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CHM556 Organic Chemistry Ii Laboratory: The Techniques
CHM556 Organic Chemistry Ii Laboratory: The Techniques
The Techniques
Students are required read and understand the various techniques that will be covered
in the laboratory sessions from the textbook.
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Techniques
Laboratory Safety
Laboratory Glassware: Care and Cleaning
Measurement of Volume and Weight
Heating and Cooling Methods
Reaction Methods (Eg: Distillation, Reflux)
Filtration
Physical Constants of Solids: The Melting Point
Crystallization: Purification of Solids
Extractions, Separations and Drying Agents
Simple Distillation
Thin Layer Chromatography
Infrared Spectroscopy
NMR Spectroscopy (Proton NMR)
NMR Spectroscopy (Carbon-13 NMR)
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6
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90
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141
179
261
311
346
383
laboratory preparations must include not only procedural notes but also reactions and
calculations.
Pre-laboratory preparations
(assessed from the lab note books)
Laboratory techniques
(performance in the lab)
Laboratory reports
(all reports are individual work)
Total
2 marks
1 marks
17 marks
20 marks
A well written report is vital in achieving a good grade. Besides conducting the
experiments carefully, the students are expected to write a good report which will
reflect a good understanding of chemistry behind the experiments.
1. All laboratory reports must be typed and submitted one week after the
experiments.
2. The cover page should contain the following information: Course name,
Course code, number and title of experiment, name of student, name of
partners (for group work), name of lecturer, and date of experiment and date
of submission of report.
3. The following marking scheme table must be included with the laboratory
report.
4. Should the student fail to submit the weeks report, the student is given
maximum of 3 marks (for prelab and technique). Marks will also be
deducted for late submission of report.
5. No report will be accepted (no marks given) from students who did not
perform the weeks experiment.
6. Students who missed any lab session (with medical certificate) will be
graded based on the remaining number of experiments.
Full
Mark(s)
1.0
2.0
1.0
3.0
3.0
2.0
1.0
3.0
1.0
2.0
1.0
20
Marks
(to be filled by lecturer)