CP16(PG)
I CPOl (AG)
CP07 I DG I Digital grounding
CP OS - -
CP09
CPlO
CPl l
CP12
CP13
CP14
CP15
CP16
CP17
Analog grounding
X-ray tube voltage monitor
X-ray tube voltage command
DAC standard voltage
X-ray tube current monitor
-
5V
I5
IG
+ 12
- 12
+ 15
- 15
24
PG
INT
I
-
- 1OV
CP19 I PRN l Pirani gauge signal
CP20
CP2 1
CP22
CP23
CP24
CP25
CP26
CP27
CP28
-
Digital power supply W-
Insulation digital power supply (5V)
Insulation digital ground
+ 24V control power supply
+ 24V control power supply grounding
X-ray generation interlock signal
I CPOl (AG)
-
f 0. l V
-
+ 8
PH
PL
SE
R5
+ 5
- 5
DG
AD
-
CPOl (AG)
CPOl (AG)
CPOl(AG)
CPOl (AG)
+ 5 V
+ 5V
+ 12V
- 12V
+ 15V
- 15V
+ 24V
-
Pirani gauge high gain signal
Pirani gauge low gain signal
Air sensor signal
ADC standard voltage
Digital grounding (same with CP07)
ADC input signal
- . + 0 2 5 ~
f 0.25V
-
f 0.6V
+ 0.6V
f 0.75V
+ 0.75V
f 1.2V
-
CPlO (IG)
-
CPOl (AG)
CPO l (AG)
CPOl (AG)
CPOl (AG)
CP16 (PG)
-
CP 1 6 (PG)
+ 8V
+ 5V
+ 12V
- 12V
-
+ 0.4V
+ 0.05V
f 0.25V
f 0.254
-
CPOl (AG)
CPOl (AG)
CPOl (AG)
CPOl (AG)
CPOl (AG)
CPOl (AG)
CPOl (AG)
-
CPOl (AG)
3.3 AMP PCB (only EDX-700HSl800HS)
3.3.1 Adjusting the gain of the amplifier
Coarse adjustment
Getting instrument environment>
1. To open the "Extras" of the "EDX-Main Menu", exit the EDX software
screen other than the "EDX-Main Menu" window.
2. Click on the "Extras" to display the "Extras".
3. On the "Environment" panel, click on the "Instrument" to display the
"Extras" window.
4. Set 127 for each of Gain and Offset of 0-40 keV and 0-20 keV of the
- -
"Detector" panel.
5. After that, click the "Save" button to close the window.
Creating an adjustment group>
6. Click on the "Condition" of the "EDX-Main Menu" window to display the
"Select Group" window.
7. Select the "Qual-Quant" of the "Select Group" window. Set "User Group"
for the "Owner of Analytical Group" and after that, click on the "Create" to
display the "Create As New Group
7
' window.
8. Input "Adjust AMP" for the "Group Name" on the "Create As New Group"
window and click on the "OK".
9. Set group conditions in accordance with the following.
AMP adjustment group measurement condition (Qual-Quantitative)
<Adjustment setup>
10. Detach the cover of the left side face and the upper cover.
11. Start the instrument from the "Maintenance" window.
Detector HT : ON
X-ray : 50 kV- 100 pA
Adjustment
sample
A750
Atmosphere
Air
AMPPCB
Channel
Ti-U
Voltage
50
Current
100
Auto
Current
control
0
Integration Time
Acq.
Range
0-40
Real Live l m e
Real Time
Display
Range
0-40
sec
100
Analysis
Range
040
DT
%
25
<Reading the analytical groups>
12. Click on the "Analytical Group" of the "Next sample" panel of the
"Analysis" window.
13. Read the group "Adjust AMP" made by the steps above.
<Displaying the KLM marker>
14. Open the "KLM Marker" through the "View" of the "Analysis" window.
15. Display Sn (50), A1 (13), and Cu (29).
Fig. 2.40
<Starting an analysis>
16. Set A750 and click on the "START".
<Adjusting the amplifier gain>
17. Adjust it so that the spectrum of SnKb is centered on the SnKb line of the
KLM maker by rotating the controller VR2 on the amplifier PCB.
(Clockwise rotating the controller raises the energy position of the peak. On
the other hand, counterclockwise rotating lowers the energy position of the
peak.)
After rotating the controller, be sure to restart the analysis.
Fine adjustment (Instrument Calibration)
<Carrying out energy calibration>
18. Set A750 and then, click on the "Instrument Calibration
yy
of the
"Maintenance" window.
19. Set the "Yes" for the "EnergyIEWHM Calibration" and click on the "Start".
20. On completion of the calibration operation, exit the "Instrument
Calibration" window.
<Confirm>
21. On the "Data Process Environment" of the "Extras" window, change the
- p - -- -- --pp-- -- -
quantitative group and data to the directory below.
Qual-Quant. Condition : c X edx Y user Y test
Qual-Quant. Data : c Y edx Y user B test
22. Using the group "Inspection: Energy Position", measure the standard sample
A750. As a result, the energy position of FeKa should be within 6.336 to 6.464
(KeV) and the spectra of SnKa (L line included) AlKa, CuKa, and NiKa should
be identified.
3.3.2 AMP PCB Display LED Function Table
I Reference No. I Dis~lav Function Linhtina condition I
I 1 I I exist or thermal sensor is disconnected. 1
LD 1
LD2
LD3
LD4
TEMP. L
PUR DISC
ERROR RESET
DET. BIAS ON
TEMP. H
Detector low temperature error
X-ray signal exists
Detector high voltage reset signal
Detector high voltage ON
Detector high temperature error
Lights up when thermal sensor is
short-circuit. I
I LD6
Lights up when X-ray signal is input.
Extinguishes at reset
Lights up when high voltage is ON
Lights up when liquid nitrogen does not
2014OkeV AMP channel change-over Lights up when full scare is 40keV.
l
3.3.3 AMP PCB Check Terminal Function Table
CP14
CP15 BUSY
Function I Standard value
P
Input buffer output
AMP initial output (?)
AMP calibration output
AMP gain change-overladjustment output
Filter 1 output
Filter 2 output
AMP output
Analog COM I
Digital COM
Pulse output for rate meter (TTL level) H at pulse count
AID conversion prohibition signal H when AID conversion is prohibited.
While X-ray signal is being outputheset H while signal is being output or reset.
Reset pulse of detector is input H during reset
- 12V -12V f 0.6V
+ 12V +12V + 0.6V
- 24V -24V f 1.2V
Detector tem~erature monitor I 0 . 8 ~ at - 175C
Gain calibration standard voltage I 0-- 1OV
+ ~ O V standard voltage I + ~ O V f 0 . 1 ~
Slow discriminator innut I
Offset calibration standard voltage - 0.1--+ 0.1V
First discriminator output (TTL level)
Slow discriminator output (TTL level)
Discriminator automatic level 5-20mV
3.4 PS PCB
3.4.1 Adjusting the detector bias
phis is not necessary in the case of EDX-SOOHS]
a
Connect the GND and + of the tester to TS3 and CP7, respectively. Measure
a range with DC.
@
Detach the right side face cover.
@
Remove the connector 54 of the prearnplifier.
@
Turn ON the power of the PS PCB.
@
Set " ON for the "Detector HT" of the "Manual Control" through the
"Maintenance".
@
Adjust the voltage at CP7 within 0.8 V f 10 mV by rotating the controller
R27. (The set voltage is common to the EDX7001800.)
@l
After the adjustment, set OFF for the Detector and turn off the power.
@
Connect the connector to 54 of the preamplifier.
Mount back the right side face cover.
3.4.2 PS PCB Check Terminal Function Table
Ref. No. Display
+
Function Standard Value
+ 15V + 15V f 0.75V
Detector bias monitor value I 0.8V f lOrnV I
Detector bias monitor set value I 0.8V f lOmV I
3.5 Stepping drive motor
Driver function selector switches and current setting controller
The switches and dial of the driver should be used without changing setting done
before shipment. Check that it conforms to the following. The (white) of the
function selector switch signifies the protruded part.
Automatic current down function selector switch - ACD
-
Step angle selector switch - F/H
-
Pulse inqutmethod selector switch -
~ - pp -------p 1PI2P
Supply voltage selector switch - 2 4 1 3 6 ~
Display
ACD
F / H
1P/ 2P
24 /36V
Switch name
Automatic current down function selector switch
Step angle selector switch
Pulse input method selector switch
Supply voltage selector switch
Setting
ON
F
2P
24V
ONIOFF
ON
ON
OFF
ON
4.1 Mounting the turret drive unit
1 . Detach the right, left and front covers of the instrument.
2. Find the lid at the turret shaft position of the casting in the analysis chamber.
Detach it from below. (M4,4 pieces)
Note: The 0 rings and bolts are used again. Be carehi not to contaminate
them.
3. Apply vacuum grease to the working faces of the 0 rings. After that, mount
the 0 rings and introducing shaft Assy (212-22332) from the bottom.
4. Replace the sample plate and mount the ring onto the analysis position.
Align the disk with the pin-split position of the disk mounting face.
Align the position No. 1 of the disk with the inner side of the analyzer.
5. Secure the four legs of the spacer for the drive (motor).
Rotate the gear to allocate the sector around the center of origin sensor.
Analysis Position No
Fig. 2.42
6. Bring the sensor toward you and mount the drive (motor) to the casting in
the analysis Chamber. (M4 X 10, 3 pieces).
Wire the sockets (212-22697). (CN13/Motor, CN12/0rigin, CNI 11Pitch)
7. Operation check
Carry out "Extras", initialize the turret (the number of turret pan) and check
that Pan No. 1 is brought to the analysis position.
Also, check for feed operation.
8. If the evacuation system is provided, carry out vacuum production to check
that 30 pa is reached in three minutes.
If it has been open to atmosphere for a long time, continue vacuum
production about one hour and then, check the degree of vacuum.
If leakage is found, check the 0 rings for debris, flaws, etc.
P p P - P -P
4.2 Installation orders of collimator
Installation contents
1. Installing the origin sensor and the limit sensor.
2. Installing the collimator plate.
3. Installing the collimator rod.
4. Installing the motor driver.
5. Installing the collimator motor and the timing belt.
6. Installing the PPMC.
7. Offset adjustment of collimator.
8. Registering values of collimator standard intensity.
1. Installing the origin sensor and the limit sensor.
Fix the "S2l"(left side: origin) and the "S22"(right side: limit). And then fix
the extra part by using the band and connect this ASSY with the H4 of hermetic
seal connector.
Fig. 2.43
Next, we wire from the cast metal of sample compartment to the CTRL PCB
ASSY.
l~ollimator Sensor ~ 4 1 - > - > - > b30 (CTRL PCB ASSY I
2. Installing the collimator plate.
Insert the collimator plate into the upper row of the guide roller from right
side.
3. Installing the collimator rod.
Grease the BARRIERTA grease at the 0-ring part of collimator rod. While
turning the collimator rod with your hand, insert the collimator rod from
collimator plate and fix it.
Note) when turning the collimator rod with your hand, confirm if it can
move smoothly.
If it is hard to turn the collimator rod, loosen the screws of base below the
guide roller and adjust the screws so that the guide roller can be parallel with
the collimator plate.
4. Installing the motor driver.
Install the motor driver next to the standard motor driver.
5. Installing the collimator motor and the timing belt.
Install the motor on the right of cart metal of sample compartment. And
install the timing belt so that the edge of timing belt can be at about 5mrn to the
edge of wheel on the side contrary to the motor.
Next wire according to below figure.
Motor Driver CN~ ] - > m1- > - > bollimator motod
r I
6. Installing the PPMC.
Install the PPMC for collimator. (M65)
Fig. 2.44
7. Offset adjustment of collimator.
7.1 Turn on the EDX main body. And select the "4-Type Changeable" in
the ''Instrument Environment" and save it.
7.2 Initialization of collimator moves to the origin sensor (LED15) at first,
and moves to the direction of the limit sensor secondary.
At this time, install the limit sensor at the most right position so as not
to sense the limit sensor (LED14).
Note 1) at this time, if the limit sensor is sensed, the
"Acceleration/reduction operation error" happens.
Note 2) when both these sensors are sensed, the LED14 and LED1 5 are
turned off.
7.3 Adjusting using the Jigs for collimator adjustment.
Refer the "2.5 Offset adjustment of shutterlfilter and collimator".
Note 3) plus offset is good. To be plus offset, you should move the origin
sensor.
8. Registering values of collimator standard intensity.
Refer the "5.2 Registering collimator standard intensity".
4.3 Mounting the X-ray indication lamp
1. Detach the left side face from the instrument.
2. Put the cable inside and attach the indication lamp on the rear side. (M4 X 8,
2 pieces)
3. Disconnect the socket at 527 of the control panel and insert the indication
lamp socket. (cf 2 12-22702)
4. Mount back the cover.
5. Check the instrument for operation. After that, check that the lamp lights up
after the X-ray operation starts.
Fig. 2.45
2 - 47
5.1 FP Sensitivity Coefficient Input Method
<Information of Sensitivity Coefficient Measurement Group and Standard Sample for
No.
1
2
3
4
5
6
7
8
9
10
11
(14 samples, 18 elements)
12
13
14
Group Name
CaCO3-15-Air
Ti-50-Air
SUS2-50-Air
Cu-50-Air
Zr02-50-Air
Measurement
Element
C, F
Na
AI
Si
S
P, K
For 700HSl800HS
CF2-15-Vac
NaC1-1 5-Vac
A1203-15-Vac
Si-15-Vac
Na2S04-15-Air
KH2P04-15-Air
Sn-50-Air
BaC03-50-Air
Pb-50-Air
For 9OOHS
9-CF2-15-Vac
9-NaC1-15-Vac
9-A1203_15-Vac
9-Si-15-Vac
9- Na2S04-15-Air
9- KH2P04-15-Air
9- CaC03-15-Air
9- Ti-50-Air
9- SUS2-50-Air
9- Cu-50-Air
9- Zr02-50-Air
Standard
Sample Name
CF2
NaCl
A1203
Si
Na2S04
KH2PO4
9- Sn-50-Air
9- BaC03-50-Air
9- Pb-50-Air
Ca
Ti
Fe, Ni, Cr
Cu
Zr
Sample Form
Teflon, plate
Salt, powder
Alumina, bead
Silicon wafer
Sodium sulfide, powder
Disodium hydrogen
Sn
Ba
Pb
Remarks
only
800HS
All
All
All
All
All
CaC03
Ti
SUS2
Cu
Zr02
Sn
BaC03
Pb
phosphate, powder
Calcium carbonate,
powder
Titanium, plate
Stainless, plate
Copper, plate
Ziroconium oxide,
powder
All
All
All
All
All
Tin, plate
Barium oxide, powder
Lead, plate
All
All
All
<Updating sensitivity coeficient>
1. On the "Data Process Environment" of "Extras", record the current
quantitative group and data directories. After that, change them to the
directories below.
Quant Condition : c\edx\user\fp
Quant Data : c\edx\user\fpdata
Fig. 2.46
2. Read fp 700.blk through the "Fi1e""Read Routine" of the "Sample
Schedule" window in case of the EDX-700HS, and read fjI 800.blk in case of
the EDX-800HS, and read fjI-900.blk in case of the EDX-900HS.
Fig. 2.47
3. In order of the read analysis sample name, set a standard sample to measure it.
4. After the measurement, run the "Calculate Theoretical Intensity" for each group.
Fig. 2.48
*
Regarding SUS, input the standard value again and then, run the "Calculate
Theoretical Intensity". (The standard value of the SUS2 is registered as the default.)
5. Calculate a sensitivity coefficient for the element measured for each group
and set it.
Fig. 2.49
6. Select the quantitative system group, sysmetal, and display the "Sensitivity
Coefficient List".
7. On the "Sensitivity Coeficient List" window, confirm that "Measurement"
is set for elements actually measured and "Interpolation" is set for other
elements. (EDX-700HSl900HS are 16 elements. EDX-800HS is 18 elements.)
If not, change setting and click on the "Register Coefficient".
Fig. 2.50
2 - 51
8. From the "Sensitivity Coefficient List" tab, select the measured group for
the measured element. Selecting it automatically updates its coefficient.
Fig. 2.51
9. After that, run the "Interpolate". After interpolation calculation finishes,
click on the "Register Coefficient".
10. Print out the Sensitivity Coefficient List of quantitative system group, sysmetal.
Fig. 2.52
2 - 52
11. Next, you should run sscopysys.exe. To do it, open the "Explorer", double
click on the file, sscopysys.exe, which resides in c\edx\bin\sscopysys.exe.
JGKB Application Extension 31'10/99 12:OOAM
41KB Applidon Extension 3tl W99 1200AM
42KB Applicatin 3lW9912OOAM
2KB Application 3 1 0/99 1200 AM
31KB Application 3/1 0199 12:OOAM
34KB Application WW9912:OOAM
328KB Application 31'10/99 1200AM
24KB Application
8KB Application
45KB Application
11 4KB Application
28XB Application 3/1 0199 12:OOAM
75KB Applicalion 31'10199 lZOOAh4
25SKB Application 3?10/99 12:OOAM
Fig. 2.53
As a result, the sensitivity coefficients made by sysmetal are copied into five
files below.
sysoxide, sysmetal 15kV, sysmetal50kV, sysoxide 1 5kV, sysoxide 50kV
12. On the "Data Process Environment" of the "Extras" window, return the
quantitative group and data into the original directory recorded by Step 1.
<Confirmation>
quantitative group and data to the directory below.
Qual-Quantitative condition : c\edx\user\test
Qual-Quantitative data : c\edx\user\test
14. Using the group "Inspection: FP Qual-Quantitative", measure the FP
standard sample SUS to check that the quantitative value of each of four
elements Fe, Cr, Ni and MO is within a range of a standard value + 2%.
15. Next, you should back up six system groups which reside in the (C:)\edx\
shimadm \grp with updated sensitivity coefficients, onto the "Device
Information" sheet.
Load the sheet into the floppy disk drive and update and using the
"Explorer", save the six system groups on it.
Atmosphere I vacuum I vacuum I vacuum I vacuum I vacuum
<Measurement condition list of each element>
AI
Ka
Element
Spectrum
Filter
Tube voltage (kV)
Tube current (uA)
Current auto control
Energy of neighbor peak setting
Energy of neighbor peak value
Si
Ka
F
Ka
C
Ka
Nothing
15
100
OK
Real Time
Live Time
lOOsec
40sec
25%
10%
Fitting
0.17-0.4
Integration method
Integration Time
DT%
Element
Spectrum
Atmosphere
Filter
Tube voltage (kV)
Na
Ka
700HSl800HS
900HS
700HSl800HS
900HS
700HSl800HS
900HS
-
-
Nothing
15
100
OK
Real Time
Live Time
l OOsec
40sec
25%
10%
Fitting
0.44-0.84
Intensity calculation method
Analysis range
P
Ka
Air
Nothing
15
Tube current (uA)
-
-
100
OK
Real Time
Live Time
lOOsec
40sec
25%
10%
Fitting
1.82-2.22
Integration method
Integration Time
DT%
Nothing
15
100
OK
Real Time
Live Time
100sec
40sec
25%
10%
Fitting
0.8-1.24
S
Ka
Air
Nothing
15
700HSl800HS
900HS
700HSl800HS
900HS
700HSl800HS
900HS
-
-
OK
0.88
100
OK
Real Time
Live Time
l OOsec
40sec
25%
10%
Fitting
2.12-2.52
Analysis range
Nothing
15
100
OK
Real Time
Live Time
l OOsec
40sec
25%
10%
Fitting
1.3-1.7
K
Ka
Air
Nothing
15
-
-
Nothing
15
100
OK
Real Time
Live Time
l OOsec
40sec
25%
10%
Fitting
1.54-1.94
-
-
Ca
Ka
Air
Nothing
15
100
OK
Real Time
Live Time
lOOsec
40sec
25%
10%
Fitting
3.12-3.52
-
-
100
OK
Real Time
Live Time
l OOsec
40sec
25%
10%
Fitting
3.5-3.86
-
-
-
-
Current auto control I OK I OK I OK I OK I OK
Element
Spectrum
Atmosphere
Filter Nothing
Tube voltage (kV)
Tube current (uA)
Ti
Ka
Air
Nothing
50
10
Integration method
Integration Time
I Element Zr Sn Ba Pb I
Cr
Ka
Air
Nothing
50
20
700HSl800HS
900HS
DT%
I Filter
700HSl800HS
900HS
Tube voltage &V)
Tube current (uA)
Integration Time 700HSl800HS
Fe
Ka
Air
Nothing
50
20
Real Time
Live Time
700HS/800HS
900HS
lOOsec
40sec
Analysis range
lOOsec l OOsec lOOsec lOOsec
40sec 40sec 40sec 40sec
N i
Ka
Air
Nothing
50
20
Real Time
Live Time
25%
10%
1 G,
Air
1 Ni
50
3
OK
Intensitv calculation method
Cu
Ka
Air
Nothing
50
1
l OOsec
40sec
Fitting
4.32-4.72
-
-
Analvsis range
Real Time
Live Time
25%
10%
Real Time Real Time Real Time Real Time
Live Time Live Time Live Time Live Time
Ka
Air
Nothing
50
100
OK
l OOsec
40sec
Fitting
5.22-5.62
-
-
Real Time
Live Time
25%
10%
La
Air
Nothing
50
17
OK
Fitting
15.34-16.1
Real Time
Live Time
l OOsec
40sec
Fitting
6.18-6.62
-
-
Lbl
Air
Nothing
50
100
OK
lOOsec
40sec
25%
10%
Fitting
24.66-25.72
25%
10%
Fitting
7.26-7.72
-
-
I
-
Fitting
7.68-8.28
-
-
Fitting
4.26-4.64
-
Fitting
12.4-12.86
-
-
- -
- -
<Standard sample information>
I Standard
No
I sam~l e name
Measured element:
content (%)
C : 24.02
F : 75.98
Salt, powder
Alumina, bead
Unmeasured element:
content (%)
Teflon, plate
Na : 39.34
A1 : 52.93
Si : 100.00
S : 22.57
K : 28.73
Silicon wafer
Sodium sulfide, powder
Disodium hydrogen
Sample form
C1 : balance
0 : balance
Li2B407 : l 0 times
Na204 : balance
H2O4 : balance
Ca : 40.04 I CO7 : balance I Calcium carbonate, powder
P : 22.76
Ti : 100.00 I I Titanium. dat e
I phosphate, powder
Cr : each determination I Si : each determination
Fe : each determination 1 Mn : balance
Zr : 74.03 I 0 : balance
Ni : each determination
Cu : 100.00
Stainless, plate
MO : each determination
Copper, plate
Zirconium, vowder
Sn : 100.00 I I Tin, vlate
Ba : 74.28 1 CO2 : balance 1 Barium oxide. ~owder
Pb : 100.00 I I Lead, alate
(14 Samples, 18 elements)
Registering collimator standard intensity
<Setup>
1. Collimator Standard Intensity Measurement Groups (4 Groups: collimator 10,
collimator5, collimator3, collimatorl) reside in the a:\collimator directory of
the "EDX (DXP) Adjustment Group Program V1.OO". Using the "Explorer",
copy them into c\edx\user\test.
quantitative group to the directory below.
Qual-Quant Condition : c\edx\user\test
Qual-Quant Data : c\edx\user\test
3. Check that the "4-type Changeable" is set for the "Collimator" on the
"Instrument Environment" of the "Extras" window.
<When "4-type Changeable" is not set>
Give a check mark to the "4-type Changeable" on the "Collimator" panel.
After checking, set it by clicking on the "Save".
<Measurement>
4. Set a SUS sample.
5. Select collimator 10 from the Quantitative Group of the "Analysis" window
and measure the sample.
6. After the measurement, note down the FeKa intensity displayed on the
"Result Display".
7. In the same manner, carry out measurements regarding groups collimator5,
collimator3, and collimatorl and note down the resulted intensities.
<Register>
8. For registration, you should run c\edx\bin\eu smzbat using the
"Explorer". Double click on the file eu srnzbat which resides in c: \edx\
bin\.
9. Click on the "Options" of the "Instrument Environment" of the "Extras"
window to display the "Instrument Environment: More Options" window.
10. Click the "Intensity Calibration" button on the lower right of this window to
display the "Intensity Calibration Information" window.
11. Input the previously measured intensity for the "Standard Intensity" column
of each collimator. (Values to be input for the Standard Intensity column should
be the same.)
Fig. 2.54
12. On completion of the input, click on the "OK". After that, exit this window
to exit the "Instrument Environment: More Options" window.
13. Click on the "Save" of the "Instrument Environment" window to save the
setting.
14. Exit the "Extras" window.
<Confirm>
15. Open the quantitative group, collimatorl0, on the "Condition" window and
change collimator dia. to 5 mm.
16. Check that the coefficient value of calibration curve of Fe is set at the value
(Standard Intensity by 5 mdstandard Intensity by 10 mm).
Note: Do not save this group.
5.3 Checking the PV ratio
Set Discrete level at 10 mV. Measure C using a styrene sample (a hard case of a
floppy disk) to check the PV ratio.
After that, set the Discrete level again. Regarding the setting method, refer to the
"3.1.2 Adjusting the LLD level controller W'.
<Setting Discrete level at 10 mV>
1. Connect the GND of the tester to the CP5 [AG] and + of the tester to the
CP4 [LLD] on the MCA PCB. Measure a range with DC.
2. Set voltage between CP5 and CP4 at 10 mV by rotating the LLD level
controller R2. (Setting should be done with the MCA PCB stable (15 minutes
after power-ON).
<Setup>
3. On the "Data Process Environment" of the "Extras", record the current
quantitative group and data directories. After that, change to the directory below.
4. Click on the "Analysis" of the "EDX-Main Menu" window. (Usually, the
"Analysis" window has been already booted.)
5. Click on the "Analytical Group" of the "Next sample" panel of the
"Analysis" window.
6. Click on the "Qual-Quant" on the "Select Analytical Group" window. Set
the "User Group" for the "Owner of Analytical Group".
7. From the group names, find "Inspection: Carbon Analysis" and click on it.
(After that, the group is highlighted in blue.) Then, click on the "OK".
8. Do not set a sample name. Accordingly, a date of measurement is
<Measurement>
9. Place a styrene sample on the measurement position.
10. Click on the "START" of the "Analysis" window.
<Data processing after measurement>
11. Click on the "Data Process" on the "Current Sample" panel of the
"Analysis" window. Then, the "Profile [Qual-Quant] [Dater window appears.
12. On the "Profile [Qual-Quant] [Dater' window, left click on the "Display
(D)" and also, left click on the "Channel Single (S)".
13. Left click on the "Display (D)" and then, left click on the "Display Region
Setting (R)". On the appeared "Display Region Setting" window, change
setting for the X-axis to 0.0-1.0. Then, click on the "OK". By this operation,
the value for "Width" is updated.
14. Left click on the "Display (D)" and then, left click on the "Vertical Axis
Unit (U)" to set "Counts m'.
15. Next, to adjust the display scale, click on the icons (a) and (m) so that
the peak of C (0.277 keV) may be displayed at a position nearly half of the full
scale of the vertical-axis.
16. Click on the Icon for the printer or left click on the "File (F)" and then, left
click on the "Print m'. Then, the "Print: [Qual-Quant][Single Profile] window
appears.
17. On the "Print Item" panel, set four items, "Measurement Condition",
"Profile", "Qualitative Result", and "Peak List".
18. After setting, click on the "Print". After printing finishes, click on
thenClose" to exit the "Print: [Qual-Quant] [Single Profile] window.
<Confirm>
19. Plot the profile and calculate the P N ratio. Check that the result is 1.4 or
more.
<How to calculate the P N ratio>
[Counts]
Fig. 2.55
a
Draw the vertical Line A which goes through the CKa peak using a ruler.
@
Measure the distance (dl) between the CKa peak and the point where Line
A crosses the X-axis using a ruler.
Draw the vertical Line B which goes through the bottom of the valley made
by the CKa peak and the noise.
@
Measure the distance (d2) between the bottom of the valley and the point
where Line B crosses the X-axis using a ruler.
@
Calculate the P N ratio by the calculation formula below.
PN=d l Id2
5.4 Procedure of installing the EDX software
EDX software (DXP-700) is installed using CD-R media after Ver.l .OO Re1 .Ol3. This
section is explained about how to re-install or do version-up.
And when you do the version-up, do backup the files in "c:Xedx~shimadzu" directory
copying to other directory.
(1) Inserting the CD-R media.
Insert the CD-R media in the CD-ROM drive and then display the content in
the CD-R media by using explorer of Windows.
(2) Executing set-up.
Double-click "setup" or "setup.exe" and then set-up program starts. after
starting, the below window is displayed. Click the "OK" button.
Fig. 2.56
And after a while, the set-up window is displayed.
Fig. 2.57
Go to the next window by clicking the "Next" button.
(3)
Selecting how to set up.
When you install this software for the first time, select the "Custom". When
the software is already installed, select the "Minimum". And for version-up,
select the "Minimum".
Fig. 2.58
If you select the "Custom", the all values of instrument adjustment file
are initialized. So select the "Minimum" when you do version-up.
When below window is displayed, click the "Next" button.
Fig. 2.59
(4) End
After finishing set-up, below window is displayed.
Fig. 2.60
(5) Note
When the EDX software before Ver. 1 .OO Re1.012 or of Ver 1 .OO Re1.012 is
installed, the "EDX" icon is newly made in "desk-top". If there is already the
"EDX icon in "desk-top", delete the "EDX icon before installing the
software.
5.5 Settings for Windows XP
Overvi ew
Here explains how to setup Windows XP for EDX.
Following settings are for better performance and for setting appearance to the
same as Windows 2000.
These setup is not having not set up so that it may be easy to manage, and surely,
not operating, unless it makes it this setup, when there are some troubles when there
is a certain question about PC from a user or.
These settings are set up so that it may be easy to manage when there is a question
about PC from a user, or when there are some troubles.
* means that it is a required setting.
For other items, you do not necessarily need to setup.
L i s t of settings
Here lists the items to be set. See the next section "Instruction for settings" for
how to set these items.
[General Settings]
1. Computer Name
*Computer Name edxpc
2. User Account
*Add "edx" user as Administrator.
Empty password and it never expires.
Default user is "edx" when logon.
Use "Welcome" screen.
3. LAN Settings
DHCP Do not use
IP Address 192.168.100.100
[Settings for edx user]
4. Display Properties
Theme Windows Classic
Background None
Screen Resolution 1024 X 768
Color Quality 16bit
*Font size Normal(96dpi)
5. Start Menu
Classic start menu
6. Control Panel
Switch to Classic View
7. Performance
Virtual Memory
Set about 1.5 times to real memory
Visual Effects
Adjust for best performance
Error Reporting
Disable
8. Windows Messenger
Do not run this program when Windows starts
Do not allow this program to run in the background
9. Power Options
*Power Schemes : Always ON
[Settings after EDX software installation]
10. Installing ASP1 driver
[EDX software Ver. l .OORe1.013 or later]
*Execute "c:XedxXdriverXaspi-v47 1Yinstall-xp.bat" to install ASP1 driver.
Ex e c u t e aspichkexe to check if the version of wnaspi32.dll is 4.71.2 or
not.
[EDX software Ver. l .OO Re1.0121
Floppy disk for Windows 2000 includes the above files.
Install ASP1 driver as the above.
1 1. Internet Explorer
Set initial page to "c:YedxXhelpYindex.html".
W Instruction for settings
Appearance of Control Panel is different in Windows2000 between WindowsXP.
So change appearance of Control Panel of WindowsXP to the same as
Windows2000.
Create "edx" first, because each user can have its own display settings.
A. User Accounts
A- 1. Add edx user
A-11. Shows "User Accounts" by the following operations.
Start Menu
Control Panel
User Accounts
A-1-2. In "User Accounts" window, click "Create a new account".
A- 1-3. Input "edx" in "Type a name for the new account".
Then click [Next].
A- 1-4. Pick an account type.
Select "Computer administrator". Then click [Create Account].
A-2. Log on as "edx" user
A-2-1. Log off from start menu.
A-2-2. Logon as edx user.
A-3. Set password
When you create a new "edx" user in A-l, settings will be the following.
Empty password
Password never expires
If you want to change or confirm the settings, operate as the following order.
[Control Panel is in Category View]
Start Menu
Control Panel
Performance and Maintenance
Administrative Tools in "or Pick a Control Panel icon"
Computer Management
Local Users and Groups
Users
edx
edx Properties
[Control Panel is in Classic View]
Start Menu
Control Panel
Administrative Tools
Computer Management
Local Users and Groups
Users
edx
edx Properties
A-4. Initial user
If only "edx" user exists, usually logon as "edx" user when Windows starts.
A-5. "Welcome" Screen
"Welcome screen" is enabled by default when you create "edx" user in A- l .
If you want to change or confirm the settings, operate as the following order.
Start Menu
Control Panel
User Accounts
Click "Change the way users log on or off".
Check "Use the Welcome screen" in "Select logon and logoff options".
( If the window for offline file settings appears, cancel it. )
B. Display Properties
B-1. Display Properties
Show "Display Properties" window by the following operation.
Show right-button-menu in the screen background and select "Properties".
Or the following operations also can show the "Display Properties" window.
[Control Panel is in Category View]
Control Panel
Appearance and Themes
"Display" in "or Pick a Control Panel icon"
[Control Panel is in Classic View]
Control Panel
Display
B-2. Select Theme
Select "Themes" tab in "Display Properties" window.
Then select "Windows Classic" in "Theme".
B-3. Background
Select "Desktop" tab in "Display Properties" window.
Then select "None" in "Background".
B-4. Resolution and color quality
Select "Settings" tab in "Display Properties" window.
Select " 1024x768" in "Screen resolution".
(You can select bigger resolution when you use LCD which has bigger
resolution than 1024x768.)
Select " 16-bit" in "Color quality".
(Software works in 24-bit mode or 32-bit mode. But if you use USB capture
cable, you must select 16-bit here.)
B-5. Font size
Select "Settings" tab in "Display Properties" window.
And click [Advanced].
In advanced window, select "General" tab.
Select "Normal size(96dpi)" in "DPI settings" of "Display".
And click [OK].
B-6. Apply changes
Click [OK] in "Display Properties" window to apply changes.
C. Control Panel Display
C- l . Switch to Classic View
Show "Control Panel" fiom Start menu.
Click "Switch to Classic View" at the left part of the Control Panel.
If "Switch to Classic View" or "Switch to Category View" is not displayed
at the left part of the Control Panel, the setting of "Show common tasks in
folders" might be disabled. To enable "Show common tasks in folders", select
"Tools" -- "Folder Options" -- "General tab".
D. Settings of Start Menu
D- l . Display Start Menu Properties
Select "Properties" in right-button-menu of "Start" to show "Taskbar and
Start Menu Properties" window.
Select "Classic Start menu" in "Start Menu'' tab.
Or you can show "Taskbar and Start Menu Properties" window from the
"Taskbar and Start Menu" of the "Control Panel".
Then select "Classic Start menu" in "Start Menu" tab.
E. Performance settings
E- l . System Properties
Display system properties from "System" of the "Control Panel".
E-2. Performance Settings
Select "Advanced" tab in "System Properties" window.
Then click [Settings] of "Performance" to show "Performance Options"
window.
Select "Adjust for best performance" in "Visual Effect" tab.
And click [OK].
E-3 .Virtual Memory
Then click [Change] of "Virtual Memory" to show "Virtual Memory"
window.
Select "custom size" and input "initial size" as about 1.5 times of real
memory.
And input "maximum size" as two times of "initial size".
(How to know the size of real memory)
The size of real memory is shown in the lower part of "System Properties".
But this value is less than the size of real memory in some hardware.
E-4. Error Reporting
Then click [Error Reporting] to show "Error Reporting" window.
Select "Disable error reporting" and select "But Notify me when critical
errors occur".
F. Power Options
F- l. Power Options
Click "Power Options" of the "Control Panel" to show "Power Options
Properties" window.
Select "Always On" of "Power Schemes" and click [OK].
G. Windows Messenger
G- l. Windows Messenger
If you find an icon of "Windows Messenger" from the lower right end of the
screen, click it to open "Windows Messenger". (In case of "<<" mark is
displayed in that region, some icons are hidden, so display all icons and check
them.)
If ".NET Passport Wizard" window appears, ignore and cancel it.
G-2. Settings of Windows Messenger
Select "Options" of "Tools" menu in Windows Messenger to open "Options"
window.
Select "Preference" tab and check off the first two items of "General".
"Run this program when Windows starts" -- OFF
"Allow this program to run in the background" - OFF
H. LAN settings
H- l. Network Connections
Open "Network Connections" window from "Network Connections" of
"Control Panel".
H-2. Local Area Connection Properties
Click "Local Area Connection" of "LAN of High-speed Internet" to open
"Local Area Connection Properties".
H-3. TCP/IP Settings
Double-click "Internet Protocol(TCP/IP)" in "General" tab.
Select "Use the following IP address" and input IP address.
I. Computer name
I- l. System Properties
Open "System Properties" from "System" of "Control Panel".
1-2. Computer name
Select "Computer Name
tt
tab.
Click [Change] of "To rename this computer or join a domain, click
Change".
Input computer name in "Computer Name Changes" window and click
[OK1
1-3. Restart
When you change computer name,
"You must restart this computer for the changes to take effect" message
appears.
Click [OK] here and click [OK] in "System Properties".
"Do you want to restart your computer now ?" message appears, then click
[Yes] to restart computer.
J. Install ASP1 driver
ASP1 driver must be installed before using EDX software.
EDX software Ver.l.OO Re1.013 includes installer of ASP1 driver, so install the
EDX software first.
J- 1. Install ASP1 driver
[EDX software Ver. 1 .OO Re1.013 or later]
Execute "c:XedxXdriverYaspi-v47 l%install-xp.batU to install ASP1 driver.
Execute aspichkexe to check if the version of wnaspi32.dll is 4.71.2 or not.
[EDX software Ver. l .OO Re1.0 121
Floppy disk for Windows 2000 includes the above files.
Install ASP1 driver as the above.
K. Internet Explorer Settings
K- l. Initial Page
Show right-button-menu at the icon of Internet Explorer and select
''Properties
tt
to open "Internet Options" window.
Select "General" tab and input "c:XedxXhelpXindex.html" in "Home Page".
Then click [OK].
M. Connection to EDX instrument
M- l . Recognition of EDX instrument
M- l - l . Found New Hardware Wizard
In case of EDX instrument is connected for the first time, system detects
EDX instrument as a new device and shows "Found New Hardware
Wizard".
M- 1-2. Select installation type
Select "Install from a list or specific location" and click [Next].
M- 1-3. Search and installation options
Select "Search for the best driver in these locations".
And check "Include this location in the search".
Then select a "c:XedxXdriver" directory from [Browse]. And click [Next].
M- 1-4. Finish installation
During the installation, Windows will give a warning that the driver does
passed the Windows Logo test, select "Continue Anyway".
Then the installation will complete.
M-2. Confirmation
If the installation successes, EDX-7001800 appears in the "Other device" as
"Device Manager" from "Hardware" of "System Properties".
N. Register a printer
You must register a printer for EDX software.
[Reference] Settings of Administrator (Normally you do not need to set.)
1. Logon as Administrator
When you set the above operations, you will not see the window for logon as
Administrator.
Normally you do not need logon as Administrator because "edx" user has
"Administrator" account type.
But there may be a case you have to logon as Administrator for trouble- shooting
or any reasons. You can logon as Admistrator as the following procedure.
Click "Change the way users log on or off' in "User Accounts" of "Control
Panel".
Turn off "Use the Welcome screen" in "Select logon and logoff options" and click
[Apply Options].
Select "Logoff' from Start Menu. Then "Log On to Windows" appears and you
can input logon name as "Administrator".
If "Logoff" menu does not appear in Start Menu, select "Shutdown" then select
"Logoff' in "Shut Down Windows".
[Reference21 Comparison Window style (English)
Default
Fig. 2.61
After changing styles
Fig. 2.62
5.6 EDX series
The EDX series are displayed as follows
It is EDX HS Series to which it was formally announced below the doublet by business report (200319126).
I I P/N I PM I Ai h me I Airfr;ime serial number seal I X-ray I X-ray filter I P/N of MCA I
ROM 1 ROM P/N I Fan guard to cool l
I for Japan I f;OE~gn I nameplate 1 I I outpit 1 -l 1 PCB As, I version I
Model name Number Thickness Polymera
tube
I
.
Custom-designed
EDX-900 (for I - I I EDX-900 I
Pannnn Tnr 1
EUA-aUU \ LE)
-
94
CUA-OUU CUA-OUU VL I J LJW LUUUl l Vl U
92
L.Ul
Custom-designed 212-22204-
2 12-22204- --a Custom-desipned - - - - - - - - , S 212-22525-
3.03B
212-22525-
I Q234 I 50w 1 1 0 1 MO l 97 1 4.00 1
I
Front, back, left and
212-29273 right sides (4 places)
EDX-700
(Standard)
EDX-800
(Standard)
EDX-900
(Standard)
EDX-700 (Custom-
designed HS)
EDX-800 (Custom-
designed HS)
EDX-900 (Custom-
designed HS)
EDX-700 (CE)
. . . . X7 "nn fr...\
Ll L- LYLLt Y
212-29271
CUA- I UUIlJ
2 12-22202-
9 1
212-22203-
91
212-22204-
0 1
212-22202-
98
212-22203-
98
212-22204-
08
-
(2 places)
right sides (4 places)
EDX-700HS
EDX-8OOHS
2 12-22202-
92
212-22203-
92
212-22204-
02
212-22202-
99
212-22203-
99
212-22204-
10
212-22202-
94
212-22203-
EDX-900HS
212-23702-
EDX-900HS EDX-900HS50 Q227 50w 20um MO
212-22525- , ,,, , , , ,,,,, Front, back, left and
212-23702
o1 95
212-23700
212-23701
EDx-700
EDx-800
EDx-900
EDX-700
EDX-800
EDx-900
EDx-700
,,, ,,,
212-23700-
o1
212-23701- o1
EDX-700
EDX-800
EDX-900
EDX-700HS
EDX-8OOHS
EDX-900HS
EDX-700
FT\- onn
EDX-700HS
EDX-800HS
Q207
Q208
Q209
Q223
Q224
Q212
nnqq
EDX-700HS50
EDX-800HS50
25w
25w
25w
45w
4 5 ~
45w
25w
* C___
Q225
Q226
of NI filter
2Oum
20um
20um
20um
20um
2Oum
20um
-R___
5 0 ~
50w
Mn
MO
MO
MO
MO
M0
MO
MO
20um
20um
212-22525-
9 1
212-22525-
9 1
212-22525-
93
212-22525-
98
212-22525-
98
212-22525-
99
212-22525-
92
212-22525-
MO
( 1 2 5 ~ )
MO
3.03
1.09A
1.09A
3.03A
2.01
, ,,
212-22525-
94
212-22525-
94
212-29225-
91
212-29225-
91
212-29265
212-29266
212-29266
212-29267
212-29249
, , , ,,,,,
1.U3.D
1.09B
Front and back sides
(2 places)
(2 places)
(2
(2
laces
(2
l_
Ll L- LYLI V
212-29270
About the identification of the instrument
In the case of "700" case, it is not possible to distinguish Standard EDX and
custom-designed HS, using the name plate attached with the lid of sample compartment.
Identify it by confirming type-identifier that has been described to the airfiame
number seal.
In the case of standard EDX-700, "EDX-700" as type-identifier is written on the
airframe number seal. In the case of custom-designed EDX-700 HS, "EDX-700HS" as
type-identifier is written on the airfi-ame number seal.
Difference of instruments
X-ray output
A special type for 45W and the HS specification and Canon Inc. is 50W output
in a standard type to 25W and request for price quotation HS specifications as
understood fiom the above-mentioned table.
Standard instruments are 25 W, custom-designed HS instruments are 45 W and
both HS and custom-designed HS for Cannon Inc. are 50W as understood from
the above-mentioned table.
Airfiame nameplate
The airframe nameplate becomes HS from HS.
Airframe number seal
It identifies it as shown in the above-mentioned table as it becomes easy to
identifl.
Thickness of Ni filter
In a custom-designed instrument for Canon Inc., the thickness of the Ni filter is
100um. The setting is set on the eu3 window. Refer to "Setting of environmental
setting eu3 at 2.5.2 installations" for the use of eu3.
There are about five instruments that are adopted lOOum for the Ni filter
besides custom-designed instruments for Canon Inc. in custom-designed HS
produced at the early times.
(The corresponding instruments are below. It is necessary to note the instruments
before and behind that for attention though it is considerably thought the accurate
intelligence. )
However, the lOOum filter absorbs X rays much stronger than the 20um filter.
So the intensity of X-rays may not be enough to measure Cd or Pb. We again
changed from the 100um filter to the 20um filter.
I think that there is a customer who changes the Ni filter from 100urn to 20um.
EDX-700 Q20741000446, 447
EDX-700 (request for price quotation HS specification) Q2234 100000 1-3
MO filter
The latter products of a standard type and HS use the MO filter instead of the
Polymer filter. Below instruments numbers display the numbers of the latter
products of a standard type.
a MCAPCB Assy
It is not possible to change a setting of an X-ray maximum output by using
software only. The ROM must be changed to raise the X-ray power. Confirm
using the upper table in the details. Therefore, if you exchange MCA PCB Assy,
the ROM loaded on the broken PCB may be used.
If the MCA PCB Assy of HS specification breaks down and the new MCA
PCB Assy loads the ROM of standard specification, the maximum output
becomes 50Wa25W regardless of the setting of the maximum output by eu3
(software).
Fan guard for tube cooling
If the X-ray output is 25W7 fan guard is none. If 45W, fan guard are the back
and forth (two places). If 50W, fan guard is the front, back, left and right (four
places). Adding fan guard raises the air volume. I think that you consent upper if
you see the instrument though it becomes such this expression in the word.
About the custom-designed instrument of EDX-900 for Canon Inc.
The following work is separately done compared with standard 900.
1)
To adjust the X-ray tube output to 50W or less, ROM is assumed to be
3.03B.
2)
The leakage inspection of X-rays is executed by 50W output.
3)
The added guards of right and left make the temperature raise of tube
cooled.
4)
A special inspection is executed. The calibration curve is made with the Cd
standard samples and the lower limit of detection is found. Moreover,
repeatability is confirmed.
5)
The result of a special inspection is appended to the device.
6)
The calibration curve group made at 4) is copied in the Device Information
sheet disk.
When installing, the inspection similar to 4) is done. So use the calibration
curve group then. Moreover, the data of the inspection in the factory becomes
reference when installing.
7)
X-ray output (50W) and filter (Ni:lOOum) are set by device environment
setting software, "eu3 " .
(When installing, it is necessary to set the setting of an X-ray output again.)
8)
Device type-identifier of the instrument number seal is assumed to be
custom-designed EDX-900 type.
About notes when installing
Using device environment setting software, "eu3" sets the maximum value of
X-ray output.
And, please confirm the kind and the thickness about the setting of the filter. (If
HS, the filter is MO and the thickness of Ni filter is 20um.)
See the "2.5.2 Environment utility "eu3" setting" about "eu3".
1) Chapter 3 Consumable and Maintenance Parts )I
1. 1 EDX Assembling structure (EDX-700HS El800HS E) .................................................... 3 - 2
.................................................................... 1.2 EDX Assembling structure (EDX-900HS E) 3 - 4
1.3 EDX Assembling structure (EDX-700HS CE1800HS CE) ........................................ 3 - 6
................................................................. 1.4 EDX Assembling structure (EDX-900HS CE) 3 - 8
2 . Consumables List ............................................................................................................ 3 - 10
.................................................................................................... 3 . Maintenance Parts List 3 - 11
1 .l EDX Assembling structure (EDX-7OOHS E1800HS E)
EDX-700HS/800HS(Assembling structure)
2 12-22209-04
-
EDX I1S WI N
I N T ASSY
A 212-22210-01 3 A 2 12-222 12-04
PCDASR ASSY 11s
1 PC FAN ASQY E
A 212-22225 A 2 12-22650-91
PC MEASIJMENT 1 PC SAMPIX 130\57, WELDING ASY
CI umvx ASSY
A 212-22236
I PC SENSOR ASSY(%,SB)
A 212-22237 F
1 PC SENSORASSY(S10)
A 212-22240 3
A 212-22241.
PC CCIVER OPENING A S Y
' ~ C P C C O V E R WEJ ,111NC.r ASSY
A 2 12-22300
"-"""""
PC SHUTTER FIL'I'EI2 ASSY
A 2 12-22450-9 l
-
PC WAR PANEL ASSY
A 212-22550-92
-
WIIUNG DIAGRAM
A 212-22620
K 5 0 W 50W INVERTER
ASSY
A 212-22529-91
-
1 PC C'I'E PCB ASSY
A 21 2-22SS-!N
-
1 PC W A PCU ASSY EIS
A 212-22533-91
I PC AMI) PC13 ASSY
31 A 212-2235
1 PC SENSOR ASSYfS7,SS)
3 A 212-22212
1 Yil FAN ASSY
FOR XRM GROUNIlING
3 2 12-22598-9 1
CABLE ASSY 13
3 212-22599-91
CALIIX ASSY 14
3 2 12-22600-91
CAWE ASSY 15
3 212-22601-91
CABLE ASSY 1 G
3 212-221@2-9 1
CABLE ASSY 17
3 212-22603-91
CABLE ASSY 18
- #
2 12-22Cfi3-92
CABLE ASSY 19
3 2 12-22604-9 1
CAR1.E ASSY 20
3 232-22Cfi5-91
CAll1.f: ASSY 21
3 2 12-22(i06-9 1
CARIX A S Y 22
3 2 12-22607-91
CABI'F, ASSY 23
3 212-2261 5-91
I PC SCSI CA131,E FOR BDX
A 212-22621
-f--T- I PL > O N KWEK.RTER PCB ASSI'
A 212-22470
Ec o VER ASSY
A 2 3 2-22575-9 1
-
A 212-22537-91
1 PC POWER SUPPLY ASSY
A 212-22576-91
A 21 2-22590-91
I PC TRANSFOMLR ASSY
3 't A 212-22588-91
1 PC POWER SUl'I'LY
WI KING IIXOIIAM
A 2 12-22552-91
-
3 A 212-22557
1 PC CONTROL UNIT
1 W 13RACKF1'4 ASSY
CFIMSIS ASSY
1 PC PANEL El3ASSY
A 2 1 2-22490-9 1
-
A 2 12-2 1650-02
1'C EDX STANllAK1> KIT
1 PC S'I'ANIMRD SAMPIX ASSY SIR32
A 2212-216513-17
l PC STANDARD SAW1 ,E ASSY A73)
A 2 12-22687-9 1
1 IT LIQUID SAMI'IE AIIAP'WK
A 202-85501 -55 E I I)(: MILER
A 212-22W-91 2 A212-2241-91
A 2 12-22567-9 1
PC DE'TEC'TOR ASSY
1 I T l'lU3AMPLIFIEK ASSY
1 PC PWAM13LIFIER KB ASSY
(FOR 700) A 212-22402-91
2 2 2-22400-92
1 PC CONNECVXnK Fl ANOE ASSY
I)EI'I~C?'OK ASSY
F A 2 1 2-22566-9 1
{FOR 800) 1 PC PML~MYI~IFIER
2 A 212-22407-91 WIRING IIIGRAM
~ P C ~ ~ T E C ' T I N G IXNtT
2 A212-22421-91 3 A 21 2-22322-92
1 PC JOINT HANGH ASSY HI.: 1 K JOINT FLANGl:'
(FOR 700) WEX.1IING ASSY
21 2-2242 1 -92
IODiTI:LANGE ASSY tl' l W (FOR 800)
2 A 212-22427-91
-
1 re VAI , ~ : FLANGE ASSY
2 A 212-22429-91
~ w F K I W ~ WIRE ASSY
2 A 212-22439-93
~ W I N I X ) W CAP ASSY
2 A212-22719-91
P A C K A G E IIE'IXCTOIl
A 212-225 10-93 A 212-22510
~ Dx P - 7 OOE ASSY
EOX X>AVI'A P1tOCBSSINli ASSY E
A 2 12-29232-9 1
1 PC 13XP-70E MIUIA ASSY
A 212-29769-91 E
1 PC 11x1'-7001' 1XISTRIIC'IION KI T
A 212-22512-91
-
I PC El3X 1)EVICE f;l,CtPPY ASSY
A 212-22219-91
1.2 EDX Assembling structure (EDX-9OOHS E)
EDX-900HS(Assembling structure)
3 A 2 12-222 12-04
1 PC FAN ASSY 11
3 A 2 12-22650-71
2
2
2
2
2
2
2
2
3 1 A 2 12-22237
1 PC SENSOR ASSY(SI0)
3 A 212-22241
=COVER WEI.DWG ASSY
C
-
11
1
-
l
-
I 5 5 0 k V SOWINVERTER
ASSY
A 212-22529-91
1 PC CTRL PCN ASSY
A 232-22525-95
~ M C A PCU ASSY 9001iS
A 212-22885-91
1 PC S10 K W ASSY
1 PC MCYI'OR ASSY
3 A 212-22364
(SYCW'I'EIZI FIL'TEK PLATE ASSY
. ,
3 L A 212-22395
1 PC SENSOR ASSYW7Sg)
3 1.3 2 12-22212
1 PC FAN ASSY
31 A 212-22615-91
1 PC SCSl CABLE FOR EllX
A 212-22621
NYER7'lR PCA ASRY
A 212-22470
I'CC'OVI:R ASSY
A 212-22575-91 A 212-22537-91
I PC ITIWER SIIPIJI,Y ASSY l I'C 1's PCB ASSY
A 2 12-22576-9 1
l 1%CASE ASSY
A 212-22471
I PC COVHl (COVER)
A 212-22472
-
I 1'0 COVER (~mmt')
A 212-22473
-
1 IT COVER (arorrr)
A 2 12-22474
-
I X' C CC)VX (X,! 'F7)
A 2 1 2-22475
I I'C COVER (IPPI3K)
A 21 2-22476
-
I PC COVER
A 2 12-2247'7
1 I T TA131X l:K/\hE
A 212-22571-9I
I PC PANX!I, t'CH ASSY
1.3 EDX Assembling structure (EDX-700HS CE1800HS CE)
EDX-700HS/800HS(Assembling structure)
A 2 12-22300
1 PC SEJUTlER FIL'IEK ASSY
t
3 A 2 12-22212-04
1 PC FAN ASSY E
2
2
2
3 A 212-22241
ICCOWR WEI.,DRJCr ASSY
A 212-22450-YI
1 PC WAK PANEL ASSY
A 2 12-22550-91
WIRING IIIAGIZAM
A 212-22620
A 212-22250
2 PC SFSTSOR hSSY
3 A 212-22390
'k 1 PC MO'I'OR ASSY
1 PC 5OkV SOW MVERTEK
ASSY
3
I PC SENSOR ASSYfS7,SS)
3 A 2 12-22212
1 PC FAN ASSY
A 212-22550
WIKINC IIIAGIUM
A 2 12-22595-06
1 PC CABLE ASSY
FOR XRM GROWI NG
A 2 12-22598-91
I PC CABLE ASSY 13
h 2 I2-22W-9l
l PC CABLE ASSY l4
3 A 2 12-22600-9 1
1 PC CAt3LE ASSY 15
I PC SCST CABLE FOR EllX
A 212-2262]
INVERTER PCB ASSY
3 1 A 21 2-22630
1 PC 50kV CASCADE ASSY
A 212-22471)
ITCOVfiN ASSY
( 2 lZ-23O80
1 PC CE IEIvlODEJJNG KIT
2 A 212-22471
~ C O W , k (COVER)
A 2 12-22472
1 PC C O I ~ (FRONT)
A 2 12-22473
-
1 PC COViiK (IUtiIl'l')
A 212-22474
-
1 PC COW'K (1,EFl.)
A 2 32-22475
1 PC COVER ( IIIYBK)
A 2 12-22476
-
1 PC COVER
A 2 12-22477
1 PC 'CAI3XE FRAME
A 212-22371-91
I PC PANEL I'CR ASSY
3 A 212-22537-91
IPS PCB ASSY
3 A 212-22557
1 X BKACWX 4 ASSY
R 212-2251043 2 A212-22510
1 1YDXP-7Wfi ASSY -EDX UrZ'I'A PIIOCESSING ASSY I!
l .4 EDX Assembling structure (EDX-9OOHS CE)
EDX-900HS(Assembling structure)
lJMT ASSY
A 212-22210-01
PCDAST! ASSY I IS
A 212-22225
PCmm~mr
C1 IAMBER ASSY
A 212-22240
-
PC COVET\. OPmVXNO ASSY
(AUTOMATIC)
A 2 12-22620
ETsnw sow INVERTER
ASSY
A 212-23010-91
K C ~ ' I % L ~ K13 ASSY
3 A 2 12-22212-04
1 PC FAN ASSY E
3 A 212-22241
~ C O W R WF;I.,DXNCI ASSY
A 212-22391
1 PC MUI'OR ASSY(h42) 'l-
3 ( A 212-22'395
l PC SENSOR ASSY(S7S8)
3 A 212-22212
1 PC FAN ASS Y
3 1 A 212-22630
1 PC 5OkV CASCADE ASSY
A 2 12-23035
-
A 212-22537-91
1 PC POWER SUPPLY2 ASSY 1 PC PS PCR ASSY
A 2 12-22576-9 1
1 PC CASE ASSY
A 2 12-22590-91
1 PC TRANSFOMER ASSY
A 212-22588-91
1 PC POWER SUPPLY
WRMG DIGRAM
A 2 12-23003
-
3 A 2 12-22557
1 PC CONTIiQL UNIT
1 PC BRACKET 4 ASSY
CHASSIS ASSY
A 212-22470
-
PC COVER ASSY
A 2 i 2-22490-9 1
A 212-22510-93
-
1 PC DXP fTS E ASSY
[[ 1 PC COVER 212-22471 (COVER)
A 21 2-22472
1 PC COVER (FRONT)
A 212-22473
1 PC COVER (RIGHT)
A 2 12-22474
I PC COVER (LEFT)
A 21 2-22475
t IJC COVER (Ul'PI'R)
A 21 2-22476
1 IT COVER
2 A 212-22477
1 PC' TA1 ?I ,l 3 12RrZMI'
2 A 212-22571-91
A 212-22512-91
1 PC EDX IXVICE FI.OF'PY ASSY
2. Consumables List
Standard unit
ShutterIFilter ASSY 2 12-22300
Cover open/close ASSY 2 12-22240
Parts name I PIN I Remarks I
I 1 I Grease, silicon H.V.G. 57G 1 0 17-308 12-0 1 1 1 pclyear, Grease for vacuum I
No.
1
2
Option unit
PIN
0 17-27014-05
2 12-22688
Parts name
LG grease
Leadnut
Remarks
1 pclyear, Molykote grease
2 pcs17 year
Vacuum exhaust unit 2 12-22460
Small sample cover 2 12-22290
4 types collimator automatic change-over unit 21 2-22320
I No. I Parts name I PIN I Remarks I
No.
1
2
3
PIN
017-30163-01
040-82712 .
036-15502-78
Parts name
RP oil, Ultragate 19
MS, FCT-150-20
0 ring, AS568A-278-1A
No.
1
Remarks
1 pc16 months
Oil mist trap
1 pclyear, 0 ring for cover of analysis chamber
PIN
01 7-308 12-01
Parts name
Grease, silicon H.V.G 57G
1
Remarks
1 pclyear, Grease for vacuum
Grease, silicon H.V.G 57G 1 017-30812-01 1 l pclyear
3. Maintenance Parts List
Base ASSY 2 12-222 10-0 1
I No. I Parts name I PIN I Remarks I
Measuring chamber 2 12-22225
1
2
3
4
5
6
1 2 1 Sensor ASSY (S6, S9)
FanASSY E
Fan, 9 6 12246402
Rubber foot, UK- 12
Driver, CSD2 1 12-P
Socket, relay PYF08A
Amplifier. E2C-GE4A
No.
1
1 3 I Sensor. E2C-X1A 1 066-81532
1 4 1 Plug. socket CN-834-7 1 071-60645
2 12-222 12-04
042-60475 11
037-30023-04
077-79704-92
070-73013-01
066-8 1532- 12
Parts name
Sample bowl welding ASSY
1 5 1 Switch. micro S-5GL-2A 1 064-33003
For cooling of X-ray tube
Rubber foot for EDX main unit
For shutter and filter
For detection of liquid sample
For detection of liauid sample
PIN
2 12-22650-91
1 14 1 Fastner seal, DS-1-4SUS 1 036-2220 1-01
6
7
8
9
10
11
12
13
1 15 1 Grease. silicon H.V.G 57G 1 017-30812-01
1 16 I Hose. spring l 5 x 22 1 035-91091-06
Sensor ASSY (S10)
Sensor, FRIEBC
Amplifier, F2R
X-ray tube, XTF-501 1A
PB- l Pirani tube filament
0 ring, 1A P12.5
0 ring, 1A P6
0 ring, 1A G40
1 17 1 Hose clamn 22 1 037-61002
2 12-22237
070-70630-1 1
070-70630-01
219-91001
200-47686
036-10214
036- l0204
036- l2004
p-
Remarks
Sample vlate (standard)
19
20
21
S6: Shutter close,
S9: For liquid sample adapter detection
Valve, check CV-1-0.01
Thermal switch ASSY
Sensitivity switch, TR-50B-50
S6: Shutter close I
040-045 1 1-7 1
212-22613-91
2 19-9200 1-0 1
Pirani filament
For shutterlfilter shaft
Fix turret unit I
For fixing detector I
For vacuum seal I
For vacuum hose main unit (700 mm) I
For vacuum hose main unit I
Cover openlclose ASSY 2 12-22240
3
4
5
6
7
8
9
10
11
12
13
14
ShutterIFilter ASSY 2 12-22300
Remarks
Cover close detecting sensor (Left and right, 2 pcs)
15
16
17
18
19
20
21
Parts name
Shutterlfilter plate ASSY 2 12-22364
212-22391
Motor, PK245-01A 077-79099-55
PIN
212-22287-01
064-33805-01
No.
1
2
Sensor ASSY S4R
Sensor ASSY S4L
Photo interrupter
Timing pulley 1
Collar, SCS15-12
Timing pulley 2
Lock ring PT008 X 021RE.S
Lead nut
Motor ASSY
Motor, 5RK60A-AF
Sensor ASSY NC
Sensor, SS-5GL2-F
4 1 Sensor ASSY 6 7 . S8) 1 212-22395
Parts name
Sensor ASSY NO
Sensor, SS-5GL2-F
Ball bush, SMK20W
Shaft clamp, SHF20
BRG, DDRF- 1980HHR
BRG, DDRF-228OHHR
Screw, TM16 X 3-L394
0 ring, AS568A-278-1A
Timing belt, 396 X T9.5
5 1 Photo interrunter. TLP1 OO6A 1 06 1-7 15 1 8-04
212-22250-0 1
2 12-22250-02
061-71518-03
212-2225 1
026-68003-1 6
2 12-22252
032-47205-03
212-22688
212-22390
077-40391-01
2 12-22287-02
064-33805-0 1
Cover tilting detecting sensor (Right)
Cover tilting detecting sensor (Left)
For cover opedclose motor
Cover opedclose screw unit (2 pcs)
Cover opedclose screw unit (2 pcs)
2 pcs17 years
Cover opedclose motor
Cover open detecting sensor
03 1-41235-06
03 1-690 12-05
03 1-20624
03 1-20423
219-83029
036-15502-78
032-22870-03
Remarks
Cover opedclose shaft unit (upper)
Cover opedclose shaft unit (lower)
Cover openlclose screw unit (upper)
Cover opedclose screw unit (lower)
Screw
0 ring for cover sample chamber
Timing belt for cover open/close
6
7
8
9
--
Motor for shutterlfilter
S7: Origin, S8: Limit
S7: Origin
S8: Limit Photo interrupter, TLP-1007A
Oring 1AP6
Belt, 106M X L6.4
Sensor ASSY (S6,S9)
0 ring for shutterlfilter shaft (2 pcs)
061-715 18-03
036-10204
032-21922-03
2 12-22236
Timing belt for shutterlfilter
S6:Shutter close
S9:Liauid sample adapter detecting
Rear panel ASSY 2 12-22450-91
No.
1
2
3
4
5
50KV50W Inverter ASSY 212-22620
20 1 LED, GL-8KG21 1 061-78044-01 I D l (POWER)
I I I
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Parts name
Fan guard T30F
FanASSY F
Fan, 9G1224G402
SCSI cable, for EDX
Ferrite, SCF-8
Remarks
Inverter power (Shimadzu)
Shimadzu inverter
No.
1
2
2 1 LED, GL8HY2 1
PIN
042-609 14-05
2 12-222 12-05
042-60452-08
212-22615-91
075-08032-04
Parts name
50KV50W ASSY for exchange
50KV Inverter ASSY Okl type
Remarks
For EDX-700HS E1800HS El900HS E
For EDX-700HS CEl800HS CEl900HS CE
For EDX-700HS EI800HS El900HS E
MCA ROM for EDX-700HS E/8OOHS E
MCA ROM for EDX-900HS CE
MCA ROM for EDX-700HS CE 1800HS CE
MCA ROM for EDX-900HS CE
For EDX-700HS CEJSOOHS CEl900HS CE
F1, F2 (for vacuum pump)
F3, F4
F5, F6 (k 24V DC)
F7, F8 (k 15V DC)
Buttons only for panel
BZ l (BUZZER)
Parts name
CTRLPCBASSY
CTRL2 PCB ASSY
MCA PCB ASSY HS
MCA HS ROM ASSY
MCA 900HS ROM ASSY
MCA HSCE ROM ASSY
MCA 900HS ROM ASSY
IC, M27C512-15F1
AMPPCBASSY
POWER SUPPLY ASSY
POWER SUPPLY2 ASSY
PS PCBASSY
Fuse, 216 010
Fuse, 218 3.15
Fuse, DMlO
Fuse, DM32 3.2A
PANEL PCB ASSY
Button, LZlllO
BUZZER, TMB-05
22
23
24
25
26
27
28
29
Remarks
For cooling of power supply unit
Connection cable between EDX main unit and data
vrocessing svstem
Ferrite core
PIN
212-22619
212-22620-88
PIN
212-22529-91
2 12-2301 0-91
212-22525-94
212-29270
212-29271
2 12-29272
212-29273
075-26458-02
212-22533-91
212-22575-91
21 9-85000-5 1
212-22537-91
072-02004-26
072-02004-21
072-013 19-03
072-013 19-06
212-22571-91
064-53205-14
078-20159-01
,
LED, GL-8KG21
LED, GL-8KG21
LED, GL-8KG21
LED, GL-8HD21
SW, LTM-01
SW, LTM-01
SW, LTM-01
SW, LTM-01
061-78044-01
061 -78044-0 1
061-78044-01
061-78044-05
064-53205-05
064-53205-05
064-53205-05
064-53205-05
D 3 (SHUTTER CLOSE)
D 4 (READY)
D 5 (LIQUID MODE)
D 6 (ERROR)
S l (CLOSE)
S 2 (START)
S 3 (OPEN)
S 4 (STOP)
2 1 Cover (fiont) 1 212-22472
Cover ASSY
5 1 Cover (upper) 2 12-22475
No.
1
3
4
EDX standard kit 2 12-22490-9 1
PIN
2 12-2247 1
Parts name
Cover (cover)
No. I Parts name
Remarks
Cover (right)
Cover (left)
1 Standard sample, SUS
2 Standard sample, A1
3 Driver
4 Liquid sample adapter ASSY
5 Sample container, 3527 large quantity
6 Samele container. 3529
2 12-22473
2 12-22474
7 1 Sarnele container. 3561 with color
8 1 Samde container. 3577 trace auantitv
9 1 Sam~l e container. 3571 oDen
10 Mylor 6mm
l l Handle
Remarks I
Standard sample (SUS)
Samvle container lOOPCs I
500 sheets I
Grease for vacuum
Oil brush I
73mm (width) X 92m role
Detector ASSY (EDX-700HS EI700HS CEI800HS El800HS CE)
No.
-
1
-
2
3
4
-
5
-
6
Parts name I PIN 1 Remarks
Detector ASSY
Detector ASSY
0 ring. 1A V34 1 036-13003 I Insulation bush unit
Detector ASSY
Detector ASSY
Insulation bush
Bush
0 ring, lAPlO
2 12-22400-92
2 12-22400-88
Detector ASSY (EDX-900HS El900HS CE)
For EDX-800HS El800HS CE
O/H ASSY
2 12-22400-9 1
2 12-22400-87
2 12-22435
212-22707
036-1 0208
0 ring, 1A P6
Svacer
for EDX-800HS El800HS CE
OlH ASSY
for EDX-700HS El700HS CE
For fixing detector (2 pcs)
Detector side to bush (2 pcs)
036-10204
212-22708
No. I Parts name
1
Fastener seal, DS- 1H-6
Analysis side to bush (2 pcs)
Insulation bush side
1
2
3
Sample compartment side to
bush (2PCs)
PIN
Other
Remarks
X-ray detector D3 12-130-50
0-ring,lAPlO
0-ring, 1A V34
I No. I Parts name I PIN I Remarks
239-45300
036-10208
036-13003
8 1 EDX device floppy ASSY 1 212-22512-91 I Characteristics information of device (l sheet)
Detector side to bush (2PCs)
0 ring of bush part for heat
insulation
1
2
3
4
5
6
7
1 9 1 MOLY-LG Grease. Cartridge 1 017-27014-05 1 MOLYKOTE
1 10 1 Grease. Silicone H.V.G 57G 1 017-30812-01 1 Grease for vacuum
DXP-700 media ASSY
EDX-HS instruction manual
Label, EDX-800HS
Label, EDX-800HS
Name Plate, EDX-900HS
Cap
BOX, EDX
2 12-29232-9 1
305-32102
212-21057-37
212-21057-36
212-21057-38
2 12-22652-01
2 12-22698
EDX program sheet (4 sheets)
Instruction manual
Label (EDX-800HS50)
Label (EDX-700HS50)
Name Plate (EX-900HS50)
Cap of detector
BOX
Vacuum exhaust unit 2 12-22460
~- - - ~ - -
No. I Parts name
1
2
PIN
3
4
5
Sample for FP Sensitivity Coefficient
Remarks
RV3
RV3
6
7
8
9
10
RV31-lOOVR.PO/H
RP oil, Ultragate 19
Bonded valve ASSY (V1)
5 l Siwafer 1 017-47005-01 1 I
042-00 146-0 1
042-00146-1 1
EFM 10
MS, FCT-150-20
Centering, KF25 18327
Clamp NW20125954-7886
Fuse, 218 010
No.
1
2
3
4
6 1 Sample, press Na2S04 1 212-22704-94
I
AC lOOV
AC l OOV with a mist trap (EFM- 10)
210-14120-87
017-30163-01
2 12-22467
for Overhaul
Oil for pump
Leak valve for ~o we r failure
042-00124-32
040-82712
035-02404-04
035-29414-03
072-02004-26
Parts name
Standard Sample set FP
SamplePETE
Sample, press CaC03
Samde. bead A1701
Auto Selection Unit of 4 Types of Collimators 212-22320, -03
Mist-filter
Oil mist trap
F1, F2 (2 pcs)
7
8
9
10
11
12
13
14
15
PIN
2 12-22706-92
2 12-2248 1-07
212-22704-93
212-22705-91
1 I Sensor ASSY (S2 1, S22) 1 212-22396 I S2 1 :origin, S22:limitation
l
Remarks
14 Sample set for FP Sensitivity Coefficient
Sample, press KH2P04
Sample, press NaCl
Sample Ti
Sample SUS
Sample Cu
Sample, press Zr02
Sample Sn
Sample, press BaC03
Sample Pb
Parts name
1 2 I Belt. 106MXL6.4 1 032-21922-03 1 I
212-22704-95
2 12-22704-98
212-22653-9 1
2 12-2248 1-0 1
2 12-2248 1-04
2 12-22704-96
212-22481-08
2 12-22704-97
212-22653-93
1 3 I Motor ASSY (M1 1) 1 212-22391-01 1 I
I
PIN
4 l 0 ~ i n ~ lAP6 1 036-10204 I Collimator Shaft 0 Ring (2 pieces) I
Remarks
Turret Drive Unit 2 12-22685-91
No. I Parts name I PIN I Remarks I
1
2
3
4
5
6
Motor ASSY (M12)
Sensor ASSY S23
Sensor ASSY S24
Helium Purge Unit 2 12-22495
-
0 Ring, 1AP6
Ring
Sensor ASSY (S10)
2
3
4
2 12-22392
212-22344-91
2 12-22344-92
No.
1
Cover for small samples 2 12-22290
X-ray polot lamp 212-22454, -01
Origin
Limitation
036-1021 1
2 12-22694
2 12-22237
PIN
040-7201 6-52
Parts name
Regulator, YBR-250 1 CGA
Flow Meter, RK1650- 100B-*
TaigonT3/32~1/32~5/32
Vinyl hose, 6x2 CL
Sample Observation Camera Unit 2 12-22750-94
S 10:Amplifier for detecting liquid sample
disk.
Remarks
Remarks No.
1
080-685 16- 18
016-3 1425
016-31329
No.
1
2
No.
l
Piping in Sample Compartment
Connecting Regulator and Helium Purge main
unit
Parts name
0 Ring, 1A G75
PIN
212-22753-01
046-6 1824-0 1
Parts name
Window
Camera, CCD GP-KX12 1
PIN
036-12012
Remarks
Parts name
Lamp, For MS-12
PIN
062-6202 1-01
Remarks
Chapter 4 Electronical Circuit Diagram
Fig. 4.1.1
Fig. 4.1.2
Fig. 4.1.3
Fig. 4.1.4
Fig. 4.1.5
Fig. 4.1.6
Fig. 4.1.7
Fig. 4.1.8
Fig. 4.2
Fig. 4.3
Fig. 4.4
Fig. 4.5.1
Fig. 4.5.2
Fig. 4.6.1
Fig. 4.6.2
Fig. 4.7.1
Fig. 4.7.2
Fig. 4.7.3
Fig. 4.7.4
Fig. 4.7.5
WIRING (Standard)
WIRING (Standard)
WIRING (Standard)
WIRING (Standard)
WIRING (CE)
WIRING (CE)
WIRING (CE)
WIRING (CE)
PREAMP PCB ASSY
PREAMP PCB
PREAMP WIRING
50KV INVERTER
SCHEMATIC
50KV CASCADE
SCHEMATIC
CTRL PCB ASSY
CTRL2 PCB ASSY
CTRL PCB SCHEMATIC
(Standard)
CTRL PCB SCHEMATIC
(Standard)
CTRL PCB SCHEMATIC
(Standard)
CTRL PCB SCHEMATIC
(Standard)
CTRL PCB SCHEMATIC
(Standard)
Fig. 4.7.6
Fig. 4.7.7
Fig. 4.7.8
Fig. 4.7.9
Fig. 4.7.10
Fig. 4.7.1 1
Fig. 4.8
Fig. 4.9.1
Fig. 4.9.2
Fig. 4.10
Fig. 4.11.1
Fig. 4.11.2
Fig. 4.11.3
Fig. 4.12
Fig. 4.13.1
Fig. 4.13.2
Fig. 4.13.3
Fig. 4.14.1
Fig. 4.14.2
Fig. 4.15
Fig. 4.16
Fig. 4.17
CTRL PCB SCHEMATIC
(Standard)
CTRL2, PCB
SCHEMATIC (CE)
CTRL2, PCB
SCHEMATIC (CE)
CTRL2, PCB
SCHEMATIC (CE)
CTRL2, PCB
SCHEMATIC (CE)
CTRL2, PCB
SCHEMATIC (CE)
MCA PCB ASSY
MCA PCB SCHEMATIC
MCA PCB SCHEMATIC
AMP PCB ASSY
AMP PCB SCHEMATIC
AMP PCB SCHEMATIC
AMP PCB SCHEMATIC
PS PCB ASSY
PS PCB SCHEMATIC
PS PCB SCHEMATIC
PS PCB SCHEMATIC
POWER SUPPLY WIRING
(Standard)
POWER SUPPLY WIRING
(CE)
PANEL PCB ASSY
PANEL PCB SCHEMATIC
S10 PCB ASSY
Fig. 4.18 S10 PCB SCHEMATIC
X-Rr/ Tube
XTFSDl IA
Fan
-
Fig. 4.1.1 WIRING (Standard) 212-22550 (114)
4 - 3 - 4
I I I I I " i I I l l I I I
--
L i d h;+ SW t N3
I
Fan - Lid t$-br
- :q
4 - 5 - 6
Fig. 4.1.3 WIRING (Standard) 21 2-22550 (314)
4 - 7 - 8
4 - 9 - 1 0
Fig. 4.1.5 WIRING (CE) 212-23050 (114)
4 - 11 - 12
I/ Attached Cable
CABLE ASSY 101
CSO2Il2-P
Fig. 4.1.6 WIRING (CE) 212-23050 (214)
4 - 13 - 14
n n n n n 1-4
Fig. 4.1.7 WIRING (CE) 21 2-23050 (314)
4 - 15 - 16
Fig. 4.1.8 WIRING (CE) 212-23050 (414)
4 - 17 - 18
--
--L-
L 3 C24
---I
( ~ 4 ) @SH I MADZU
us
MADE I N JAPAN
Fig. 4.2 PREAMP PCB ASSY 212-22567 (111)
--
--L-
'L - C24
--d
CJ4> R43 ~ S H I M A D Z U
us c25 MADE IN JAPAN
Fig. 4.2 PREAMP PCB ASSY 212-22567 ( I l l )
J2
INHIBIT
Fig. 4.3 PREAMP PCB 212-22570 (111)
4 - 21 - 22
HERMFiTC SEAL
P I N 1 CYV)
DETAIL l3
212- 2256'7 REAMP PC8 ASSY
I
DETAIL 8
-
=P@
DETAIL E
76
OUT
52
m1 eIT
33
PowER
SUPPLY
L
swfs! -- 55
TO LNz
JS- GND TERMINAL GLQ%& <FFr7Dlk!)
3s - ENTER CMJTACT r p r I I q ? C
LUG -ER
TO PCB W E P N
SCHEMATIC DIAGRAM @B@
m T
~Ee hEnc
DETAIL F
Fig. 4.4 PREAMP WIRING 212-22566 (111)
4 - 23 - 24
Fig. 4.5.1 50KV INVERTER SCHEMATIC 212-22622 (111)
4 - 25 - 26
Fig. 4.5.2 50KV CASCADE SCHEMATIC 212-22631 (111)
4 - 27 - 28
Fig. 4.6.1 CTRL PCB ASSY 212-22529 (1/1)
4 - 29 - 30
Fig. 4.6.2 CTRL2 PCB ASSY 212-23010 (111)
4 - 31 - 32
Fig. 4.7.1 CTRL PCB SCHEMATIC (Standard) 212-22532 (116)
4 - 33 - 34
X-ray Pi l ot Lamp
4 - 35 - 36
4 - 37 - 38
PourEft
'X- RAY
RWY
W
C LOSE
4 - 39 - 40
4 - 41 - 42
Fig. 4.7.7 CTRL2 PCB SCHEMATIC (CE) 212-23012 (115)
4 - 45 - 46
4 - 47 - 48
CCD
Fig. 4.7.9 CTRL2 PC6 SCHEMATIC (CE) 212-23012 (315)
4 - 49 - 50
THETA
TftETFF
RWY
LIQUID NODE
4 - 51 - 52
4 - 53 - 54
S I L K PARTS
c : c33 m1
il- 4%
m' ??
il- C75
1
S
2
i t -
'II
I J MCA PCB
f 26 (.171 2 BOARD 212-22526A
._.I
ASSY 212-225250
Fig. 4.8 MCA PCB ASSY 212-22525 (111)
4 - 55 - 56
AC~P, ~@, ~R, R~Y ,
m. C M OUT
Fig. 4.9.1 MCA PCB SHEMATIC 212-22528 (112)
4 - 57 - 58
, 31s, LcU( .Cm m, my J
ncsP,PCSj,@,M I
Fig. 4.9.2 MCA PCB SHEMATIC 212-22528 (212)
4 - 59 - 60
Fig. 4.10 AMP PCB ASSY 212-22533 (111)
Fig. 4.11.1 AMP PCB SCHEMATIC 212-22536 (113)
4 - 63 - 64
39 CRM
Fig. 4.11.2 AMP PCB SCHEMATIC 212-22536 (213)
Fig. 4.12 PS PCB ASSY 212-22537 (111)
4 - 69 - 70
Fig. 4.13.2 PS PCB SHEMATIC 212-22540 (213
4 - 73 - 74
Fig. 4.13.3 PS PCB SHEMATIC 212-22540 (313)
4 - 75 - 76
POWER SUPPLY PCB ASSY
1 63 l-q~~--r
--
-- 7- -+-I-!== CPS l
L ~ - { T + - -
--
-- 7- -+-I-!== CPS l
TI;AME ASSY
Fig. 4.14.1 POWER SUPPLY WIRING (Standard) 212-22588 (IH)
COM
P9
C
CM1 Cl41
7\ ? T ~ I 1 ACt u U3
3
3 IG/Y
3 AEm L ~ ~ ' ~
\S 5 - FG
CABLE ASY 10
5v> /,to#+
RECEPTACLE ASSY luY
Fig. 4.14.2 POWER SUPPLY WIRING (CE) 212-23039 (111)
4 - 79 - 80
Q
\
m m m m o m m m m a m m m m m
BOARD 272-22572
Fig. 4.15 PANEL PCB ASSY 212-22571 (111)
Fig. 4.16 PANEL PCB SCHEMATIC 212-22574 (111)
4 - 83 - 84
Fig. 4.17 S10 PCB ASSY 212-22886 (111)
OND
S*) m
aoa
U)
y.
l c M
U N
ONO
DID
m1
om
DBI
m4
m
W
on
mu
IIIFIUA.
Fig. 4.18 SIO PC6 SCHEMATIC 212-22889 (111)
4 - 87 - 88
Chapter 5 Trouble Shooting
1. Error message ..................................................................................................... 5 - 2
l. Error message
X-ray generator 1 106 1 Maximum output setting error
ShutterIFilter 1 201 1 PPMC status read error at initialization
Power supply of detector 1 604
Collimator 1 70 1
Collimator 1 705 1 Constant speed operation error
r-a stage 1 801 1 PPMC status read error at initialization of r drive
Room temperature warning (Cooling)
PPMC status read error at initialization
Collimator
Collimator
Collimator
r-q stage 1 804 l PPMC error r drive
r-q stage 1 805 1 Constant speed operation error q drive
702
703
704
1 V
r-q stage
r-q stage
High speed operation error
Acceleration/reduction operation error
PPMC error
802
803
r-q stage
r-q stage
r-q stage
r-q stage
High speed operation error of r drive
Acceleration/reduction operation error r drive
r-q stage
Turret
Turret
81 1
8 12
8 13
8 14
PPMC status read error at initialization of q drive
High speed operation error of q drive
Acceleration/reduction operation error q drive
PPMC error q drive
8 15
100 1
1002
Constant speed operation error q drive
Initialization time out error
Time out error during drive

EDX-700HS 800HS 900HS SM Rev0ocr

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Shimadzu Energy Dispersion

Fluorescence X-ray Spectrometer

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