Professional Documents
Culture Documents
Refference For Mineral Reserves and Resources
Refference For Mineral Reserves and Resources
This Reference for Mineral Reserves and Resources is the sole property of
Barrick Gold Corporation and has been prepared by the employees of
Barrick solely for their own reference in preparing internal reports and
analyses. Except by employees of Barrick in the performance of their
employment or with the prior written permission of an authorized officer of
Barrick, no part of this Reference volume may be (a) reproduced, stored in
a retrieval system or transmitted in any form or by any means, electronic,
mechanical, photocopying, recording or otherwise, or (b) adapted, quoted,
referenced or otherwise used by any person.
The purpose of this Reference volume is solely to provide an easily
accessible collection of resource materials relevant to the various Barrick
professionals involved in estimating mineral resources and reserves. The
procedures and specifications described in this Reference volume do not,
and are not intended to, establish fixed policies or standards of practice
applicable at all times or in all situations.
ACKNOWLEDGEMENTS
The initial basis for this reference volume was the excellent and comprehensive
Operations Geology Procedures Manual that was assembled by Homestake Gold of
Australia. Maurice Rowley and Alex Mandyczewsky were instrumental in compiling and
editing the Homestake work, and Maurices guidance during the early stages of this
Barrick Reference for Mineral Reserves and Resources is greatly appreciated.
The editors wish to thank the other Barrick employees who contributed to this volume,
including Chris Bostwick, John Frostiak, Patrick Garver, Bob Leonardson, John
McDonough, Ren Marion, Craig Munson, Sybil Veenman, Jeff Volk, Martin Wafforn,
and Cindy Winwood. Independent contributors included David Tutton of DAT Mine
Consulting, John Goode of J.R. Goode and Associates, Ian McBride of Davies, Ward,
Phillips, and Vineberg, Richard West, Ron Crouse, and Joyce Austin of Call & Nicholas
Inc., and Chris Lattanzi of Micon International. Thanks are also due to Jane Spooner
and Lynn Mortimer of Micon International for final review of the volume.
Rick Sims of Barrick and Don Earnest of Resource Evaluation Inc. authored portions of
the reference and also served as editors of the volume.
List of Abbreviations
Abbreviation
Unit or Term
Abbreviation
Unit or Term
US$
US$/g
US$/oz
US$/st
US dollar(s)
US$ per gram
US dollars per ounce
US dollars per short ton
kg/t
km
lb
LHD
US$/t
LMIS
%
<
>
3-D
m
AAS
Ag
ANFO
ARD
LOM
M
m
mg
mil
mm
Mt
Mt/y
NaCN
NPV
Au
Barrick
BD
percent
less than
greater than
three-dimensional
microns, micrometres
atomic absorption spectroscopy
silver
ammonium nitrate-fuel oil
acid rock drainage
American Society of Testing and
Materials
gold
Barrick Gold Corporation
bulk density
NSR
oz
oz/t
cfm
P90
CIL
CN
cm
CMS
cm3
CRM
d
D
DC
DCF
DDH
DTH
ft
carbon-in-leach
cyanide
centimetre(s)
cavity monitor survey(s)
cubic centimetre(s)
continuous flow ring mill
day
density
diamond core
discounted cash flow
diamond drill hole
down-the-hole
foot, feet
PGM
pH
ppb
PPE
ppm
psi
PVC
QA
QC
RC
RD
ROM
RQD
grams
SEM
G&A
g/t
g/t Au
HDPE
SG
SMU
t
UCS
US
United States
USC
VCR
vol %
percent by volume
wt%
y
percent by weight
year
ASTM
HQ
ICP
ICP-AES
ICP-MS
in
kg
Section 1
REPORTING CODES
(NI 43-101)
(JORC)
(SEC)
Reference for Mineral Reserves and Resources
PART 2
2.1
2.2
2.3
2.4
PART 3
3.1
3.2
3.3
3.4
3.5
PART 4
4.1
4.2
4.3
PART 5
5.1
5.2
5.3
PART 6
6.1
6.2
6.3
PART 7
-ii7.1
PART 8
8.1
8.2
8.3
PART 9
9.1
EXEMPTION
Exemption
PART 10
10.1
EFFECTIVE DATE
Effective Date
PART 1.
1.1
Application - This Instrument applies to all oral statements and written disclosure
of scientific or technical information, including disclosure of a mineral resource or
mineral reserve, made by or on behalf of an issuer in respect of a mineral project
of the issuer.
1.2
(b)
(c)
"data verification" means the process of confirming that data has been generated
with proper procedures, has been accurately transcribed from the original source
and is suitable to be used;
"development property" means a property that is being prepared for mineral
production and for which economic viability has been demonstrated by a feasibility
study;
"disclosure" means any oral statement or written disclosure made by or on behalf
of an issuer and intended to be, or reasonably likely to be, made available to the
public in a Canadian jurisdiction, whether or not filed under securities legislation,
but does not include written disclosure that is made available to the public only by
reason of having been filed with a government or agency of government pursuant
to a requirement of law other than securities legislation;
"disclosure document" means an annual information form, prospectus, material
change report or annual financial statement filed with a regulator pursuant to a
requirement of securities legislation;
-3(a)
gross revenues, derived from mining operations, of at least $30 million for
the issuer's most recently completed financial year; and
(b)
(b)
(c)
(d)
(b)
has experience relevant to the subject matter of the mineral project and the
technical report; and
(c)
-4"technical report" means a report prepared, filed and certified in accordance with
this Instrument and Form 43-101F1 Technical Report;
"USGS Circular 831" means the circular published by the United States Bureau
of Mines/United States Geological Survey entitled "Principles of a
Resource/Reserve Classification for Minerals", as amended or supplemented; and
"written disclosure" includes any writing, picture, map or other printed
representation whether produced, stored or disseminated on paper or
electronically.
1.3
1.4
1.5
Interpretation
(1)
(2)
(b)
(c)
-5(i)
(ii) the votes carried by such securities entitle the second person
or company to elect a majority of the directors of the
company;
(3)
(b)
(c)
(4)
the issuer,
(c)
(d)
(e)
-7PART 2.
2.1
2.2
2.3
(a)
(b)
(c)
Prohibited Disclosure
(1)
(2)
(b)
-8-
(3)
(a)
(b)
the basis on which the disclosed potential quantity and grade has
been determined.
(b)
(c)
(4)
An issuer shall not use the terms preliminary feasibility study, prefeasibility study or feasibility study when referring to a study unless the
-9study satisfies the criteria set out in the definitions of the applicable terms
in section 1.2.
2.4
(b)
PART 3.
3.1
- 10 3.2
3.3
(b)
describes the nature of, and any limitations on, the verification of
data disclosed; and
(c)
(2)
(b)
(c)
(b)
3.4
(c)
(d)
(e)
(f)
(b)
(c)
(d)
(e)
- 12 3.5
PART 4.
4.1
4.2
(1)
(2)
2.
(b)
- 13 (c)
3.
4.
An offering memorandum.
5.
6.
(b)
(c)
7.
8.
9.
(3)
Subject to subsections (4), (5), and (6), the technical report required to
be filed under subsection (1) shall be filed not later than the time of the
filing of the document listed in subsection (1) that it supports.
(4)
(5)
(a)
(b)
- 15 file the technical report required by subsection (1) within 30 days of the
date that the property first became material to the issuer.
(6)
4.3
PART 5.
5.1
5.2
5.3
2.
3.
- 16 4.
Reporting Issuer in
an Additional Canadian Jurisdiction - Subsection 4.1(2)
(2)
(3)
PART 6
6.1
6.2
6.3
Maintenance of Records - The issuer shall keep copies of assay and other
analytical certificates, drill logs and other information referenced in the technical
report or used as a basis for the technical report for 7 years.
PART 7
7.1
- 17 (2)
PART 8
8.1
An issuer shall, when filing a technical report, also file a certificate of each
of the individuals who are qualified persons and who have been primarily
responsible for the technical report, or a portion of the technical report,
dated, signed and, if the signatory has a seal, sealed, by the signatory.
(2)
(b)
(c)
the date and duration of the qualified person's most recent visits
to each applicable site;
(d)
(e)
- 18 (f)
(g)
what prior involvement, if any, the qualified person has had with
the property that is the subject of the technical report; and
(h)
that the qualified person has read this Instrument and Form 43101F1, and the technical report has been prepared in compliance
with this Instrument and Form 43-101F1.
8.2
8.3
(b)
PART 9
EXEMPTION
9.1
Exemption
(1)
(2)
Despite subsection (1), in Ontario, only the regulator may grant such an
exemption.
- 19 (3)
Despite subsection (1), in Alberta, only the regulator may grant such an
exemption.
PART 10
EFFECTIVE DATE
10.1
Effective Date - This Instrument shall come into force on February 1, 2001.
PART 2
DISCLOSURE
2.1
Disclosure is the Responsibility of the Issuer
2.2
Use of Plain Language
2.3
Prohibited Disclosure
2.4
Materiality
2.5
Material Information not yet Confirmed by a Qualified
Person
2.6
Exception in Section 3.5 of the Instrument
2.7
Meaning of Current Technical Report
2.8
Exceptions from Requirement for Technical Report with
Annual Information Form, Annual Report and Preliminary
Short Form Prospectus if Information Previously
Disclosed
PART 3
PART 4
PART 5
USE OF INFORMATION
5.1
Use of Information
- ii PART 6
PERSONAL INSPECTION
6.1
Personal Inspection
6.2
Exemption from Personal Inspection Requirement
6.3
Responsibility of the Issuer
PART 7
REGULATORY REVIEW
7.1
Review
PART 1
1.1
Purpose - This companion policy sets out the views of the Canadian Securities
Administrators (the "CSA") as to the manner in which certain provisions of
National Instrument 43-101 (the "Instrument") are to be interpreted and applied.
1.2
1.3
1.4
-21.5
1.6
(b)
(c)
-3(b)
PART 2
DISCLOSURE
2.1
2.2
2.3
Prohibited Disclosure
(1)
-4resources.
(2)
2.4
Materiality
(1)
(2)
(3)
(4)
(5)
-52.5
2.6
2.7
Meaning of Current Technical Report - In the view of the CSA, the "current
technical report" referred to in sections 4.2 and 4.3 of the Instrument is a technical
report that contains all information required under the Form 43-101F1 in respect
of the subject property as at the date on which the technical report is filed. A
technical report may constitute a current technical report, even if prepared
considerably before the filing date, if the information in the technical report remains
accurate and does not omit materially new information as at the date of filing.
2.8
-6PART 3
3.1
3.2
Qualified Person - Section 2.1 of the Instrument requires that all disclosure be
based upon a technical report or other information prepared by or under the
supervision of a qualified person and section 5.1 of the Instrument provides that
a technical report must be prepared by or under the supervision of one or more
qualified persons. The Canadian securities regulatory authorities recognize that
certain individuals who currently provide technical expertise to issuers will not be
considered qualified persons for purposes of the Instrument. These individuals
may have the necessary experience and expertise but may lack the professional
accreditation because of differences in provincial registration requirements or for
other reasons. Application can be made by an issuer under section 9.1 of the
Instrument for an exemption from the requirement for involvement of a qualified
person and the acceptance of another person. The application should demonstrate
the person's competence and qualification to prepare the technical report or other
information in support of the disclosure despite the fact that he or she is not a
member of a professional association or otherwise does not meet the requirements
set out in the definition in the Instrument of qualified person.
3.3
(2)
PART 4
4.1
"Best Practices" Guidelines - Issuers and authors shall follow the Mineral
Exploration "Best Practices" Guidelines prepared on the recommendation of the
TSE-OSC Mining Standards Task Force by a committee comprised of mining and
exploration industry professionals and regulators. These Guidelines were
published in June, 2000.
PART 5
USE OF INFORMATION
5.1
PART 6
PERSONAL INSPECTION
6.1
6.2
-8inspect the property. In such instances the qualified person or the issuer should
apply in writing to the securities regulatory authority for relief, stating the reasons
why a personal inspection is considered impossible or not beneficial. It would
likely be a condition of any such relief that the technical report state that no
inspection was carried out by a qualified person and provide reasons.
6.3
Responsibility of the Issuer - The requirement set out in section 6.2 of the
Instrument sets a minimum standard for personal inspection. The issuer should
have property inspections conducted by one or more qualified persons as
appropriate, taking into account the work being carried out on the property and
the technical report being prepared by the qualified person or persons.
PART 7
REGULATORY REVIEW
7.1
Review
(1)
Disclosure and technical reports filed under the Instrument may be subject
to review by Canadian securities regulatory authorities.
(2)
An issuer that files a technical report that does not meet the requirements
of the Instrument will be in breach of securities legislation. The issuer may
be required to issue or file corrected disclosure, file a revised technical
report or file revised consents, and may be subject to other sanctions.
APPENDIX
TO
COMPANION POLICY 43-101CP
Mineral Resource
Mineral Resources are sub-divided, in order of increasing geological confidence, into
Inferred, Indicated and Measured categories. An Inferred Mineral Resource has a lower level
of confidence than that applied to an Indicated Mineral Resource. An Indicated Mineral
Resource has a higher level of confidence than an Inferred Mineral Resource but has a lower
level of confidence than a Measured Mineral Resource.
A Mineral Resource is a concentration or occurrence of natural, solid, inorganic or
fossilized organic material in or on the Earths crust in such form and quantity and of such
a grade or quality that it has reasonable prospects for economic extraction. The location,
quantity, grade, geological characteristics and continuity of a Mineral Resource are
known, estimated or interpreted from specific geological evidence and knowledge.
The term Mineral Resource covers mineralization and natural material of intrinsic economic
interest which has been identified and estimated through exploration and sampling and
within which Mineral Reserves may subsequently be defined by the consideration and
application of technical, economic, legal, environmental, socio-economic and governmental
factors. The phrase reasonable prospects for economic extraction implies a judgement by
the Qualified Person in respect of the technical and economic factors likely to influence the
prospect of economic extraction. A Mineral Resource is an inventory of mineralization that
under realistically assumed and justifiable technical and economic conditions, might become
economically extractable. These assumptions must be presented explicitly in both public and
technical reports.
Inferred Mineral Resource
An Inferred Mineral Resource is that part of a Mineral Resource for which quantity and
grade or quality can be estimated on the basis of geological evidence and limited sampling
and reasonably assumed, but not verified, geological and grade continuity. The estimate
is based on limited information and sampling gathered through appropriate techniques
from locations such as outcrops, trenches, pits, workings and drill holes.
-2Due to the uncertainty which may attach to Inferred Mineral Resources, it cannot be
assumed that all or any part of an Inferred Mineral Resource will be upgraded to an
Indicated or Measured Mineral Resource as a result of continued exploration. Confidence
in the estimate is insufficient to allow the meaningful application of technical and economic
parameters or to enable an evaluation of economic viability worthy of public disclosure.
Inferred Mineral Resources must be excluded from estimates forming the basis of feasibility
or other economic studies.
Indicated Mineral Resource
An Indicated Mineral Resource is that part of a Mineral Resource for which quantity,
grade or quality, densities, shape and physical characteristics, can be estimated with a
level of confidence sufficient to allow the appropriate application of technical and
economic parameters, to support mine planning and evaluation of the economic viability
of the deposit. The estimate is based on detailed and reliable exploration and testing
information gathered through appropriate techniques from locations such as outcrops,
trenches, pits, workings and drill holes that are spaced closely enough for geological and
grade continuity to be reasonably assumed.
Mineralization may be classified as an Indicated Mineral Resource by the Qualified Person
when the nature, quality, quantity and distribution of data are such as to allow confident
interpretation of the geological framework and to reasonably assume the continuity of
mineralization. The Qualified Person must recognize the importance of the Indicated Mineral
Resource category to the advancement of the feasibility of the project. An Indicated Mineral
Resource estimate is of sufficient quality to support a Preliminary Feasibility Study which
can serve as the basis for major development decisions.
Measured Mineral Resource
A Measured Mineral Resource is that part of a Mineral Resource for which quantity,
grade or quality, densities, shape, physical characteristics are so well established that
they can be estimated with confidence sufficient to allow the appropriate application of
technical and economic parameters, to support production planning and evaluation of the
economic viability of the deposit. The estimate is based on detailed and reliable
exploration, sampling and testing information gathered through appropriate techniques
from locations such as outcrops, trenches, pits, workings and drill holes that are spaced
closely enough to confirm both geological and grade continuity.
Mineralization or other natural material of economic interest may be classified as a
Measured Mineral Resource by the Qualified Person when the nature, quality, quantity and
distribution of data are such that the tonnage and grade of the mineralization can be
-3estimated to within close limits and that variation from the estimate would not significantly
affect potential economic viability. This category requires a high level of confidence in, and
understanding of, the geology and controls of the mineral deposit.
Mineral Reserve
Mineral Reserves are sub-divided in order of increasing confidence into Probable Mineral
Reserves and Proven Mineral Reserves. A Probable Mineral Reserve has a lower level of
confidence than a Proven Mineral Reserve.
A Mineral Reserve is the economically mineable part of a Measured or Indicated
Mineral Resource demonstrated by at least a Preliminary Feasibility Study. This Study
must include adequate information on mining, processing, metallurgical, economic and
other relevant factors that demonstrate, at the time of reporting, that economic extraction
can be justified. A Mineral Reserve includes diluting materials and allowances for losses
that may occur when the material is mined.
Mineral Reserves are those parts of Mineral Resources which, after the application of all
mining factors, result in an estimated tonnage and grade which, in the opinion of the
Qualified Person(s) making the estimates, is the basis of an economically viable project after
taking account of all relevant processing, metallurgical, economic, marketing, legal,
environment, socio-economic and government factors. Mineral Reserves are inclusive of
diluting material that will be mined in conjunction with the Mineral Reserves and delivered
to the treatment plant or equivalent facility. The term Mineral Reserve need not necessarily
signify that extraction facilities are in place or operative or that all governmental approvals
have been received. It does signify that there are reasonable expectations of such approvals.
Probable Mineral Reserve
A Probable Mineral Reserve is the economically mineable part of an Indicated, and in
some circumstances a Measured Mineral Resource demonstrated by at least a
Preliminary Feasibility Study. This Study must include adequate information on mining,
processing, metallurgical, economic, and other relevant factors that demonstrate, at the
time of reporting, that economic extraction can be justified.
Proven Mineral Reserve
A Proven Mineral Reserve is the economically mineable part of a Measured Mineral
Resource demonstrated by at least a Preliminary Feasibility Study. This Study must
include adequate information on mining, processing, metallurgical, economic, and other
-4relevant factors that demonstrate, at the time of reporting, that economic extraction is
justified.
Application of the Proven Mineral reserve category implies that the Qualified Person has
the highest degree of confidence in the estimate with the consequent expectation in the
minds of the readers of the report. The term should be restricted to that part of the deposit
where production planning is taking place and for which any variation in the estimate would
not significantly affect potential economic viability.
FORM 43-101F1
TECHNICAL REPORT
TABLE OF CONTENTS
Item 26:
Title Page
Table of Contents
Summary
Introduction and Terms of Reference
Disclaimer
Property Description and Location
Accessibility, Climate, Local Resources, Infrastructure and Physiography
History
Geological Setting
Deposit Types
Mineralization
Exploration
Drilling
Sampling Method and Approach
Sample Preparation, Analyses and Security
Data Verification
Adjacent Properties
Mineral Processing and Metallurgical Testing
Mineral Resource and Mineral Reserve Estimates
Other Relevant Data and Information
Interpretation and Conclusions
Recommendations
References
Date
Additional Requirements for Technical Reports
on Development Properties and Production
Properties
Illustrations
FORM 43-101F1
TECHNICAL REPORT
INSTRUCTIONS
(1)
(2)
Terms used and not defined in this Form that are defined or
interpreted in National Instrument 43-101 Standards of
Disclosure for Mineral Projects (the "Instrument") shall bear
that definition or interpretation. In particular, the terms
"mineral resource" and "mineral reserve" and the categories
of each are defined in the Instrument. In addition, a general
definition instrument has been adopted as National
Instrument 14-101 Definitions which contains definitions of
certain terms used in more than one national instrument.
Readers of this Form shall review both these national
instruments for defined terms.
(3)
(4)
(5)
Item 1:
Title Page - Include a title page setting out the title of the technical report, the
general location of the mineral project, the name(s) and the professional
designation(s) of the authors and the effective date of the technical report.
Item 2:
Item 3:
Summary - Provide a summary which briefly describes the property, its location,
ownership, geology and mineralization, the exploration concept, the status of
exploration, development and operations and the author's conclusions and
recommendations.
Item 4:
(b)
(c)
(d)
Item 5:
Disclaimer - If the author of all or a portion of the technical report has relied on
a report, opinion or statement of legal or other experts who are not qualified
persons for information concerning legal, environmental, political or other issues
and factors relevant to the technical report, the author may include a disclaimer of
responsibility in which the author identifies the report, opinion or statement relied
upon, the maker of that report, opinion or statement, the extent of reliance and the
portions of the technical report to which the disclaimer applies.
Item 6:
(b)
Item7:
(c)
(d)
the nature and extent of the issuer's title to, or interest in, the property
including surface rights, the obligations that must be met to retain the
property, and the expiration date of claims, licences or other property
tenure rights;
(e)
(f)
(g)
to the extent known, the terms of any royalties, back-in rights, payments
or other agreements and encumbrances to which the property is subject;
(h)
(i)
to the extent known, the permits that must be acquired to conduct the
work proposed for the property, and if the permits have been obtained.
Accessibility, Climate, Local Resources, Infrastructure and Physiography With respect to each property reported on, describe
(a)
(b)
(c)
(d)
to the extent relevant to the mineral project, the climate and the length of
the operating season; and
(e)
Item 8:
-4to the extent relevant, the sufficiency of surface rights for mining
operations, the availability and sources of power, water, mining personnel,
potential tailings storage areas, potential waste disposal areas, heap leach
pad areas and potential processing plant sites.
History - To the extent known, with respect to each property reported on,
describe
(a)
(b)
(c)
(d)
INSTRUCTION:
Item 9:
Item 10:
Deposit Types - Describe the mineral deposit type(s) being investigated or being
explored for and the geological model or concepts being applied in the
investigation and on the basis of which the exploration program is planned.
Item 11:
Item 12:
Exploration - Describe the nature and extent of all relevant exploration work
conducted by, or on behalf of, the issuer on each property being reported on,
including
(a)
(b)
(c)
(d)
Item 13:
Drilling - Describe the type and extent of drilling including the procedures
followed and a summary and interpretation of all results. The relationship between
the sample length and the true thickness of the mineralization must be stated, if
known, and if the orientation of the mineralization is unknown, state this.
Item 14:
Item 15:
(a)
(b)
(c)
(d)
(e)
-6reduction, and the security measures taken to ensure the validity and integrity of
samples taken, including
Item 16:
Item 17:
(a)
(b)
(c)
(d)
(b)
whether the author has verified the data referred to or relied upon,
referring to sampling and analytical data;
(c)
(d)
(b)
the source of the information and any relationship of the author of the
information on the adjacent property to the issuer is identified;
(c)
the technical report states that its author has been unable to verify the
information and, in bold face type, that the information is not necessarily
indicative of the mineralization on the property that is the subject of the
technical report;
(d)
(e)
Item 18:
Item 19:
use only the applicable mineral resource and mineral reserve categories set
out in sections 1.3 and 1.4 of the Instrument;
(b)
(c)
(d)
disclose the name, qualifications and relationship, if any, to the issuer of the
qualified person who estimated mineral resources and mineral reserves;
(e)
(f)
(g)
(h)
-8identify the extent to which the estimates of mineral resources and mineral
reserves may be materially affected by mining, metallurgical, infrastructure
and other relevant factors;
(i)
(j)
state the grade or quality, quantity and category of the mineral resources
and mineral reserves if the quantity of contained metal is reported; and
(k)
INSTRUCTIONS
Item 20:
(1)
(2)
(3)
Item 21:
Item 22:
Item 23:
References - Include a detailed list of all references cited in the technical report.
Item 24:
Date - Include the effective date of the technical report on both the title page and
the page of the technical report that is signed. The date of signing must also be
included on the signature page.
Item 25:
(b)
(c)
(d)
Item 26:
(e)
(f)
Taxes - a description of the nature and rates of taxes, royalties and other
government levies or interests applicable to the mineral project or to
production, and to revenues or income from the mineral project;
(g)
(h)
(i)
(j)
Illustrations
(a)
(b)
(d)
Maps shall include a scale in bar form and an arrow indicating North.
Information taken from government maps or from drawings of other
engineers or geoscientists shall be acknowledged on the map.
19
9
9E
dit
ion
THE 1999 AUSTRALASIAN CODE FOR REPORTING OF MINERAL RESOURCES AND ORE RESERVES (JORC CODE)
FOREWORD
1.
2.
3.
4.
PAGE 2
Note: Code is in normal typeface, guidelines are in indented italics, definitions are in bold.
THE 1999 AUSTRALASIAN CODE FOR REPORTING OF MINERAL RESOURCES AND ORE RESERVES (JORC CODE)
6.
7.
9.
Note: Code is in normal typeface, guidelines are in indented italics, definitions are in bold.
PAGE 3
THE 1999 AUSTRALASIAN CODE FOR REPORTING OF MINERAL RESOURCES AND ORE RESERVES (JORC CODE)
REPORTING TERMINOLOGY
12. Public Reports dealing with Mineral Resources and/
or Ore Reserves must only use the terms set out in
Figure 1.
Figure 1 sets out the framework for classifying
tonnage and grade estimates so as to reflect
different levels of geological confidence and
different degrees of technical and economic
evaluation. Mineral Resources can be estimated
mainly by a geologist on the basis of geoscientific
PAGE 4
Note: Code is in normal typeface, guidelines are in indented italics, definitions are in bold.
THE 1999 AUSTRALASIAN CODE FOR REPORTING OF MINERAL RESOURCES AND ORE RESERVES (JORC CODE)
Figure 1. General Relationship between Exploration Results, Mineral Resources and Ore Reserves.
Exploration Results
Mineral Resources
Ore Reserves
Inferred
Increasing level
of geological
knowledge and
confidence
Indicated
Probable
Measured
Proved
REPORTING GENERAL
13. Public Reports concerning a companys Mineral
Resources or Ore Reserves should include
a description of the style and nature of
mineralisation.
14. A company must disclose relevant information
concerning the status and characteristics of a mineral
deposit which could materially influence the
economic value of that deposit. A company must
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THE 1999 AUSTRALASIAN CODE FOR REPORTING OF MINERAL RESOURCES AND ORE RESERVES (JORC CODE)
TABLE 1
CHECK LIST OF ASSESSMENT AND REPORTING CRITERIA
Table 1 is a check list and guideline which those preparing reports on exploration results, Mineral Resources and
Ore Reserves should use as a reference. The check list is not prescriptive and, as always, relevance and materiality
are overriding principles that determine what information should be publicly reported. It is, however, important
to report any matters that might materially affect a readers understanding or interpretation of the results or
estimates being reported. This is particularly important where inadequate or uncertain data affect the reliability
of, or confidence in, a statement of exploration results or an estimate of Mineral Resources and/or Ore Reserves.
The order and grouping of criteria in Table 1 reflects the normal systematic approach to exploration and
evaluation. Criteria in the first group Sampling Techniques and Data apply to all succeeding groups. In the
remainder of the table, criteria listed in preceding groups would often apply to succeeding groups and should
be considered when estimating and reporting.
CRITERIA
EXPLANATION
SAMPLING TECHNIQUES AND DATA
(criteria in this group apply to all succeeding groups)
Drilling
techniques
Drill type (eg. core, reverse circulation, open-hole hammer, rotary air blast, auger,
Bangka etc.) and details (eg. core diameter, triple or standard tube, depth of diamond tails, facesampling bit or other type, etc.). Measures taken to maximise sample recovery and ensure
representative nature of the samples.
Logging
Whether core and chip samples have been logged to a level of detail to support appropriate
Mineral Resource estimation, mining studies and metallurgical studies. Whether logging is
qualitative or quantitative in nature. Core (or costean, channel etc.) photography.
Drill sample
recovery
Whether core and chip sample recoveries have been properly recorded and results assessed. In
particular whether a relationship exists between sample recovery and grade and whether sample
bias may have occurred due to preferential loss/gain of fine/coarse material.
Other sampling
techniques
Nature and quality of sampling (eg. cut channels, random chips etc.) and measures taken to
ensure sample representivity.
Sub-sampling
techniques
and sample
preparation
If core, whether cut or sawn and whether quarter, half or all core taken. If non-core, whether
riffled, tube sampled, rotary split etc. and whether sampled wet or dry. For all sample types, the
nature, quality and appropriateness of the sample preparation technique. Quality control procedures
adopted for all sub-sampling stages to maximise representivity of samples. Measures taken to
ensure that the sampling is representative of the in situ material collected. Whether sample sizes
are appropriate to the grainsize of the material being sampled.
Quality of
assay data and
laboratory tests
The nature, quality and appropriateness of the assaying and laboratory procedures used and whether
the technique is considered partial or total. Nature of quality control procedures adopted (eg.
standards, blanks, duplicates, external laboratory checks) and whether acceptable levels of accuracy
(ie. lack of bias) and precision have been established.
Verification of
sampling and
assaying
Location of
data points
Accuracy and quality of surveys used to locate drill holes (collar and down-hole surveys), trenches,
mine workings and other locations used in Mineral Resource estimation. Quality and adequacy of
topographic control.
Data density
and distribution
Data density for reporting of exploration results. Whether the data density and distribution is
sufficient to establish the degree of geological and grade continuity appropriate for the Mineral
Resource and Ore Reserve estimation procedure(s) and classifications applied. Whether sample
compositing has been applied.
Audits or reviews
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Type, reference name/number, location and ownership including agreements or material issues
with third parties such as joint ventures, partnerships, overriding royalties, native title interests,
historical sites, wilderness or national park and environmental settings. In particular the security
of the tenure held at the time of reporting along with any known impediments to obtaining a
licence to operate in the area.
Exploration done
by other parties
Geology
Data aggregation
methods
In reporting exploration results, weighting averaging techniques, maximum and/or minimum grade
truncations (eg. cutting of high grades) and cut-off grades are usually material and should be
stated. Where aggregate intercepts incorporate short lengths of high grade results and longer
lengths of low grade results, the procedure used for such aggregation should be stated and some
typical examples of such aggregations should be shown in detail. The assumptions used for any
reporting of metal equivalent values should be clearly stated.
Relationship
between
mineralisation
widths and
intercept lengths
These relationships are particularly important in the reporting of exploration results. If the geometry
of the mineralisation with respect to the drill hole angle is known, its nature should be reported.
If it is not known and only the down-hole lengths are reported, there should be a clear statement
to this effect (eg. downhole length, true width not known).
Diagrams
Where possible, maps and sections (with scales) and tabulations of intercepts should be included
for any material discovery being reported if such diagrams significantly clarify the report.
Balanced
reporting
Where comprehensive reporting of all exploration results is not practicable, representative reporting
of both low and high grades and/or widths should be practised to avoid misleading reporting of
exploration results.
Other substantive
exploration data
Other exploration data, if meaningful and material, should be reported including (but not limited
to): geological observations; geophysical survey results; geochemical survey results; bulk samples
- size and method of treatment; metallurgical test results; bulk density, groundwater, geotechnical
and rock characteristics; potential deleterious or contaminating substances.
Further work
The nature and scale of planned further work (eg. tests for lateral extensions or depth extensions
or large-scale step-out drilling).
Measures taken to ensure that data has not been corrupted by, for example, transcription or
keying errors, between its initial collection and its use for Mineral Resource estimation purposes.
Data validation procedures used.
Geological
interpretation
Nature of the data used and of any assumptions made. The effect, if any, of alternative interpretations
on Mineral Resource estimation. The use of geology in guiding and controlling Mineral Resource
estimation. The factors affecting continuity both of grade and geology.
Estimation
and modelling
techniques
The nature and appropriateness of the estimation technique(s) applied and key assumptions,
including treatment of extreme grade values, domaining, interpolation parameters, maximum
distance of extrapolation from data points. The availability of check estimates, previous estimates
and/or mine production records and whether the Mineral Resource estimate takes appropriate
account of such data. The assumptions made regarding recovery of by-products. In the case of
block model interpolation, the block size in relation to the average sample spacing and the search
employed. Any assumptions behind modelling of selective mining units (eg. non-linear kriging).
The process of validation, the checking process used, the comparison of model data to drillhole
data, and use of reconciliation data if available.
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Cut-off grades
or parameters
The basis of the cut-off grade(s) or quality parameters applied, including the basis, if appropriate,
of equivalent metal formulae.
Mining factors
or assumptions
Assumptions made regarding possible mining methods, minimum mining dimensions and internal
(or, if applicable, external) mining dilution. It may not always be possible to make assumptions
regarding mining methods and parameters when estimating Mineral Resources. Where no
assumptions have been made, this should be reported.
Metallurgical factors The basis for assumptions or predictions regarding metallurgical amenability. It may not always
be possible to make assumptions regarding metallurgical treatment processes and parameters
or assumptions
when reporting Mineral Resources. Where no assumptions have been made, this should be reported.
Tonnage factors (in
situ bulk densities)
Whether assumed or determined. If assumed, the basis for the assumptions. If determined, the method
used, the frequency of the measurements, the nature, size and representativeness of the samples.
Classification
The basis for the classification of the Mineral Resources into varying confidence categories. Whether
appropriate account has been taken of all relevant factors. ie. relative confidence in tonnage/
grade computations, confidence in continuity of geology and metal values, quality, quantity and
distribution of the data. Whether the result appropriately reflects the Competent Person(s) view of
the deposit.
Audits or reviews
Description of the Mineral Resource estimate used as a basis for the conversion to an Ore Reserve.
Clear statement as to whether the Mineral Resources are reported additional to, or inclusive of,
the Ore Reserves.
Cut-off grades
or parameters
The basis of the cut-off grade(s) or quality parameters applied, including the basis, if appropriate,
of equivalent metal formulae. The cut-off grade parameter may be economic value per block
rather than metal grade.
Mining factors
or assumptions
The method and assumptions used to convert the Mineral Resource to an Ore Reserve (ie either
by application of appropriate factors by optimisation or by preliminary or detailed design). The
choice of, the nature and the appropriateness of the selected mining method(s) and other mining
parameters including associated design issues such as pre-strip, access, etc. The assumptions
made regarding geotechnical parameters (eg. pit slopes, stope sizes, etc.), grade control and preproduction drilling. The major assumptions made and Mineral Resource model used for pit
optimisation (if appropriate). The mining dilution factors, mining recovery factors, and minimum
mining widths used and the infrastructure requirements of the selected mining methods.
Metallurgical
factors or
assumptions
The metallurgical process proposed and the appropriateness of that process to the style of
mineralisation. Whether the metallurgical process is well-tested technology or novel in nature.
The nature, amount and representativeness of metallurgical testwork undertaken and the
metallurgical recovery factors applied. Any assumptions or allowances made for deleterious
elements. The existence of any bulk sample or pilot scale testwork and the degree to which such
samples are representative of the orebody as a whole.
The derivation of, or assumptions made, regarding projected capital and operating costs. The
assumptions made regarding revenue including head grade, metal or commodity price(s), exchange
rates, transportation and treatment charges, penalties, etc. The allowances made for royalties
payable, both Government and private.
Market
assessment
The demand, supply and stock situation for the particular commodity, consumption trends and
factors likely to affect supply and demand into the future. A customer and competitor analysis
along with the identification of likely market windows for the product. Price and volume forecasts
and the basis for these forecasts. For industrial minerals the customer specification, testing and
acceptance requirements prior to a supply contract.
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Others
The effect, if any, of natural risk, infrastructure, environmental, legal, marketing, social or
governmental factors on the likely viability of a project and/or on the estimation and classification
of the Ore Reserves. The status of titles and approvals critical to the viability of the project, such
as mining leases, discharge permits, government and statutory approvals.
Classification
The basis for the classification of the Ore Reserves into varying confidence categories. Whether
the result appropriately reflects the Competent Person(s) view of the deposit. The proportion of
Probable Ore Reserves which have been derived from Measured Mineral Resources (if any).
Audits or reviews
Primary sources of diamonds in nature are variable and complex. Accordingly, information relating to
primary sources should contain details of the nature of the rock type together with its form, shape and size.
Diamond value
Diamond valuation is a highly specialised process and is only possible on parcels containing
appropriate numbers of macrodiamonds. It is not possible to evaluate diamond quality from
microdiamonds. Classification of diamonds as, for example, gem, near gem and industrial should
be made by recognised experts who should be identified in the valuation report and their
independence stated. The number of stones, the total carat weight and size range for the parcel
valued should be stated.
Secondary rock
source
Secondary sources of diamonds in nature, including alluvial deposits, are variable and complex.
Accordingly, information relating to secondary sources should contain details of the nature of the
geological environment together with its form, age and size.
Microdiamonds
Current practice in Australia defines microdiamonds as diamonds which will pass through a screen
with 0.4 mm aperture, ie. diamonds weighing less than 0.001 carats. Reports of microdiamond
recoveries should specify both the number of stones recovered and the top and bottom screen or
crushing sizes used in the recovery process.
Macrodiamonds
Macrodiamonds are defined as diamonds larger than 0.4 mm in size. Reports of macrodiamond recoveries
should specify both the number of stones and the total carat weight recovered above a specified screen size.
Indicator minerals
Conventional indicator minerals include garnet, ilmenite, chrome spinel and chrome diopside
having the requisite chemical and physical attributes that distinguish them from otherwise similar
minerals found in non-diamond associated rock types. Reports of indicator minerals should be
prepared by a suitably qualified laboratory.
Sampling
parameters
Reported discoveries of diamonds or indicator minerals from all samples must be accompanied
by details of the sampling parameters and sampling equipment used. Type of sample (stream
sediment, soil, bulk, rock etc.) as well as sample size, sample density and screening or jigging
parameters are required.
Cut-off grades
Carat
Grades
Internationally, diamond grades for primary deposits are stated both in carats per tonne and carats per
100 tonnes. The Joint Ore Reserves Committee recommends the use of carats per tonne. In the case of
alluvial deposits, industry practice is to quote grades in carats per tonne or carats per cubic metre.
Volumes: state bank or loose cubic metres and basis of volume to tonnage conversions.
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APPENDIX 1
THE JORC CODE AND AUSTRALASIAN STOCK EXCHANGES
The Australian and New Zealand Stock Exchanges
(ASX and NZSX) have, since 1989 and 1992
respectively, incorporated the Code into their
listing rules. Under these listing rules, a Public
Report must be prepared in accordance with the
Code if it includes a statement on exploration
results, Mineral Resources or Ore Reserves. The
incorporation of the Code imposes certain specific
requirements on mining or exploration companies
reporting to the ASX and NZSX. The guidelines in
this section of the Code which paraphrase these
requirements should not be used as a replacement
for the relevant listing rules, and it is strongly
recommended that users of the Code familiarise
themselves with those listing rules which relate to
Public Reporting of exploration results, Mineral
Resources and Ore Reserves.
ASX listing rules require the Competent Person(s),
on whose work the Public Report of Mineral
Resources or Ore Reserves is based, to be named
in the report. The report or attached statement must
say that the person consents to the inclusion in the
report of the matters based on their information in
the form and context in which it appears, and must
include the name of the persons firm or employer.
Refer also to Clause 8 of the Code.
Appropriate forms of compliance statements may
be as follows (delete bullet points which do not
apply):
If the required information is in the report:
The information in this report that relates to
Mineral Resources or Ore Reserves is based
on information compiled by (insert name
of Competent Person), who is a Fellow or
Member of The Australasian Institute of Mining
and Metallurgy or the Australian Institute of
Geoscientists (select as appropriate): or
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Page 1 of 5
Introduction
Through the years, geologists, mining engineers, and others operating in the minerals field have used
various terms to describe and classify mineral resources, which as defined herein include energy
materials. Some of these terms have gained wide use and acceptance, although they are not always used
with precisely the same meaning.
Staff members of the U.S. Bureau of Mines and the U.S. Geological Survey collect information about
the quantity and quality of all mineral resources, but from different perspectives and with different
purposes. In 1976, a team of staff members from both agencies developed a common classification and
nomenclature, which was published as U.S. Geological Survey Bulletin 1450-A - "Principles of the
Mineral Resource Classification System of the U.S. Bureau of Mines and U.S. Geological Survey."
Experience with this resource classification system showed that some changes were necessary in order
to make it more workable in practice and more useful in long-term planning. Therefore, representatives
of the U.S. Geological Survey and the U.S. Bureau of Mines collaborated to revise Bulletin 1450-A
Long-term public and commercial planning must be based on the probability of discovering new
deposits, on developing economic extraction processes for currently unworkable deposits, and on
knowing which resources are immediately available. Thus, resources must be continuously reassessed in
the light of new geologic knowledge, of progress in science and technology, and of shifts in economic
and political conditions. To best serve these planning needs, known resources should be classified from
two standpoints: (1) purely geologic or physical/chemical characteristics - such as grade, quality,
tonnage, thickness, and depth-of the material in place: and (2) profitability analyses based on costs of
extracting and marketing the material in a given economy at a given time. The former constitutes
important objective scientific information of the resource and a relatively unchanging foundation upon
which the latter more variable economic delineation can be based.
The revised classification system, designed generally for all mineral materials, is shown graphically in
figures 1 and 2 (see page 5); its components and their usage are described in the text. The classification
of mineral and energy resources is necessarily arbitrary, because definitional criteria do not always
coincide with natural boundaries. The system can be used to report the status of mineral and energy-fuel
resources for the Nation or for specific areas.
Resource/Reserve Definitions
A dictionary definition of resource, "something in reserve or ready if needed," has been adapted for
mineral and energy resources to comprise all materials, including those only surmised to exist, that have
present or anticipated future value.
Resource.-A concentration of naturally occurring solid, liquid, or gaseous material in or on the Earth's
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Page 2 of 5
crust in such form and amount that economic extraction of a commodity from the concentration is
currently or potentially feasible.
Original Resource. - The amount of a resource before production.
Identified Resources. - Resources whose location, grade, quality, and quantity are known or estimated
from specific geologic evidence. Identified resources include economic, marginally economic, and
subeconomic components. To reflect varying degrees of geologic certainty, these economic divisions
can be subdivided into measured, indicated, and inferred. (The terms "proven," "probable," and "possible", which are commonly
used by industry in economic evaluations of ore or mineral fuels in specific deposits or districts, have been loosely interchanged with the terms measured, indicated,
and inferred. The former terms are not a part of this classification system.)
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Marginal Reserves. - That part of the reserve base which, at the time of determination, borders on being
economically producible. Its essential characteristic is economic uncertainty. Included are resources that
would be producible, given postulated changes in economic or technologic factors.
Economic. - This term implies that profitable extraction or production under defined investment
assumptions has been established, analytically demonstrated, or assumed with reasonable certainty.
Subeconomic Resources. - The part of identified resources that does not meet the economic criteria of
reserves and marginal reserves.
Undiscovered Resources. - Resources, the existence of which are only postulated, comprising deposits
that are separate from identified resources. Undiscovered resources may be postulated in deposits of
such grade and physical location as to render them economic, marginally economic, or subeconomic. To
reflect varying degrees of geologic certainty, undiscovered resources may be divided into two parts:
Hypothetical Resources. - Undiscovered resources that are similar to known mineral bodies and
that may be reasonably expected to exist in the same producing district or region under analogous
geologic conditions. If exploration confirms their existence and reveals enough information about
their quality, grade, and quantity, they will be reclassified as identified resources.
Speculative Resources. - Undiscovered resources that may occur either in known types of
deposits in favorable geologic settings where mineral discoveries have not been made, or in types
of deposits as yet unrecognized for their economic potential. If exploration confirms their
existence and reveals enough information about their quantity, grade, and quality, they will be
reclassified as identified resources.
Restricted Resources/Reserves. - That part of any resource/reserve category that is restricted from
extraction by laws or regulations. For example, restricted reserves meet all the requirements of reserves
except that they are restricted from extraction by laws or regulations.
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7. The reserve base is an encompassing resource category delineated by physical and chemical criteria.
A major purpose for its recognition and appraisal is to aid in long-range public and commercial
planning. For most mineral commodities, different grades and tonnages, or other appropriate resource
parameters, can be specified for any given deposit or area, or for the Nation, depending on the specific
objectives of the estimators; therefore, the position of the lower boundary of the reserve base, which
extends into the subeconomic category, is variable, depending on those objectives. The intention is to
define a quantity of in-place material, any part of which may become economic, depending on the
extraction plans and economic assumptions finally used. When those criteria are determined, the initial
reserve-base estimate will be divided into three component parts: reserves, marginal reserves, and a
remnant of subeconomic resources. For the purpose of Federal commodity assessment; criteria for the
reserve base will be established for each commodity.
8. Undiscovered resources may be divided in accordance with the definitions of hypothetical and
speculative resources, or they may be divided in terms of relative probability of occurrence.
9. Inferred reserves and the inferred reserve base are postulated extensions of reserves and of the
reserve base. They are identified resources quantified with a relatively low degree of certainty.
Postulated quantities of resources not based on reserve/reserve-base extensions, but rather on geologic
inference alone, should be classified as undiscovered.
10. Locally, limited quantities of materials may be produced, even though economic analysis has
indicated that the deposit would be too thin, too low grade, or too deep to be classified as a reserve. This
situation might arise when the production facilities are already established or when favorable local
circumstances make it possible to produce material that elsewhere could not be extracted profitably.
Where such production is taking place, the quantity of in-place material shall be included in the reserve
base, and the quantity that is potentially producible shall be included as a reserve. The profitable
production of such materials locally, however, should not be used as a rationale in other areas for
classifying as reserves, those materials that are similar in thickness, quality, and depth.
11. Resources classified as reserves must be considered economically producible at the time of
classification. Conversely, material not currently producible at a profit cannot be classified as reserves.
There are situations however, in which mining plans are being made, lands are being acquired, or mines
and plants are being constructed to produce materials that do not meet economic criteria for reserve
classification under current costs and prices, but would do so under reasonable future expectations. For
some other materials, economic producibility is uncertain only for lack of |detailed engineering
assessment. The marginal reserves category applies to both situations. When economic production
appears certain for all or some of a marginal reserve, it will be reclassified as reserves.
12. Materials that are too low grade or for other reasons are not considered potentially economic, in the
same sense as the defined resource, may be recognized and their magnitude estimated, but they are not
classified as resources. A separate category, labeled other occurrences, is included in figures 1 and 2.
13. In figure 1, the boundary between subeconomic and other occurrences is limited by the concept of
current or potential feasibility of economic production, which is required by the definition of a resource.
The boundary is obviously uncertain, but limits may be specified in terms of grade, quality, thickness,
depth, percent extractable, or other economic-feasibility variables.
14. Varieties of mineral or energy commodities, such as bituminous coal as distinct from lignite, may be
separately quantified when they have different characteristics or uses.
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15. The amount of past cumulative production is not, by definition, a part of the resource. Nevertheless,
a knowledge of what has been produced is important to an understanding of current resources, in terms
of both the amount of past production and the amount of residual or remaining in-place resource. A
separate space for cumulative production is shown in figure 1. Residual material left in the ground
during current or future extraction should be recorded in the resource category appropriate to its
economic-recovery potential.
16. In classifying reserves and resources, it is necessary to recognize that some minerals derive their
economic viability from their coproduct or byproduct relationships with other minerals. Such
relationships must be clearly explained in footnotes or in an accompanying text.
17. Considerations other than economic and geologic, including legal, regulatory, environmental, and
political, may restrict or prohibit the use of all or part of a deposit. Reserve and resource quantities
known to be restricted should be recorded in the appropriate classification category; the quantity
restricted and the reason for the restriction should be noted.
18. The classification system includes more divisions than will commonly be reported or for which data
are available. Where appropriate, divisions may be aggregated or omitted.
19. The data upon which resource estimates are based and the methods by which they are derived are to
be documented and preserved.
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Section 2
Section 3
DISCUSSION OF NI 43-101
Section 4
DRILLING METHODS
AND PROCEDURES
4.2.
4.3.
4.4.
4.5.
REPORTING OF DRILLING ACTIVITIES AND RESULTS ....................................... 4-4
4.5.1.
DRILLING ACTIVITIES ........................................................................................ 4-4
4.5.1.1. Daily Shift Reports ............................................................................................. 4-4
4.5.1.2. Weekly Drilling Reports (Optional) ..................................................................... 4-5
4.5.1.3. Monthly Drilling Reports ..................................................................................... 4-5
4.5.2.
UPDATING OF WORKING MAPS AND SECTIONS ........................................... 4-5
4.6.
4.7.
4.8.
4.9.
4.10.
APPENDICES
Appendix 4-1
Appendix 4-2
Appendix 4-3
4.1. INTRODUCTION
Drilling is a key part of both the resource definition and grade control processes and is the
highest cost component of a Geology Departments budget. It is therefore essential that the
supervising geologist is completely familiar with all aspects of the drilling program, and that
the program is adequately planned and supervised and the results interpreted in a timely
manner.
This section outlines the procedures for the two most common forms of drilling used for
exploration and at the mine sites reverse circulation (RC) and diamond coring (DC), also
referred to as diamond drilling (DD). A third form of drilling conventional open hole - is
nowadays generally only used to drill open pit blast holes. The diagram below shows the
differences between the three systems.
4-1
Reference for Mineral Reserves and Resources
Most exploration offices and mine operations will have a formal system for approving drilling
expenditures. Exploration and development drilling programs typically require approval to
spend capital funds and must be reviewed by Barrick senior management. Grade control
drilling programs, if in addition to normal blast hole drilling and sampling, are usually funded
from the mine operating budget and must be reviewed and approved by appropriate
department manager(s). If a written proposal for the drilling is required, the following table is
provided as an example of a general guide for summarizing the proposed holes:
Hole
Number
Northing Easting
Elev.
Dip
Azim
RC
Depth
Dia
Depth
Geologist ..
Total
Depth
Comments
Date ..
Once agreement has been reached with the appropriate department manager(s), an
Authorization/Authority for Expenditure (AFE) is usually required, especially if capital funds
are to be used for the drilling program.
An alpha prefix should consist of 2 to 3 letters for location (e.g. NHS for New Holland
South) followed by 2 to 4 letters indicating the hole type (e.g. DD for diamond, RC or
GC for reverse circulation or grade control).
For ease of future electronic data entry, at least 4 numerals should be used (e.g.
NHSRC0005, not NHSRC5).
Drill hole re-entries (where RC holes are deepened by diamond drilling) should retain
the original hole numbering with the prefix modified (e.g. RC hole NHSRC0005 reentered as a diamond tail becomes NHSRCD0005).
4-2
Reference for Mineral Reserves and Resources
The project geologist must be familiar with the contracts payment (remuneration)
schedule and the specifications schedule in order to be able to run the drilling
operation efficiently and cost effectively.
If required, the contractor must submit an Environmental Health and Safety (EH&S)
Management Plan to the Project Geologist, Chief Mine Geologist, or the mine site
EH&S Manager for review.
The Project Geologist or Drilling Supervisor should ensure that the contractor has
Material Safety Data Sheets (MSDS) on the drill rig.
The Project Geologist must ensure that the contractors personnel undertake and
complete the appropriate site-specific safety training. (MSHA training in the U.S. In
Australia, such training is referred to as Inductions and Pit Passes). Care should be
taken to schedule any required training in advance as classes may only be conducted
on specific days.
If the drilling project is at a mine site, the contractors personnel must be shown the
locations and instructed in the procedures for using mine facilities that are commonly
required during the course of a drilling project, including the equipment lay-down
area(s), the wash-down area, the fuel farm, the source for drilling water, and the waste
area (rubbish tip).
If the drilling project is distant from a mine site, the Project Geologist must establish
locations for obtaining drilling water, fuel, and for disposal of waste. These locations
must then be identified to the contractor.
All Barrick personnel working near a rig should complete any safety training and/or
orientation (rig induction in Australia) required by the contractor.
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DRILLING ACTIVITIES
4.5.1.1.
Daily drilling activities are typically reported by drilling shift on a shift report form supplied by
the contractor. Prior to starting the project, the Project Geologist or Drilling Supervisor should
review the format of the shift report to ensure that it is sufficient for reporting the desired
drilling data. The following list of information that should be included on a typical shift report
is provided as a guideline:
Date.
Drilling progress (metres or feet drilled per shift, from and to).
It is very important that the Project Geologist or Drilling Supervisor obtain and sign the
contractor shift reports in a timely manner, in order to avoid disagreements with respect to rig
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delay (standby) time and drilling materials used (mud and other additives, cement, bits and
reamer shells, casing, casing bits and casing shoes) when the contractors invoice is issued.
If possible, the shift report should be signed at the end of each shift in the presence of the
driller submitting the shift report, so that any disagreements can be resolved promptly face-toface.
4.5.1.2.
HOLE NUMBER
Planned
4.5.1.3
COORDINATES
Actual
Northing
Easting
DEPTH (metres)
Elev.
Planned
HOLE
STATUS
Actual
A monthly report summarizing the drilling progress and results is usually required for the
monthly mine site department reports or exploration reports. Typically the minimum
information in the monthly drilling report includes:
A summary table in a format similar to the Weekly Drilling Report shown above.
A table summarizing significant assays from the drill intervals sampled, similar to the
following suggested form:
LOCATION
HOLE
NUMBER
COORDINATES
Northing
Easting
El
INTERVAL
From
To
LENGTH
Metres
GRADE
g/t
COMMENTS
A brief text that addresses areas where drilling was conducted, the type of drilling,
number of holes, and number of metres or feet completed in each area relative to the
project plan. The text should also comment on the significant assays and the
relationship of these assays to the current geologic interpretation.
4.5.2.
- The Geologist must plot geology and assays on working maps and cross
sections as soon as these data become available At a minimum, the data plotted should include:
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Timely plotting of these data ensures that the drilling program can be modified to take into
account the new information, while ongoing planning for subsequent drilling programs can
take advantage of new data and interpretations. It also provides information that is readily
available for review by supervisors and management.
Ensure that holes are drilled in accordance with the agreed drilling program.
Visit the drill rig at least once during day shift and at least once during night shift
(except underground drilling projects, where a mine Shift Boss may assume this
responsibility).
Issue all instructions to the drill crew and field assistants and handle disputes.
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Instruct the Driller to immediately stop drilling if any of the following occur:
Examine the core/RC chips at the end of the hole prior to stopping the hole at its final
depth.
- There are very few good reasons for stopping a drill hole in mineralization Depending on the location, the Project Geologist may have to meet the qualifications of a
Qualified Person or Competent Person (see Section 1 of this reference volume) for drill rig
supervision.
General housekeeping.
Sample size (RC drilling) and core recovery (DC drilling).
Core run blocks and sample bag labeling.
Cleaning of RC holes after each sample is taken.
Cleaning of rig sample cyclone (RC).
Cleaning and packing (boxing) of drill core.
Core orientation marks in place.
Check core/RC cuttings lithology.
Monitor hole deviation (where down-hole surveys are taken).
Anticipate possible changes to target depth.
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For diamond core holes, allow enough space on the site for all of the contractors
equipment, including core storage and sumps.
Arrange for site preparation equipment (if needed), and ensure that the site
preparation is completed as specified before equipment leaves the drill site. Site must
be level to prevent trip hazards.
Where necessary, flag off the drill site to limit the area covered by personnel and
equipment, particularly inside an active pit with mining equipment working nearby.
Request surveyors to set the drill collar location and hole azimuth line (foresight and
backsight).
- Allow enough time for site preparation to avoid costly drill rig standby time For underground drill sites, the following typical site layouts are provided for reference:
Site With Light Vehicle and IT Access
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For a surface diamond drill site, the following typical layout is provided for reference:
Suggested Site Layout for a Surface Diamond Drill Rig (Barrick Australian Version):
Note: In terrain of high relief, site width can be reduced to 10-12m and site length to 30m.
Sump 2 can be located in a separate cut below the drill site.
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Hole number.
Location of collar.
Hole dip and azimuth.
Expected hole depth.
Allowable deviation for dip and azimuth.
Prescribed depths for down-hole surveys (if single-shot survey tools used).
Although different Barrick operating locations may have site-specific procedures for setting
and aligning drill rigs, the following suggested procedures are provided as a guide for sites
where specific procedures are not in place:
The rig should be aligned on a surveyed azimuth complete with foresight (collar) and
backsight (sighter) stakes (pegs). Aligning rigs with Brunton transits or other handheld compasses should be avoided if at all possible.
The hole should be collared within 0.2m (1.0 ft) of the surveyed collar location.
The hole dip (inclination) must be set by placing an accurate clinometer (such as a
SOLA or equivalent clinometer with magnetic base) on the starter (quill) rod that is
tightly secured in the drill chuck.
The following diagrams show several methods for aligning different drill rig types:
CAB
DRILLER LINES
BY DRIVING
FLAGGING
1.24m
COLLAR STAKE
FLAGGING
TAPE
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STRING LINE
DRILLER LINES UP
ON STRING LINE
COLLAR STAKE
STEEL PIN
DEVIATION LIMITS
All drill holes deviate, depending on the lithology drilled, the presence of structures, the dip
(inclination) of the hole, and the skill of the driller. Drill hole deviation must stay within certain
limits, depending on the depth, size, and orientation of the targets. Depending on the project,
sometimes hole deviation limits are set in the Specification Schedule of the drilling contract.
These examples of deviation limits is presented for reference:
at collar
each 100m
each 100m
each 100m
The Project Geologist and Chief Geologist should carefully consider what if any deviation
limits should be addressed by a Specification Schedule.
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4.11.2.
CONTROLLING DEVIATION
In general, hole deviation can be controlled to some extent by a competent driller without
having to resort to the more expensive directional (Navi) drilling techniques. Skilled drillers
typically control deviation using methods that include:
Controlling the down-pressure (weight) on the drill bit. Down-the-hole hammers tend
to drill straighter holes because too much down-pressure impedes hammer action.
To assist with monitoring deviation, a stainless steel rod can be used behind the RC hammer
or diamond barrel to allow an accurate azimuth to be read from an Eastman camera.
A more detailed account of the techniques used to control deviation is presented in Appendix
4-1.
4.11.3.
REMEDIAL ACTION
If the permissible deviation limits are exceeded, the following course of action is
recommended:
The driller must notify the Project Geologist or Drilling Supervisor immediately and the
rig should be placed on non-chargeable standby (as provided in the drilling contract).
The Project Geologist must quickly make the decision whether or not to continue
drilling, having plotted the hole on the working maps and sections and consulted with
management, if necessary.
If additional decision time is required, the Project Geologist may wish to consider
moving the rig to a different hole location.
If necessary, the deviated hole may be re-drilled. Depending on the provisions of the
drilling contract, re-drilling may be at the contractors expense.
The Project Geologist must not over-emphasize penetration rates because most
drillers gladly will react and increase the rate (especially if contract price is based on
hole advance), and deviated holes are the predictable result.
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4.12.1.
Eastman camera surveys generally are conducted by the drilling contractor or Barrick site
technicians in order to monitor hole deviation. Originally designed as a rapid way to track
hole deviation in oil exploration, Eastman survey tools consist of either single shot or multishot camera systems. Typically, single shot cameras have been used for mineral exploration
because of camera durability and the substantially lower replacement cost.
The
recommended procedure for conducting Eastman single shot surveys is as follows:
Single shots should be taken at regular, pre-determined intervals in the hole (typically
every 30m or 100ft of hole depth).
The survey disc should be presented to the Project Geologist in a paper envelope
labelled with drill hole number, date, depth, dip, azimuth and camera number.
The Geologist should always verify the survey readings on each disc. Care should be
taken to adjust the magnetic azimuth readings on the discs for the magnetic
declination appropriate for the project location.
If the survey shot is taken with the camera situated inside the drill rods or in magnetic
ground, the azimuth reading will be incorrect, and should be disregarded.
Dip readings should always be correct, since the clinometer in the survey tool is not
affected by magnetics.
An example of a single-shot survey disc is shown in the diagram below. Note that the
inclination numbers (18) represent units of 10o. These are measured from the vertical and
are subtracted from 90o to calculate the dip of the hole (e.g. 8 = 10o dip). The bearing
numbers represent units of 10o and are equivalent to the magnetic azimuth.
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36
26
34
4.12.2.
28
32
30
Other commonly used down-hole survey instruments that measure dip and azimuth include:
MAXIBOR Systems Like GYRO systems, these unique down-hole survey tools can
be used inside drill rods and casing and are not affected by magnetic constituents in
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the rock. Arguably the simplest of all survey tools in concept, a number of mining
companies have selected MAXIBOR systems in order to provide the greatest inhouse flexibility for obtaining down-hole surveys on a project. The MAXIBOR
system is the best for all types of holes, but is superior to the other systems in holes
flatter than 45o.
4.12.3.
Arrange and execute a formal contract agreement and complete required safety and
mine site orientations (inductions).
Safeguard the hole collars prior to surveying to prevent accidental loss of hole access.
Complete a written checklist of hole conditions that could increase the risk of tool loss
(old stopes and other underground workings, broken ground and problematic
geological formations) and provide it to the contractor before surveying commences.
Obtain preliminary survey results before the contractor leaves the site, examine the
results and resolve any obvious errors with the contractor.
Ensure that the correct and final survey data are entered into the drill hole database.
DUST SUPPRESSION
Dust produced by RC drilling affects general visibility and is a hazard to the health of Barrick
and contractor employees. The following systems and practices are used on RC drill rigs to
suppress dust. These systems must be maintained in good working order:
The outside air return at the drill collar must be dampened by water injection or
passed through the fines cyclone.
The dust from the top outlet on the sampling cyclone must be removed by the fines
cyclone. Water MUST NOT be sprayed into the cyclone inlet to suppress dust, since
wetting the sample passing through the cyclone causes contamination of the sampling
equipment.
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- Water MUST NOT be sprayed into the cyclone inlet to suppress dust
The dust at the sample splitter can be minimized by ensuring that the upper door on
the collection box is always closed when the sample is dropped through the splitter.
An approved dust mask must be worn by all personnel who are exposed to dust where
adequate dust control is not practical.
The Project Geologist or Drilling Supervisor should shut the rig down if the dust
suppression equipment is not working correctly.
4.13.2.
WASTE CONTROL
For drilling projects at operating mine sites, washing down and servicing of equipment, cleanup of hydrocarbon or other chemical spills, and trash (rubbish) disposal should be performed
in accordance with site-specific regulations and policies in order to avoid contamination of drill
sites. In particular, oil or fuel leaks from machinery should not be tolerated in areas of gold
mining and processing at any time, since hydrocarbon contamination of ore feed can cause
gold loss in CIL plants.
The recommended procedures to be followed at remote drilling locations, where site-specific
procedures may not be in place, include:
In the event of fuel or oil spillage at the drill site, the driller should immediately notify
the Project Geologist or Drilling Supervisor, who will advise on the procedure to collect
and dispose of the contaminated rock or soil. Clean up of spills should be at the
contractors cost, if not otherwise specified in the drilling contract.
- Oil or fuel leaks from machinery should NOT be tolerated in areas of gold
mining and processing at any time
Water generated from drilling operations must be contained in sumps at the drill site.
4.13.3.
SITE REHABILITATION
Site-specific procedures should be followed for rehabilitation of drill locations. Generally, sitespecific procedures will contain guidelines or policies for:
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Backfilling of sumps.
The samples are mixed up, damaged, contaminated, lost, or poor (unacceptable)
sample recovery has occurred.
The hole did not reach its target because drilling equipment (rods, core barrels,
hammers, or bits) lost down-hole could not be recovered.
The contractor did not inform the Geologist of dangerous drilling conditions.
The decision to re-drill a hole should be based on consultations with project management and
the contractors on-site representative. During these discussions it should be determined if
the cost of re-drilling the hole should be borne by the contractor.
4.15. RC DRILLING
4.15.1.
4.15.1.1.
4.15.1.2.
Compressed air is forced down between the inner and outer walls of the drill rod to the
hammer.
The hammer typically activates at 30 strokes per second (at 600 psi).
The high-pressure air passes through the inside of the hammer and out through holes
in the face of the drill bit. The air is directed back in through holes in the centre of the
drill bit, transporting the drill cuttings into the innermost pipe in the drill rod string.
The air and drill cuttings then travel from the drill bit up the inner pipe of the drill rods
to the surface.
The drill cuttings are discharged through the rotary top drive, the bullhose, and into the
cyclone assembly.
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4.15.1.3.
Produces a larger sample than diamond core, which can result in improved sampling
statistics under normal conditions. Provides drier samples than open hole drilling.
Much less risk of contamination than open hole drilling methods (such as rotary air
blast holes).
4.15.1.4.
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Sample interval breaks are less accurate. Unique samples of narrow features cannot
be obtained.
4.15.1.5.
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c) Tri-cone bits
Tri-cone bits are used in lieu of a hammer for a limited number of applications. These include
drilling of clay formations, badly fractured ground and where excessive water can cause
hammers to experience hydraulic lock. Large diameter tri-cone bits are also used to ream out
holes prior to casing.
The RC tri-cone has a wider centre channel to increase the flow of sample up the central
pipe.
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4.15.1.6.
RC Drilling Equipment
Compressor onboard the rig rated at 250 to 350 psi and 500 to 800 cfm.
Auxiliary compressor and booster on a separate truck, capable of boosting air to 750 psi
and 1800 cfm. This is required to speed up penetration and maintain dry samples.
Rod string of 4.5-in diameter. Smaller rods cause greater hole deviation.
Support vehicles.
4.15.2.
An organized geologist will have a checklist of personal equipment that should be carried in
the truck when visiting the drill rig. This will save unnecessary trips back to the office for
forgotten items. A typical checklist will include the following:
PPE (steel-capped boots, hard hat, reflective vest, ear plugs, safety glasses, dust masks,
sunscreen, and gloves. For underground projects, a safety belt, cap lamp and self
rescuer should be included).
Drilling program particulars (hole numbers, azimuths and dips, projected depths).
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Sieves.
Tape measure.
Hand lens.
Acid bottle.
Weighing scales.
Clinometer.
Compass.
Geology pick.
Flagging tape.
4.15.3.
RC SAMPLING
Sampling on RC drill rigs will always be accomplished using a cyclone and splitter. There are
many different sampling systems available on the market and attached to drill rigs. Not all of
these perform adequately and the sampling system should be approved before drilling starts.
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This type of system can deliver 99% of the sample to the splitter but has the disadvantage of
being large in size and weight.
4.15.3.1.
Cyclone
The cyclone must be matched to the air capacity of the drill rig. It should be capable of
reducing dust loss from the top vent to less than 5%. The operating principle of a cyclone and
critical dimensions are shown in the two figures below.
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4.15.3.2.
Splitter
Either a riffle splitter or a cone splitter should be used in each RC sampling system
a) Riffle Splitter
A riffle splitter can be manually operated as a separate unit, or built into a vertical
arrangement beneath the cyclone as a multi-tiered splitter.
The riffle width must accommodate the largest particle in the sample.
The sample must be put evenly through all the riffles simultaneously in order to
achieve a representative split.
The riffles in each tier must be easily accessible for cleaning after each sample is
taken. This is usually performed either by spraying the splitter with compressed air or
vibrating the splitter with a rubber mallet.
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b) Cone Splitter
The principal features of a cone splitter are:
It is necessary to have a collection box and a delivery box above the cone splitter so
that the sample is dropped evenly over the cone.
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The width of the hood below the cone determines the weight of the sample split
(subsample). The size of the hood cannot be easily altered as it is welded into place.
It is necessary to have a rotary vibrator on the delivery opening above the cone in
order to facilitate cleaning, particularly with damp or wet samples.
Two or more hoods of any size can be built into the cone splitter allowing additional
sample splits (subsamples) to be taken which are all representative and thus usable
for check sampling.
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4.15.3.3.
Wet Samples
Collection of wet samples should be avoided if at all possible by the use of an auxiliary
compressor and booster. Where wet samples are unavoidable due to ground water inflow,
the following recommended procedure should be considered in the absence of site-specific
procedures.
During initial collection of the sample, the splitter should be removed and the entire
sample collected in a plastic bag. If the riffle splitter has been contaminated, it should
be thoroughly cleaned.
If the assay of the preliminary sample is greater than 0.2g/t, the entire remaining
contents of the plastic bag should be dried thoroughly, then broken up and passed
through the riffle splitter in order to provide a more representative assay split
(subsample). The assay of the second split should then be tagged as wet and used
to replace the original assay in the database.
Wet splitting can be conducted safely through a cone splitter, provided the system is
monitored after every sample for possible contamination and hang-up of sample in the
cone.
The driller should be instructed to record the hole depths at which detectable water
inflow is encountered, and to estimate the flow rate in litres per second or gallons per
minute.
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The geologists responsible for logging the cuttings should ensure that this information
is transferred to the logging sheets (under Comments, or other appropriate heading).
At the end of the drilling program, the Project Geologist should ensure that a summary
of the water inflow data is provided to the mine engineers responsible for mine
planning and dewatering.
If an RC hole encounters a stope or cavity and there is no sample return, the following
recommended procedures should be followed, if there are no site-specific procedures in
place:
Continue the sample number sequence by placing empty numbered bags in with the
bags containing samples.
-The driller must be instructed to spend as much time as required to reestablish full sample return when the hole once again encounters good ground4.15.3.5.
Drilling must stop while air circulation is maintained in order to flush out all remaining
portions of the sample at the end of each prescribed sample interval.
The inside of the cyclone and the collection box must be thoroughly cleaned out once
per shift when drilling in fresh rock, and more often, as required, in oxide rock or when
drilling under wet conditions.
Sample bags must be tied off immediately after filling to prevent external
contamination.
4.15.3.6.
The sample interval is usually 1.0 or 2.0m (5.0 or 10.0ft in U.S.), or as determined by project
management.
After each sample interval, the driller must stop drilling for 5 to 15 seconds, without turning the
air off, in order to allow any of the sample remaining in the hole to be blown into the cyclone.
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4.15.3.7.
Samples for assay should be collected at the rig in accordance with established site- or
project-specific procedures. The general procedure is as follows:
Normally one split (subsample) of 3 to 4kg is designated as the assay split (assay
subsample) and is collected in a calico or heavy-duty plastic bag for assay. The
assay split (subsample) weight may need to be greater than 3 to 4kg for problematic
ore types, if routine check sampling so indicates. If this is the case, further evaluation
of the sample size is warranted, including construction of a sampling nomograph.
The bags containing the assay split (assay subsample) are numbered according to
site-specific procedures.
The remainder of the sample from the splitter is called the sample reject or rig reject
in the U.S. (field residue in Australia). This sample is handled or stored according to
site-specific procedures. If retained for storage, the bags containing the sample
rejects (field residue) should be labelled with hole depths.
If not collected separately at the splitter, the samples used for logging and for chip
trays must be taken from the sample reject (field residue) bags only.
A consistent sample weight in fresh rock must be obtained. This can be monitored by
weighing samples on a set of scales on a regular basis. Note that it is impossible to
collect the entire sample from the hole interval, since some loss will occur from the
outside return (at the collar) and from the sampling cyclone vent (as dust).
Where no sample is recovered (i.e., when the drill passes through stopes or other
voids), it is good practice to continue the numbering sequence uninterrupted through
the void area. Although this results in empty numbered bags, it helps to avoid
confusion and inconsistencies when data are entered into the drill hole database.
4.15.3.8.
The insertion of standard (SRM) and blank samples into the sample preparation and
analytical stream is an excellent way to monitor laboratory accuracy. Although a given
Barrick property may have its own set of guidelines for submitting standards and blanks with
sample lots dispatched from a project site, a recommended industry-accepted procedure is
outlined in Section 7, QA/QC for ASSAYING AND SAMPLING, of this reference volume.
4.15.3.9.
Sample Dispatch
Careless dispatch of samples to the laboratory can be a common source of problems such
as lost samples, incorrect sample numbers and sample damage during transport. Here are
some recommended guidelines for proper dispatch of samples:
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Prior to dispatch to the laboratory, a Sample Manifest must be prepared for each drill
hole that includes the following:
A listing of the assay split (subsample) numbers that corresponds to the numbers
written on the sample bags.
Alongside the sample numbers, the sample interval corresponding to that sample.
Slots on the sample list every 20th sample number for the insertion of a blank
sample (see Section 7, QA/QC for ASSAYING AND SAMPLING)
Sample bags should not be picked up for transport to the laboratory until a responsible
person has checked off the number on each bag against the log sheet. If a numbering
error is found, it must be resolved before the bags are dispatched to the laboratory.
Likewise, samples should not be dispatched until the numbers on the sample sacks
are checked against the Sample Manifest in order to account for all samples.
On the day that samples leave the project site a dispatch sheet should be faxed to the
laboratory before the end of shift.
4.15.4.
For every RC drilling program, 5% of the samples should be checked as part of the quality
control program.
a) Check Assaying
This is required to monitor potential assay bias at the Primary (Principal) Laboratory. A
selected number of pulps from the assay splits (subsamples) analyzed by the primary
laboratory are sent to a second laboratory for re-assay.
b) Check Sampling
This is required to verify that the assay subsample that is split from the original sample is
representative of that sample.
Instructions for performing Check Assaying and Check Sampling are outlined in Section 7,
QA/QC for ASSAYING AND SAMPLING, of this reference volume.
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4.15.5.
Rejects and pulps from the various stages of the sampling and analytical processes should be
stored for future re-assaying, metallurgical testing (see Section 10, METALLURGICAL DATA
COLLECTION AND TESTWORK), or reference purposes. These rejects (residues) and
pulps include:
a) Assay splits (subsamples)
d) Metallurgical samples
See Section 10
4.15.6.
RC CHIP LOGGING
The Project Geologist should make sure that the chips collected at the RC rig are logged
promptly using the standard log sheet established for the particular site or project. The
degree of detail in the logs will depend on the local geology and the purpose of the drilling
program. For example, programs designed for resource definition and site condemnation
typically require a lower level of logging detail.
4.15.6.1.
Alteration.
Contacts between alluvium and bedrock, the base of the zone of complete oxidation
and mixed (transition) zone, and the contact between the mixed (transition) zone and
sulphide (sometimes referred to as fresh rock) zone.
Other features that may be relevant to interpreting local geology, such as veining, rock
texture and fabric (if distinguishable), and grain size.
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4.15.6.2.
During mining of a deposit, the geology is usually reasonably well understood, and
logging of chips where RC drilling is used for grade control does not need to be done
in great detail. Because speed is normally of the essence, only the features that are
locally critical to grade control should be logged.
Diamond core drilling has been used for more than 100 years to discover, delineate and
define ore deposits throughout the world. As a result of technical advances, it remains the
primary method for providing data used by geologists, mining engineers, and metallurgists to
discover and develop mines.
4.16.1.1.
The principal features of the diamond drilling (diamond core) method are listed below:
The core is forced from inside the bit into the core barrel (which rotates with the drill
rods) where it is collected and protected inside a non-rotating inner tube.
Water and mud additives are pumped down the rods in order to:
The additives can also stabilize the wall of the hole in bad ground by forming a mud
cake on the surface of the wall. Sumps at the surface of the drill rig are used to
contain the return water and mud so that there is no contamination of the drill site, drill
cuttings can settle out of the mud and the mud can be re-circulated.
When drilling conventionally, the rod string must be pulled to retrieve the core. With
more common wireline systems, the core is removed from the core barrel without
having to pull the rod string by using an overshot assembly, which is sent down the
rods and attached to the head of the inner tube. A wireline cable attached to the
overshot then pulls the inner tube and core out of the hole.
The wireline is also used to run down-hole survey tools and core orientation tools
down the drill rods (See Section 4.16.9).
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4.16.1.2.
The force required to advance the drill bit through the rock is supplied by the hydraulic
head and the weight of the drill rods.
Impregnated diamond (most commonly used) while the bit rotates, the matrix
holding the diamonds slowly erodes, exposing new diamonds which continue the
cutting process.
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The reamer shell is located between bit and core barrel and is used to maintain hole
gauge.
The drilling medium is water, with mud additives as required for hole stability.
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Conventional
The entire rod string is pulled to retrieve core from the core barrel.
Wireline
The inner tube holding the core is recovered from the core barrel by lowering an
overshot on a wireline through the rod string (the rod string is not pulled).
4.16.1.3.
Compared to the RC drilling method, diamond coring offers the following advantages:
It is the only drilling method that allows collection of structural orientation data.
Diamond rigs can be more portable than RC rigs and require less support when
operational.
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4.16.1.4.
4.16.1.5.
Core Sizes
Not To Scale
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4.16.1.6.
The equipment normally supplied by a contractor to perform diamond drilling consists of the
following:
The following equipment is supplied by Barrick for collecting, processing and storing the core:
Core trays.
Marker (paint) pens for labelling run blocks, core boxes and blocks that note where
samples are removed for making thin sections or performing geotechnical tests.
Logging table.
Sample bags.
4.16.2.
An organized geologist should have the proper personal equipment when visiting the diamond
drill rig or logging core in the core shed or core yard. This will save on unnecessary trips back
to the office for forgotten items. The following typical checklist is provided as a guideline:
PPE (steel-capped boots, hard hat, reflective vest, ear plugs, safety glasses,
sunscreen, gloves). If the project is underground, include a cap lamp and self rescuer.
Drilling program particulars such as hole azimuths, dips and drill site locations.
Data logger or appropriate laptop computer and spare battery (if electronic logging).
Pencil, eraser.
Tape measure.
Hand lens.
Acid bottle.
Core protractor strip for measuring structure angles with core axis.
Clinometer.
Compass.
Geology pick.
Flagging tape.
Camera.
Spare film.
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4.16.3.
Diamond core holes are sometimes pre-collared to reduce overall drilling costs per hole. Precollaring is simply the drilling of the upper alluvial or unmineralized portion of a core hole
using open hole rotary or RC methods. Pre-collars are usually drilled using an RC rig or a
multi-purpose diamond drill rig capable of RC drilling.
Choosing the pre-collar depth depends on:
Hole deviation in the pre-collar portion of the hole must be carefully monitored so that the
diamond core portion will reach the target. (In Australia, this portion of the hole is called the
diamond tail). Pre-collars are usually cased to prevent diamond drill rod vibration and
degradation of the alluvial portion of the hole, and to seal off weathered ground.
Reaming and casing are usually performed to protect the diamond hole from collapsing in
poor ground. Reaming is simply the enlarging of the diameter of the hole in order to allow
installation of the larger-diameter pipe that serves as the hole casing.
4.16.5.
CORE RECOVERY
The goal of a diamond drilling program should be to obtain maximum core recovery at all
times. Poor core recovery raises doubts that the recovered portion of the sample is
representative of the drilled interval. Unfortunately, some drillers prefer to push for maximum
drill advance, often to the detriment of recovery. This can often happen when a rig is run 24
hours per day and the different shift crews tend to compete for footage. The Project
Geologist or Drilling Supervisor should always be aware of declining core recovery or
sporadic poor recovery and how these may relate to drilling advance rates.
The language of the drilling contract should make it clear that maximizing core recovery is a
prime consideration for the drilling contractor.
be recorded as a length measurement for each drill run and should not be logged as a visual
estimation of percentage recovery.
If poor core recovery is due to soft or broken ground, a triple tube core barrel will help
maximize core recovery. When electing to use triple tube tools, the contractor should be
asked to supply two additional sets of tube splits for the innermost barrel.
If triple tube core barrels are used, the Geologist should perform the following logging
operations while the core is still in the split tube, before the core is disturbed or transferred
into a separate core tray or box:
4.16.6.
4.16.6.1.
Driller Tasks
The driller should present the diamond drill core for logging/sampling as follows:
Core should be free of oil and grease and placed in appropriate core trays or boxes.
Core is placed in the box or tray like the lines of text in a book, with an arrow on the
tray at the start of the sequence.
Hole number
Tray/box number
Depth from / to
EOH (End of Hole) written on last tray or box.
Run (marker) blocks should be placed after each drilled interval and labelled with the
drillers depth measurement.
START
0.0m
1.50m
3.00m
4.25m
CAVITY
4.50m
4.90m
PLAN VIEW
HOLE NUMBER
DEPTH FROM/TO
BOX NUMBER
SIDE VIEW
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- Check that the driller measures depth based on length of drill steel down
the hole, NOT length of core
Where possible, place TD (True Depth) on marker block where drill runs end with a
face break (i.e., core broke off even with the face of the core bit).
The position of known core loss should be clearly indicated with marker blocks.
4.16.6.2.
The Geologist or Field Assistant should use site- or project-specific procedures, or the
following recommended procedures when marking up diamond drill core:
For core that is to be oriented, remove the core from the tray or box and place it on an
orientation rack (usually a piece of upturned angle iron).
Where possible, fit the core back together in the orientation rack. If core is broken or
has been ground, use any geological features observed (rock type, foliation, colour,
veining) in order to assist with fitting the core back together.
For oriented core, draw a reference line along the bottom (lowest point) of the core,
i.e. closest to the orientation mark, and draw arrow marks pointing in the down-hole
direction.
- The orientation line should always indicate the BOTTOM of core in the hole
Where the orientation mark is of good quality and core fits well, draw a solid reference
line. If poor, draw a dashed line.
Non-oriented core should also be fitted and splitting (sawing) lines drawn, if required.
While splitting lines should be as consistent as possible down the entire drill hole, the
lines should ensure that each half core is a mirror image of the other half after splitting
to the extent possible.
Once fitted, the core is then marked up with sample metre or footage interval marks.
Look for face breaks, as these will be the only accurate depths in the hole.
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Face breaks have a ridge that protrudes from the core circumference and the face
is commonly convex. This results from the core breaking directly off the bottom of
the hole when the rods are pulled and the core lifter contracts around the core
More commonly, the core breaks off some distance above bottom and is picked
up in the next drilled interval.
BREAK OFF
FACE BREAK
DEPTH ON
MARKER BLOCK
At a face break, the depth written by the driller on the run (marker) block is equal to
the length of drill steel in the hole.
Mark-up work should progress up and down the hole from selected face breaks.
Metre/footage intervals on the core should be marked using a permanent marker.
Note that the depth on the run (marker) block may not match up with measurements
because:
Core from the run above the marker block may have broken short and be
included in the next run (sometimes referred to on drillers logs as stick-up).
The driller has rounded the depth measurement to the nearest foot or 10cm.
On the half of the core that is to be retained after splitting or sawing, write all
metre/footage marks and geological labels on the right-hand side of the reference line
where the line is uppermost when the core is held in front of the Geologist and the
down arrow is pointing away.
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4.16.7.
CORE PHOTOGRAPHY
For exploration and pre-development diamond drill holes, all core should be photographed
prior to splitting, sawing, or sampling, using either a conventional camera or a digital camera.
When practical from a logistics standpoint, production (stope delineation) holes should also
be photographed if whole core is sent for assay. If site- or project-specific procedures are not
in place, the following recommended procedures should be followed:
Do not photograph or record digital image of core until mark-up has been completed.
Keep tray out of direct sunlight to prevent harsh shadows and reflection.
When using a conventional camera, a 28mm lens allows for a closer distance
between camera and tray.
Store digital images in a permanent directory as .jpg files. If necessary, the images
can be cropped and plotted using a program such as CorelDraw.
4.16.8.
CORE ORIENTATION
Oriented diamond drill core can provide valuable structural information for interpreting
geology and providing geotechnical evaluation of ground conditions.
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It is best to consider collecting oriented core data only for holes with dips (inclinations)
between minus-30o and minus-80o (approximately) since most orienting methods rely on
gravity to properly position the apparatus that indicates the bottom side of the hole.
Typically, one orientation reading is taken every one to three runs. However, the frequency
for taking orientations is also highly dependent on:
The importance of the structural data to be measured (i.e. faults/jointing that could
seriously affect pit slope stability or the safety of underground openings.
How easily the core can be fitted together between drill runs.
a) Spear device.
In addition to the spear and Van Ruth devices, the Christensen scribe (generally the most
reliable), the ball-mark method and the simple use of modeling clay to take an impression of
the bottom of the hole, are alternative methods for orienting core.
4.16.9.
All diamond core should be logged prior to splitting, sawing, or sampling for assay. The
degree of detail will depend on the local geology and the purpose of the drilling program. For
example, exploration and pre-development holes typically are logged in greater detail than
production (stope definition) core holes.
The core log sheet that is standard for the site or project should be used. In the absence of
site- or project-specific logging procedures, the following recommended guidelines should be
used:
Check that core mark-up is complete and correct (see Section 4.16.6).
Always wet the core to better reveal colour, alteration and textural features.
Briefly examine the entire hole to get a feeling for the overall geology.
Proceed to log in detail.
- When logging, the Geologist must strike a balance with respect to detail - DO NOT LOSE SIGHT OF THE BIGGER PICTURE!!!
If the unit or lithology is the same as one already described in the hole, then the
notation as from interval ___-m (ft) to ___-m (ft) will suffice for a description.
4.16.9.1.
When logging core from exploration or pre-development resource definition drill holes, siteor project-specific logging procedures should be followed. In the absence of these
procedures, as a minimum the following items should be logged:
Structure.
Alteration.
Contacts between alluvium and bedrock, between the base of any zone of complete
oxidation and mixed (transition) zone and between the mixed (transition) zone and
sulphide (sometimes referred to as fresh rock) zone.
Non-mineralized structures, including angles with longitudinal core axis (alpha and
beta angles) as described in the following Section 4.16.10, gouge and/or clays along
structure surfaces, striations and slickensides. When using triple tube core barrels,
see guidelines in Section 4.16.10.
Veining.
Core recovery.
4.16.9.2.
At the mine production stage, the geology is usually reasonably well understood, and the
logging of holes designed to aid stope development and design does not need to be as
detailed as for exploration. With production drilling, also, speed is usually of the essence.
Hence, only those features that are critical to better definition of stope shape or possible
ground problems must be logged as a minimum, such as mineralization contacts, structures,
and alteration. However, if time and manpower permit, a detailed log for all diamond core
holes is warranted.
4.16.10.1. Guidelines
The determination of which structures should be logged and how many dip and dip direction
measurements should be recorded is often confusing. Prior to logging, it often helps to first
broadly scan the entire hole and determine which structure types are present (such as quartz
veins), make a rough assessment of how many sets of a particular type are present, and
structures that are important enough to log. It is also important to develop consistent codes
for structure types such as foliation, veins and joints, as well as for geological contacts.
Once detailed structural logging begins:
For each structure logged, record a dip and dip direction whenever there is a
change in orientation.
For important structures, such as major faults or veins, be sure also to record the
dips and dip directions of these structures on the graphic portion of the log sheet
so that the information is readily available later when using the log to interpret
sections.
- Always keep the big picture in mind when logging structures 4.16.10.2. Measurement of Dip and Dip Direction
The true bearing of any geological feature, contact or structure can be determined from
oriented core obtained from an inclined hole. Two common approaches are:
This device imitates the orientation of the drill hole. It has the advantages that:
The dip and azimuth of a structure can be measured directly off the core.
The true bearing of important geological features can be recorded as they are
logged. This gives the geologist a better understanding of key structural
relationships as logging proceeds.
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All diamond core should be sampled for assaying throughout the entire hole, even if
in waste rock, except by direction from the Geology Superintendent.
As a general rule, sample interval breaks should respect the contacts between
significant geologic units or zones based on:
Mineralization.
Rock type.
93.7 to 94.7m
94.7 to 95.6m
95.6 to 96.0m
96.0 to 97.0m
Except where breaks are necessary because of geology, sample intervals are
commonly set at regular 1.0m or 2.0m lengths (2.0 ft or 5.0 ft in the United States).
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Except under special circumstances, the minimum sample interval length should not
be less than 0.25m (0.50 ft in the United States).
In order to avoid contamination between ore and waste, sample interval breaks should
be marked just outside of the ore contact in the waste.
In order to avoid confusion in marking core, the colour used to note sample intervals
should not be used for any other marks.
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Outlined below is the procedure which should be followed when cutting core with a saw:
Be familiar with the standard operating procedure for using a diamond saw (an
example is shown in Appendix 4-3).
Lay the core trays out in the order they are to be cut.
Check that the core has a line drawn along its length by the geologist, indicating the
cutting position. This may be different from the reference line used in core orientation.
Check that there are arrows along the line that indicate the down-hole direction.
The cut should be placed 5mm to the left of the line (when holding the line uppermost
and the arrow pointing away from you) and should follow the line consistently.
Place both halves of the cut core back together in the tray.
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Conventional screw-type or hydraulic splitters break the core between two hardened knife
blades. In very competent rock such as granites, monzonites, or other intrusives, nearly
identical core halves can be obtained with these traditional tools. However, when attempting
to split core that has been drilled through bedded or foliated rock, conventional splitters tend
to induce fracturing along the weaker bedding and foliation planes, and the core is often
broken into disc-shaped pieces or reduced to fragments or rubble.
Care must be taken in certain cases when rock quality or mineralogy may cause sample loss
in the form of sludge into the water basin beneath the diamond saw. Under these conditions,
core splitting is absolutely necessary in place of sawing.
A Sample Manifest must be prepared for each drill hole that includes the following:
A listing of the assay split (subsample) numbers that corresponds to the numbers
written on the sample bags.
Alongside the sample numbers, the sample interval corresponding to that sample.
Slots reserved on the sample list every 20th sample number for the insertion of a
blank core sample (see Section 7, QA/QC for ASSAYING AND SAMPLING).
Always sample the left side of the core (the one without the marked line).
For mineralized core, place a plastic bag inside the calico or canvas bag to prevent
gold or other metal loss through the pores in the bag.
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Samples should not be dispatched until the numbers on the sample sacks are
checked against the Sample Manifest in order to account for all samples.
Dispatch the unprepared primary samples, check assay splits (if any), SRM pulp splits
and blank samples to the laboratory.
a) Check Assaying
This is required in order to monitor potential assay bias at the primary laboratory. A
selected number of pulps from the assay splits (subsamples) analyzed by the primary
laboratory are sent to a second laboratory for re-assay.
b) Check Sampling
This is required in order to verify that the assay subsample that is split from the original
sample is representative of that sample.
Instructions for performing Check Assaying and Sampling are outlined in Section 7, QA/QC
for ASSAYING AND SAMPLING, of this reference volume.
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APPENDICES
APPENDIX 4-1
CONTROL OF HOLE DEVIATION
INTRODUCTION
Drill holes deviate in both dip and azimuth. The course of a drill hole is affected by ground
conditions, down-hole equipment and operator techniques.
The ground conditions that affect the course of a hole are angle of incidence of the bit to the
bedding or schistosity, variations in hardness of rock layers and erosion of soft formations by
drilling fluids.
Aspects of down-hole equipment which can influence the course of a diamond drill hole
include the bit profile and the core barrel design or configuration. In RC drilling, the number,
weight and location of stabilizers and subs have an influence.
The driller can cause holes to deviate from their intended course by applying too much downpressure (weight) on the bit, by continuing to drill too long with a worn bit, or by tolerating
excessive vibration in the drill string when drilling soft formations.
Two methods are available to direct the drill hole to the target zone. The first is to make use of
natural factors or drilling techniques. The second is to change the course of the hole artificially
by wedging.
NATURAL DIRECTIONAL CONTROL
The geologist should first check what hole deviation occurred in any earlier drilling in the area
before siting the hole and determining its angle. Consultation with the drilling contractor at this
time is essential, as his experience in deviation control will be required to get the hole to its
target. As a general rule, the larger the diameter of the hole, the straighter it should be. The
cost of the larger diameter hole must be weighed against the necessity for achieving the
straightest possible hole.
Once the hole has been collared, the following equipment and techniques will assist to keep
the hole straight:
Hole flattening may be induced by reversing the above. Hole steepening is more difficult, but
may be achieved by use of a heavy barrel and appropriately placed stabilizers.
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Frequent hole surveys are essential to keep geologist and driller aware of the course of the
hole, and to initiate corrective measures if necessary.
ARTIFICIAL DIRECTIONAL CONTROL
Methods of correcting an off-course hole are arc cutting, wedging or using a down hole-motor.
Because arc cutting is seldom used today, no description is provided for this method.
Wedging a hole can achieve a maximum of about 1.5o deflection per wedge, and although
repeated wedgings are an option, proper minimum intervals between wedges must be
maintained to avoid a severe a dog leg in the hole.
There are three types of wedge:
The Casing wedge is simple. Because the wedge is screwed on to the bottom of the casing,
a reduction in hole size is required. After setting the wedge, drilling continues normally with
the wedge deflecting the smaller-diameter hole.
The Hall Rowe wedge consists of a steel deflecting wedge which remains in the hole. A
drive wedge is first placed in the hole at the appropriate depth and its orientation checked.
The steel deflecting wedge is set at the surface so that when its lower end mates with the
drive wedge, it will be at the required orientation. The deflecting wedge is lowered into place
on the rod line and detached by shearing brass rivets. Drilling off the wedge is done initially
with a bull nose non-core bit for approximately one metre. The hole is then reamed to full size,
and drilling can continue with the full-size bit. A number of trips into and out of the hole are
necessary. The complete wedging operation can mean a delay of two or more shifts
depending on the depth of the hole and the competence of the drill crew. A disadvantage with
this wedge is that some 4 to 5 metres of original hole are lost.
The Clappison Retrievable wedge has several advantages over the Hall Rowe wedge.
These are:
Wedging takes place at the bottom of the hole, with no loss of sampling ability.
Speed of installation (at 300m, setting of the wedge and a 3m hole advance takes
about one and a half shifts).
The equipment consists of a wedging assembly and a reaming assembly. The operation
consists of lowering the wedging assembly, orienting the deflecting wedge and locking it in
position, and drilling a pilot hole for 1.5m. The full assembly is then retrieved from the hole.
The reaming assembly is lowered and the pilot hole reamed to full gauge. Wedge orientation
is achieved by alignment clamps, acid etch method, mule shoe or Unger device.
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The simple and inexpensive Unger device consists of an orientation sub attached to the
wedge. A steel rod (similar to an inverted billiard cue) with a wad punch on the tip is lowered
on the wire-line to obtain a symbol from the orientation disc. The wedge can be rotated until
the symbol from the wad punch indicates the wedge is in its intended orientation.
Bottom Hole Motors The Dyna-drill and the Navi-drill are both bottom hole turbine units
with a non-core bit attached to the drill string (which does not rotate). Drilling fluid is pumped
down the drill rods causing the turbine rotor, with the bit attached, to rotate and the hole to
advance. By incorporating a bent sub above the tool, a lateral force between the tool and the
rock formation causes the hole to develop an arc. The Unger device can be used to orient the
bent sub and therefore the course of the arc that is cut by the bit.
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APPENDIX 4-2
MAXIMIZING CORE RECOVERY
Maximum penetration rates and high core recovery are not necessarily complementary. To
maximize penetration, the driller uses various methods that are not necessarily independent
of each other. These are:
Core Loss
There are three main ways in which core is lost:
Soft core (or loosely held material held in a softer matrix) is washed away.
The core meets resistance to entry into the core barrel inner tube. This can be the
result of an undetected core blockage caused by a piece core that jams and does not
feed into the inner tube. If drilling continues while core is jammed, core below the jam
is ground to rubble by the bit.
Specify equipment that enhances core recovery, particularly barrel or bit type.
Consult the driller, or his supervisor, when problems arise before taking drastic action.
While drillers typically are more experienced and should know what steps to take to
reduce core loss, often they may be reluctant to implement them.
Be familiar with the equipment and techniques available to the driller to reduce loss.
Driller Action
To reduce core loss in drilling, the driller should:
Use a face discharge bit. This type has holes that direct the water or other drilling fluid
to the face of the bit, in lieu of conventional waterways, which allow drilling fluid to
wash the surface of the core, causing erosion of soft core as it enters the inner tube. A
face discharge bit is normally standard with a triple tube barrel, and is a major reason
for the better core recovery attributed to the triple tube barrel.
Reduce fluid circulation to a safe minimum to flush cuttings away, thus reducing
washing of the core.
Maximize advance per revolution to reduce time available for washing core.
Reduce the gap between the core lifter case and bit.
Use a shorter core barrel (say 1.5m). A shorter barrel is better stabilized, and will
frequently result in longer drilling runs than a 3m barrel.
Adjust the shut-off valve to make it easier to detect core blockage by the rise in fluid
pressure.
Use chromed or stainless steel inner tubes. This reduces the friction of core sliding up
the tube.
Use soluble oil (Ro-lub or Torq-trim) to reduce friction of core sliding up the tube,
provided it is not a contaminant to the material being sampled.
Pull the inner tube at frequent intervals, e.g. 50cm, or when water pressure rises,
engine labours, penetration rate drops, or bit weight increases.
Check the inner tube for damage when out of the hole.
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Consider dry blocking, which consists of spinning the rods for a short interval without
circulating drilling fluid so that the cuttings wedge the core solidly in the bit.
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APPENDIX 4-3
EXAMPLE OF STANDARD OPERATING PROCEDURE FOR USING A DIAMOND SAW
1.
Inspect the core saw mechanisms and blade for any defects or hazards.
2.
Make sure that you wear a full-face shield or goggles (safety glasses are not
acceptable), a PVC bib or raincoat, and hearing protection (earplugs or earmuffs).
When wearing goggles and dust mask, change the dust mask regularly when it
becomes wet or dusty.
3.
Make sure that all belts, clothing, jewellery, and hair are fastened/tucked away so that
there is no danger of any items getting entangled with the core saw machinery. Rings
should be removed from fingers before cutting.
4.
Lay the core trays out in the order that they are to be cut.
5.
Inspect and check the oil and water in the generator, and top off as necessary. If the
generator is cold, it should be preheated before starting.
6.
Make sure that the water supply (lubrication) to the core saw is turned on.
7.
After inspecting the core saw, and checking that the blade is free and not restricted by
any core or rubble in the cradle, turn it on.
8.
Place the core in the cradle and commence cutting along side the orientation mark. Do
not push too hard otherwise the blade will start to dig in. If this happens pull the cradle
and core back towards you. If the blade stops, turn the saw off and remove the core.
When cutting the metre marks on the core, make sure that the core is in the side
cradles and held firmly, and that hands are kept away from the blade.
10.
The core should be cut 5mm to the LEFT of the reference line (when you are holding
the core with the reference line facing up, and the arrow is pointing away from you).
The section of core with the reference line STAYS in the core tray, the unmarked core
will be sent off for assaying. After cutting the core, put it back in the original position in
the core tray (2 pieces together, orientation mark at the top).
11.
If you are unfamiliar with the rock type being cut, or with operating a core saw, work
slowly until you have gained confidence with the operation.
12.
Do not hesitate to ask any questions, no matter how minor they may seem.
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Section 5
REFERENCES ....................................................................................................................5-19
APPENDIX
Appendix 5-1
5.1. INTRODUCTION
This section addresses the collection of geotechnical and geologic data from drill core, RC
cuttings, and open pit and underground geologic mapping and sampling. Although
geotechnical data are in fact a subset of the broader category termed geological data, the
methods used and the degree of detail required in the collection of geotechnical data differ, so
this subject is addressed separately in this section. It is important to understand that, for
geotechnical applications, the focus should be on the identification of rock characteristics that
may impact slope stability or underground opening size during the operational life of the mine.
In order to approach this problem correctly, the general geology of the deposit, as well as the
surrounding host rock and structural setting, must be understood. For example, for a
porphyry copper deposit, a successful slope design is a function of an achievable bench
design. In this case, orientation of discrete fracture sets, length and spacing characteristics
and filling types may be the most important geotechnical features. However, for a
disseminated gold deposit in sedimentary host rocks, zones of intense argillic alteration may
be the most important geotechnical feature affecting slope stability and design of underground
openings. The basic approach for collection of geotechnical data will be somewhat different
for each of these two cases.
This reference volume does not address the collection of geologic data that typically takes
place prior to initial drilling in the earliest stages of exploration, and which includes activities
such as reconnaissance sampling and mapping, geochemical soil or rock chip sampling and
geophysical surveys. These data, while critical to exploration success, generally play a minor
role in subsequent resource modeling and ore reserve estimation.
As described in Sections 4.16.11 and 11.2.1 of this reference volume, the collection of
geotechnical data is very important for the determination of open pit slope angles and the
design of bench configurations, and for determining the maximum opening sizes of
underground workings and the spacing between sublevels. The descriptions and procedures
described below for the collection of geotechnical data have been designed to provide the
user with the basic tools for gathering and presenting meaningful information. It is not the
intention of this reference volume to turn Barrick geologists and engineers into geotechnical
engineers, nor to replace the third party consultant or geotechnical specialist when it comes to
making the final decisions on critical issues. Rather, it is intended to ensure consistent
collection of initial data (and most often this is the responsibility of the Project Geologist), and
to provide the mining engineers involved in project development with sufficient information to
make an early assessment of possible geotechnical problems.
Some of the descriptions of procedures provided in this section can also be found in other
sections of this reference volume. The purpose of this duplication is for ease of reference. A
discussion of the interpretation of geotechnical data by third party consultants or Barrick inhouse geotechnical specialists, and a description of the industry-accepted methods of rock
mass characterization and excavation design, can be found in the Appendix to Section 11,
MINING DATA COLLECTION, SELECTION OF MINING METHOD, AND MINE PLANNING.
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Log geotechnical data before any core is removed from split inner tubes (if triple-tube
core barrels are in use).
Transfer remaining core to boxes or core trays, leaving room for the return of the
geotechnical samples from the laboratory and marking the core where it has been
deliberately broken.
Prepare core as appropriate for sampling for assay and metallurgical testing.
5.2.1.
GEOTECHNICAL LOGGING
As discussed above, drill core recovered via triple-tube core barrels is best logged and
marked up for sampling after each drill run and before the core is removed from the innermost
(split) tube. This ensures that no core is lost or disturbed during transfer to a core box or tray
prior to logging. To avoid rig stand-by time, the drilling contractor will need to have enough
sets of split inner tubes to allow time for the logging and sampling, thus enabling the driller to
continue drilling without significant delays.
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After the removal of each run of core from the hole, the triple-tube split should be carefully
removed from the inner tube. The core-filled split inner tube should then be placed on a rack
and the top split should be removed carefully so that the remaining core is left undisturbed in
the bottom split for logging. In cold weather environments, if the core is to be sampled for
geotechnical laboratory testing, it should be protected from freezing. This can be done by
covering the core with a large plastic sheet and keeping it warm using a portable gas heater.
Prior to geotechnical logging, carefully fit together any broken sections of core. Samples for
geotechnical laboratory testing should be very carefully removed, then wrapped in plastic food
wrap and aluminum foil. Samples with high clay content, usually destined for triaxial testing,
will require extreme care. Be sure to mark the drill interval, rock type and nature of the
sample on the outer layer of wrapping!
There has been interest in the determination of in-situ rock fragment size distribution from drill
core at some mines in recent years for use in both blasting and leachability studies. This
trend is likely to continue as more mining companies realize the benefits of these data. As
the data required for this type of analysis are an extension of the data required for
determination of RQD value, a summary of the data collection procedure is provided in the
following section.
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Reference for Mineral Reserves and Resources
RQD Defined as Rock Quality Designation, RQD represents the percentage of a drill core
interval that is composed of whole pieces with lengths greater than 10cm (4in), excluding
drilling breaks, measured along the centerline of the core. Material with an estimated rock
hardness designation of less than 2 should be assigned an RQD value of zero. Core intervals
composed of soft rock generally coincide with zones of fault gouge, intensely-argillized rock,
or highly weathered, near surface rock. Deere and Deere (1988) provide recent commentary
on the practical use of RQD.
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Reference for Mineral Reserves and Resources
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Reference for Mineral Reserves and Resources
Fracture Spacing - The measure of true spacing between structures (faults, fractures, joints,
veins, and bedding planes) of the same structural set. Where the intersection between the
structures and the core axis is oblique, spacing = L sin , where L = Length along the
orientation reference line, and = the acute angle between the discontinuity plane and the
core axis as determined for orientation.
Persistence - This refers to the persistence of a particular discontinuity along strike and/or
down dip. It usually cannot be determined from a single drill hole, unless the structure in
question can be correlated reasonably with other data, such as pit bench (detail line) mapping
or underground mapping.
Roughness - This parameter describes the surface of the structural discontinuity with respect
to two categories: planarity and smoothness. Planarity is classified as planar, stepped,
irregular, undulating, or curved. Smoothness is classified as slickensided, polished, smooth,
or rough.
Roughness Profiles
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Reference for Mineral Reserves and Resources
Wall Rock Strength - This parameter is the same as overall rock strength as discussed
below, and is important only if the material in the wall of the discontinuity differs from the
overall rock strength. This can occur when alteration or weathering halos are present (see
Table of Soil and Rock Strength Classification following definition of Rock Strength).
True Width (Aperture) This is the measured true width of a structural discontinuity
containing a filling such as quartz, calcite or barite, or fault gouge. The measurement is taken
normal to the wall(s) of the structure and may include void space if the extent of the void can
be determined in the core or from the drillers shift reports. Typically, no true width is
recorded for structures such as non-filled fractures or fractures with only slickenside breaks.
Filling Type - A description of the material, if any, that fills the discontinuity.
Seepage - Evidence of water flow from structures based on core or drilling shift reports
should be recorded. Reported water flow can sometimes be correlated to individual
structures based on the presence of vugs, voids or other signs of dissolution.
Number of Structural Sets This differs from structure frequency in that it is the
determination of the number of structural sets (two or more joints, faults, fractures, or veins
having a similar attitude) recognizable within the core.
Structural Block Size - Based on the number of structure sets, the spacing of the sets, the
persistence of the structure sets and individual major structures, and orientations of the
structure sets, it may be possible to define structural blocks and estimate the size of these
blocks.
Rock Type These data are typically recorded as part of detailed geological logging. For
geotechnical and development engineering purposes, it is often necessary for the geologists
to combine rock types into more general zones, often referred to as engineering rock types.
The early understanding of the variations in rock types across a deposit is very important for
preliminary slope stability evaluations and bench configurations.
Degree of Weathering Also recorded during detailed geologic logging, the following simple
index is provided for making a visual assessment of the degree of weathering.
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Reference for Mineral Reserves and Resources
DESCRIPTION
Fresh
W2
Slightly weathered
W3
Moderately weathered
W4
Highly weathered
W5
Completely weathered
W6
Residual soil
DEFINITION
Parent rock shows no discolouration, loss of strength or any
other weathering effects.
Rock may be slightly discoloured, particularly adjacent to
defects, which may be open and have slightly discoloured
surfaces; rock is not noticeably weaker than the fresh rock.
Rock is discoloured; defects may be open and have
discoloured surfaces with alteration starting to penetrate
inwards; intact rock is noticeably weaker that the fresh rock.
Rock is discoloured; defects may be open, clay rich and
have discoloured surfaces and the original fabric of the rock
near to the defects may be altered. Alteration penetrates
deeply inwards but less altered fragments are still present.
Rock is discoloured and changed to a soil but original fabric
is mainly preserved. The properties of the soil depend in
part on the nature of the parent rock.
Rock is completely changed to a soil and all original rock
fabric has been destroyed.
Rock Strength - A rough guide to rock strength is shown below. Note that index tests must
not be performed on any core that will subsequently be sent for laboratory testing.
DESCRIPTION
Very soft soil
DEFINITION
Easily penetrated several centimetres by fist
UCS RANGE
(MPa)
<0.025
X2
Soft soil
0.025 0.05
X3
Firm soil
0.05 0.10
X4
Stiff soil
X5
H1
0.45 1.25
H2
Weak rock
1.25 5.0
H3
5.0 12.5
12.5 50
H5
Moderately weak
rock
Moderately
strong rock
Strong rock
50 100
H6
100 200
H7
Extremely hard
rock
>200
H4
0.10 - 0.2
0.2 0.45
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Reference for Mineral Reserves and Resources
- Informed estimates are acceptable: guesses are not 4. Geological information should be recorded only if it has geotechnical significance.
The logger should remember that a separate geological log will be prepared after
geotechnical logging is completed.
A suggested form to use for geotechnical loggings is included in Appendix 5-1. Note that the
Comments column on the log form sheet is very small. This is intentional in order to
emphasise the logging of concise, factual data. Where an extended comment is necessary
(such as recording the removal of a sample for laboratory testing), this information can be
included in the margin of the form. Note: never write important information on the back of the
sheet since it is easy for this information to be lost.
5.2.2.
Prior to the collection of laboratory samples for geotechnical testing, the core should be
photographed to allow maximum enhancement of discontinuities in the photos. The core may
be photographed dry or wet, whichever visually enhances the most important features in the
core. It is best to do this while the core is still undisturbed in the split tubes, especially if poor
ground conditions have been encountered.
The photos can be taken using either a
conventional camera or a digital camera. The advantage of a digital camera is that the digital
images can be stored in a permanent directory as .jpg files and, if necessary, the images can
be cropped and plotted using a program such as CorelDraw.
The following steps can enhance the quality of the photos:
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Reference for Mineral Reserves and Resources
Orient the camera at right angles to the centre point of the split tube.
5.2.3.
Samples for laboratory testing should be selected as soon as possible after drilling, while the
core is as close to in-situ condition as possible. Generally, the stronger and more competent
the rock, the longer the available time for sampling, provided the core is protected from
extremes of weather. This also applies to samples other than drill core (surface samples and
samples collected from open pit bench faces or from underground workings). Generally, the
greatest threats to the integrity of the samples after collection are:
Laboratory tests to determine physical properties of intact rock samples may include uniaxial
compression test, triaxial test, tensile test, direct shear test, and a combined test for Youngs
Modulus (E) and Poissons Ratio (). Other tests may include drillability of intact rock. It is
important that the core loggers have a basic understanding of the type of tests that are likely
to be used for the core samples at that site, so that the specific requirements of sample size
and quality are understood. A visit to a local geotechnical testing laboratory may be in order,
if there is one within a reasonable distance from the site.
According to ISRM suggested methods, reliable results from a minimum of five discrete
samples for each test type are adequate (for each rock type). Since it is common for a
number of samples to break either during shipment, during preparation, or during the actual
testing, at least two to three times the number of core samples required for the testing
program should be collected at the mine or project site. The number of samples submitted for
laboratory testing should reflect the observed variability of the material, as well as its relative
importance as a potential stability problem in pit wall exposures or underground openings. A
rock type that is fairly localized may require only a few successful sample tests, whereas a
rock type with a range of alteration intensities that will occur throughout the mine may require
a number of tests for each alteration type.
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Reference for Mineral Reserves and Resources
Sampling must be undertaken in a manner that does not compromise the integrity of
the subsequent test work. The following procedure is recommended to ensure that
the samples collected are suitable for testing:
Samples should be collected for testing as soon as possible after the core is removed
from the hole or the samples are taken from pit bench or underground working faces.
Care should be taken to ensure that the samples are clearly labelled with a permanent
marker at points positioned 120 around the core or hand specimen. Whiteout, paint,
or engraving tools should not be used for labelling. The label should include the
sample number and, if the sample is core, the hole number, down-hole direction and
depth. The source location of surface samples should also be recorded.
Core samples should have a minimum length to core diameter ratio in the range of
2.5:1 to 3.0:1. For example, for HQ3 core, 180mm should be considered the standard
minimum sample length for sample collection. See Section 4.16.1.5 for standard core
diameters. Sample ends must be flat and perpendicular to the core axis or long axis of
the hand specimen for testing. Core samples may be prepared prior to shipment if a
rock saw is available and it can be done properly. However, as a general rule, it is
preferable to have the samples prepared at a rock mechanics testing facility.
Samples should not be taken from core that has been broken by a hammer or other
percussion means.
For shipment to the test laboratory, packaging requirements vary with the type of test
to be done on the sample. For UCS testing, the individual samples should first be
wrapped in a thin layer of paper, sealed with plastic wrap, and then packed in a
suitable strong container surrounded by sufficient packing material. The preparation
of porous rock samples, in which moisture content may be significant, should include
several wet paper towels in the wrapping to help preserve the in-situ moisture of the
sample. For triaxial and direct shear testing, the sample should be sealed in several
layers of paraffin and cheesecloth, in order to preserve the in-situ moisture content of
the sample.
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Reference for Mineral Reserves and Resources
vehicle should be avoided. For projects in Australia, a plastic esky of 201 to 261
capacity is ideal for shipping samples.
The laboratory chosen to perform the testwork should be a facility registered with the
appropriate Federal or independent testing agency (ASTM in the United States, NATA
in Australia, and ISRM in Canada). The laboratory should also be instructed to
photograph all cores before and after testing, and to indicate on each photo which test
is being performed.
The laboratory should be instructed to return all samples in individually labelled bags
to the project site, so that complete geological logging, density measurements,
assaying and metallurgical testing can take place. Supplying pre-labelled bags for this
purpose when the samples are submitted can help expedite the return of the tested
samples.
5.3.1.
This form of geotechnical mapping is based on the same parameters as geotechnical core
logging. The mapping occurs along a single line marked on the wall of the excavation at a
constant height or slope, be it an open pit bench face, underground drift or crosscut face, or
other underground opening or surface excavation. Only those features that intersect the line
are recorded on the map. The main emphasis is on the recording discontinuities. In open
pits, particular attention is paid to those discontinuities whose lengths are on the order of the
bench height, as these are the features (when coupled with orientation measurements) that
will have the greatest impact on slope stability and the determination of slope angles. Good
survey control of the mapped line is required to ensure that the data are recorded in the
correct spatial orientations and relationships. To maintain this control, survey control points
should be placed approximately 30m (100ft) apart. Mapping should be performed at 1m (3-ft)
intervals from a defined starting point on the line, similar to logging core.
Certain geotechnical parameters that are a primary focus in core logging may not be required
as part of the geotechnical mapping. One such parameter is RQD. At first glance it might
seem that RQD could be recorded as a function of geotechnical mapping, as it is based on
the number of structures present in a defined linear distance. However, the blasting required
to establish the pit benches or underground workings can create unnatural localized fractures,
which can skew RQD determinations on open rock faces. The geologist should bear this in
mind before making the decision to include RQD measurements on field mapping sheets.
The remaining parameters recorded in core logging (orientation, spacing, persistence,
roughness, wall strength, aperture, filling, seepage, and number of sets and block size) are
also recorded during geotechnical mapping. Orientation can be measured directly as a dip
and dip direction using a Brunton compass or similar pocket transit. Structure orientations
should always be recorded relative to true north, rather than to mine north. Other
5-12
Reference for Mineral Reserves and Resources
parameters such as persistence, seepage and block size that are difficult to measure in drill
core are much more obvious in open pits and underground workings, and thus easier to
record during mapping.
Because only those features that intersect the mapping line are recorded, and only at the
point of intersection with the line, the choice of mapping line orientation should take into
account obvious significant features visible in the bench face or underground face or rib. Any
such features that do not intersect mapping lines should be described in map side notes, but
these cannot be included in the data set defined by the mapping line.
In conjunction with geotechnical mapping, a photograph should be taken of the pit bench face
or underground face or rib that is mapped. Although these photos do not record the detail
that is possible when photographing drill core, they do provide a simple and practical visual
record of the structural features. It is important that exposures are clean prior to
photographing, which usually requires washing down of the face or rib with water. However,
extreme caution is warranted when washing down faces or underground backs and ribs,
especially those that contain poor quality rock. Water sprayed for cleaning purposes can
easily dislodge sizeable rock fragments, and even cause significant local rib and back failures
in underground workings.
- Safety is a primary concern when washing and mapping surface and underground
exposures -
5.3.2.
CELL MAPPING
Cell mapping and bench-scale stability analysis are techniques developed by Call & Nicholas,
Inc. (CNI), a geotechnical firm located in Tucson, Arizona. This technique is designed to
allow a statistical approach to analyse the impact of joint sets on open pit bench-scale
stability. Structure set mapping is done utilizing a series of cells, which have a horizontal
dimension on the order of the bench height. Structure data collected include the orientation
and statistical fracture count-length parameters of discrete structure sets identified in each
cell. Mean orientation, lengths and spacings are then determined for each structure set.
Areas within which resident structure sets have a similar orientation are called structural
domains. Structures within each domain have a unique impact on slope stability. A benchscale stability analysis can be conducted that predicts the probability of achieving a desired
catch bench width, given the orientation of the wall, and based on the distribution of joint
orientation, joint length, spacings and probability of occurrence, for each set of joints
observed.
CORE LOGGING
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Reference for Mineral Reserves and Resources
program. For example, exploration and pre-development holes typically are logged in greater
detail than production (stope definition) core holes. This is because the geology of a mine is
usually reasonably well understood at the production stage, so that the logging of holes that
are drilled to aid stope development and design does not need to be as detailed. Also, with
production drilling, speed is usually of the essence, so only those features that are critical to
better definition of stope shape or possible ground problems are typically logged in detail.
These features include mineralization contacts, structures, limits to alteration and bedding.
However, if time and manpower permit, a detailed log for all diamond core holes is
recommended. If time and manpower restraints significantly affect the ability to maintain upto-date core logs, computerization of core logging should be seriously considered.
For logging, geologists should use the core log sheet or computerized spreadsheet file that is
standard for the site or project. In the absence of site or project-specific logging procedures,
the following recommended guidelines should be followed:
Check that core mark-up is complete and correct (see Section 4.16.12).
Always wet the core to better reveal colour, alteration, and textural features.
Before logging, briefly examine the entire hole to get a feeling for the overall geology.
Proceed to log in detail.
The determination of which structures to plot on the graphic portion of the log and to
describe in the log text is often confusing. Prior to logging, it often helps to first
broadly scan the entire hole and determine which structure types are present, develop
a rough idea of how many sets of a particular type are present (such as quartz veins),
and identify structures that are important and require logging. It also helps to use
consistent codes for different structure types, such as foliation, veins, joints, contacts
and bedding.
For the structures selected, record the angle of intersection between the structure and
the longitudinal axis of the core (the angle).
Where bedding is present, select a nominal distance (10m or 30ft) to record the angle
of intersection between the bedding and the longitudinal axis of the core. Abrupt local
changes to bedding should be recorded as required.
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Reference for Mineral Reserves and Resources
Describe any structure filling (gouge, quartz, calcite or other gangue mineral and/or
sulphides) present in the structures logged.
If the core in the hole is oriented (see Section 4.16.8), the following methods can be used to
determine true dip and dip direction of structures.
The dip and azimuth of a structure can be measured directly off the core.
The true bearings of important geological features can be recorded as they are
logged. This gives the geologist a better understanding of key structural relationships
as logging proceeds.
5.4.1.4. Input of Alpha and Beta Angle Data into a Computer Program
This approach requires measurement of the following:
Alteration.
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Reference for Mineral Reserves and Resources
Contacts between alluvium and bedrock, the base of the zone of complete oxidation
and the mixed (transition) zone, and the mixed (transition) zone and the sulphide
(sometimes referred to as fresh rock) zone.
Non-mineralized structures, including the angles these structures make with the
longitudinal core axis (alpha and beta angles) as described in Section 5.2.1.1, gouge
and/or clays along structure surfaces, and striations or slickensides.
Veining.
Core recovery.
5.4.2.
Section 5.2.2 describes the procedure for photographing core for geotechnical purposes. If
the geotechnical photos do not provide the needed detail, a separate set of photos should be
taken after wetting the core in order to highlight rock texture, alteration, and mineralization.
These photos should be taken using either a conventional camera or a digital camera after
geotechnical logging has been completed and the core has been transferred to core boxes or
trays, but prior to splitting, sawing, or sampling. Where practical from a logistical standpoint,
the same approach should be considered for underground production (stope delineation)
holes, especially if whole core from these holes is sent for assay. If site or project-specific
procedures are not in place, the following recommended procedures should be followed:
Do not photograph or record digital images of core until it has been fully marked-up.
Keep the tray out of direct sunlight to prevent harsh shadows and reflection.
Orient the camera at right angles to the centerpoint of the tray or box.
When using a conventional camera, a 28-mm wide-angle lens provides the best
undistorted close-up view of the core.
Avoid the use of flash since this reflects off wet core surfaces.
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Reference for Mineral Reserves and Resources
5.4.3.
CORE SAMPLING
Mineralization.
Rock type.
Alteration.
93.7 to 94.7m
94.7 to 95.6m
95.6 to 96.0m
96.0 to 97.0m
Except for where breaks are necessary because of geology, sample intervals are
commonly set at regular 1.0m or 2.0m lengths when using the metric system. For
projects in the United States and some other locations, regular sample breaks are
usually 2.0ft and 5.0ft, respectively.
Except for special circumstances, the minimum sample interval length should not be
less than 0.25m (0.50 ft).
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Reference for Mineral Reserves and Resources
To avoid confusion with other marks on core, the colour used for noting sample
intervals should not be used for any other marks.
The splitting and sawing of core for assay is described in detail in Section 4.16.12 of this
reference volume.
Lithology
Alteration
Mineralization
Other than the ability to detect some of the stronger structures intersected based on the
presence of gouge or clays in with the larger chips or the presence of vein gangue minerals,
little can be ascertained about structures intersected by the RC drill.
The Project Geologist should make sure that the chips collected at the RC rig are logged
promptly using the standard log sheet established for the particular site or project. The
degree of detail in the logs will depend on the local geology and the purpose of the drilling
program.
For example, resource definition drilling, stope margin test drilling and
condemnation drilling programs typically require less detailed logging than for resource
estimation.
Section 4.15.3 describes sample collection at RC rigs in detail.
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Reference for Mineral Reserves and Resources
There must be consistency established for the level of mapping detail required and for
descriptions and classifications used in core logging and geologic mapping. These
include a common understanding of lithologic units and contacts, alteration types
(especially silicification), structure (particularly breccia) classifications and any other
geologic factors of particular local importance.
Correlation of structures and geological contacts must be made in the field during the
mapping process, not in the office after the mapping data have been collected. An
interpreted map of the benches immediately above the bench being mapped should
be taken into the field, and used as part of the mapping process.
If time and manpower restraints significantly affect the ability to maintain up-to-date
core logs, geologic plan maps and geologic cross sections, the relative importance of
various geologic features should be categorized, so that the most important features
continue to be mapped, even if the less important features are not recorded.
Computerization of these tasks should also be seriously considered.
5.7
REFERENCES
BADGLEY, PC, Structural Methods for the Exploration Geologist, Harper, New York.
BARTON, N, LIEN, R and LUNDE, J. 1974. Engineering classification of rock masses for the
design of tunnel support. Rock Mechanics. Vol 6, Number 4.
BERKMAN, DA, 1976, Field Geologists Manual, Monograph Series #9, Australasian Institute
of Mining & Metallurgy.
BIENIAWSKI, Z. T, 1973. Engineering classifications of jointed rock masses. Transactions of
the South African Institution of Civil Engineers. Vol 15, Number 12.
BIENIAWSKI, Z. T, 1989. Engineering Rock Mass Classifications. John Wiley. New York.
BRIDGES, M. C, 1993. Assessments of Ground Conditions for Exploration Prospects and
Mines. In, Proceedings of the International Mining Geology Conference (I. Robertson and W.
Shaw Eds). Pp 243-254. The Australasian Institute of Mining and Metallurgy, Melbourne.
BROWN, E. T, 1981. Rock Characterisation Testing and Monitoring IRSM suggested
methods. Pergammon Press. Oxford.
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Reference for Mineral Reserves and Resources
DEER, D. U and DEERE, D. W, 1988. The Rock Quality Designation (RQD) Index in
Practice. In, Rock Classification Systems for Engineering Purposes, ASTM STP 984. (L.
Kirkaldie Ed). Pp 91-101. American Society for testing and Materials. Philadelphia.
HOEK, E and BRAY, J.W., 1981. Rock Slope Engineering. The Institution of Mining and
Metallurgy. London.
HOEK, E and BROWN, E. T, 1980. Underground Excavations in Rock. The Institution of
Mining and Metallurgy. London.
HOEK, E and BROWN, E. T, 1997. Practical Estimates of Rock Mass Strength. International
Journal of Rock Mechanics, Min. Sci., 34:8, 1165-1186.
KIRKALDIE, L 1988. Rock Classification Systems for Engineering Purposes.
Society for Testing and Materials. Philadelphia.
American
LAHEE, FH, 1952, Field Geology, 5th Ed, McGraw-Hill, New York.
LAUBCHER, D. H and TAYLOR, H. W, 1976.
The Importance of Geomechanics
Classification of Jointed Rock Masses in Mining Operations. Proc. Symposium on
Exploration for Rock Engineering Vol 1. Johannesburg.
NICHOLAS, D., and SIMMS, D., Collecting and Using Geologic Structure Data for Slope
Design. In: Slope Stability in Surface Mining. SME, Littleton Co.
PETERS, W. C., 1978. Exploration and Mining Geology. John Wiley. New York.
PRIEST, S. D., 1985. Hemispherical Projection Methods in Rock Mechanics. George Allen
and Unwin. London.
ROBERTS, C. M., 1992. Core Drilling as a Geomechanical Tool. In Western Australian
Conference on Mining Geomechanics. (T Szwedzicki, GR Baird and TN Little Eds.) Curtain
University of Technology. Kalgoorlie.
STILLBORG, B., 1986.
Sweden.
Atlas Copco.
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APPENDIX
Filling
Block Size
Roughness
Type
Persistence
Spacing (cm)
Depth (m)
Frequency
Rock
Type
RQD (%)
Rec
(%)
Strength
To
(m)
Weathering
From
(m)
Hole No.
Page of
Seepage
Discontinuities
Orientation
Aperture (mm)
Lithology
Wall Strength
Drilling
Project
Number of
Sets
Appendix 5-1
Comments
Section 6
SAMPLE PREPARATION
AND
ASSAYING
APPENDICES
Appendix 6-1
Appendix 6-2
Appendix 6-3
Analytical Techniques
Appendix 6-4
Appendix 6-5
Appendix 6-6
Heterogeneity Testwork
6.1. INTRODUCTION
The assay value of a sample received from a laboratory is the end result of a multi-step
process of sample preparation and analysis. This exacting process is a specialized field in
which the laboratory provides most of the expertise. However, care should be taken by
Barrick personnel not to leave all decisions relative to sample preparation and analysis to the
laboratory. Laboratories typically are under severe competitive pressure and often look for
ways to cut costs, and these cost cutting procedures can compromise the quality of the assay
results that Barrick receives. Barrick project personnel should determine the accuracy of the
results that is required and then determine a reasonable price for that accuracy.
For large drilling and assaying programs, project managers should consider setting up a
contract with the primary analytical laboratory. The basic points to be considered for such a
contract are outlined in Appendix 6-1. A form that can be used to help evaluate prospective
primary laboratories can be found in Appendix 6-5.
6.2. TERMINOLOGY
The common terms used in assaying are explained below. It is recommended that all Barrick
personnel adopt this terminology when issuing reports and other communications.
6.2.1.
Accuracy in assaying is a measure of the ability to determine the true grade of the primary
sample. Precision in assaying refers to the ability to consistently repeat the assay results for
a sample within required limits. Accuracy and precision are the means by which the quality of
a laboratorys work is judged. The following diagram illustrates the concepts:
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Reference for Mineral Reserves and Resources
Good precision
Good accuracy
Good precision
Poor accuracy
Poor precision
Good accuracy
Poor precision
Poor accuracy
The variance of the results is a direct consequence of the many errors that can be introduced
during the sampling and assaying stages.
6.2.1.1. Accuracy
Accuracy is a measure of the closeness of the assay result to the true grade of the primary
sample. It is affected by:
The ability to achieve an assay result which is close to the true grade of the assay split
(subsample).
The introduction of a systematic error in any of the above processes will produce a biased
and inaccurate result. Laboratory accuracy can only be verified by using Standard Reference
Materials (SRMs) of known grade, in the manner described in Section 7, QA/QC for
ASSAYING AND SAMPLING, of this reference volume.
6.2.1.2. Precision
Precision in assaying is the ability to consistently repeat an assay result. It is affected by
random errors generated in:
Field sampling.
Sample preparation.
Assaying.
Precision can be determined by examining the standard deviation, variance and coefficient of
variation of the results of check samples and check assays.
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6.2.2.
SAMPLING TERMINOLOGY
There is a unique set of terms that applies to sample preparation and assay procedures.
These terms are described in the flow charts below, with the recommended standard
terminology shown in boxes.
P R IM AR Y SA M P LIN G AN D A S SAYIN G
D R ILLIN G
RC
DIAM O N D
SPLIT
SPLIT
A SS A Y
SP LIT
R IG
S PLIT
R ETA IN ED
H A LF C O R E
C RU SH
SA M P LE
S TO R A G E
TO TA L S A M PLE
P R EP A R A TIO N
SPLIT
C O A R SE
R EJE C T
PULVERIZE
SPLIT
PU LP
SP LIT
(300g)
R E PE A T(s)
ASSAY(Au1,Au2,etc)
PU LP
R EJEC T
50g C H A R G E
ASSAY(Au)
PR IM A R Y
LA B
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Reference for Mineral Reserves and Resources
CHECK ASSAYING
CHECK SAMPLING
DRILLING
RC
DRILLING
DIAMOND
RC
DIAMOND
RIG
SPLIT
RETAINED
HALF CORE
PRIMARY LAB
RETRIEVE
PULP SPLIT (300g)
RE-SPLIT
RE-SPLIT
Quarter Core
ASSAY
SPLIT
50g CHARGE
CHECK
ASSAY
ASSAY
SECONDARY
LAB
PRIMARY
LAB
6.3.1.
SAMPLE MANAGEMENT
Sample management is the procedure for maintaining physical control of samples from the
drill rig, underground face, or surface collection site until the samples arrive at the laboratory,
ensuring that proper recording and accounting of the samples takes place. The term that
refers to the control of the samples from source to the laboratory is chain of custody. Since
the Bre-X scandal several years ago, maintaining chain of custody of samples between the
point at which the samples are taken and the laboratory has become a critical issue in the
eyes of the various regulatory agencies that oversee the mining industry. While it is not
always possible for Barrick to maintain direct physical control over samples at all times until
delivery to the laboratory, steps must be taken to ensure that samples are well-packed and
transported via reputable common freight carriers.
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Reference for Mineral Reserves and Resources
6.3.2.
SAMPLE TRACKING
Each operation or project site should maintain a planning chart to keep track of the samples in
the sampling and assaying process. The planning chart is separate from the geologic data
base and should include fields or space for each of the following:
Sample source (i.e. underground working, drill hole number, or open pit bench).
Assay sample numbers dispatched to laboratory.
Assays received from laboratory.
Problems identified from examining SRM and blank sample results.
Problems resolved.
Database updated.
Check samples selected.
Check samples dispatched to laboratory.
Check samples received from laboratory.
Check assay pulps selected.
Check assay pulps dispatched to secondary laboratory.
Check assay results received from secondary laboratory.
Statistical analysis of check samples, check assays, standards and blanks.
Problems identified from statistical analysis.
Problems resolved.
Samples returned to operation or project site for storage.
In general, it is best if one person on the project or at the operation is designated to track
samples.
6.4.1.
OBJECTIVE
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It is essential for the geologist to ensure that these objectives are being met by conducting the
appropriate testwork and/or by regular analysis of quality control checks.
6.4.2.
TYPES OF SAMPLES
The types of samples generated at operations sites and by exploration drilling programs can
be quite varied. These include:
RC drill chips.
Diamond drill core.
Open pit blast hole samples.
Underground and open pit rock face chips.
Underground muck samples.
Stockpile samples.
SRMs and blanks.
The collection of these samples is discussed in this reference volume in Section 4, DRILLING
METHODS AND PROCEDURES, and Section 15, PRODUCTION RECONCILIATIONS. The
treatment of these samples prior to assaying depends on their total size and maximum
particle diameter. Because of particle size differences within samples, a suitable sample
preparation protocol must be developed.
6.4.3.
The sample preparation normally consists of particle size reduction, followed by splitting. The
end product of the sample preparation process is a very small sample split (on the order of 30
to 50g) that is then assayed. This sample split must be representative of the larger sample
that was collected at the drill rig or in the mine.
Factors to consider when determining a sample preparation protocol include:
Different ore types can have vastly different gold distribution and gold particle sizes.
Because the density of gold is so much greater than its host rock, this can easily
cause gravity segregation during sample handling.
Each sample preparation stage increases the total assaying cost per sample.
- Incorrect sample preparation leads to incorrect assays! Particle size reduction is far more effective than increasing sample size to reduce sampling
errors. This is because reducing the particle size reduces the variance at a much greater rate
than increasing the sample weight. The critical step in the preparation process, therefore, is
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Reference for Mineral Reserves and Resources
determination of the acceptable minimum sample split weight (at a particular particle size) that
is required before allowing the next split to take place. Because this is not readily apparent
early in the evaluation of an orebody, these guidelines should be followed:
Examine the exploration QA/QC data carefully to determine if the sampling techniques
used produce representative assay splits.
Evaluate the check sampling results on a regular basis (see Section 7, QA/QC for
ASSAYING AND SAMPLING, in this reference volume).
Be prepared to modify the sample preparation protocol if the check sampling results
indicate that a problem exists.
The sample preparation protocol should be fully documented and communicated to all
geologists working on the project and also to the laboratory.
The following examples of sample preparation flowcharts illustrate the way that an instruction
should be issued to the laboratory. These flowcharts, which are an extension of the sampling
protocol developed by the geologists, can then be used for auditing the laboratory:
RC SAMPLES (CO ARSE GOLD)
ASSAY
SPLIT
(~ 7 kg)
DRY
DRY
NUGGET CRUSHER
(<2mm)
GRIND
CHECKS
(1 in 100)
SPLIT
3.5kg
LM5
GRIND
CRUSH
REJECT
(~ 3.5 kg)
SCOOP
PULP
SPLIT
(300g)
SCOOP
(50g)
FA 50
AAS
PULP
REJECT
(~ 3.2 kg)
STORE
3 MONTHS
then
RETURN
TO SITE
LM5
GRIND
SCOOP
(300g)
STORE
3 MONTHS
then
DISCARD
PULP
SPLIT
(300g)
GRIND
CHECKS
(1 in 100)
SCOOP
(50g)
STORE
3 MONTHS
then
DISCARD
FA 50
PULP
REJECT
( ~ 3.2kg)
STORE
3 MONTHS
then
RETURN
TO SITE
GRIND
CHECKS
(1 in 100)
STORE
3 MONTHS
then
DISCARD
AAS
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Reference for Mineral Reserves and Resources
6.4.4.
A large variety of sample preparation equipment is used in laboratories to perform the various
prep functions. A detailed description of equipment available on the market and the
advantages and disadvantages of each is presented in Appendix 6-2. The choice of
equipment to be used in each sample preparation procedure will depend on the following:
6.4.4.1. Drying
Since the metal content of samples must be reported on a dry weight basis, each entire
sample must be thoroughly dried to zero percent moisture content prior to preparation.
Drying is typically done for up to 12 hours at 120C to 130C in an oven specifically designed
for drying rock samples. For samples with high sulphide content, or if the presence of mercury
is known or suspected, lower drying temperatures may be required. Once dried, samples
should be prepared as soon as possible to avoid the drawing of moisture from the
atmosphere, particularly in humid climates. For an illustration of a drying oven and additional
discussion, see Appendix 6-2, Sample Preparation Equipment.
6.4.4.2. Crushing
A crusher is used to reduce the original sample to a smaller particle size in as short a time as
possible. The broad categories of crusher types are:
Jaw Crusher.
Used for core, rock samples from underground faces and for stockpile samples.
Final product size is around 12mm (in).
Roll Crusher.
Nugget or Rhino Crusher.
For illustrations of these crushers and additional discussion, see Appendix 6-2, Sample
Preparation Equipment.
6.4.4.3. Pulverizing
A pulverizer grinds the sample to pulp size, which is suitable for assaying. This is usually 90%
passing 75m to 106m. It is the final stage of sample preparation and achieving a suitable
grind size can be time consuming. The broad categories of pulverizer types are:
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Reference for Mineral Reserves and Resources
Uses a vertically rotating spindle to drive a plate which grinds the sample against a
stationary plate as the sample flows through the mill.
Uses a horizontally rotating spindle to drive a disc that grinds the sample against a
stationary disc as the sample feeds from above.
Similar to a Keegor mill, except the discs are smooth (see Appendix 6-2)
For illustrations of these pulverizers and additional descriptions of each, see Appendix 6-2,
Sample Preparation Equipment.
Periodic checks should be conducted after each grinding stage to ensure that the required
particle size is being achieved. Although grind checks are typically performed by laboratories
as part of routine internal quality control, Barrick geologists should also obtain pulps
unannounced from the laboratory for grinding checks by an independent laboratory. Further
details on grinding checks are described in Section 7, QA/QC for ASSAYING AND
SAMPLING, of this reference volume.
6.4.4.4. Splitting
Splitting normally is conducted after each stage of sample particle size reduction to reduce
the sample weight. The following techniques and equipment are commonly used in
laboratories:
Riffle Splitter - This is the most common device used for splitting samples. A riffle
splitter has the advantage that a sample can be repeatedly split (halved) until a
required amount is obtained. This method can be used in all sample preparation
stages, except the splitting of pulp(s) for assay.
Rotary Splitter This device is suitable for most splitting applications, but has the
disadvantage that once the splitting ratio is set, it cannot be adjusted. Like a riffle
splitter, a rotary splitter can be used in all sample preparation stages except for
obtaining a pulp split.
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Reference for Mineral Reserves and Resources
Cone Splitter This type of splitter is suitable for most splitting applications, but like
the rotary splitter, once the splitting ratio is set, it cannot be adjusted. Cone splitters
are not widely used today.
Scoop Scoops typically are used to produce the 30 to 50g assay charges from the
300 to 500g pulp splits.
Scoops should only be used where samples are
homogeneous.
6.4.5.
There is potential for cross-sample contamination in the sample preparation area if strict
measures are not taken to clean the equipment thoroughly between samples and to control
airborne dust. Good housekeeping and equipment maintenance are reflections of the
laboratorys professionalism and must be taken into account when evaluating bids or cost
proposals for sample preparation and assay work and conducting lab audits (see Section
6.6). The following areas, equipment, and procedures must be monitored for evidence of
possible contamination:
a) Sample receiving area
b) Drying area
c) Crushing equipment
d) Pulverizing equipment
e) Splitting and storage of pulps
f)
g) Dedicated preparation areas (i.e. separate preparation areas for samples of varying grade
that have varying accuracy requirements, such as mill carbons, development/exploration
samples and grade control samples.)
Further details are contained in Section 6.6, Laboratory Audit, below.
6.4.6.
CHECK SAMPLING
Check sampling is conducted to verify that the assay split that was sent to the laboratory was
representative of the original sample. Check sampling should commence after the results of
the first round of assaying have been returned to the project site.
Further details on check sampling are described in Section 7, QA/QC for ASSAYING AND
SAMPLING, of this reference volume.
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Reference for Mineral Reserves and Resources
6.5. ASSAYING
Assaying is a historical term referring to the determination of metal content in samples by
using particular quantitative techniques such as fire assay with gravimetric finish. In practice,
the terms assaying and analysis are used somewhat interchangeably.
Assaying for gold is a specialized procedure for which the geologist relies on the expertise of
the laboratory. However, it is important for Barrick geologists to have a basic understanding
of the assaying process in order to maintain control over the quality of the results received
from the laboratory.
6.5.1.
OBJECTIVE
Assaying in the laboratory must accurately determine the quantities of each metal or element
present in the sample, as specified in the instructions from the Project Geologist to the
laboratory.
This objective is accomplished in stages that include:
Fusing.
Cupelling.
Weighing.
Finishing.
- The assay technique used must be capable of reporting all of the gold in the
assay charge It is essential for the Project Geologist to ensure that the assay objectives are being met by
conducting the appropriate testwork and/or by regular analysis of quality control checks. See
Section 7, QA/QC for ASSAYING AND SAMPLING, of this reference volume.
6.5.2.
ASSAYING TECHNIQUES
Choosing the appropriate assaying technique for the ore type or mineralization sampled is
critical.
Ore type.
Level of accuracy required.
Detection limit required.
Required turnaround time for results.
6-11
Cost.
The differences between the four techniques lie in the ways by which the gold is extracted
from the sample. It must be stressed that each technique has disadvantages. The merits and
disadvantages of each technique are summarized below. A detailed description of each is
presented in Appendices 6-3 and 6-4. Further reading on this subject is recommended in
Eames, 1999.
Ore type:
Fire assay has the advantage over other techniques in that it is least affected by
ore mineralogy (with some exceptions, such as certain ferro-titanate ore types and
ores having very refractory mineralogy).
An expert fire assayer can tailor the flux to optimize gold extraction from different
ore mineralogies.
Fire assay determinations are not skewed by gold particle size in the assay
charge.
Level of accuracy:
Not as rapid as cyanide leach or acid digestion when dealing with oxide ore
bodies.
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Reference for Mineral Reserves and Resources
Cost:
Ore type:
As with standard fire assaying, screen fire assaying has the advantage over other
techniques in that it is least affected by ore mineralogy (with some exceptions,
such as certain ferro-titanate or highly refractory ore types).
Screen fire assay determinations are not skewed by gold particle size in the assay
charge.
Level of accuracy:
When coarse gold is present, screen fire assay produces the most accurate result
of all of the gold assaying techniques.
A lower detection limit (0.01 0.02g/t Au) is achievable using an AA finish (see
Section 6.5.3).
Screen fire assay is the most time consuming of all assay techniques.
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Reference for Mineral Reserves and Resources
Cost:
Ore type:
Acid digestion is not as effective as fire assay or screen fire assay at breaking
down gangue minerals, but it is generally more effective than the cyanide leach
method.
Gold associated with copper and tellurium can be lost through fuming if digestion
is done improperly.
Highly ferruginous ores can cause gold recovery problems with acid digestion.
Level of accuracy:
As with fire assay and screen fire assay, if the pulp is not homogeneous, the level
of accuracy will suffer.
Lower detection level when used with AA finish, depending on assay grade and
dilution requirements.
More rapid than fire assay or screen fire assay, but not as rapid as cyanide leach,
when dealing with oxide material.
Ore type: Cyanide leach is not as effective as the fire assay or acid digestion methods
in breaking down gangue minerals.
Level of accuracy.
Cost:
6.5.3.
If the pulp is not homogeneous, the size of the charge can be increased more
readily than with the fire assay methods.
Large gold particles require a longer time to leach than smaller gold particles.
The cyanide leach method is more expensive than acid digestion and the fire
assay methods.
FINISHING TECHNIQUES
The finishing technique refers to the final step in the assay process when the amount of gold
dissolved in solution is determined. Finishing techniques include:
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Reference for Mineral Reserves and Resources
This is the most commonly used finishing technique with the fire assay methods.
The acid solution containing the dissolved gold is aspirated directly into the AAS
machine.
This method is commonly used in conjunction with acid digestion and cyanide
leach analysis.
Gold from the acid solution is first extracted and concentrated into an organic
solvent before aspirating into the AAS machine.
This method provides good accuracy for samples in lower grade ranges,
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Reference for Mineral Reserves and Resources
This traditional technique involves placing the fire assay prill in nitric acid, which
dissolves the silver but leaves the gold. Platinum group metals are only partially
soluble in nitric acid, and the presence of these will be indicated by discolouring of
the nitric acid solution to brown/black (indicating platinum) or orange (indicating
palladium). After dissolution of the silver, the prill is annealed.
This is a very accurate method for determining the gold content of high grade
samples.
6.5.4.
CHECK ASSAYING
Check assaying is required to monitor for potential assay bias at the primary laboratory.
Normally, a minimum of 5% of the samples analyzed are checked as part of a quality control
(QA/QC) program. The original pulp splits from the primary laboratory are sent to a secondary
laboratory for reassaying. Check assaying should be undertaken after results for the first
round of assaying have been received.
Further details on check assaying are described in Section 7, QA/QC for ASSAYING AND
SAMPLING, of this reference volume.
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Reference for Mineral Reserves and Resources
6.6.1.
For a first time audit of a laboratory that is under consideration as a primary or secondary lab,
contact the laboratory manager and arrange for an appointment. By making arrangements in
advance, it can be made certain that all of the sections of the laboratory (sample preparation,
fire assay, wet chemical, and cyanide leach sections, along with the weighing room,
instrument facility, and sample storage area) will be in operation at the time of the visit. It is
likely that during this visit the laboratory will be in its best condition. If it is not, it serves as a
warning with respect to managements dedication to housekeeping and quality work.
The first-time audit should proceed in the following order:
The size and layout of the area and note the size of the area with respect to the
efficiency of handling and sorting of samples as they are received.
How the samples are sorted and the sample numbers are recorded into the laboratory
system (i.e. is there a possibility of mixing job lots or switching individual samples?).
Are the sample numbers, sample preparation and assay methods to be used entered
into a Laboratory Information Management System (LIMS) that will allow them to be
tracked through the laboratory?
Housekeeping in the receiving area. A messy receiving area warns of overall poor
operating practices.
Sample preparation section - The sample preparation section should be in a separate room
with tight-fitting doors to prevent migration of dust created during crushing, pulverizing, and
splitting. The Barrick auditor needs to observe the procedures being used by the sample
preparation technicians.
- Most important, make sure that equipment is routinely cleaned between each
sample 6-18
Reference for Mineral Reserves and Resources
General housekeeping:
Sample dryers:
Crushers:
Dust should not be excessive, and sample fragments should not be lying on the
floor, work tables, or hung up on the crushers, pulverizers, and splitters.
The types of crushers (i.e. jaw crushers, roll crushers, or hammer mill). A onestage crusher (Nugget Crusher or equivalent) is preferable, since this can reduce
the particle size to 2mm in one stage, thus avoiding the extra sample handling
needed for two-stage crushing, which provides an additional source of error.
Crusher trays should be large enough to hold the sample without overflowing.
Splitters:
The type and size of splitters being used and their compatibility with the particle
sizes in the sample being split.
The construction of the splitter (should be made from smooth stainless steel).
If a riffle splitter is used, note the number of riffles and whether they are evenly
spaced.
Pulverizers:
Is pulverizing done in one stage, or is the sample being divided and then
recombined (a possible source of sampling errors and/or sample loss).
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Reference for Mineral Reserves and Resources
How are the pulp splits are taken for assay (scooped or split?).
Removal of pulp residue from pulverizers before cleaning (i.e., pulp residue must
not be left in pulverizers due to carelessness, resulting in pulp loss).
Whether two or more pulverizers are being used in parallel by one operator to
save time (a possible source of sample contamination or error).
How is the grind size tested (i.e. are sieves used, or is test simply by feel)?.
Frequency of screen (sieve) tests; these should be done several times per day.
Results of previous checks on other client samples.
Fire assaying section - The fire assaying section should be in a separate room in the
laboratory. Check the following:
Furnaces:
Maintenance
Condition of furnace liners
The normal batch size used (i.e. 25 or 50 crucibles).
The sample identification system used when batching samples.
Batch makeup:
Number of samples for assay
Number of duplicates
Number of SRMs
Number of blanks.
Assaying:
Crucible size and compatibility with required Barrick sample charge size.
Flux composition, sample to flux ratios and flux mixing procedures (see Appendix
6-3).
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Reference for Mineral Reserves and Resources
Reuse of crucibles (new crucibles should be used for samples from resource
estimation and development drilling).
Acid digest (wet) section - A separate part of the laboratory should be set aside to carry out
acid digestions and wet assay analyses. Assay equipment, including all glassware, should be
clean and stored under cover. Acid digestion and hot plate areas should be contained within
enclosed fume hoods. Check the following:
General:
Housekeeping.
Distilled water source is handy.
Bench space is adequate.
The range of elements that the section is capable of analyzing.
Acid Digestion:
Batch makeup:
Number of assay samples
Number of duplicates
Number of SRMs and grades of SRMs
Number of internal blanks
The sample tracking system used when placing a batch of samples onto the
hotplate.
Digestion times.
If gold is extracted into an organic solvent, what solvent is used, and how the
mixing is performed to achieve complete extraction.
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Internal fire assay checks should be performed in order to monitor gold recovery
from acid digestion.
Method for identifying problem samples and what remedial action is taken.
Cyanide leach - The cyanide leach section should be in a separate area of the laboratory
building. Check the following:
General.
Housekeeping.
Distilled water source is handy.
Bench space is adequate.
The range of elements that the section is capable of analyzing.
Cyanide leach.
Batch makeup:
Number of assay samples
Number of internal duplicates
Number of internal SRMs and grades of SRMs
Number of internal blanks
The sample tracking system used when placing a batch of samples onto rollers or
into tumblers.
Agitation times.
If gold is extracted into an organic solvent, what solvent is used, and how the
mixing is performed to achieve complete extraction.
Checks with fire assay should be performed in order to determine gold remaining
in residue.
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Reference for Mineral Reserves and Resources
Weighing room - Balances and scales for measuring weight should be set up in a separate
room. Check the following:
Whether balances are linked to the LIMS (if in place), and if the accuracy of the
weighing is preserved by this link.
Whether gold calculations are done manually or by computer via a link to the
LIMS.
If the grades of the standards are appropriate for the grades of the samples to be
analyzed.
That storage of calibration standards is appropriate (i.e. within a dark sealed area).
The upper grade limit when dilution of a sample is required to keep within the
calibration range.
Sample storage - The storage of sample pulps and sample rejects is important as these may
need to be retrieved for check assaying by either by the primary laboratory if assay problems
are detected or by the secondary laboratory in order to confirm assay accuracy. Other uses
for stored samples include metallurgical testwork and making site-based SRMs (see Section
7.3.1.2 of this reference volume). Check the following:
Storage area:
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Reference for Mineral Reserves and Resources
Samples should be stored under cover and organized to allow easy access and
retrieval.
How samples are identified in storage (e.g. by numbered job lots or individual
samples).
Condition of samples in storage (e.g. pulp envelopes sealed, reject bags tied).
There should be an effective computerized index for stored pulps and rejects.
Internal laboratory quality control (QA/QC) procedures - Laboratories should have their
own comprehensive QA/QC programs that monitor all stages of their analytical procedures.
An important part of an audit for selection of a laboratory is the review of the QA/QC program,
including the following components:
Accreditation:
The in-house and SRMs used and the grades of these standards.
The checking of in-house SRMs via a round robin, or similar program, with other
laboratories.
The types and limits of errors allowed before a sample batch is re-assayed, and
the individual who makes this decision.
Duplicates:
How and when duplicate samples are prepared and assayed. These should cover
both the sample preparation and analytical stages in order to enable the
laboratory to monitor internal precision.
How the laboratory monitors and assesses its internal QA/QC results.
Actions taken in response to QA/QC data.
Data should be made available for inspection by Barrick personnel.
Data handling - Data handling includes the laboratorys procedures for recording and
transmitting analytical results to clients. The ability of the laboratory to provide timely assay
reports to Barrick is dependent on having an efficient data transfer system in place. In order
to assess the capabilities of the laboratory in this area, the following should be checked:
The performance of the LIMS in order to determine that the laboratory databases and
recording systems are working well.
Verification that the laboratory reporting format meets, or can be revised to meet,
Barricks requirements.
The laboratory data transmission facilities and capabilities. The laboratory should be
able to transmit analytical results electronically (e-mail), by fax, and by mail (hard copy
or disc).
During the audit for laboratory selection, the following should be checked:
The number of personnel (both full time and part time) employed.
The shift schedules for the laboratory. Long shifts (over 10 hours) can be another
source of error in all sections of the laboratory.
The ability of the laboratory to quickly increase staff levels with experienced workers if
workloads increase.
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Reference for Mineral Reserves and Resources
6.6.2.
During the course of a drilling project, Barrick personnel should conduct ongoing laboratory
audits of the primary laboratory at least once every 3 months. Unlike an initial audit for
selection of a laboratory when it is appropriate to first schedule the audit, ongoing periodic
audits must be done on a random basis, without prior warning. The purpose of these audits is
to observe the operation of the laboratory and its adherence to procedures under normal
operating conditions. Scheduling an audit in advance, or performing the audit on the same
day or week of the same month defeats the purpose of an ongoing audit, since it is logical for
the laboratory to present itself in the best light possible by ensuring that correct procedures
are in use and that the laboratory is clean at the time of the expected visit.
To perform these audits, always arrive unannounced at the laboratory and immediately
contact the manager, informing him/her of the purpose of the visit. Always request that the
manager or a senior technical person accompany you during the audit, and conduct the
examination in a thorough but expedient manner, so that the person(s) accompanying you
can return to their normal duties as soon as possible.
This audit should start at the sample receiving area and then progress through the sample
preparation, fire assay, acid digestion, cyanide leach, weighing room, instrument facility and
data handling sections of the laboratory. The final step of the audit is a conference with the
laboratory manager to discuss briefly the audit findings, any results of the laboratorys internal
quality control program, and any results of Barricks QA/QC monitoring program. The
checklist of items to examine, which is shorter than what was defined for initial assessment
audits in Section 6.6.1, immediately above, is as follows:
6.6.2.1. Housekeeping
All sections of the laboratory should be checked to insure that the facilities meet reasonable
standards for cleanliness during a working shift.
The sample preparation area, in particular, should receive special scrutiny, since more errors
typically arise in this area than all others combined. The area should be reasonably free of
standing dust. Airborne dust should be brought to the attention of the laboratory manager
immediately. Watch for fragments of sample on benches, in and around equipment, and on
the floor, and bring these to the attention of the lab representative assisting with the audit.
Wet chemical areas also should be carefully examined for evidence of spills, beakers boiling
over on hotplates during digestions, or sloppy handling of dry chemicals.
The weighing (balance) room and instrument rooms should be briefly checked. If both are not
spotless, report this to the laboratory manager immediately.
6.6.2.2. Procedures
Adherence to specified procedures should be checked throughout the laboratory, with
particular focus, again, on the sample preparation area, where shortcuts are most likely to
occur. Also check fire assay and wet chemical areas, paying particular attention to flux
formulae and acid mixtures, respectively.
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6.6.2.3. QA/QC
Review the results of the internal laboratory QA/QC for the period between the last audit and
the current examination. Discuss any issues observed in the data with the laboratory
manager as part of the post-audit conference. At the same time, share with the manager the
results of any Barrick QA/QC check sampling sent to a secondary laboratory, as well as data
from blanks and SRMs submitted blind by Barrick to the primary laboratory.
There should be no serious QA/QC issues to discuss at this point, since any potential
problems revealed by QA/QC programs should have been discussed with the laboratory
immediately after detection.
Resource RC
Diamond core
Grade control
ASSAY PULPS
Resource RC
Diamond core
Grade control
PULP REJECTS (300g)
Resource
Grade control
STORE AT LAB
DISPOSAL
3 months
3 months
3 months
Discard
Discard
Discard
3 months
3 months
3 months
Discard
Discard
Discard
3 months
3 months
Return to site
Discard
If the pulps and rejects are to be saved and stored at the mine or project site, the
recommended procedure for storing these is as follows:
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Reference for Mineral Reserves and Resources
The Project Geologist should designate one person to coordinate the return and
storage of any pulps and rejects from the laboratory. This person will maintain an
electronic database of all pulps, pulp rejects and coarse rejects, including the storage
location for each sample.
The pulps and pulp rejects must be stored under cover in a low-moisture environment
Coarse rejects may be stored outside in sealed barrels or other weather proof
containers.
In general, once mining takes out the area drilled or sampled, the pulps, pulp rejects
and coarse rejects from that area may be destroyed.
6.8.1.
If at all possible, assays should be received from the laboratory in digital format (rather than
hard copy) and first stored in a separate temporary database. Prior to merging the temporary
assay data files into the main geologic database, the following steps are recommended:
The database manager should download the assays received from the laboratory into
the temporary database files.
The geologist responsible for the project must then check the assays for:
Acceptable comparison between assay values and logged or mapped geology.
This is an important check for sample switching errors.
The laboratory must be contacted immediately with respect to any problems found.
When confirmed to be correct, the temporary assay data file should be merged into
the geologic database.
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6.8.2.
Mine and project site-specific procedures will govern how assay and drilling data are to be
entered into the geologic database. Although different from site to site, these procedures
should include the following general steps:
A designated person should be responsible for merging the assays into the database.
Assay uploading should be automated in order to avoid corruption of digital data.
Sample numbers should be entered in the database prior to merging of assays.
- Once entered into the geologic database, assays should not be changed or
deleted without the approval of the Project Geologist If there are no site-specific procedures in place for the recording of QA/QC assay data (check
sample assays from the secondary laboratory, check assays from the primary laboratory,
SRM and blank assays from either), it is recommended that these data be downloaded into a
different file in the geologic database. Analysis of these data should be performed at least
every three months using the recommended methods of data analysis described in Section 7,
QA/QC for ASSAYING AND SAMPLING, of this reference volume.
After receiving results for check samples sent to the secondary laboratory and check assays
received from the primary laboratory, a decision must be made with respect to each final
assay that is to be entered into the geologic database for use in resource modeling. It is
recommended that the database have an assay field designated as the final assay (for
example, AuFinal) for this purpose. The method used to determine the final assay to be
used for resource modeling when more than one assay is available should conform to
Barricks corporate or site-specific policy.
6.8.3.
This is the process by which the integrity of the data that are entered into the geological
database is checked. It must be performed before the data are used for resource modeling or
other purposes. The validation should be conducted as follows:
Each batch of results from the laboratory must be checked as soon as received by
the geologist responsible for the project.
Use the standard validation tools available in the database software to check for
misplaced decimals, missing assays, or codes for assays below detection limits (such
as -9) that may not be compatible with resource modeling software:
Print out the laboratory data sheet and check the position and grades of the standards
and blanks.
Cross check the sample numbers on the laboratory data sheet with the sample
numbers in the drill logs, underground sample logs, or relevant field sheet (blasthole
location map, bench face map, or ditch-witch sample sheet).
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Ensuring that the data were imported into the correct assay field.
A check against geological logs for compatibility (this can be achieved by plotting
assays and geology on cross sections or base plan maps).
6.9. DOCUMENTATION
Documentation of sample preparation and assaying procedures and QA/QC programs is an
important part of the audit trail of an operation or project. This documentation should be
readily available for any technical audits required by Barrick management, to satisfy bank
financing requirements, for possible joint ventures, sale of a project, or in potential legal
proceedings. The documentation should be in the form of written reports and should include:
Assaying procedures.
Actions taken as a result of issues revealed by QA/QC data analyses, such as rerunning of sample lots, deletion of biased or erroneous data from the geologic
database, or revision of laboratory procedures.
Analysis of mineralogy
This allows the laboratory chemist to make informed judgments regarding possible
problems that may arise in relation to certain assaying techniques. Such problems can be
related to the chemical nature of the deposit, where certain contained elements may
cause spectral interferences in the analyses, resulting in what is commonly referred to as
assay robbing. Problems can also arise due to the mineralogical nature of the deposit,
where the mineral containing the element(s) of interest is difficult to digest. An example of
this is refractory gold.
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These tests (which include screen fire assays) determine precious metal particle size and
the distribution of the various sizes. The tests are useful for indicating potential problems
associated with coarse gold and whether an ore will be free milling or refractory.
Heterogeneity testwork on the mineralization will provide data for the development of a
Sampling Nomograph, from which the optimum sample preparation sequence can be
determined (see Appendix 6-6). Other types of testwork can be performed to determine
appropriate operating practices during individual sample preparation stages, such as the
optimum grind times required when pulverizing.
This involves running a suite of samples using fire assay, acid digestion (aqua regia) and
cyanide leach techniques in order to determine if gold losses are likely to occur with any
particular technique.
In order to determine the best assay finishing method, the solutions extracted from the
various fire assay methods should be subjected to several different finishing methods to
determine if gold losses are occurring with any one method.
6.11. REFERENCES
Eames, J, 1999. Unrealistic expectations of assay results, in Good Project Wrong Assays,
Getting Sample Preparation and Assaying Right, papers presented at a Seminar on Quality
Assurance in Mineral Assaying (AusIMM AIG: Sydney).
Menne, D M, 1992. Assaying cyanide-extractable gold within an hour, and addressing effects
of preg- and assay-robbing, in Proceedings International Conference on Extractive Metallurgy
of Gold and Base Metals pp 369-380 (AusIMM: Melbourne).
Pitard, F, 1993. Pierre Gys Sampling Theory and Sampling Practice, Second Edition, CRC
Press, 528 p.
Radford, N W, 1987. Assessment of error in sampling, in Meaningful Sampling in Gold
Exploration, Bulletin No 7, pp 123 (AIG: Perth).
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APPENDICES
APPENDIX 6-1
SPECIFICATIONS FOR ANALYTICAL CONTRACT
All analytical work carried out by a commercial Laboratory should be detailed in an analytical
contract agreed upon between Barrick and the Laboratory. This can be prepared by the sites
using a template obtained from the appropriate Barrick Department.
A section called Specification in the contract will need to be prepared by the Geologist and
this should clearly outline the following:
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Insert clause in contract that Barrick will monitor the Labs performance with its own
QC program.
Checks initiated by Barrick which subsequently show problems with the original
Lab results will be paid for by the Lab.
Checks initiated by Barrick that are subsequently shown to verify the original Lab
results will be paid for by Barrick.
The Schedule of Rates should provide details of the following unit rates:
All sample preparation procedures which are likely to be used during the term of
the contract
All analytical procedures which are likely to be used during the term of the contract
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APPENDIX 6-2
SAMPLE PREPARATION EQUIPMENT
DRYING OVEN
An oven is used in the Lab to dry the samples prior to sample preparation and assaying. This
is necessary because the metal content of the samples must be reported on a dry weight
basis.
SPECIFICATIONS
Must be capable of taking the full sample submitted by Barrick
Lower drying temperatures may be required for samples with high sulphides,
metallurgical concentrates, carbons or if mercury is present
Drying time is normally 12 hours but can vary depending on sample size and moisture
content
Samples are sometimes tipped into metal trays if bags are torn or if faster drying times
are required
If metal trays are used then metal identification tags are placed in each tray
The oven should have a thermostat, timer, fan and an air extraction system
Once dried, the samples should be processed quickly so they do not draw in
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ADVANTAGES
DISADVANTAGES
Use of metal trays can introduce handling errors and contamination problems
Wet, clayey samples will require >>12 hours of drying time
Placing samples into open trays can lead to mix-ups and cross-contamination
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JAW CRUSHER
A jaw crusher is used in the lab to reduce the size of large fragments in a sample. It is an
intermediate stage where the sample is reduced to a smaller particle size in as short a time as
possible.
SPECIFICATIONS
ADVANTAGES
A jaw crusher is a very quick method of reducing large rock fragments to a size which
can be put directly into a pulverizer.
3
Easy to clean.
DISADVANTAGES
Sample hang-up can lead to cross-contamination if the crusher is not inspected and
cleaned between samples.
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NUGGET CRUSHER
A nugget crusher is used in the Lab to crush large samples prior to splitting. It can be used an
intermediate stage between jaw crushing and pulverizing.
SPECIFICATIONS
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ADVANTAGES
A nugget crusher is a very quick method of reducing large samples to a size which can be
put directly into a pulverizer
Can reduce fragment size to around 3mm compared with a 12mm product from a jaw
crusher
Provides a cost effective intermediate crushing stage compared to pulverizing the total
sample
Easy to clean
DISADVANTAGES
Maximum rock fragment size into a nugget crusher is much smaller than into a jaw crusher
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The sample is placed in the bowl with the puck in place and the lid is locked on with a
pneumatic clamp
The sample falls through a hole in the puck and is ground between the puck and the
base and walls of the bowl by the vibrating action of the bowl
The LM2 is run for a preset time
The operator should check the pulp by feel and if still too coarse, continue grinding
The puck is removed with a crane
300g of pulp split is taken with a scoop and placed in a pre-numbered paper packet
As much as possible of the remaining pulp reject is scooped into the original sample
bag
The entire assembly is cleaned after each sample by vacuuming and/or by
compressed air
The LM2 is flushed, as required, by grinding a barren material, such as quartz, to
remove smeared gold
ADVANTAGES
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Can pulverize up to 1.2kg of sample allowing total sample preparation for Grade
Control at a reasonable cost
Easy to clean
DISADVANTAGES
The grinding action on large gold particles is not as efficient as that of the Keegor mill,
causing smearing and requiring longer grinding times to break down the gold
Loss of sample can be considerable if long grinding times are employed (> 12
minutes)
Complete sample loss occurs on rare occasions when the seal on the lid disintegrates
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The sample is placed in the bowl with the puck in place and the lid is locked on with a
pneumatic clamp
The sample falls through a hole in the puck and is ground between the puck and the
base and walls of the bowl by the vibrating action of the bowl
The operator should check the pulp by feel and if still too coarse, continue grinding
300g of pulp split is taken with a scoop and placed in a pre-numbered paper packet
As much as possible of the remaining pulp reject is scooped into the original sample
bag
The LM5 is flushed, as often as required, by grinding with a barren material such as
quartz to remove smeared gold
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ADVANTAGES
DISADVANTAGES
The grinding action on large gold particles is not as efficient as that of the Keegor mill,
causing smearing and requiring longer grinding times to break down the gold
Loss of sample can be considerable if long grinding times are employed (> 12
minutes)
Complete sample loss occurs on rare occasions when the seal on the lid disintegrates
Not all pulp can be retrieved as the bowl is fixed and cannot be up-ended
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The Mixermill has a large and small grinding ring and a center puck
The sample is placed in the bowl with the puck and rings in place and the lid is locked
on with a pneumatic clamp
The sample is ground between the puck, rings and the base and walls of the bowl by
the vibrating action of the bowl
The operator should check the pulp by feel and if still too coarse, continue grinding
300g of pulp split is taken with a scoop and placed in a pre-numbered paper packet
As much as possible of the remaining pulp reject is scooped into the original sample
bag
ADVANTAGES
DISADVANTAGES
The grinding action on large gold particles is not as efficient as that of the Keegor mill,
causing smearing and requiring longer grinding times to break down the gold
Not all pulp can be retrieved as the bowl is fixed and cannot be up-ended
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KEEGORMILL PULVERIZER
A pulverizer grinds the sample to a size that is suitable for assaying. It is the final stage in the
sample preparation process. The Keegor mill is a vertical spindle pulverizer. It can be used for
total sample preparation.
SPECIFICATIONS
The Keegor mill has 2 grinding discs near its base, the top disc is fixed to the body and the
bottom disc is attached to a vertical spindle which rotates the disc
The gap between the grinding discs is preset to give a consistent grind size
The sample is introduced through the top feed chute and falls through a hole in the top
disc
The sample is ground between the 2 discs by an extremely abrasive shearing action
The sample is collected from the bottom chute into a tray and transferred into its original
bag
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ADVANTAGES
Can process any size sample because the process is continuous feed
Produces better grinding and less smearing of large gold particles than a puck, ring and
bowl pulverizer
DISADVANTAGES
Does not homogenize the sample as it grinds (the pulp must be roll-mixed on a rubber
mat after pulverizing)
Retains some sample in the cone and requires thorough cleaning between each sample
The grinding action is very abrasive on the discs which can lose 1-2g of steel per kg of
sample
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RIFFLE SPLITTER
A riffle splitter is used in the Lab to reduce the volume of the assay split after each grinding
stage.
SPECIFICATIONS
The riffle splitter must produce a sample which is representative of the original sample
It is necessary to have at least 12 riffles in the splitter
There must be an equal number of riffles directed towards each split
The riffle width must be at least twice the largest particle in the sample
All riffles must be of equal width
The riffles must be easily accessible for cleaning after each sample
The entire sample must be put evenly through all the riffles at the one time
Each passage through the riffles reduces the sample by half, this is continued until the
required final size is reached
The halves are taken from alternate sides to avoid any bias in the equipment
The riffle splitter and the trays are cleaned with compressed air after each sample
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ADVANTAGES
Simple to use
Easier to vary size of final split than with a rotary splitter or cone splitter
DISADVANTAGES
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ROTARY SPLITTER
A rotary splitter is used in the Lab to reduce the volume of the assay split after a grinding
stage. This type of splitter is usually attached to a feeding device, for example, a nugget
crusher.
SPECIFICATIONS
The rotary splitter must produce a sample which is representative of the original
sample
The rotating speed must match the incoming sample stream from the feeding device
The rotary splitter receivers are usually pre-set to the required split proportions
The sample enters the rotating receivers of the splitter and is automatically split into
the required proportions
The machines are switched off and the assay split and crush residue are bagged and
labeled
The rotary splitter and receivers are cleaned with compressed air after each sample
The following photograph illustrates a rotary splitter mounted underneath a nugget crusher:
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ADVANTAGES
DISADVANTAGES
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CONE SPLITTER
A cone splitter is used in the Lab to reduce the volume of the assay split after a grinding
stage. This type of splitter is usually attached to a feeding device, for example, a crusher.
Cone splitters are not widely used.
SPECIFICATIONS
The cone splitter must produce a sample which is representative of the original
sample
The sample must be dropped evenly over the point of the cone
The width of the receiver below the cone determines the weight of the split
ADVANTAGES
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DISADVANTAGES
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APPENDIX 6-3
ANALYTICAL TECHNIQUES
FIRE ASSAY
INTRODUCTION
Fire assay is the oldest and, in most circumstances, still the best method for the determination
of precious metals in ores and metallurgical products. It is known that man had the capability
of refining metals from ores in the third millennium (2,600) BC and the basic procedures
employed in fire assay have not changed markedly since then.
Essentially the method consists of two consecutive pyrochemical separations. First, the finely
ground sample is fused with a suitable flux under reducing conditions, which promotes the
separation of the precious metals from the gangue, with simultaneous collection as a lead
alloy. Second, the lead is removed by an oxidizing fusion (cupellation) and the precious
metals are isolated and available for determination.
Fire assaying does not always guarantee full determination of the gold in the sample because
some ores contain minerals that can cause interferences and gold loss. A skilled fire assayer
can add flux reagents to overcome most of these problems. It is important to tell the Lab the
mineralogy of the ore type as this will allow them to modify their flux mixture as required.
PREPARING THE ASSAY CHARGE
Flux is added to the pulp split, the ideal sample to flux ratio being 1 : 5
The sample and flux charge is then transferred into clay crucibles
1
The crucibles are always arranged in the same order each time a batch is made up to
prevent mistakes in sample ordering during handling
A flux is a material (reagent) mixture that converts the minerals and complexes in the sample
into soluble forms which separate into molten metal and slag phases. A number of flux
reagents are used and these are classified as acid, basic or neutral and as oxidizing or
reducing.
Acids and bases in fire assay do not fit most of the usual acid-base definitions. The general
property that an acid plus a base gives a salt still partly applies, for example, when sodium
carbonate (a base) is fused with silica (an acid) the following occurs:
Na2CO3 + SiO2
Na2SiO3 + CO2
Silica (SiO2) is the strongest acid reagent. It combines with the metal oxides to form
silicates which are the foundation of most slags.
Borax (Na2B4O7) is also a strong acid and fluxes all the metallic oxides, both acids and
bases. It has a relatively low melting point of 742C and effectively lowers the fusing
point of all slags.
Litharge (PbO) is a readily fusible basic flux and oxidizing agent and on being reduced
provides the lead necessary for the collection of gold, silver and PGMs. It melts at
883C and contains 92.8% lead.
2
Flour (C6H10O5) is a reducing agent and is used in the flux to take up the oxygen from
litharge to produce lead:
12PbO + C6H10O5
As2S3 + 13Fe
2Fe5As + 3FeS
4KNO3 + 5C
Silver (Ag) is added to the flux to increase the size of the prill so that it is easier to
handle. It also acts as a collector of Au and PGMs during fusion and cupellation.
THE FUSION
During the fusion the flux combines with the gangue to form a fluid slag, and the litharge in
the flux is reduced to minute globules of lead which are significantly more dense than the
molten flux. The rain of lead globules falling through the molten mass collects the particles of
precious metals and coalesces into a liquid button at the bottom of the crucible. The formation
of a good-sized lead button containing a minimum of contamination is the primary objective of
the fusion.
The batch of crucibles containing the sample and flux charges is placed in a furnace
The crucibles are removed from the furnace five at a time and the molten material is
poured into an iron mould
It is at this stage that the fire assayer will notice any poor fusions
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The moulds are cooled and the solid contents are removed
The slag is broken to free the lead button
The lead buttons are placed into cupels, ready for the next stage
THE CUPELLATION
Cupellation is an oxidizing fusion of the lead button (which contains gold, silver and PGMs) in
an absorbent vessel called a cupel.
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A batch of cupels containing lead buttons is placed in a muffle furnace (in a highly
oxidizing atmosphere)
Most of the litharge is absorbed by the cupel and the remainder volatilized
A small bead or prill of silver, gold and PGMs is left behind in the cupel
Parting is the process by which the gold and PGMs contained in the prill are separated from
the silver. During the prill formation, the gold and PGMs form a sponge-like lattice within the
larger bulk of the silver. Nitric Acid, which dissolves silver but not gold, is used to take the
silver into solution, leaving a gold sponge.
The PGMs are partly soluble in nitric acid and give indication of their presence at this stage.
Platinum gives the parting acid a brown to blackish colour and in alloy with gold produces a
steel grey instead of yellow sponge. Palladium yields an orange coloured solution in nitric
acid. Iridium appears in the parted gold as detached black specks.
Two alternative finishing methods are used gravimetric or AAS.
Gravimetric Part and Weigh Finish:
This is the traditional method for determining the gold content of the prill
The gold sponge which was produced by the parting process is washed with distilled
water
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The gravimetric part and weigh finish is considered to be more accurate than an AAS finish
for grades > 0.2g/t. The micro-balance is prone to less calibration errors than an AAS
machine. This is more so for higher-grade samples outside the calibration range of the AAS
machine where dilution of the gold bearing solution has to take place.
AAS Finish:
The parting solution (containing nitric acid) is treated with hydrochloric acid to dissolve
the gold sponge and PGMs
This solution is directly aspirated into an AAS machine to read the gold concentration
COMMON INTERFERENCES
The following elements can cause interference or gold loss (assay robbing) during fire
assaying:
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Nickel and Zinc are partially collected in the lead button and interfere during
cupellation when a ring of metallic oxide forms around the prill. This ring, called a
scoria, retains some of the gold.
Copper also collects with lead during cupellation and causes freezing of the copper lead - gold - silver alloy. Gold cannot be easily determined from the resulting prill.
Arsenic and Antimony form metallic arsenides and antimonides during fusion,
producing a spiesse phase on the lead button. Spiesse invariably contains some gold
and silver.
Tellurium interferes with cupellation by reducing the surface tension of the molten prill.
Gold is therefore lost by cupel absorption.
Carbon remaining unoxidized in the fusion forms a layer between the lead and slag
phases resulting in lead loss into the slag.
Several techniques are available to overcome interferences in fire assay. The choice of the
technique may be problematic, especially when dealing with a material of unknown
composition. However, the assayer learns, from experience, which technique is most suitable
for specific ore types.
Fusion with Special Fluxes, combined with a reduction in sample weigh, is the most
practical way of overcoming interferences. The addition of reagents (other than those
necessary for the formation of a slag) provides enough excess reagent in the fusion to
neutralize the interference.
Potassium Nitrate is a powerful oxidizing agent and can be used to oxidize metallic
sulphides and carbon.
and limiting the litharge and borax. An iron matte is formed by the action of metallic
iron on the sulphide and this matte is dissolved by the excess alkaline flux.
Cu2S + Fe
2Cu + FeS
Once any of the interfering elements mentioned above (and particularly the metals) enter the
percent range, interferences with the gold determination can occur. Spot tests for the
presence of sulphides or carbonates are routinely performed by the Lab and quickly give the
assayer estimates of the interfering elements present.
General information regarding expected values of interfering elements can save the
Laboratory and the Geologist time and money.
LOWER LIMIT
OF DETECTION
Lead
Gravimetric part and weigh
0.2 g/t *
Lead
Flame AAS detection
0.01 g/t **
Lead
DIBK extraction, flame AAS detection
0.001 g/t **
Lead
Graphite furnace, AAS / ICP-MS detection 0.001 g/t **
* (K. Renton, pers. comm.)
** (Eames, 1999)
PRECISION OF THE FIRE ASSAY TECHNIQUE
PRECISION
10%
FINISH
CONFIDENCE LEVEL
95%
GOLD CONCENTRATIONS
>50 times the detection limit
(Eames, 1999)
Where:
The precision at the detection limit is very poor because errors are amplified,
therefore the calculation should not include replicates below a certain gold
concentration
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ACID DIGEST
INTRODUCTION
Acid digest is also known as aqua regia digest and refers to the 2 acids used to dissolve the
gold in the sample nitric acid and hydrochloric acid. It relies on chemical dissolution of the
sample which in some cases is not as effective as the fusion performed in fire assay.
The technique is often used for grade control and mill samples because it is cheaper to use
than fire assay at a commercial laboratory. Many minesites set up their own site labs with acid
digest facilities because of the low capital outlay, simplicity of operation and faster assay
turnaround.
Care must be taken with certain ore types because the digest is affected by some minerals
and elements. A strict adherence to procedures must be followed during routine analysis to
prevent only partial digestion of the sample.
PREPARING THE ASSAY CHARGE
A batch of samples is made up, the number usually determined by the size of the hot
plate
PRE-ROAST
It is necessary to pre-roast samples containing elevated sulphides and carbon to liberate the
gold:
Care must be taken not to overcook iron sulphides as this can cause gold lockup in
the resulting iron oxide
THE DIGEST
The digestion process relies on free chlorine provided by the aqua regia to dissolve the gold:
Concentrated nitric acid is added first and this will commence dissolution of sulphides,
etc
Once the reaction has subsided, concentrated hydrochloric acid is added and this
forms aqua regia with the nitric acid
The beakers are removed from the hotplate and allowed to cool
The solution is further treated with acids to remove interferences (e.g. orthophosphoric
acid is added to suppress iron)
THE EXTRACTION
Gold is extracted and concentrated from the aqueous solution into an organic solvent to
produce a solution that is free of elements which can cause major interferences during
measurement:
The test tubes are shaken in a mechanical mixer for a set period of time to ensure full
extraction
THE DETERMINATION
The DIBK solution is aspirated directly into an AAS machine to measure the gold
concentration.
COMMON INTERFERENCE AND EXTRACTION PROBLEMS
The following procedures, minerals and elements can cause incomplete digestion and
extraction of the gold:
Inadequate shaking of the aqueous/DIBK mixture will cause poor gold extraction
Silicates and carbonaceous minerals are not attacked by aqua regia and may enclose
gold particles
Significant quantities of sulphides and carbonates can require extra reagent for
complete dissolution
Sulphides can cause acid overflow (and gold loss) on the hotplate
Gold associated with copper and tellurium can be lost through fuming of the
dichlorides in a poorly executed digest
Samples high in iron oxides (particularly magnetite) will cause inadequate digestion
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Acid digest results need to be regularly checked by fire assaying. Eames, 1999, states that a
comparison of acid digest results with fire assay results over several years has shown that
acid digest only recovers about 90% of the gold. High-Fe matrix samples (such as laterites)
commonly show aqua regia Au results which are only 70 - 90% of fire assay results.
TYPICAL ACID DIGEST DETECTION LIMITS
EXTRACTION
25g, DIBK
50g, DIBK
25g, DIBK
50g, DIBK
25-100g, DIBK
FINISH
LOWER LIMIT
OF DETECTION
0.02 g/t
0.01 g/t
0.001 g/t
0.001 g/t
0.0001 g/t
(Eames, 1999)
CONFIDENCE LEVEL
95%
GOLD CONCENTRATIONS
>50 times the detection limit
(Eames, 1999)
Where:
The precision at the detection limit is very poor because errors are amplified,
therefore the calculation should not include replicates below a certain gold
concentration
CYANIDE LEACH
INTRODUCTION
The cyanide leach technique was developed as a cost-effective method of determining gold in
large samples. In Exploration, the Bulk Leach Extractable Gold (BLEG) method is used on
soil samples up to 10kg in size. The mill uses Bottle Rolls in testwork on ore samples to
simulate gold recovery in a CIP plant.
For grade control, some mining operations use an accelerated cyanide extraction technique
for assaying gold. This is known by various names, such as:
Gold extraction is performed in less than 1 hour, thus allowing a quick turnaround time for
results. The advantage over other assaying techniques is the ability to use large assay
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charges up to 1kg in weight. However, the cyanide extraction is only partial, so is not suitable
when a total gold content is required. The partial extraction mirrors the performance of a CIP
or CIL plant.
PREPARING THE ASSAY CHARGE
The standard assay charge weights used are 250g, 500g or 1000g
A batch of samples is made up, the number usually determined by the size of the
mixing machine
THE LEACHING
4NaAu(CN)2 + 4NaOH
Only gold particles that come into physical contact with the cyanide solution are available to
be taken into solution. Gold bound in a mineral matrix is not available for dissolution.
A catalyst called LeachWELLTM 60X is used to accelerate the normal cyanidation reaction
time by 60 times. The leaching procedure is outlined below:
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THE EXTRACTION
Gold is extracted and concentrated from the aqueous solution into an organic solvent to produce a
solution that is free of elements which can cause major interferences during measurement:
The test tubes are shaken in a mechanical mixer for a set period of time to ensure full
extraction
THE DETERMINATION
The DIBK solution is aspirated directly into an AAS machine to measure the gold concentration.
COMMON INTERFERENCE AND EXTRACTION PROBLEMS
The following procedures and minerals can cause incomplete leaching and extraction of the gold:
Inadequate shaking of the aqueous/DIBK mixture will cause poor gold extraction
Gold which is refractory (no exposed surfaces) such as in arsenopyrite cannot be leached
Cyanide and oxygen consuming minerals such as malachite, azurite, pyrrhotite and pyrite
can deplete the reagents so that leaching of the gold is incomplete
Normal cyanide extraction can suffer from the following additional problems:
Very coarse gold particles are not dissolved in the time allocated to a standard extraction.
Preg-robbing can occur where the extraction process proceeds for too long allowing
dissolved gold to be progressively locked up by gold-attracting minerals. This has been
documented with certain ores containing clays, Fe, Cu, Co and Ni (Menne, 1992).
The fast action of LeachWELLTM 60X plus high cyanide concentration will generally prevent these
two problems from developing.
CHECKS WITH FIRE ASSAY
Cyanide extraction results need to be regularly checked by fire assaying.
An alternative technique to screen fire assaying for determining total gold in a large sample, but at
a lower cost is:
13
Reference for Mineral Reserves and Resources
However, the accuracy will be high with regard to cyanide extractable gold (e.g. if
comparing to a CIP plant)
Accuracy will also be improved (e.g. compared to fire assay) if the pulp is not homogeneous
because a large sample size is used.
14
Reference for Mineral Reserves and Resources
APPENDIX 6-4
SCREEN FIRE ASSAYING
INTRODUCTION
The first sign of coarse gold in an ore type is poor repeatability of the 50g fire assay replicates
in a quality control campaign. Screen Fire Assaying is a technique that can accurately
determine the gold grade of a sample containing coarse gold particles (or nuggets). It also
gives an indication of the amount of the problematic coarse gold, as a proportion of the total
gold in the sample.
The coarse sizing (containing the coarse gold particles) and sieve cloth are fire
assayed in total using 50g charges
The grade of the fine sizing (which forms the largest proportion of the split by weight)
is determined by taking 3 x 50g assay charges and averaging their grades
The grades of the coarse sizing and fine sizing are combined in proportion to their
original weights to give the grade of the 1kg pulp split
Additional information on gold distribution can be obtained if 2 or more sieves are used.
Screen fire assaying is an expensive but necessary part of any orientation testwork. The cost
of a screen fire assay is determined by the time taken to grind, sieve and weigh the sample
and the number of fire assays in each sample. Care must be taken to outline the exact Barrick
required procedure to the lab as there are many shortcuts that the Labs use to keep their
costs down.
PROCEDURE USING 2 SIEVES
The procedure described below is the usual format that should be requested at Barrick
minesites for orientation-type testwork.
1. Grind Check
It is necessary to determine how much +75 micron material will be generated. This
should be <100g to keep assaying costs down. Proceed as follows:
Take 100g of pulp and determine the grind size by wet sieving
If <90% passing 75microns, the pulp will need to be pulverized further
1
Reference for Mineral Reserves and Resources
2. Screening
Split out approximately 1kg of pulp and record the pulp weight
Screen the pulp using 106 and 75 sieves
Screen entire pulp
Weigh each sizing:
+106
-106 + 75
-75
Fire assay the entire +106 sizing and use a gravimetric finish. Do not regrind and
resieve this sizing to make it smaller. Calculate the grade of the +106 sizing
Fire assay the entire -106 + 75 sizing and use a gravimetric finish. Do not
regrind and resieve this sizing to make smaller. Calculate the grade of the -106 +
75 sizing
Perform 3 fire assays on the -75 sizing using 50g assay charges and a
gravimetric finish. Calculate the grade of this sizing as an average of the 3 x 50g
assay charges
Calculate the weighted average grade of each pulp by combining the grades of the
+106, the -106 + 75 and the -75 sizings using the sizing weights as weighting
factors
4. Presentation of Results
SCREEN FIRE ASSAYS
Deposit:
SIZINGS
Column 1
+106
-106+75
-75
TOTALS
Pulp Number:
Pulp Weight:
50g
50g
50g
WEIGHTED AVERAGE GRADE Au (g/t)
Notes:
Column 2: Weight of entire sizing
Column 9: Add Columns 6, 7, 8
Column 10: Weight of Au (mg) in entire sizing = [Column 9 x Column 2]
[Columns 3+4+5]
Column 11: Grade of Au (g/t) in entire sizing = [Column 10 x 1000]
Column 2
WEIGHTED AVERAGE GRADE Au (g/t) = average the sizing grades in Column 11 using the sizing
weights in Column 2 as weighting factors
2
Reference for Mineral Reserves and Resources
ORIGINAL
GRADE
(for comparison)
+106
SIZING GRADES
Au (g/t)
-106+75
-75
WEIGHTED AVERAGE
GRADE
Au (g/t)
The 3 assay charges from the fine sizing may be assayed by acid digest, however, this
is not recommended as additional errors are introduced by mixing 2 assaying
techniques
3
Reference for Mineral Reserves and Resources
APPENDIX 6-5
LABORATORY AUDIT FORM
Laboratory Name:
Laboratory Manager:
Address:
Phone:
Fax:
E-mail:
DATE
ACTION LIST
Deadline Completed
1.
2.
3.
4.
1
Reference for Mineral Reserves and Resources
5.
Size:
Layout:
HANDLING &
SORTING
PROCEDURE
System:
Sample No Recording:
LIMS
Data Tracking:
STAFFING
Numbers:
No Samples:
AREA
Size:
Layout:
CLEANLINESS
General:
Dust Control:
Ventilation:
SAMPLE
DRYING
Type:
Capacity:
Method of Loading and Unloading:
FACILITIES
Drying Time:
Drying Temperature:
2
Reference for Mineral Reserves and Resources
EQUIPMENT
CRUSHERS
Type:
Condition:
PULVERIZERS
Type:
Condition:
SPLITTERS
Type:
Condition:
EQUIPMENT SPECIFICATIONS
3
Reference for Mineral Reserves and Resources
CRUSHERS
PULVERISERS
No Pulverising Stages:
Grind Time:
Grind Size:
SPLITTERS
EQUIPMENT CLEANING
CRUSHERS
Method:
Cleaning Material:
PULVERIZERS
Method:
Cleaning Material:
SPLITTERS
Method:
Cleaning Material:
Frequency of Testing:
- CRUSHERS
- PULVERIZERS
RECORDING OF
QC RESULTS
STAFFING
Numbers:
4
Reference for Mineral Reserves and Resources
No Samples:
AREA
Size:
Layout:
FUSION
Type:
FURNACES
Batch Size:
Condition:
CUPEL
Type:
FURNACE
Cupel Capacity:
CRUCIBLE SIZE
Catch-Weight or Exact:
CHARGE SIZE
FLUX
Composition:
Mixing System:
Sample : Flux Ratio
No Assay Samples:
o
N Standards:
No Duplicates:
o
N Blanks:
Grades of Standards:
FUSION TIME
CRUCIBLE REUSE
Grade(g/t):
PRILL DIGEST
Acid Mix:
Condition:
Time:
5
Reference for Mineral Reserves and Resources
No Samples:
AREA
Size:
Layout:
Cleanliness:
Fume Hoods:
Distilled Water Source:
PRE-ROAST
Crucible Capacity:
FURNACE
Condition:
Catch-Weight or Exact:
CHARGE SIZE
DIGEST MAKEUP
Temperature:
Acids:
Batch Size:
No Assay Samples:
No Duplicates:
No Standards:
No Blanks:
Grades of Standards:
DIGEST
Digest Time:
Hotplate Temperature Monitoring:
FURTHER TREATMENT
Orthophosphoric Acid:
EXTRACTION
Frequency:
6
Reference for Mineral Reserves and Resources
INSTRUMENT FACILITIES
CLEANLINESS
WEIGHING BALANCE
Type:
Manual/Auto to LIMS:
MICRO-BALANCE
AAS MACHINE
Make/Model:
OTHER INSTRUMENTS
CALIBRATION OF
AAS MACHINE
Type of Standards:
Grade of Standards:
Storage of Standards:
Manual/Auto to LIMS:
SAMPLE STORAGE
AREA
Size:
Layout / Access:
PULP STORAGE
Storage Period:
ID / Layout / Access:
Dispatch System:
REJECT STORAGE
Storage Period:
ID / Layout / Access:
ORGANIZATION
General:
SAFETY ISSUES
GENERAL
7
Reference for Mineral Reserves and Resources
Type:
Frequency of use:
Grades used:
ACID DIGEST
Type:
Frequency
Grades used:
CYANIDE LEACH
Type:
Frequency
Grades used:
AAS MACHINE
Type:
Frequency
Grades used:
Other
Type:
Frequency
Grades used:
Which Stage:
Frequency of use:
PULP DUPLICATES
Which Stage:
Frequency of use:
INTERLABORATORY TEST
PROGRAM PARTICIPATION
Outside:
In-house:
QC MANAGER
QC DATA
8
Reference for Mineral Reserves and Resources
DATA HANDLING
LABORATORY INFORMATION
MANAGEMENT SYSTEM (LIMS)
Type:
LABORATORY
DATABASES
AND RECORDS
REPORTING
FORMAT
Assays:
Grind Checks:
QC Results:
DATA
TRANSMISSION
Email:
Fax:
Post:
INVOICING
SYSTEM
9
Reference for Mineral Reserves and Resources
LABORATORY PERSONNEL
TOTAL NUMBERS
WORKING SHIFTS
Chemist:
JOB
CLASSIFICATIONS
AND PERSONNEL Fire Assayer:
QUALIFICATIONS
Supervisors:
TRAINING
TURNOVER
10
Reference for Mineral Reserves and Resources
APPENDIX 6-6
HETEROGENEITY TESTWORK
The three areas that affect assay quality are sampling, sample preparation and analysis. In
general terms, the errors in sampling are the largest, but are often difficult to reduce. With
good laboratory practices, errors in analysis should be small, but the errors in sample
preparation are often much higher. Improving sample preparation is the easiest way to
achieve an overall improvement in data quality.
SAMPLING THEORY
How can sample preparation be improved? There are three basic areas to be critically
examined; sample size, the fineness of the sample at each split and the method used to split
the sample. Also to be considered is the cost of any improvements, in terms of the capital
cost for any additional equipment and any extra labor cost for processing each sample.
The effects of increasing sample size and reducing particle size are both included in Pierre
Gys equation:
For any given mineral deposit; the two factors that can be varied are the weight MS to be
taken as a sample and the top particle size d (usually at the 95% passing screen size). The
variance S2FE is reduced as sample weight MS is increased and particle size d is reduced.
What is often overlooked is that the factor d is cubed in the equation.
Doubling the sample weight halves the variance, reducing the particle size by half reduces the
variance by a factor of 8. Particle size reduction is far more effective than increasing
sample size if you want to reduce errors.
The steps in a sample preparation procedure can be quantified in a sampling nomograph.
HETEROGENEITY TESTWORK
Heterogeneity testwork is carried out on an ore type to provide the base information (i.e. S2FE ,
C and d) from which a sampling nomograph can be constructed using Gys sampling formula
described above.
1
Reference for Mineral Reserves and Resources
A heterogeneity test is usually performed on a large ore sample (>200kg) and is carried out
by a Reference Laboratory. The cost of each test is about usually several thousand dollars.
Further costs are incurred producing the nomograph. A format which can be followed for a
heterogeneity test can be obtained from the following internal company report:
Mandyczewsky, A and Rowley, M. 1999. Report on Heterogeneity Testwork, New Holland
South Ore. Lawlers Gold Mine.
SAMPLING NOMOGRAPH
It can be used to design a sample preparation procedure that obeys the rules of
sampling theory
It can be used to estimate the sampling errors associated with each sample
preparation step
0.100000
FE)
1.000000
0.010000
0.001000
0.000100
1.7
6.3
3.3
mm
5m
5m
(10
m
m(
me
6m
sh
es
)
1.0
h
)
mm
(16
me
sh
0.7
)
1m
m(
24
me
sh
0.4
)
25
(35
me
0.3
sh
mm
)
(48
me
0.2
sh
12
)
mm
(
6
0.1
5m
5m
es
h)
m(
10
0m
0.1
06
esh
mm
)
(15
0.0
0m
75
es
mm
h)
(20
0m
es
h)
1
10
.5m 2.7m
m
m
25
.4m
m
50
mm
Split to 3kg
Safety Line(FE=+/-16%)
Safety Line(FE=+/-10%)
30kg Drill
Sample
Pulverize
in LM5
Fire
Assay
0.000010
Subsample
50g
0.000001
10
10
0
1,0
00
10
,00
0
10
0
,00
0
1,0
00
,0
10
00
,00
0,0
00
Note: This nomograph indicates that the first sampling step (splitting the RC sample to 3kg) introduces an
unacceptable sampling error because the sample is now well above the safety line. The last sampling step
(splitting the RC sample from 3kg to 50g) will generate a very low sampling error because the entire sample was
pulverised to 75 microns and this is well below the safety line.
2
Reference for Mineral Reserves and Resources
Section 7
QA/QC
for
REFERENCES ............................................................................................................7-43
APPENDICES
Appendix 7-1
Appendix 7-2
7.1. INTRODUCTION
The concept of Quality Assessment and Quality Control (QA/QC) can be applied to any form
of data collection, data or geological interpretation, estimation, planning, scheduling, or design
process. For example, the daily execution by the operators of a mine plan and schedule is an
activity that requires constant evaluation by both the Mine and Mine Engineering
Departments. The mine engineers must confirm that the mine foreman and shift bosses are
implementing the mine plan and schedule as designed. If the shift bosses are constantly
having to juggling the plan in order to meet the schedule, then the two departments have to
determine the reason (Quality Assessment, or QA). Once the problem is identified, steps
then are taken either to revise the plan and schedule or, perhaps, to add an additional truck to
night shift (Quality Control, or QC).
Although QA/QC can be applied to any operating activity, it is most commonly applied to
sampling and assaying, as discussed in this section of this reference volume. Here, QC is
achieved by following good work practices and set procedures. Examples of these activities
include:
Cleaning out the splitter on the drill rig after each sample to control contamination.
Ensuring that the sample preparation section of the assay laboratory is following
prescribed procedures.
An integral part of Barricks quality control procedures are the checks that have been put in
place to monitor the accuracy of the primary assay data produced by a laboratory. Although
each laboratory will have its own quality control procedures, these procedures are separate
from the quality control measures undertaken by Barrick, and at no time should the laboratory
QC procedures supplant Barricks own.
Quality assessment is the interpretation of the quality control data to determine if the results
(in this case, assays) meet the required minimum standards set by Barrick.
REVERSE CIRCULATION
DRILL
GENERATION
DIAMOND CORE
Split
Insert Standards
and Blanks
Primary
Assay
Split
Field
Reject
PRINCIPAL
PRIMARY
LAB
LAB
PRIMARY
ASSAY
Select 5% of
Pulp Split
(insert Standards
and Blanks)
Sample
Farm
Select 5% of RC
Field Rejects
UMPIRE
SECONDARY
LAB
LAB
Select 2 - 5% of
Half Core
CHECK ASSAYS
Resplit
Insert Standards
and Blanks
Assay
Split
PRINCIPAL
PRIMARY
LAB
LAB
CHECK
SAMPLE
7-2
Reference for Mineral Reserves and Resources
Assay
Split
.
Total
Sample
Prep
Crush
Split
GRIND CHECKS - are performed after each crushing and pulverising stage to
determine if the particle size reduction is adequate. The particle size is critical
to achieving a homogeneous pulp split.
Pulp
Split
Assay A
Au 1
Au 2
Au(etc)
Assay B
Au 2
Au(etc)
7-3
Reference for Mineral Reserves and Resources
The suggested quality control measures that should be undertaken at each site are shown
below.
SECTION
DEVELOPMENT
GRADE
CONTROL
STANDARDS BLANKS
(SRMs)
GRIND
CHECKS
CHECK
SAMPLING
CHECK
ASSAYING
DRILLING
(RC & DC)
5%
2%
1%
RC 5%
DC 2%
5%
DRILLING
(RC & DC)
5%
2%
1%
RC 5%
DC 2%
5%
SLUDGE
DRILLING
5%
2%
1%
5%
UG FACE
SAMPLING
5%
2%
1%
5%
BLAST
HOLES
5%
2%
1%
5%
5%
DITCH
WITCHING
5%
2%
1%
5%
5%
STOCKPILE
SAMPLING
5%
2%
1%
5%
The percentage shown indicates the number of checks to be performed per 100 primary samples.
For example, the 5% insertion rates for SRMs, as shown above, equates to one standard per
20 samples submitted to the laboratory. The percentages for check samples and check
assays are considered to be the industry-accepted minimum for a QA/QC program.
SRMs and blanks should be submitted blind where possible, since the intent of a QA/QC
program is to check the laboratory under normal operating conditions, with the laboratory
giving no more attention to a blank or standard than to any other sample. This is easier said
than done, as a single SRM sample pulp envelope stands out when submitted with 20 sample
sacks containing random-sized pieces of diamond drill core, for example. This easily flags
the SRM for the laboratory, and may result in the laboratory giving the SRM special attention
and care (such as running duplicates of the SRM pulp) relative to the other samples. Little
can be done about this, since it is important for the standard to be included in the lot of 20 drill
core samples, in this particular example.
It is easier to submit blanks blind to the laboratory. Samples known to lack any gold from
previous sampling, for example, drill core splits of quarter core or rig splits of RC samples
(see Section 4.15.3.2 of this reference volume), can be used for this purpose. Because the
blanks have the appearance of a routine sample, there is less chance of the laboratory
identifying them.
7-4
Reference for Mineral Reserves and Resources
- SRMs are used to monitor the assaying accuracy of the laboratory As general rule, an SRM should always be submitted along with any set of samples that is
sent to the laboratory, particularly if Barrick has not used the laboratory previously.
The following diagram shows the location in the Quality Control Flowchart of insertion points
for SRMs.
REVERSE CIRCULATION
DRILL SAMPLE
GENERATION
DIAMOND CORE
Split
Insert Standards
and Blanks
Primary
Assay
Subsamples
INSERT
Field
Residue
PRINCIPAL
PRINCIPAL
LAB
LAB
PRIMARY
ASSAYS
Select 5% of
Pulp Subsamples
(insert Standards
and Blanks)
Sample
Farm
STANDARDS
Select 5% of RC
Field Residues
UMPIRE
UMPIRE
LAB
LAB
Select 2 - 5% of
Half Core
CHECK ASSAYS
Resplit
Insert Standards
and Blanks
Assay
Subsamples
PRINCIPAL
PRINCIPAL
LAB
LAB
CHECK
SAMPLES
7-5
Reference for Mineral Reserves and Resources
7.3.1.1.
Properties
An SRM must have the following properties for it to be able to perform its function:
The value of the SRM must be accurately determined and the standard deviation of
the various splits that are run to determine the value must be low.
The SRM must be a homogeneous pulp - it cannot be made from ore containing
coarse gold.
The SRM must remain stable over the length of time it is used as a standard. Stability
issues include:
The presence of particles with a wide range of densities should be avoided in the
preparation of SRMs. SRMs containing sulphides are discussed in more detail below.
The SRM should consist either of an ore type from the project site or, if a commercial
SRM is used, it should consist of a rock type similar to the samples being assayed.
Commercial SRMs must have a certificate that specifies all the details of the
validation process used to establish the grade of the SRM.
A sufficient number of SRMs must be available for monitoring the assaying of the important
ore types and grade ranges at each operation or project site. These include but are not
limited to:
A variety of grade ranges in order to support future production cutoff grade decisions
and to provide a check against sample dilution required for atomic absorption (AA)
analyses of samples having grades near or beyond the upper range of detection.
Unless site- or project-specific guidelines are in place, the following describes the minimum
recommended suite of SRM samples that should be established and maintained at a Barrick
project for insertion into the sample stream on a rotating basis:
7-6
Reference for Mineral Reserves and Resources
Where possible, the SRMs should consist of visually similar material, although this will
be difficult when dealing with ores having high sulphide content.
If applicable, these SRMs should have oxide and fresh (sulphide) versions.
If required, special SRMs should be prepared to address unique or problem ore types
(such as highly refractive material, or material with high-carbon content).
7.3.1.2.
SRMs may be purchased from a reliable supplier, or prepared at the operation/project site
using material from the deposit to provide custom site-based standards. The advantage of a
site-based SRM is that it will have the same mineralogy as the samples sent for assay.
The preparation and assaying of a site-specific SRM generally takes a minimum of two
months. At operating mines, material can be collected in bulk from the pit or underground
workings for preparation of a SRM. On projects in the pre-development stage, SRMs
normally are developed as composites of numerous individual sample rejects from either drill
core or RC cuttings. The preparation procedure is as follows:
Select a suitable laboratory for preparing the SRM, ensuring that the laboratory has
the right equipment to prepare a large sample. SRMs can be prepared on-site
provided that the operation or project laboratory has the necessary equipment,
including:
Screens (45m, 75m and 106m) for testing the grind size.
Select a material type suitable for the desired SRM. This should take into account :
The maximum sample fragment size that can be run through the crusher of the
primary laboratory.
The size and distribution of gold particles (again, samples containing coarse gold
are not acceptable for use as SRMs).
The grade of the individual sample rejects to be composited. If the sample rejects
used for the composite have a wide range of grades, the individual weights of the
samples used must be known so that the target grade of the SRM can be
achieved.
Pulp rejects that are no longer needed for QA/QC check assays may be combined
to create a composite that can be used as an SRM. This is the quickest method
7-7
for creating an SRM, but has the disadvantage that the resulting size of the SRM
will be limited, compared to a complete SRM prepared from drill core or RC
cuttings rejects.
Collect at least 50kg (110lb) of material for the preparation of each SRM, or at least
enough to last several months, as drawn from experience over time.
Submit the entire SRM sample for preparation and assay to the laboratory chosen as
the primary laboratory for the operation or project. During preparation of the SRM, it is
essential that the grind size be monitored to ensure the homogeneity of the SRM:
Take 5 random samples of pulverized material, each weighing 100g, and submit
these to a third party (secondary) laboratory.
The secondary laboratory should pass each sample, wet, through 3 screens
(45m, 75m and 106m), calculate the percent of sample passing through each
screen, and determine if the grind is sufficient (90% passing 45m).
Fire assay five pulp splits using the finishing technique generally employed by the
laboratory. If the SRM is high-grade, a gravimetric finish must be used. The results of
these analyses establish the preliminary value of the SRM.
Determine the true or recommended grade and confirm the homogeneity of the SRM
as follows:
Take 20 100-g pulp splits of the SRM and submit five each to four third party
(secondary) laboratories. Secondary laboratories may include laboratories at
other Barrick operations.
Each laboratory should assay the samples as one batch, employing the same
finishing technique used by the primary laboratory.
For the SRM to pass the homogeneity test, all of the results must fall within 10% of
the mean value (calculated using all results), and 90% of the results must fall
within 5% of the mean value.
If this test is not passed, check to see that the reason is not due to the results of
one laboratory being skewed relative to the other laboratories. This may indicate
contamination of the SRM in that laboratory, or some other procedural error.
Whatever the reason, known or otherwise, the laboratory in question should re-run
the five pulps. If satisfied that all laboratory procedures are correct, but the
homogeneity test is still not passed, that SRM should be discarded.
Calculate the standard deviation using all data, then discard all values more than three
standard deviations from the mean value (if any) and recalculate the standard
deviation. This value should be used to establish the Warning Lines and Action
7-8
Reference for Mineral Reserves and Resources
Lines in graphs used to evaluate sampling and assaying QC results (see Section
7.4.4).
The SRM must be packaged at the laboratory into containers no larger than 2.5kg
(5.5lb) before being transported in order to minimize the effect of gold segregation
during transport.
When needed, the containers should be picked at random and not in the sequence
they were packaged at the laboratory.
Another option is to send a bulk sample from the site to a commercial supplier of SRMs for
preparation. The cost for this alternative will exceed the cost of buying a commercial SRM,
but it provides a site-based SRM while freeing site personnel for other project tasks.
7.3.1.3.
Date of certification.
Reference to special properties of the SRM (such as contains sulphides or, should
not be subjected to temperatures over 50oC, et cetera).
7-9
Reference for Mineral Reserves and Resources
7.3.1.4.
Standard Reference Materials should be inserted into the sample submittal and analysis
stream on a regular basis. As a general rule, at least one SRM must be included in each
assay batch (a batch normally contains 25 or 50 samples). However, for simplicity of
discussion, the rate of SRM sample submittal should be set at one standard per 20
samples, as previously mentioned.
The following recommended procedure for submitting SRMs should be followed, unless a
different site- or project-specific procedure is in place:
Place approximately 250g of the SRM in a paper pulp envelope and then insert the
envelope into a numbered sample bag.
The sample number assigned to the SRM must be in sequence with the samples for
assay.
If possible, match the rock type of the SRM with the rock type of the sample lots.
Care must be taken to keep track of which SRMs are assigned to which sample
numbers.
The assays for the SRM samples will be reported in sequence along with the samples
submitted for assay on each assay report.
7.3.2.
BLANKS
Blanks are samples of material known to be void of gold mineralization. These samples are
useful for monitoring both the sample preparation and assay sections of a laboratory.
Contamination of sample preparation equipment is one of the most common sources for
assay laboratory error. Because gold is very soft and malleable compared to the gangue or
other material that commonly serves as its host, coarser gold particles can be smeared by the
much harder working surfaces of the preparation equipment (i.e., crusher jaws, pulverizer
plates, et cetera) such that it adheres to these surfaces. Unless the sample preparation
technicians routinely clean the equipment by passing barren silica sand through it between
the samples submitted for assay, any gold adhering to the working surfaces usually is
knocked loose during the preparation of the next sample.
In general it is good practice to include blanks with any samples that are sent to the
laboratory. Insertion of blanks will identify poor cleaning practices within the sample
preparation sections, but only if the blank samples are not visually different from the other
samples in the lot. As with SRMs, the purpose of running blank samples is to check the
laboratorys procedures and accuracy under normal operating conditions. If a laboratorys
sample preparation technicians are easily able to detect potential blank samples, the
possibility that the blanks will receive special treatment during preparation increases, and the
purpose of the QC procedure is defeated.
The diagram in the following section shows the location in the Quality Control Flowchart of
recommended insertion points for blanks:
7-10
Reference for Mineral Reserves and Resources
7.3.2.1.
Properties
A blank must have the following properties in order for it to be able to perform its function:
It should resemble the primary samples in sample weight, particle size and sample
type (prepared from split or sawn drill core, RC cuttings, rock chips or grab material).
- Blanks are used to monitor the sample preparation and assaying accuracy of
the laboratory -
REVERSE CIRCULATION
DRILL SAMPLE
GENERATION
DIAMONDCORE
Split
Insert Standards
and Blanks
Primary
Assay
Subsamples
INSERT
Field
Residue
PRINCIPAL
PRINCIPAL
LAB
LAB
PRIMARY
ASSAYS
Select 5%of
Pulp Subsamples
(insert Standards
and Blanks)
Sample
Farm
BLANKS
Select 5%of RC
Field Residues
UMPIRE
UMPIRE
LAB
LAB
Select 2 - 5%of
Half Core
CHECK ASSAYS
Resplit
Insert Standards
and Blanks
Assay
Subsamples
7.3.2.2.
PRINCIPAL
PRINCIPAL
LAB
LAB
CHECK
SAMPLES
Preparation of Blanks
Unlike SRMs, blanks can be easily prepared at a mine or project site. The guidelines for
choosing material for blanks are as follows:
7-11
Reference for Mineral Reserves and Resources
Blanks should be comprised of material that is hard enough to remove any gold
contamination which remains in the sample preparation equipment from the previous
sample.
Diamond core blanks can be developed by splitting or sawing core that the geologists
believe to be barren and then having the core prepared and assayed under controlled
conditions, where great care is taken by sample preparation and analytical personnel
to ensure that no contamination takes place during analysis.
At least five separate samples should be taken from the material selected as a
possible source for sample blanks.
The samples can be prepared and assayed either at a Barrick operations laboratory or
by an independent laboratory. It is best to choose a laboratory other than the one
chosen as the primary laboratory.
Inform the laboratory of the nature of the samples. This is very important, since the
principal objective is to confirm that the potential blank material contains no gold
above laboratory detection limits. Thus, the material must be prepared and assayed
under carefully controlled conditions:
Both an AA finish and a gravimetric finish should be used, since there is a chance
for noise in the AA finish to provide a false indication of the presence of gold. A
gravimetric finish will show gold if any is present (see Section 6, SAMPLE
PREPARATION AND ASSAYING, of this reference volume for a discussion of
assay finishing techniques).
If any of the five samples show detectable gold, the blank material must be discarded
and new material selected.
7.3.2.3.
As with SRMs, blanks should be inserted into the sample submittal and analysis stream on a
regular basis. As a general rule, at least one blank should be included in every other sample
batch (approximately one every 50 samples).
7-12
Reference for Mineral Reserves and Resources
The following recommended procedure for submitting blanks should be followed, unless a
different site- or project-specific procedure is in place:
Place the blank into a numbered sample bag, using a number that is in sequence
with the other samples in the lot.
In addition to the blanks submitted under a Barrick QC program, most laboratories insert a
pulp blank with each assay batch as part of internal quality control programs. Check to see
that these data are available and review the results regularly.
The assays for the blank samples will be reported in sequence along with the samples
submitted for assay on each assay report.
7.3.3.
GRIND CHECKS
Grind checks are tests done on the products of crushing and pulverizing to determine if the
sample preparation procedures at the laboratory are adequate for producing assay pulp splits
of uniform particle size. Grind specifications are set as part of the Sample Preparation
Protocol that is developed at the beginning of a project (see Section 6, SAMPLE
PREPARATION AND ASSAYING, of this reference volume), and the laboratory must be
regularly checked for compliance with these specifications.
The areas where grind checks should be performed are indicated on the Quality Control
Flowchart below.
7-13
Reference for Mineral Reserves and Resources
REVERSE CIRCULATION
DRILL SAMPLE
GENERATION
DIAMOND CORE
Split
Insert Standards
and Blanks
Primary
Assay
Subsamples
GRIND
Field
Residue
PRINCIPAL
PRINCIPAL
LAB
LAB
PRIMARY
ASSAYS
Select 5% of
Pulp Subsamples
(insert Standards
and Blanks)
Sample
Farm
CHECKS
Select 5% of RC
Field Residues
UMPIRE
UMPIRE
LAB
LAB
Select 2 - 5% of
Half Core
CHECK ASSAYS
Resplit
Insert Standards
and Blanks
Assay
Subsamples
7.3.3.1
PRINCIPAL
PRINCIPAL
LAB
LAB
CHECK
SAMPLES
Usually, grind checks are made at two points in the sample preparation sequence:
The most important point at which to regularly perform grind checks is after pulverizing, since
this is the final stage of size reduction of a sample prior to splitting for assay. Pulps that have
poor homogeneity as a function of inadequate pulverizing are much more likely to produce
erratic assay results. Grind checks made after coarse crushing are useful for determining any
adjustments required to crushing equipment that could facilitate pulverizing and improve
pulverizer performance. Also, if the size product of the crushing step does not meet sample
preparation protocols, the splitting of the coarse reject material may be adversely affected.
Unless a mine or site-specific grind check procedure is in place, grind checks should follow
this recommended sequence of steps:
Selection of a screen size - The appropriate screen size for a particular ore type is the
one that will pass a ground product that, when continuously re-assayed, will achieve
reproducible assay results. The convention is that the screen must pass 90% of the
ground product. This is referred to as P90. Common screen sizes used for pulps are
75m and 106m.
Screening Method - The laboratory should carry out grind checks using the methods
described below:
7-14
Reference for Mineral Reserves and Resources
Pulps
Use the coarse reject (not the coarse split selected for assaying).
Split out approximately 100g of dry coarse reject and weigh accurately.
Dry sieve the coarse reject through the screen.
Weigh the oversize (Wo).
Calculate the weight of the undersize (100g Wo).
Calculate the percentage passing the screen: % = 100(100g Wo) / 100g
7.3.3.2
Secondary laboratory - One in every five check assay samples (this equates to one in
every 100 primary samples, as each check assay sample represents 5% of the total).
In addition to these prescribed grind checks, samples for random grind checks should be
collected during unannounced laboratory audits, as described in Section 6, SAMPLE
PREPARATION AND ASSAYING, of this reference volume.
7-15
Reference for Mineral Reserves and Resources
The results of both coarse crush and pulp grind checks should be reported by the laboratory
concurrently with each batch of assay results.
7.3.4.
CHECK ASSAYING
Check assaying is the process of submitting a selected set of the same pulps assayed by the
primary laboratory to a secondary laboratory for assaying. This procedure checks the
accuracy of the assay section of the primary laboratory and determines if there is an assay
bias present in that laboratorys analytical results. It should be noted, however, that check
assaying does not provide an assessment of the primary laboratorys sample preparation
process.
Selection of the secondary laboratory is important. The secondary laboratorys work must be
of demonstrated exceptional high quality, and the laboratory must use exactly the same
assaying and finishing techniques as the primary laboratory.
DRILL SAMPLE
GENERATION
DIAMOND CORE
Split
Insert Standards
and Blanks
Primary
Assay
Subsamples
CHECK
Field
Residue
PRINCIPAL
PRINCIPAL
LAB
LAB
PRIMARY
ASSAYS
Select 5% of
Pulp Subsamples
(insert Standards
and Blanks)
ASSAYING
Sample
Farm
Select 5% of RC
Field Residues
UMPIRE
UMPIRE
LAB
LAB
Select 2 - 5% of
Half Core
CHECK ASSAYS
Resplit
Insert Standards
and Blanks
Assay
Subsamples
PRINCIPAL
PRINCIPAL
LAB
LAB
CHECK
SAMPLES
7-16
Reference for Mineral Reserves and Resources
7.3.4.1.
In the absence of mine or site-specific check assaying procedures, the following suggested
procedures should be observed when submitting check assays to the secondary laboratory:
At least 5% (one in 20) of the original sample pulps should be sent for check assaying.
Using the original assay results from the primary laboratory as a guide, the geologist
should select the pulps to be submitted for check assay. The chosen suite of pulps
should be representative of the ore types present in the samples, and should include
high grade, low grade, and waste material. The waste samples should be chosen
from mineralized zones, using the geological logging as a guide.
Select 20% of the check assay pulps (this equates to one in every 100 primary
samples) for grind checks, including some pulps for which the primary laboratory has
already performed grind checks (in order to have some direct comparisons). The
secondary laboratory must use exactly the same screen sizes and screening methods
as used by the primary laboratory.
The original pulp splits must be submitted, not a duplicate split taken from pulp rejects.
The pulps should be submitted to the secondary laboratory in one batch and should
be assayed together.
At least one standard sample (SRM) pulp should be included with each lot of check
assay pulps.
Check assaying should be performed frequently, so that any problems with assay bias at the
primary laboratory can be recognized early on in the project. The results of the check
assaying should be promptly recorded and analyzed after results are received. Entry of
check assay data into electronic databases should conform to the procedures described in
Section 5, SAMPLE PREPARATION AND ASSAYING.
7.3.5.
CHECK SAMPLING
Check sampling consists of collecting a duplicate sample from material remaining from the
original sample which has not passed through the sample preparation process. For example,
check samples from diamond drill core should be obtained by sawing or splitting the half core
that remains in storage for a given sample interval. For RC drilling, check samples are
collected from the sample splits taken at the rig during drilling. For other methods of sampling
where a portion of the original sample no longer remains (such as blast hole drill cuttings,
ditch witch samples, underground face samples), where diamond drill core was sent whole for
assay or if all remaining core splits have been used, check samples can only be obtained
from coarse rejects remaining from the original sample.
Check samples must be taken from the original samples using exactly the same sampling and
splitting techniques used to collect the primary assay samples. The check samples then are
7-17
Reference for Mineral Reserves and Resources
submitted to the primary laboratory for full sample preparation and assaying. The primary
laboratory should use exactly the same sample preparation and assaying techniques that
were used on the primary samples.
The results of check sampling typically will display more erratic repeatability because of the
compounding effect of errors from sampling, sample preparation and assaying.
DRILL SAMPLE
GENERATION
DIAMOND CORE
Split
Insert Standards
and Blanks
Primary
Assay
Subsamples
Field
Residue
PRINCIPAL
PRINCIPAL
LAB
LAB
PRIMARY
ASSAYS
Select 5% of
Pulp Subsamples
(insert Standards
and Blanks)
CHECK
Sample
Farm
Select 5% of RC
Field Residues
SAMPLING
UMPIRE
UMPIRE
LAB
LAB
Select 2 - 5% of
Half Core
CHECK ASSAYS
Resplit
Insert Standards
and Blanks
Assay
Subsamples
7.3.5.1.
PRINCIPAL
PRINCIPAL
LAB
LAB
CHECK
SAMPLES
The following guidelines should be used when submitting check samples to the primary
laboratory:
7-18
Reference for Mineral Reserves and Resources
Ditch witch, blast holes, underground face samples - 5% of the original samples
(1 in 20).
Whenever possible, the check samples are collected only from the original samples.
For RC cuttings and diamond core, the same sample intervals submitted for check
assaying should be selected for check sampling. Similarly, for ditch witch, blasthole,
underground face samples, and core hole intervals where whole core was sent for
assay, the coarse rejects for the same sample intervals submitted for check assays
should be submitted for check sampling, unless a duplicate sample was collected and
saved at the time of collection of the original sample.
Diamond core - The remaining half core is split or sawn into quarter core.
Ditch, witch, blast holes, underground face samples - A second duplicate sample
is taken from the reject pile by the trench, blast hole collar, or is cut at the face.
Use a sample numbering scheme different than the one used for the primary samples.
Insert standards after every 20th sample and blanks at the rate of 1 in 50 samples.
Submit the check samples to the primary laboratory as one batch or lot.
As with check assaying, check sampling should be performed in frequent campaigns, so that
any problems with sampling protocol can be recognized early on in the project, or as soon as
they arise. The results of the check sampling should be promptly recorded and analyzed after
receipt from the laboratory. Entry of check sample data into electronic databases should
conform to the procedures described in Section 5, SAMPLE PREPARATION AND
ASSAYING. HERE
7-19
Reference for Mineral Reserves and Resources
Graphs provide quick visual indications of sampling errors, assay bias, possible switching of
sample tags in the laboratory, and other errors generated by the sampling, sample
preparation and assaying process. The graphed data then are interpreted to determine the
magnitude of any errors, and the following items are checked:
Do the checks show that some of the data are acceptable and some are outside
acceptable limits?
The geologist must then proceed to resolve any problems that apparently are affecting the
primary assays.
- Primary assay results are either accepted or rejected - They must NEVER be adjusted based on results of check assays It is important that the QC data are analyzed on a regular basis before a point of no return is
reached where assays in the database are being used for geological interpretations and
resource modeling and grade estimation.
7.4.1.
MEASUREMENT ERRORS
The errors that QC data can reveal, and which are of the most interest, are measurement
errors, because these can be remedied if identified in time. Measurement errors are
generated during the collection of assay data and can be divided into:
Sampling errors.
Assaying errors.
Random errors.
Systematic errors.
Random errors occur in every analysis, even when using the same sampling and assaying
procedures. The random error can be recognized if, in spite of using the same procedures,
the assays vary from each other by small irregular differences. As a result, the true, exact
assay of the sample is usually not known, and lies somewhere within the range of variation.
Systematic errors always affect measurements in the same way, and are usually an indication
of sampling or assaying bias, either positive or negative. These errors warrant immediate
attention, since the final assays can directly impact a resource estimate or the determination
of ore and waste classifications.
The size of the measurement errors can be determined by using accuracy and precision
functions.
7-20
Reference for Mineral Reserves and Resources
7.4.2.
Accuracy is a measure of the closeness of the assay result to the true grade of the primary
sample. Key aspects in the measurement of accuracy in assaying include:
The assay result must be close to the true grade of the assay split.
A biased result occurs if a systematic error is induced during the analysis. For
example, the primary laboratory may have a high assay bias in one grade range
compared with the secondary laboratory because one of its internal standards used
for calibrating the AA machine is too high.
Laboratory accuracy can only be verified by using standard samples of known grade.
Check assaying at the secondary laboratory will not determine which laboratory is the
more accurate.
Precision is a measure of the reproducibility of the assay results. Important aspects in the
measurement of assaying precision include:
Good precision is achieved if random errors are minimized. Random errors can occur
in field sampling, sample preparation and assaying.
Good precision may still be achieved even if a systematic error is present. For
example, the primary laboratory will produce repeatable (precise) results when
assaying a standard sample, even though the assays do not match the standard
value.
Laboratory precision can be determined by analyzing both check assay and check
sample data.
Accuracy in assaying is a measure of the ability to determine the true grade of the primary
sample. Precision in assaying refers to the ability to consistently repeat the assay results for
a sample within required limits. Accuracy and precision are the means by which the quality of
a laboratory is judged. The following diagram illustrates the concepts:
7-21
Reference for Mineral Reserves and Resources
Good precision
Good accuracy
Good precision
Poor accuracy
Poor precision
Good accuracy
Poor precision
Poor accuracy
The variance of the results is a direct consequence of the many errors that can be introduced
during the sampling and assaying stages.
In summary, the QC data can be used to evaluate:
7.4.3.
SRMs
Blanks
Check sampling.
PRESENTATION OF QC DATA
The QC data should be assessed and presented in two stages. The first, termed Immediate
Assessment and Action, takes the data as soon as they are available, graphs and assesses
the results, and formulates the action required to correct any observed irregularities. The
second, Full Documentation, compiles all analyses and actions taken into a single report
that becomes part of the backup for the Statement of Mineral Reserves and Resources.
7-22
Reference for Mineral Reserves and Resources
7.4.3.1.
Upon receipt of the QC data, the geologist should enter the data into the site database and
proceed with graphing, interpretation and follow-up action. A summary of the assessment
can be recorded on the recommended form (Data Assessment Summary Sheet), an
example of which is shown below, if no operation or site-specific procedures or forms are in
place.
All of the QC data can be summarized using this form, including short term performance of an
SRM, long term performance of an SRM showing laboratory drift, grind checks and check
assaying. This one-page summary is a simple and useful record of the action taken, and may
be circulated internally.
7.4.3.2.
Full Documentation
A full QC assessment should be presented as part of the report serving as a backup for the
Statement of Mineral Reserves and Resources. The assessment report should include:
GRAPH
ORIGINALS
SAMPLE
DETAILS:
INTERPRETATION:
SUMMARY STATISTICS
No Samples:
Mean:
Std Dev:
Max:
Min:
ACTION TAKEN:
7-23
Reference for Mineral Reserves and Resources
7.4.4.
GRAPHS
Many types of graphing techniques can be used to plot QC data. Some of these are quite
complex and beyond the scope of this reference volume. The following three types of simple
graphs have been found to be adequate for most operational and project requirements.
7.4.4.1.
Line Graphs
A simple line graph should be used for plotting data for SRMs, blanks and grind checks.
Line graphs for these data should be set up in the following manner:
For SRMs
A central line is plotted as the recommended value for the assays, this being the
mean value of the SRM.
Warning lines and action lines are plotted either side of the recommended value.
The warning lines are equal to two standard deviations of replicate assays performed
during the certification process, while the action lines are equal to three standard
deviations.
When using commercial SRMs, the mean and standard deviation of an SRM should
be obtained from the supplier of the SRM.
g/t Au
Action
Required
Action Line
Warning Line
Recommended Value
Warning Line
Action Line
3
Action
Required
7-24
Reference for Mineral Reserves and Resources
For blanks
Action
Required
0.2g/t
Action Line
0.1g/t
Warning Line
Sample Number/Time
The recommended value is set at 90% of the weight of each sample passing through
screen (P90).
Action is required if all of the samples do not equal or exceed this recommended
value.
%
Passing
75m
P100
P90
P80
Recommended Value
Action
Required
Sample Number/Time
7-25
Reference for Mineral Reserves and Resources
7.4.4.2.
Scatter Plots
A scatter plot graph should be used for plotting all assay pairs, such as check assays and
check samples. These graphs are very useful for showing assay bias between laboratories.
Scatter plots should not be used for monitoring standards.
Scatter plots should be set up in the following manner:
Assay As (original assays) are plotted on the x-axis.
Assay Bs (check assays) are plotted on the y-axis.
A reference line is plotted for x = y, reflecting exact matches between the two assays.
Warning lines are plotted on either side of the reference line. The warning lines for
check assays should be set at 10%. The warning lines for check samples should be
set at 20%.
The warning lines become meaningless for assays more than 10 times the detection
limit of the assaying technique.
Assay B
g/t Au
Warning Line
(+10%) or (+20%)
Action may
be required
10x detection
Action may
be required
Assay A g/t Au
If the assay data cover a wide range, it is best to present scatter plots over several grade
intervals so that the resolution of the data in the lower grade ranges are readable on the plots.
For a normal data set (i.e. gold grades ranging from less than detection to 100 g/t), a typical
range breakdown might be:
0 to 1g/t
1 to 10g/t
10 to +100g/t
7-26
Reference for Mineral Reserves and Resources
7.4.4.3
Thompson-Howarth Graphs
An alternative method for presenting and assessing the differences between the individual
assays in a data set of assay pairs is the Thompson-Howarth graph. These graphs are very
useful for determining the precision of the paired assays and setting pass/fail criteria.
Thompson-Howarth graphs should be set up in the following manner:
The absolute values of the difference of the assay pairs are plotted on the y-axis.
The difference of the assay pair is always positive, (i.e. the absolute difference).
A warning line is plotted to show which assay pairs have an unacceptable error. The
warning line for check assays should be set at +10%. The warning line for check
samples should be set at +20%t.
The warning lines become meaningless when the mean of an assay pair is less than
10 times the detection limit of the assaying technique.
Absolute
Assay
Difference
A-B
Action may
be required
Warning Line
+10% or + 20%
10x detection
7-27
Reference for Mineral Reserves and Resources
7.4.4.4
In addition to line graphs, scatter plots and Thompson-Howarth graphs, there are several
other ways to check the precision of paired data. These include the Dot Plot method, the
Confidence Interval method, the ANOVA method, the t-Test, and the F-test method. Easy-touse computer software is available for these methods of checking paired data.
7.4.5.
DATA INTERPRETATION
After the assay data have been displayed in the appropriate graphs, the data must be
interpreted to determine what, if any, corrective course of action is required in order to
address sampling errors, laboratory bias or assay accuracy issues.
The QC data should be interpreted in the following order, particularly when attempting to track
down an apparent error in the system:
This order is very important. The failure of a laboratory to match mean SRM values within
acceptable limits is a direct indication of a potential problem in the analytical section of the
laboratory. Similarly, unacceptable assay results for blank samples strongly suggest possible
laboratory contamination. Also, a period of poor grinding performance may relate directly to
poor precision in check assay results.
It is important to remember that a systematic approach to addressing apparent problems in
sampling or in the laboratory is absolutely essential. Change only one procedure at a time in
order to avoid further skewing of results. As with mechanical repairs to equipment:
- Determine what is broken before starting to make repairs! Each stage of interpretation of QC data should conclude with a documented statement of
action taken. For example:
The conclusion may simply be Check results are satisfactory, no action required;
or
The sampling procedure will be revised after the results of testwork are received in
early September
7-28
Reference for Mineral Reserves and Resources
7.4.5.1.
As described in Section 7.4.4.1, the results of the SRM analyses are compared against the
recommended value (mean) of the SRM by plotting the data for each standard on a separate
line graph. Once plotted, the analysis must:
Single out the results outside the action lines. All results beyond the action line are
unacceptable.
- This is a critical stage, where the primary assays are accepted or rejected
based on results of the SRMs
Promptly bring to the laboratorys attention any results falling between a warning line
and an action line as a potential problem.
Examine the long-term history of the SRM assay data, and check for assay bias over
time.
The following line graph example shows assay results obtained for an SRM having a value of
2.00g/t Au over a period of 1.5 months. The data can be divided into groups that illustrate
trends over time. The significance of these groups or trends is discussed below:
STANDARD No ... at ... LAB
GOLD - mean value 2.00g/t
- standard deviation 0.10g/t
3.00
2.80
2.60
2.40
Action Line
Warning Line
2.20
Recommended Value
2.00
1.80
Warning Line
Action Line
1.60
1.40
1.20
mean = 2.00g/t
mean = 2.33g/t
mean = 2.22g/t
mean = 2.00g/t
mean = 2.09g/t
1.00
1-Jun
11-Jun
21-Jun
1-Jul
11-Jul
DATE
The data for the above graph were compiled in an Excel spreadsheet that appears in
Appendix 7-1.
7-29
Reference for Mineral Reserves and Resources
Action Required: The geologist will have confidence in the primary assays produced
during this period. No action is required.
Group 2 (11th June to 20th June)
These data show a trend of increasing value, with four assays above the warning line
and one assay above the action line.
The laboratory should be informed immediately of the results and asked to check on
procedures in place before overall results become unacceptable.
Action Required: The batch of primary samples that included the one standard above the
action line may need to be re-assayed, depending on the laboratorys findings.
Group 3 (21st June to 30th June)
These results display good precision but unacceptable accuracy, with seven assays
above the action line. This indicates a high bias on the part of the laboratory with
respect to the SRM analyses for this period, which likely translates to a high bias in
the primary sample assays also.
The laboratory must be informed immediately and steps taken to determine and
correct the source of the bias.
Action Required: The primary sample lots that include the seven SRMs above the action
line must be re-assayed. Depending on the results of the laboratorys investigation, the
primary sample lots that include the three SRMs with results falling between the warning
line and the action line also may require re-assaying.
Group 4 (1st July to 10th July)
The data indicate that the laboratory appears to have corrected the assay bias
problem, with only one assay is above the warning line. The results are now accurate
(mean=2.00g/t), but precision is worse.
Action Required: The geologist should continue to closely monitor the laboratory.
Group 5 (11th July to 20th July)
All assays except one show good precision and good accuracy. However, one assay
is beyond the action line and warrants investigation. Because the result for this SRM
7-30
is well above the action line, laboratory bias may not be the cause.
reasons include:
Alternative
Another SRM could have been incorrectly labeled and submitted to the laboratory.
Sample swapping may have occurred on site or at the laboratory.
Action Required: The batch of primary samples that included the single SRM above the
action line may need to be re-assayed, if no other evidence for a labeling or swapping
error can be found.
To track laboratory performance over time, a moving average line can be added to the line
graph as shown below.
STANDARD No ... at ... LAB
GOLD - mean value 2.00g/t
- standard deviation 0.10g/t
3.00
2.80
Au g/t
2.60
9 point moving
average
2.40
2.20
2.00
1.80
1.60
1.40
1.20
1.00
1-Jun
11-Jun
21-Jun
1-Jul
11-Jul
DATE
The deviation of the moving average line from the mean or suggested value line shown in the
graph is sometimes referred to as laboratory drift.
7.4.5.2.
As with SRM samples, the results of blank sample assays are tracked by plotting the data on
a line graph. Once plotted, the analysis must:
Single out the results outside the action lines. All results beyond the action line are
unacceptable.
- This is also a critical stage, where the primary assays are accepted or
rejected based on results of the standards 7-31
Reference for Mineral Reserves and Resources
Promptly bring to the laboratorys attention any results falling between a warning line
and an action line as a potential problem.
The following line graph example shows assay results obtained from the routine assaying of
blanks over a one-month period. The data can be divided into groups that illustrate trends
over time. Note that the scale on the y-axis is logarithmic in order to provide better visual
resolution of the data in the lowest grade, where most blank assay data will fall:
BLANK No ... at ... LAB
10.00
Au g/t
(log
scale)
2.34
1.00
0.83
0.36
0.01
31-May
10-Jun
20-Jun
30-Jun
DATE
All blanks except one show good precision and good accuracy. One blank is
significantly high (2.34g/t Au) and warrants investigation. Because all other blanks
assayed during this period returned acceptable assays, the problem may be due
to:
Action Required: Overall laboratory performance for the period appears to be good.
However, if no evidence of sample swapping or mislabeling can be found, pulps from
the lot of primary samples that included the high assay blank (2.34g/t Au) should be
re-assayed, including the pulp for the single anomalous blank. If the results are
similar, then new assay pulps should be prepared for the entire lot using coarse
rejects (residues) and these pulps assayed.
7-32
Reference for Mineral Reserves and Resources
One blank is above the warning line and two blanks are above the action line.
Except for these three assays, all other blank results are at or below detection
limit, indicating:
Because the other blank data are all at or below detection limit, the cause of the
problem may be a particular laboratory technician who is not properly trained or
who is intentionally cutting corners. The laboratory should be informed of the
results immediately and asked to investigate.
Action Required: The pulps for the primary sample lots that which include the two
blanks above the action line will need to be re-assayed, along with the pulps from the
anomalous blanks. If the results are similar, then new assay pulps should be
prepared for the entire lot using coarse rejects (residues) and these pulps assayed. If
the laboratory determines that the source of the problem is contamination due to
laboratory technician error, then other sample lots prepared by the same operator may
need to be re-assayed.
Group 3 (21st June to 30th June)
All blanks are above the warning line and four blanks are above the action line,
indicating good laboratory precision but unacceptable accuracy. This high bias
may indicate:
The laboratory may have a chronic contamination problem, although the good
precision displayed by the data suggests that the problem is not likely to be in
the sample preparation area.
Check the standards that were submitted during the same period for evidence of a
similar increase in grade.
Action Required: Regardless of the cause of the problem, the laboratory should be
informed of the results immediately, and all of the pulps for the primary sample lots
(including the pulps for the blanks) must be re-assayed. If the results are similar, then
7-33
Reference for Mineral Reserves and Resources
new assay pulps should be prepared for the entire lot using coarse rejects (residues)
and these pulps assayed.
7.4.5.3.
Poor grinding usually results in a non-homogeneous ground product. With pulps, this shows
up as poor repeatability of assays on pulp duplicates.
As with the data on SRMs and blank samples, the results of grind tests are tracked by
plotting the data on a line graph. Separate graphs should be produced for grind checks on
pulps and checks of coarse crush material. Once plotted, the analysis and action steps must
include:
Compilation of the results at less than the recommended P90 value for the screen size
used for the grind checks. The results are unacceptable if they fall below P90. In
order for no action to be necessary, the grind for all samples must be better than P90
on the line graph. Note that to achieve the P90 designation, 90% of the pulp must
pass through the screen. The term nominal should never be accepted as defining
the pass percentage, as it means in name only.
Diligent action - even an occasional poor grind result cannot be ignored. Follow up
whenever a grind test fails to pass the P90 limit and inform the laboratory immediately
of the results.
- One grind check per 100 samples means each laboratory operator is only
being checked about TWICE per shift
With the laboratorys assistance, determine the possible reasons for the poor grind
results.
An abundance of siliceous material in the sample, which is not unusual for ore-grade
material, particularly in certain types of gold deposits. Care should be taken to ensure
that both ore and waste material are represented in the grind checks, as the grinding
index of the two material types can vary significantly.
Overloading of the pulverizer(s). Note that increasing the grind time cannot remedy
overloading. Either a smaller sample must be submitted or, if this is not possible, the
laboratory should grind each sample in two passes and then correctly recombine the
pulp product.
Solutions to poor grinding vary depending on the reason for the problem:
If siliceous material is believed to be the cause, the laboratory can either increase the
grind time on all samples, or the Barrick geologist can flag the samples thought to
7-34
Reference for Mineral Reserves and Resources
contain high levels of siliceous material so that only these samples are given a longer
grind time.
If a satisfactory explanation for the poor grinds cannot be found, the primary samples
associated with these grind checks must be reground and re-assayed. Prior to
regrinding, the assay pulp split should be remixed with the pulp reject and a new
assay pulp split produced.
Should the grind checks be consistently good but pulp duplicates continue to demonstrate
poor repeatability (i.e. the pulp is not homogeneous), then it may be that the screen size used
for the grind checks is too large.
Finally, it helps to maintain a line graph that displays the grind test results over time. These
data are useful for analyzing trends in grinding check results, which can sometimes be
correlated to QC issues revealed by other data.
7.4.5.4.
As described in Section 7.3.4, check assays are performed by a secondary laboratory on the
same pulps used for assaying the primary samples at the primary laboratory. The results are
compared against the assays generated by the primary laboratory. Interpretation of check
assay results should be completed as soon as the results have been received from the
secondary laboratory.
Both a scatter plot and a Thompson-Howarth graph should be used to analyze check assay
data, since:
The scatter plot will reveal any assay bias between the two laboratories.
However, neither a scatter plot nor a Thompson-Howarth graph can determine which
laboratory is more accurate. Accuracy can only be determined by assaying and analyzing
standard samples.
The examples on the following pages illustrate some common assaying errors that check
assaying can help identify:
7-35
Reference for Mineral Reserves and Resources
Example 1
SCATTER PLOT
THOMPSON-HOWARTH GRAPH
25.00
2.50
+10%
-10%
20.00
15.00
1.50
10.00
1.00
5.00
0.50
0.00
0.00
0.00
Warning Line
+/-10%
2.00
5.00
10.00
15.00
ASSAY A Au g/t
20.00
25.00
0.00
5.00
10.00
15.00
20.00
25.00
MEAN Au g/t
Both graphs indicate acceptable results. The scatter plot shows no laboratory bias,
and the Thompson-Howarth graph shows that the precision is acceptable, except for
two duplicates which fall above the +10% warning line.
Action Required: Investigate the two samples that fall above the +10% warning line by
looking for common characteristics such as close proximity in the deposit, similar geological
features (i.e., sulphide content, silicification, et cetera). Also, the grind may be poorer on
these two samples because of strong silicification or sample preparation error.
Example 2
SCATTER PLOT
THOMPSON-HOWARTH GRAPH
25.00
4.50
+10%
4.00
-10%
20.00
3.50
3.00
15.00
2.50
Warning Line
+/-10%
2.00
10.00
1.50
1.00
5.00
0.50
0.00
0.00
0.00
5.00
10.00
15.00
ASSAY A Au g/t
20.00
25.00
0.00
5.00
10.00
15.00
MEAN Au g/t
20.00
25.00
The scatter plot shows no evidence of bias (the data are scattered evenly about the
reference line).
The Thompson-Howarth graph indicates that the relative precision of the laboratories
is poor in all grade ranges.
Action Required: The poor precision in all grade ranges is indicative of pulps that are not
homogeneous. To determine if this is the case, examine the two laboratories in-house
duplicate checks and review the grind checks. If the grind checks appear to be
satisfactory, it may indicate that the screen used to check the grind is too coarse, and the
primary laboratory should change to a finer screen size. If the problem is not identified
7-36
Reference for Mineral Reserves and Resources
and corrected, all primary assays run by the laboratory during in this period likely will
have poor precision.
Example 3
SCATTER PLOT
THOMPSON-HOWARTH GRAPH
25.00
4.50
+10%
-10%
20.00
4.00
3.50
3.00
15.00
Warning Line
+/-10%
2.50
2.00
10.00
1.50
1.00
5.00
0.50
0.00
0.00
0.00
5.00
10.00
15.00
ASSAY A Au g/t
20.00
25.00
0.00
5.00
10.00
15.00
20.00
25.00
MEAN Au g/t
The scatter plot shows that the original assays (Assay A) have a low assay bias.
The Thompson-Howarth graph indicates that the relative precision between the
laboratories is generally good except in the 7g/t to 14g/t grade range, where four pairs
are above the warning line.
Action Required: The borderline relative precision in the 7g/t to 14g/t range may be due to
an incorrect AA calibration standard in the primary laboratory. The results of the standard
sample submittals for the lots that contain the original assays in the erratic pairs should be
examined to see if the same low bias exists in those data. If a faulty standard is found, all
primary samples that fall in the grade range affected by the calibration standard should be
re-assayed by the primary laboratory.
Example 4
SCATTER PLOT
THOMPSON-HOWARTH GRAPH
80.00
+10%
15.00
-10%
60.00
10.00
Warning Line
+/-10%
40.00
5.00
20.00
0.00
0.00
0.00
20.00
40.00
ASSAY A Au g/t
60.00
80.00
0.00
10.00
20.00
30.00
40.00
50.00
MEAN Au g/t
60.00
70.00
80.00
7-37
Reference for Mineral Reserves and Resources
The Thompson-Howarth graph shows that the relative precision between the
laboratories is good in the 0 20g/t grade range but is poor for grades above 20g/t.
Action Required: Look for a procedural problem in the laboratories. If the secondary
laboratory is using a gravimetric finish (which is preferable in the higher grade ranges) and
the primary laboratory is not, the procedural problem may be in the primary laboratory. If one
or both of the laboratories is using an AA finish, an inexperienced operator may be
introducing a number of errors, including dilution (solutions containing gold over 20g/t are
outside the calibration range of the AA machine and would have to be diluted before
analysis). If the problem is not corrected, all of the primary assays above 20g/t Au performed
during this period are likely to have poor precision, and all must be re-assayed by the primary
laboratory.
Example 5
SCATTER PLOT
THOMPSON-HOWARTH GRAPH
25.00
8.00
+10%
-10%
20.00
7.00
6.00
5.00
15.00
4.00
10.00
3.00
Warning Line
+/-10%
2.00
5.00
1.00
0.00
0.00
0.00
5.00
10.00
15.00
ASSAY A Au g/t
20.00
25.00
0.00
5.00
10.00
15.00
MEAN Au g/t
20.00
Both graphs indicate that the precision is good except for three duplicate pairs.
25.00
Action Required: Upon investigation it was found that two of the errors were introduced
by sample swapping, where two samples were interchanged (they have a similar assay
difference on the Thompson-Howarth graph), and one sample was selected from outside
the batch and mislabeled. These issues must be discussed with both laboratories
immediately, as such errors are commonly caused by:
With the sample swap corrected, the precision for this set of data becomes acceptable.
7-38
Reference for Mineral Reserves and Resources
7.4.5.5.
Check sampling consists of collecting a duplicate sample from material remaining from the
original sample that has not passed through the sample preparation process (see Section
7.3.5). Check samples are submitted to the primary laboratory and pass through the
complete sample preparation and assaying procedure. The results are compared against the
primary assays, also prepared and assayed at the primary laboratory.
Interpretation of check sample results should be completed as soon as they have been
received from the secondary laboratory.
The analysis procedure for check samples is the same one used for check assays. Both a
scatter plot and a Thompson-Howarth graph should be used to analyze check sample data,
since:
The scatter plot will reveal any assay bias between the two laboratories.
However, neither a scatter plot nor a Thompson-Howarth graph can determine which
laboratory is more accurate. Accuracy can only be determined by assaying and analyzing
standard samples.
The following examples illustrate some common errors that check sample data can identify:
Example 1
THOMPSON-HOWARTH GRAPH
SCATTER PLOT
CHECK SAMPLES at LAB
ALL GRADE RANGES
+20%
5.00
25.00
Warning Line
+/-20%
4.50
4.00
20.00
-20%
15.00
3.50
3.00
2.50
10.00
2.00
1.50
5.00
1.00
0.50
0.00
0.00
0.00
5.00
10.00
15.00
20.00
ASSAY A Au g/t
25.00
0.00
5.00
10.00
15.00
20.00
25.00
MEAN Au g/t
For this data set, both the scatter plot and the Thompson-Howarth graph show good
precision, except for one pair that falls above the +20% warning line.
Provided that all sampling and assaying procedures were strictly adhered to by the
primary laboratory, the possible reasons for the sample pair beyond the warning line
include:
7-39
Reference for Mineral Reserves and Resources
The sampling protocol is incorrect for the material represented by that sample for
reasons that may include the samples location in the deposit, possible high
sulphide content and/or the presence of silicification.
Action Required: The location and character of the sample falling above the warning line
should be checked. At the same time, a second check sample split should be submitted to
the primary laboratory to check for possible procedural errors. If the results of these
investigations are inconclusive, a larger check sample split should be submitted for screen fire
assaying to check for coarse gold (see Section 6.5.2.2 of this reference volume).
- The initial sampling and assaying protocols may not fit all mineralization in the
deposit Example 2
THOMPSON-HOWARTH GRAPH
SCATTER PLOT
CHECK SAMPLES at LAB
ALL GRADE RANGES
+20%
25.00
8.00
7.00
20.00
6.00
-20%
5.00
15.00
Warning Line
+/-20%
4.00
10.00
3.00
2.00
5.00
1.00
0.00
0.00
0.00
5.00
10.00
15.00
ASSAY A Au g/t
20.00
25.00
0.00
5.00
10.00
15.00
20.00
25.00
MEAN Au g/t
The scatter plot shows no evidence for significant sample bias in the data set.
However, both the scatter plot and the Thompson-Howarth graph of these data (which
are all from RC drill hole samples) indicate poor sampling precision for all grade
ranges. This is indicative of an incorrect sampling protocol.
Action Required: This problem is significant and must be quickly addressed, as all
primary assays are likely to demonstrate poor precision using the original protocol and
procedures. First examine the sample collection and handling practices from the drill rig
through to the sample preparation area at the laboratory to determine if established
procedures are being followed. If procedures are acceptable, then the sampling protocol
must be closely reviewed and changes made where appropriate:
Example 3A
This example represents an actual case from a Barrick project, where all data were generated
from diamond drill core samples. The data for these graphs were compiled in an Excel
spreadsheet and appear in Appendix 7-2.
THOMPSON-HOWARTH GRAPH
SCATTER PLOT
CHECK SAMPLES at LAB
ALL GRADE RANGES
+20%
100.00
70.00
60.00
-20%
80.00
50.00
60.00
40.00
30.00
40.00
Warning Line
+/-20%
20.00
20.00
10.00
0.00
0.00
+20%
0.00
20.00
40.00
60.00
80.00
ASSAY A Au g/t
100.00
120.00
0.00
20.00
40.00
60.00
MEAN Au g/t
80.00
100.00
The scatter plot for these data (all of which are from diamond core samples) shows
that there is a high assay bias in the original assays (Assay A).
Both the scatter plot and the Thompson-Howarth graph indicate a rapid decline in
precision in the high-grade range.
The possible explanations for the bias and poor precision include:
Laboratory contamination during either the primary sample or the check sample
assaying.
Preliminary Action Required: Note that the scales on both the plot and the graph are
insufficient for examining the behavior of the data in the lower grade ranges, where the
data diverge from the reference and warning lines. Before embarking on detailed
investigations to address the problem, the following steps were taken to further analyze
the problem:
The scatter plot and the Thompson-Howarth graph were regenerated for the grade
range from 0.10 g/t to 20.0g/t, as shown in Example 3B on the following page.
The assay results for the standards and blanks and the results of the grind checks
were investigated.
7-41
Example 3B
THOMPSON-HOWARTH GRAPH
SCATTER PLOT
20.00
+20%
-20%
10.00
15.00
8.00
10.00
6.00
Warning Line
+/-20%
4.00
5.00
2.00
0.00
0.00
0.00
5.00
10.00
15.00
ASSAY A Au g/t
20.00
25.00
0.00
5.00
10.00
MEAN Au g/t
15.00
20.00
The review of the assay results for the standards and blanks and the results of the
grind checks failed to reveal any problems, indicating that it did not reside in the
primary laboratory. The reasoning behind this conclusion is as follows:
If a laboratory calibration problem was the cause for the poor precision at higher
grades, the results of the high grade standard also would have been skewed.
If the grind checks corresponding to the higher grade samples were unsatisfactory,
then poor homogeneity in these pulps could have explained the poor precision.
The blank sample results were acceptable, indicating that sample contamination
was not an issue.
Final Action Required: Because preliminary analysis indicated that the problem did not
reside at the primary laboratory, the initial sampling procedures from the drill rig to the
point where the samples are dispatched to the laboratory were reviewed. This
investigation revealed that poor sampling practices at the core shed had introduced a
sampling bias. Specifically:
The primary samples (Assay A) were taken from the half core with the best looking
mineralization.
7-42
Reference for Mineral Reserves and Resources
These issues were resolved by instituting the correct sampling procedure for core and
improving supervision.
7.5. REFERENCES
MRDI, 1996. Assay Quality Assurance-Quality Control Program for Drilling Projects at the
Pre-Feasibility to Feasibility Report Level. In: Francois-Bongarcon, D.M., Long, S.D., Parker,
H.M., 1997. Bankable Ore Reserves and Feasibility Studies. Mineral Resources
Development, Inc. San Mateo, California, USA. AIC Conference, Singapore, November 1997.
Stanley, C.R., 1999. Treatment of geochemical data: some pitfalls in graphical analysis, in
Quality Control in mineral Exploration, short course, 19th IGES, Vancouver, British Columbia
(Assoc. of Expl. Geochemists).
7-43
Reference for Mineral Reserves and Resources
APPENDICES
APPENDIX 7-1
EXAMPLE OF ASSAY DATA FOR STANDARD
LAB RESULTS
DATE
ASSAY
g/t Au
1-Jun
1.93
2-Jun
1.89
3-Jun
2.12
4-Jun
1.98
5-Jun
2.04
6-Jun
2.10
7-Jun
1.95
8-Jun
2.01
9-Jun
1.96
10-Jun
2.00
11-Jun
2.09
12-Jun
2.17
13-Jun
2.13
14-Jun
2.19
15-Jun
2.15
16-Jun
2.23
17-Jun
2.29
18-Jun
2.26
19-Jun
2.27
20-Jun
2.38
21-Jun
2.28
22-Jun
2.32
23-Jun
2.41
24-Jun
2.34
25-Jun
2.28
26-Jun
2.38
27-Jun
2.42
28-Jun
2.35
29-Jun
2.22
30-Jun
2.33
1-Jul
2.12
2-Jul
2.23
3-Jul
1.93
4-Jul
2.15
5-Jul
1.83
6-Jul
2.04
7-Jul
1.86
8-Jul
2.10
9-Jul
1.80
10-Jul
1.92
11-Jul
2.01
12-Jul
1.98
13-Jul
2.04
14-Jul
1.93
15-Jul
2.11
16-Jul
2.02
17-Jul
2.01
18-Jul
2.88
19-Jul
1.99
20-Jul
1.93
STDEV
VALUE (g/t)
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
"WARNING"
"ACTION"
2.00+/-2STDEV
2.00+/-3STDEV
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
2.20
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
1.80
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
2.30
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1
Reference for Mineral Reserves and Resources
APPENDIX 7-2
EXAMPLE OF ASSAY DATA FOR CHECK SAMPLING
Warning Lines
SAMPLE ASSAY A ASSAY B MEAN Abs.Difference
No
(Original) (Check) (A+B)/2
A-B
20% of mean A=B +20% -20%
Au g/t
Au g/t
Au g/t
Au g/t
Au g/t
1
0.25
0.23
0.24
0.02
0.05 0.1 0.12 0.08
2
0.58
0.62
0.60
0.04
0.12 100
120
80
3
0.96
1.05
1.01
0.09
0.20
4
1.23
1.02
1.13
0.21
0.23
5
1.56
1.51
1.54
0.05
0.31
6
1.81
1.88
1.85
0.07
0.37
7
2.01
2.15
2.08
0.14
0.42
8
2.32
2.21
2.27
0.11
0.45
9
2.65
2.85
2.75
0.20
0.55
10
3.25
3.02
3.14
0.23
0.63
11
3.84
3.83
3.84
0.01
0.77
12
4.25
3.95
4.10
0.30
0.82
13
6.56
7.1
6.83
0.54
1.37
14
8.15
8.21
8.18
0.06
1.64
15
10.26
9.44
9.85
0.82
1.97
16
12.76
11.1
11.93
1.66
2.39
17
14.87
10.33
12.60
4.54
2.52
18
16.18
12.83
14.51
3.35
2.90
19
20.65
13.12
16.89
7.53
3.38
20
23.36
13.62
18.49
9.74
3.70
21
29.61
21.65
25.63
7.96
5.13
22
35.63
23.11
29.37
12.52
5.87
23
37.28
28.3
32.79
8.98
6.56
24
41.22
36.41
38.82
4.81
7.76
25
52.31
32.33
42.32
19.98
8.46
26
60.33
31.76
46.05
28.57
9.21
27
74.29
48.69
61.49
25.60
12.30
28
86.29
55.24
70.77
31.05
14.15
29
95.87
66.32
81.10
29.55
16.22
30
112.32
69.36
90.84
42.96
18.17
1
Reference for Mineral Reserves and Resources
Section 8
DENSITY DETERMINATIONS
8.1.1.
8.1.2.
8.1.3.
APPENDICES
Appendix 8-1
Appendix 8-2
Appendix 8-3
Appendix 8-4
8.1. INTRODUCTION
The preparation of a mineral resource estimate requires that the tonnage, grade and
contained metal in the mineral deposit be estimated as accurately as possible. When
acquiring data for the estimation of resources, much emphasis is attached to the
collection, processing and validation of numerous individual assay samples from drill holes
or rock faces to determine the grade of the deposit. As a result, it is not unusual to either
neglect altogether or to only partially sample the deposit for determination of the densities
of the material sampled. The sample densities are used to convert the measured volume
of rock (ore or waste) in the deposit into a tonnage. If adequate density data are not
collected, the deposit tonnage and, consequently, the contained metal in the deposit can
easily be over-estimated or under-estimated.
8.1.1. TERMINOLOGY
In the mining industry, it is common for the terms density and specific gravity to be used
interchangeably. However, by definition there is a distinction between these terms.
The Specific Gravity (SG) of a substance is defined as the ratio of the mass of a
quantity of a substance to the mass of an equal volume of a standard substance
(normally water at 4oC). Being a ratio, the SG is a number with no unit value. If a
mineral or rock has an SG of 2, this indicates that it has twice the mass of the
same volume of water at 4oC.
The Density (D) of a substance is defined as its mass per unit volume (density =
mass/volume) and therefore is expressed in grams per cubic centimetre when
using the metric system of measurement. In the metric system, the density of a
substance is numerically the same as its SG because the mass in grams of one
cubic centimetre of the substance is numerically equal to its ratio to an equal
volume of water at 4oC, since the same volume of one cubic centimetre of water at
4oC weighs one gram.
Although both SG and D data are commonly used in resource estimation, the preferred
methods for estimating tonnage of in situ and broken material are the following:
The apparent Relative Density (RD) of the rock accounts for the porosity, voids
and other open spaces such as fractures in the in-situ rock volume.
The Bulk Density (BD) is determined when estimating the tonnage of broken rock,
whether contained in a stope underground or in a surface stockpile. BD is defined
as the mass of crushed or broken material that occupies a specific volume.
Resource/reserve estimates are always done on a dry (moisture free) tonnage basis, so
it is essential that all samples are completely dried prior to initial weighing during density
determinations, or alternatively, that moisture content is determined and a correction made
if samples are not dried before initial weighing.
generally increases with depth below the surface as a result of a decrease in weathering
and, also, a decrease in open spaces with the increasing weight of overlying rock. In the
weathering profile, lower near-surface densities result from an increase in open space or
an increase in volume primarily due to the breakdown of certain rock minerals to clays.
Variations in mineralization content, also, can substantially affect density. For example, in
massive and semi-massive sulphide deposits, significant density variations can occur
depending on the type and percentage of sulphides present.
8-2
Reference for Mineral Reserves and Resources
A stool or table with a hole cut in it to allow the balance to rest on the table and be
placed over the hole and to allow access to the weighing hook below the balance.
A wire cage suitable to hold the rock or core samples being measured. A
suspension cable should be attached to the cage to allow it to be suspended from
the weighing hook below the balance.
A bucket of water.
W1 / (W1 W2)
W1 / (W2 W3)
8-4
Reference for Mineral Reserves and Resources
W1 / (W1 W2)
Because the weight of the wax on the sample is insignificant compared to the rest of the
sample, it is usually ignored.
8-5
Reference for Mineral Reserves and Resources
8.2.2.1
Drill core from triple-tube drilling is best logged and marked up for sampling after each drill
run before the core is removed from the innermost (split) tube. This ensures that no core
is lost or disturbed during transfer to a core box or tray prior to logging. To avoid rig standby time, the drill contractor will need to have 2 or 3 sets of split inner tubes in order to
allow time for logging and sampling while the driller continues to advance the hole.
After the removal of each run of core from the hole, the triple-tube splits should be
carefully removed from the inner tube. The core-filled split inner tubes should be placed on
8-6
Reference for Mineral Reserves and Resources
a rack, the top splits should be removed carefully, and the core should be left undisturbed
in the bottom splits for logging. The following procedure should then be followed:
1. Carefully fit together any broken sections of core.
2. Mark up and accurately measure the lengths of core to be sampled for assay.
Sampling should take into account and respect the natural geological breaks
(lithology contacts, veins or stockwork zones, for example). It is very important
that only actual lengths of core in each sampled interval are measured for the
volume calculation. It is also important to note that the cumulative length of the
core recovered in the split inner tube may not equal the length drilled according to
the drillers depth record. Core loss or core lengths that exceed the length of the
drilled interval can skew the determination of sample lengths if care is not taken to
account for these. For a description of how the cumulative length of core
recovered can exceed the length actually drilled, see Section 5, GEOTECHNICAL
AND GEOLOGICAL DATA COLLECTION, of this reference volume. Core loss
and/or overrun should be recorded separately by the geologist (see example form
in Appendix 8-1).
3. Photograph the core (see Section 4.16.7).
4. Log the core for geology.
5. Carefully clean excess drilling mud from the core and measure the core diameter
in several places with vernier calipers to obtain an average core diameter for the
run. Note where core is broken if this is likely to affect the core length
measurement. If the core is worn to less than the expected normal diameter by
washing or bit wander, then an estimate should be made of the extent of wear,
such as 4cm length of sampled interval 30% worn. This will allow an adjustment
to be made when completing the core volume calculation.
6. Whole core from each sample interval should be transferred to a large numbered
sample bag, taking care not to lose any of the sample.
7. Dispatch the samples to the laboratory for determination of RD and subsequent
assay.
8.2.2.2
Laboratory Instruction
Written instructions should be sent to the laboratory with the dispatched sample lot. The
instructions should read as follows:
1. Weigh each whole core sample (the entire contents of the sample sack before
drying and record as WW.
2. Oven-dry each whole core sample for 12 hours at 105oC.
3. Weigh each dried whole core sample and record as WD.
4. Prepare each sample for gold or other metal analysis.
The wet sample weight WW is not used for the density calculation. This measurement by
the laboratory is for the calculation of the moisture content of the rock, where:
8-7
Reference for Mineral Reserves and Resources
8.2.2.3
Density Calculation
Mass / Volume
=
Where
WD / r2 L
WD = Dry weight of sample
=
3.1416
r =
L =
The density data should be entered into a spreadsheet as shown in Appendix 8-2. An
example of a page from a Laboratory Analytical Report for density samples is shown in
Appendix 8-3.
Analysis of the density data from the diamond core holes will enable:
Density values to be assigned to the various rock types in the deposit both in the
weathered and non-weathered zones.
Separation of ore and waste densities within weathered and non-weathered zones.
In order to analyze variations in density across a deposit, all of the data for each drill hole
should be plotted on cross sections. These data include:
Sample intervals.
Weathering profile contacts, including those between the oxide and transition
zones, and the transition and sulphide zones.
In Australia and some other countries, these contacts are referred to as the Base of
Complete Oxidation (BOCO) and Top of Fresh Rock (TOFR). An example of a cross
8-8
Reference for Mineral Reserves and Resources
section of this type for the Salmon deposit at Barricks Plutonic operation in Australia is
included in Appendix 8-4.
From analysis of the data, it can be determined if uniform density values can be assigned
to entire domains based on zone of weathering (oxide, transitional, or sulphide), ore types,
lithologies, alteration types, or other geologic features, or if a more complex approach to
density determination is warranted.
8.3.2.
8.3.2.1
Once RD values are assigned to the appropriate zone of weathering (oxide, transitional, or
sulphide), ore types, lithologies, or alteration types, the interpreted outlines on the cross
sections that represent these geologic domains can be correlated or linked by wire
framing or other three-dimensional modeling techniques. The resulting three-dimensional
domains can then be used to cut the resource block model and back-code the blocks so
that an RD value can be assigned to each block in the model (see Section 9).
For example, in the Salmon deposit, it is possible to separate the densities for the various
rock types based on the geological logging (i.e., Transported Alluvium (AL), Pisolitic
Laterite (PI), Mafic and Ultramafic derived Bedrock Clays (CB/MU and CB/UM),
Sedimentary derived Bedrock Clays (CB/SU) and primary unweathered rock types
including Mafics (MU), Basalt (BV), Ultramafics (TC/TCU) and Felsics (FV). By selecting
all of the samples in these units separately, the weighted average (by sample volume) of
the densities in each rock type can be calculated. A further breakdown is also possible into
mineralized and unmineralized (waste) parts of these rock units.
The RD data can be summarized and assigned for use in the resource estimate using the
following table:
Depth Range
Mineralized
Unmineralized
AL
PI
CB/MU
CB/UM
CB/SU
MU
BV
TC/TCU
FV
8.3.2.2
For deposits having significant local density variability (such as Barricks Eskay Creek
operation in British Columbia, Canada, or massive sulphide deposits such as Bousquet in
Quebec, Canada, or Kabanga in Tanzania), statistical modeling of density values should
be seriously considered, whereby a separate estimated density value is assigned to each
block in the resource model. This should be done using all available measured RD data.
However, if measured RD or other measured density data are judged to be sparse in light
8-9
Reference for Mineral Reserves and Resources
of the variability observed in the available data, an RD value should be obtained where
possible for those samples that contain significant amounts of sulphides that might
substantially skew in situ density modeling, as determined by the geologists.
Where drill core is not available for analysis, substitute density values can be generated
mathematically using a stoichiometric algorithm. This approach, which is used at Barricks
Eskay Creek operation, considers the assay value for a sample and the presence of
individual sulphide minerals in the sample (based on the drill hole logs) to calculate a
density value that is based on the stoichiometric ratios of the assayed metals in the
individual sulphide minerals. While this approach can reasonably provide substitute
density data for a new project until additional drilling can be completed that allows
sufficient sampling of in situ density, the results must be used with extreme caution for the
following reasons:
Assay and analytical data for all major sulphide constituents must be available
(especially iron and sulphur).
The density obtained using this approach is not an RD value, as there is no way to
take into account any voids or fractures that might have been present in the
sample.
8-10
Reference for Mineral Reserves and Resources
APPENDICES
APPENDIX 8-1
EXAMPLE
HOLE NO.: FDD017
PROJECT: XYZ
HQ3 TRIPLE TUBE DRILLING
DRILLING RECORD SHEET
DRILL
FROM
TO
DRILLED
RUN
CORE
RECOVERED(M)
20.68
21.64
0.96
0.97
21.64
23.00
1.36
1.36
23.00
24.00
1.00
0.97
10
24.00
25.00
1.00
0.99
11
25.00
26.00
1.00
1.00
12
26.00
27.07
1.07
1.07
13
27.07
28.00
0.93
0.95
14
28.00
29.00
1.00
0.99
15
29.00
30.50
1.50
1.55
16
30.50
32.00
1.50
1.52
17
32.00
33.50
1.50
1.51
18
33.50
35.00 (EOH)
1.50
1.41
TOTAL
35.00m
34.94m
1
Reference for Mineral Reserves and Resources
Sample
Number
D19891
D19892
D19893
D19894
D19895
D19896
D19897
D19898
D19899
D19900
D19901
D19902
D19903
D19904
D19905
D19906
D19907
D19908
D19909
From
0.00
1.13
2.00
3.00
4.00
5.00
6.50
7.00
8.00
9.00
10.00
11.00
12.00
13.00
14.00
15.00
16.00
17.00
18.001
To
1.13
2.00
3.00
4.00
5.00
6.50
7.00
8.00
9.00
10.00
11.00
12.00
13.00
14.00
15.00
16.00
17.00
18.00
19.00
L
1.13
0.87
1.00
1.00
1.00
1.50
0.50
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
PROJECT: XYZ
Measured Core
Length
in Sample
(cm)
67
90
100
96
103
92
53
94
100
104
96
1001
105
95
100
102
97
101
102
Core
Diametre
(cm)
6.2
6.2
6.1
6.1
6.1
6.1
6.0
6.1
6.1
6.1
6.0
6.0
6.0
6.0
5.8
6.0
6.0
6.0
6.0
LOCATION:
Core
Dry
Volume
Weigh
(cm3)
t of
Core
(gms)
2022.77
2717.16
2922.46
2805.56
3010.14
2688.66
1498.53
2747.11
2922.46
3039.36
2714.33
2827.43
2968.80
2686.06
2642.07
2883.98
2742.61
2855.70
2883.98
Density
gms/cm3
(Local Grid)
496ON 4960E
Comments
Solid core
8 cm broken core
APPENDIX 8-2
,
EXAMPLE
APPENDIX 8-3
Perth W.A.
Job Number:3PE3012
O/N :2006249
ANALYTICAL REPORT
SAMPLE
Dry
D20861
D20862
D20863
D20864
D20865
D20866
D20867
D20868
D20869
D20870
D20871
D20872
D20873
D20874
D20875
P20876
D20877
D20878
D20879
D20880
D20881
D20882
D20883
D20884
D20885
D20886
D20887
D20888
D20889
D20890
D20891
D20892
D20893
D20894
D20895
D20896
D20897
D20898
D20899
D20900
UNITS
DT.LIM
SCHEME
Au Dupl.
0.17
0.04
<0.01
0.01
0.91
0.15
0.31
0.21
0.06
1.41
1.73
1.29
0.65
0.43
0.37
0.17
0.03
0.03
0.03
0.02
0.01
<0.01
<0.01
0.01
0.21
0.01
<0.01
<0.01
<0.01
<0.01
<0.01
0.81
0.04
<0.01
<0.01
0.02
<0.01
0.01
<0.01
<0.01
PPM
0.01
FA1
Au Dp2
1.04
-0.39
0.19
-1.60
1.83
1.31
0.02
--
0.32
--
0.95
--
PPM
0.01
FA1
Au Avg
0.17
0.04
<0.01
0.01
0.97
0.15
0.35
0.20
0.06
1.51
1.78
1.30
0.65
0.43
0.37
0.17
0.03
0.03
0.0'3
0.02
0.02
<0.01
<0.01
0.01
0.27
0.01
<0.01
<0.01
<0.01
<0.01
<0.01
0.88
0.04
<0.01
<0.01
0.02
<0.01
0.01
<0.01
<0.01
PPM
0.01
FA1
AU Dp3
PPM
0.01
FA1
Wt Wet
6217
5893
5920
6443
6042
6671
6545
6443
6385
6005
5776
6217
5843
6271
6704
4669
6483
8501
7391
6732
6322
7243
6441
7193
8523
6375
6173
6551
6749
6526
7168
6619
7381
7099
6739
7764
8650
7481
6812
6720
g
0.01
WAT26
Wt
4948
4718
4662
5191
5031
5732
5609
5383
5305
5091
4892
5448
4999
5480
5735
4081
5749
7890
7125
6321
5982
6654
5941
6991
8234
5714
5551
5955
6144
5951
6465
5945
6870
6781
6444
7642
8615
7231
6492
6194
g
0.01
WAT26
1
Reference for Mineral Reserves and Resources
APPENDIX 8-4
1
Section 8 Density Determinations
Ver. 1 November, 2002
Section 9
RESOURCE MODELING
INTRODUCTION ......................................................................................................1
GEOLOGIC INFORMATION ....................................................................................2
ASSAY INFORMATION ...........................................................................................3
ASSAY STATISTICS ...............................................................................................4
TOPOGRAPHY ........................................................................................................5
GEOLOGIC MODEL ................................................................................................5
ASSAY COMPOSITES ............................................................................................7
VARIOGRAMS .........................................................................................................8
GRADE MODEL.......................................................................................................8
RESOURCE CLASSIFICATION ..............................................................................9
15.1 INTRODUCTION
The resource model serves as the interface between the various disciplines involved in
defining ore reserves. All other tasks within the ore reserve process either provide
information to the resource model or depend on information provided by the resource model.
For example: The drill logs, geologic mapping, and surface topography form the basis for the
geologic framework of the resource model. The sample assays, density determinations,
geotechnical, and metallurgical tests are used to develop models of the metal grades, metal
recoveries, resource tonnage, and rock quality. The resulting resource model provides the
information necessary to permit the mining engineer to develop optimum mining limits, mine
designs, and schedules. The metallurgist can then determine the amounts and characteristics
of the various types of plant feed and thereby develop a processing strategy and plant design.
A resource model consists of spatial estimates of various important characteristics of an ore
body. A simple resource model would typically contain estimates of the rock/alteration type,
rock density, and grades for the important metals.
Early in the exploration and development of a project, the resource model is necessarily fairly
simple since sample data is limited and geologic understanding is preliminary. As drilling
progresses and the geologic framework is better understood, the resource model becomes
more complex. Care should be taken, however, to avoid over-modeling. The detail and
complexity of the resource model should be dictated by the availability and reliability of the
underlying information. The amount of information required for proper definition of a given
mineral deposit will be dictated by 1) the nature and complexity of the geology of the deposit
and 2) the complexity of the optimum mining and processing scenario. A good rule to follow
with resource models is that the simpler solution is usually the better solution.
Earlier we said that a resource model consists of a collection of spatial estimates. It is
worthwhile to look at the two words that make up that term. Spatial expresses that the
resource model provides information that depends on location in three-dimensions (or in
some cases two-dimensions). Estimate expresses the idea that the values in a resource
model are not very precise. Much time and money can be spent in trying to resolve some
aspect of a resource model to very high levels of precision. These efforts should always be
tempered with the understanding that the combined errors involved in sample location,
preparation, and assaying.
Considering the inherent errors in the input measurements, it might seem surprising that a
resource model would ever be capable of providing information of the quality needed to make
good mining and processing decisions. In this regard, the reliability of a resource model is
grounded in some fairly simple statistical concepts. The first of these concepts is the notion
of a central limit. The more times a characteristic like gold grade is measured, the more the
results will tend to group around a central limit or mean. So one way a resource model
overcomes inherent sampling variability is by using very large numbers of samples. Equally
as important as collecting and assaying huge numbers of samples, however, is ensuring that
as the sample results group around a central limit, that the central limit is not biased, in other
9-1
Reference for Mineral Reserves and Resources
words it accurately reflects the true grade of the deposit. A good discussion of precision and
accuracy is given in Section 6.2.1 of this reference volume.
Within a small portion of a resource model (a single underground stope or a single open pit
ore outline), the accuracy of an estimate can be very low. As the portion of the model
increases, the accuracy of the estimate should improve. A good rule of thumb for larger
volumes of material (a years production, a full cut back in an open pit) is that accuracy within
plus or minus ten percent should be achievable. Inaccuracy that is reflected by bias
consistently in the same direction for large volumes indicates a problem either in the reserve
estimate or in the production data used for the comparison. These types of comparisons are
called reconciliations and are discussed in detail in Section 15 of this reference volume.
Resource models can be separated into two major components; the geologic model and the
grade model. One of the most important aspects of the resource modeling process is to
ensure that these two components are linked to one another. To put it another way, the
geologic model should do a good job of identifying metal grade, namely, separating
mineralized from unmineralized material. If this is accomplished, the grade model will make
geologic sense. Because these two modeling components should be closely lnked, it is
impractical to discuss them separately. Rather the sub-headings in this section will be
organized so that the two modeling components, geology and grade, will be discussed in the
sequence that they evolve in a resource model
9-2
Reference for Mineral Reserves and Resources
The geologists use the logging information to develop plan maps of the geology at the
topographic surface or at other levels either underground or in a pit. The geologic information
is usually also compiled on cross sections at a spacing dictated by the spacing of the drilling
and at orientations dictated by the geometry of the faulting and attitudes of the rock and
alteration units . As drilling and logging information increase, section and level spacing is
reduced to add more detail to the geologic interpretation. The development of geologic level
plans and cross section should be an iterative process where geologic boundaries on levels
are projected to sections and vice-versa to ensure tree-dimensional consistency.
could have downhole survey or collar location problems. Underground drill holes should
always be checked against the drill logs to verify the inclination since these holes can have
either positive or negative inclination. Drill hole collar and surface sample locations can be
checked against topography to ensure that the elevations are consistent.
Large
discrepancies should be checked.
against the log of the grades. The resulting line provides some insights into the underlying
grade distribution. Changes in the slope of the line indicate more than one grade population.
The highest-grade portion of the line usually gets very erratic. The grade at which the line
begins to show erratic behaviour is a good indication of the grade cap that should be applied
to samples with grades higher than this value.
Both the histogram and cumulative frequency plot should be constructed individually for each
geologic zone to further assist in recognizing the important geologic controls for mineralization
15.5 TOPOGRAPHY
A key component of the resource model is the accurate definition of the pre-mining surface
topography. This surface is important for accurate assessment of tonnages in open pit
projects and for proper placement of mine and plant infrastructure in all projects.
Topography is defined through use of aerial survey flights in which closely-spaced stereo pair
photographs are taken of the area to be surveyed . Control points are marked on the ground
prior to the flights so that they can be located in the air photos. These points are also located
using conventional surveying methods or GPS. The stereo air photos are then used to
digitally contour the topography. These digital contours are adjusted in X,Y,Z using the control
points as a reference. The digital contours are provided for use, usually in the form of
Autocad DXF files. Alternatively the surface topography can also be transferred as gridded
elevation data at a fairly small grid spacing.
The contours or elevation grid are then loaded into various mining software packages to be
used as is or to create a three-dimemsional surface. The surface then forms one of the
control surfaces within the geologic model.
discussed below. A better method is to overlap polygons such that the lower priority polygon
is overlapped by all higher priority polygons. Priority will be discussed below. 4) Care should
be taken to assign the correct plane reference to each polygon. In digitizing paper sections
this is just a matter of keeping track of the elevations or sections and assigning them
correctly. Digitizing on the screen can cause the plane coordinates to change unexpectedly if
the sectional position is moved during digitizing. In either case, including the planar reference
in the name of the polygon will permit correcting mistakes.
Once digitized, the polygons can then used to create three dimensional solids. The simplest
solids are created by projecting each polygon halfway to the next adjacent section. Resulting
solids have abrupt steps between sections. The polygons can also be linked together with a
series of triangles to form three-dimensional solids with smoother transitions between
sections. These types of solids look better in three-dimensions but can have inconsistencies
if the underlying polygons are adjusted for no overlap. Small volumes between solids can
remain unaccounted for because adjacent solids usually do not link up with the same
triangles.
The three-dimensional solids provide a convenient way to reconcile sectional interpretations
to plan and vice-versa. Most mining software permits the solids to be sliced at any plane
orientation and spacing. These slices can then be used to check the exiting interpretation on
that sectional plane. Once adjustments are made, the revised slices are re-linked into a solid
and sliced on the original orientation to further reconcile the three-dimensional interpretation.
Several iterations of this kind might be necessary to develop a shape that is consistent in
three dimensions.
The three-dimensional solids or the polygons are then used to assign the relevant geologic
codes to a three dimensional block model. If the block sizes within the model are uniform,
geological assignments are usually done based on the position of the block center relative to
the solids or polygons or based on the solid or polygon that contains the majority of the block
volume. When polygons or solids overlap the assignment is made based on the priority of the
polygons or solids in question. The highest priority polygon or solid is assigned to the block.
In some cases the percentages of the block contained in the various polygons is retained
along with the appropriate geologic codes. If the block sizes are variable, then smaller
blocks, usually called subcells, are added at the polygon or solid edges to better define the
geologic contacts. These subcell models can create very large computer files so the need
for higher resolution of the geologic contacts should be honestly evaluated.
Topography is usually added to the model as a value in each block indicating the percentage
of the block that is below the topographic surface. This procedure requires that there be
sufficient blocks above topography at all positions in the model. Once the percentage value
has been assigned, they should be verified for a complete set of sections or plans at the
topographic surface.
All levels and sections of the final geologic model should be viewed in plan and section to
ensure that the block assignments have been made correctly. The importance of this visual
check cannot be over-emphasized. Care in constructing the geologic block model will save
considerable time later.
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roughly coincide. Any drift of the peak indicates a bias at the composite stage, suggesting that
a smaller composite should be used. The smaller composite and block size will prevent the
composite bias from propagating to the grade model.
15.8 VARIOGRAMS
Probably the most useful tool to come out of geostatistics is the variogram. For the theory
behind variograms the reader is referred to any of the geostatistics references. For the
purposes of this volume, the basic components of the variogram are discussed. Variograms
measure the spatial continuity of a population of sample grades. The X-axis of a variogram
denotes lag or separation distance for sample pairs. The Y-axis of a variogram denotes
variance between the paired samples at a specific separation distance. As the lag distance
increases, the variance increases until it levels off at or near the statistical variance of the
entire grade population. This variance is also known as the sill of the variogram. The lag
distance where the variance reaches the sill is known as the range of the variogram. The
variance at a lag distance of zero is known as the nugget of the variogram. One
measurement of continuity based on the variogram is the nugget:sill ratio. The lower the
nugget:sill ratio the greater the local correlation or continuity. The range of the variogram
indicates the maximum distance at which samples have some spatial correlation.
Variograms should be calculated using the composite assays after capping the raw data.
One of the powers of the variogram is that it can be calculated at specific orientations. Multidirectional variograms should be calculated on an ongoing basis to identify and confirm
preferred orientation of the ore zones. By adjusting directional windows, variograms can be
calculated for planar features such as bedding and faults. Some of the mining software
permit calculation of downhole variograms which are useful for determining the nugget
variance. Variograms will usually show improved continuity parallel to the drilling. If this
direction is one of greater grade continuity, the drilling orientation should be changed. If not,
respecting this direction in grade estimates can cause oversmoothing of grades in the grade
model.
Many alternatives to the variogram have been developed. Two that are commonly used are
the correlogram (1 minus correlation) and the indicator variogram (variogram of zero-one
indicator value at a specific cutoff). The correlogram often gives cleaner results than the
variogram. The indicator variogram is useful for determining continuity of mineralization at a
certain cutoff.
While many models exist for variograms, nested spherical models are usually adequate for
modeling most variogram data. Most of the mining software packages contain programs for
variogram calculation and modeling. Alternatively, the variogram data can be plotted and
modeled in standard spreadsheet software. It is not uncommon for variograms to not level off
at the population variance but to continue to increase with increasing lag distance. Variogram
models should be restricted to the portion of the variogram at or below the sill.
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The composite assays are used to assign grades to the model blocks contained in the
geologic model. The variogram provides guidance in determining the search distances to use
as well as the search orientation. Maximum search distances should be limited to distances
corresponding to 90 to 95 percent of the sill variance.
While the variograms can provide valuable input with regard to anisotropic search ellipses, it
is often necessary to apply search ellipses that respect the geologists interpretation of ore
geometry and continuity. Often tight structural controls are not discernible with variograms
but are observed in outcrop and in drill holes. If general orientations for these types of
controls are obtainable, tight anisotropic searches are appropriate even if they do not show up
in the variography. Other mineralization controls might also be applied based on geology
alone such as bedding plane control and mineralization in dikes or sills.
Often the drill spacing is such that searches as long as the variogram range include large
amounts of composite data. Using all this data in a block grade estimate would likely result in
grades that are much smoother than desired. Two solutions to this problem are suggested. 1)
The total number of samples should be limited as well as the total number of samples per drill
hole. 2) The blocks can be estimated using multiple estimation runs at increasing search
distances to restrict sample influence in early short-search-distance runs and extend the
sample influence in later runs. Both of these techniques serve to reduce the overall
smoothing of grades. Use of too many samples for resource model estimates is a common
problem. Model to mine reconciliations often show that the resource model predicts more
tonnage at a lower grade than is actually produced. Use of fewer samples per block in the
resource estimate is a good way to minimize that problem.
With no mining experience, measured resources and proven reserves can be difficult to
define reliably. In underground mines, the industry-accepted practice is to consider the
material that is blocked out and ready for mining as measured. Also material that has been
sampled from drifts and raises developed in the mineralization is typically considered
measured. The measured material extends only a short distance from the development. This
distance is usually equivalent to the appropriate dimension of the selective mining unit.
In open-pit mines, measured resources are defined using various methods. If the
underground conventions were applied, material could be considered proven once it has been
drilled and sampled for blasting. The bench just below a blasthole-sampled bench might also
be considered measured. Within the indicated resource, the planned blast hole spacing could
also be used to define small measured blocks around the exploration drill holes. Experience
in open-pit mines usually shows these estimates of measured resources are conservative.
With mining experience, mine-model reconciliation can be used to establish or verify the
criteria used for defining measured/proven. The method is valid as long as reconciliation of
mine production to the resource model is acceptable, the mine measurements of grade and
tonnage are unbiased, and the mine production of metal reconciles well with final metal
production. If this is the case, the 90 percent rule (item two above) can be used to calibrate
the criteria used for classifying measured/proven. In an open pit mine, for example, the
values of individual resource model blocks can be compared to the actual values of the
blocks based on blast holes. If blast hole data confirm that at least 90 percent of the resource
ore blocks ended up actually being ore, then those blocks could be considered proven. The
comparison is done selecting blocks using very strict classification criteria (for example: short
distances to nearest drill holes). If the success rate is greater than 90 percent than the criteria
are relaxed until the success rate drops to 90 percent. Those relaxed criteria can than be
used for defining measured/proven material. The test usually involves several iterations,
either relaxing or restricting the classification criteria until a 90% success rate is found. An
example of this type of study is shown in Figure 1 where measured resources and proven
reserves in the example ore deposit should be within 20 meters of the nearest exploration drill
hole.
Care should be taken in applying this test. Resource model blocks that are originally waste
but end up being ore after production sampling cannot be used to increase the success rate
in the test. These blocks, while welcome, are still misclassified. Geologic variations should
also be respected in the comparison to avoid mixing well-behaved mineralization with poorly
behaved mineralization.
In nearly all cases, stockpile material is considered proven ore. This might not apply if
stockpile re-handling and mixing makes it necessary to re-sample the pile to predict grade
and mill recovery.
In underground operations, most measured resources that meet economic criteria
automatically become proven reserves and are mined fairly quickly. One exception is pillar
material. If no plan exists to mine this material it remains a measured resource only.
Indicated Resource
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In nearly all cases, an indicated resource requires one more sampling effort that converts it to
a measured resource prior to making an ore-waste decision during mining.
It is a commonly accepted rule that a probable reserve should have at least a 75 percent
success rate.
In defining indicated resources, a metal grade variogram or an ore-waste indicator variogram
is often used to establish indicated resource criteria. The sill of the variogram or the statistical
variance of the grade data is considered the maximum variance or sill variance. A range that
corresponds to 80-85% of the sill variance is taken from the variogram plot. That range then
defines the maximum separation distance between sampled drill holes and indicated resource
blocks. Examples of this method are shown in Figures 2 and 3.
Another method for designating measured resources involves using the sample data and
geologic information to define a continuous mineralized zone. In order to be used for
indicated resources, the zone must efficiently separate mineralized material from
unmineralized material. As a rule of thumb, the mineralized / unmineralized cutoff should be
10-20 percent below the ore-waste cutoff. If such a zone can be defined, and if the geometry
of the zone is not too complex, then continuity within the zone can be assumed the zone can
be considered an indicated resource. The maximum separation distance defined from the
variogram should also be used to confirm that most (> 95%) of the material within the
mineralized zone is also within the required distance to sampling.
As with the measured/proven categories, mining experience can be used to verify and adjust
the criteria that define indicated/probable material. Mine-model reconciliation is used as
discussed above to determine the classification criteria that identify material with a 75 percent
success rate. For the ore deposit shown in the example on Figure 1, indicated resource
blocks should be within 45 meters of an exploration composite.
In nearly all mines and projects, the bulk of the resource is indicated and the bulk of the
reserve is probable. The indicated/probable criteria therefore are the most important ones to
get right.
Inferred Resource
An inferred resource will require at least two more sampling efforts prior to development. The
first infill sampling will convert it to an indicated resource. The second will convert it to a
measured resource prior to making an ore-waste decision during mining.
It is a commonly accepted rule that inferred resources should have at least a 50 percent
success rate.
The second comment above is inconsistent with the CIM statement: it cannot be assumed
that all or any part of an Inferred Mineral Resource will be upgraded to an Indicated or
Measured Mineral Resource as a result of continued exploration. The CIM statement sets a
very low hurdle for inferred resources, one that is also inconsistent with other aspects of the
CIMs own resource definition. As mentioned above the CIM requires that all resources must
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have a reasonable prospect for economic extraction. Restated in terms of the CIM standard,
all resources must have a reasonable prospect for becoming a mineral reserve, which by
definition is at least an indicated resource.
The variogram can be used to establish a reasonable limit for search distances to create
inferred resources. Many companies use the total range of the variogram as the maximum
search distance. Often the variogram model approaches the sill at a low angle (see Figure 3).
This low-angle portion should be ignored to avoid search ranges that are unreasonably long.
A variogram value that corresponds to 90-95 percent of the sill variance is usually reasonable
as an upper limit for search ranges during resource modeling (Figures 2 and 3).
Calibration of the inferred resource criteria is usually not done during mining. It would be
useful to check these criteria with production data. This would require special models with
some of the exploration samples removed to create longer block-sample separation
distances.
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Section 10
10.7.
10.1. INTRODUCTION
Estimation of mineral reserves for a new project requires knowledge of the likely metallurgical
recoveries pertaining to the metals of interest contained in the various ore types in the
deposit. Although the inaccurate estimation of resources and reserves is arguably the major
reason for the failure or poor performance of newly developed projects, the lack of adequate
metallurgical testing prior to project development also can significantly contribute to poor
project performance. Unfortunately, this problem often occurs simply as a result of the failure
of project geologists and metallurgists to maintain communication between each other. A lack
of ongoing communication results in geologists (especially those in exploration) not being
familiar with metallurgical processing issues that may have little to do with ore grade.
However, just as important, poor communication can result in metallurgists who do not
understand the geologic and mineralogical characteristics of the deposit, and thus have
trouble designing an effective metallurgical testing program. For example, zones of silica
encapsulation of gold, high clay content, or highly variable sulphide content can significantly
affect metallurgical recovery and, if these zones are not identified, defined, and understood
prior to project flowsheet design and plant construction, plant performance can be severely
affected and the success of the project may be compromised.
The collection of metallurgical data should begin during the very early stages of exploration
drilling, or as soon as grades are encountered that indicate the presence of potentially
mineable mineralization. The results of this early metallurgical sampling and testwork can be
invaluable in preventing further exploration expenditures on a project or portion of a project
that is shown to have significant recovery issues, such as high sulphide content or silica
encapsulation of gold. These early-stage metallurgical samples must be representative of
the various ore types that are known to be present in the deposit, given the level of
understanding of the deposit at that point in time.
Whether for a new project or at an existing operation, the person responsible for reporting ore
reserves should be familiar with the estimation of process operating costs. This ensures that
all appropriate costs are included in open pit floating cone or Lerchs-Grossmann simulations
and are reflected in both open pit and underground break-even cutoff calculations.
10.1.1.
TERMINOLOGY
The terms associated with metallurgical sampling, testing and the estimation of operating
costs are described below. Terms used specifically for gold have been included (for example,
the bottle roll test) but most are applicable to other metals:
Metallurgical Data - This broad term refers to any data that help define the metallurgical
characteristics of a deposit. It includes assays or analyses for recoverable metals, gangue
constituents (such as silica or carbonate), problem metals and clay minerals, estimates from
drill logs and geologic mapping of pyrite or other sulphide minerals, grinding indices and
hardness data from metallurgical testwork.
Metallurgical Sample - A sample collected for the purpose of performing metallurgical
testwork and analyses. These samples usually represent large blocks of material that fall
within a specified grade range or material type. Typically, initial metallurgical samples are
composites of smaller samples taken from drill core, RC drill cuttings, or underground channel
samples. Later-stage sampling includes bulk material from small surface sample pits,
underground workings, or large-scale multi-ton (tonne) samples for pilot plant test runs.
Bottle Roll Test - A preliminary test for gold cyanide extraction potential that involves placing
a metallurgical sample in a bottle with cyanide solution and rolling (agitating) the bottle for an
extended period of time. The solution is then decanted and analyzed for gold content.
Generally, the solids are washed free of solution and also assayed for gold content.
Column Test - An integral part of metallurgical testing for the amenability of precious metal
ores to heap leaching, column tests involve the placing of crushed or broken mine run
mineralized material into plastic pipes, or columns, of varying diameters and lengths and
subjecting the material to variable concentrations of cyanide solution at different application
rates.
Flotation test
Bench-scale Test - Bench scale tests are those tests performed in the laboratory. These
include bottle rolls, grinding tests, flotation tests, gravity tests, pressure oxidation and roasting
tests.
Pilot Plant Test - Pilot plants are small-scale versions of the projected processing plant.
Pilot plant tests are designed to determine how the ore types behave under actual milling
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conditions. Typically, the pilot test will process bulk samples selected as representative of the
various ore types. The size of a bulk sample can range from several hundred tons (tonnes)
up to more than 10,000 tons (tonnes).
NEW OPERATIONS
The collection of metallurgical data for new or undeveloped operations begins early in the
exploration drilling stage of the project. As drilling takes place, the interpretation of the
metallurgical characteristics of the deposit should be developed simultaneously with the
interpretation of structural, lithologic, alteration and mineralogical zones. These initial
metallurgical interpretations are general in nature and, typically, are based primarily on grade
and/or the oxidation state of the in situ material (for example, oxidized, transition or mixed,
and primary (unoxidized) or sulphide).
The data that are ultimately needed for the refinement of metallurgical characteristics must be
collected at the same time that lithology, structure and other geologic features are logged.
There is a risk that core or RC cuttings may not be available for re-logging if needed in the
future since it is not unusual for whole (unsplit) core to be sent for assay, or for RC sample
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In summary, comprehensive logging and mapping of these data at the same time that other
geologic features are logged and mapped will save time and possible significant expense in
the later stages of a project.
- Early collection of metallurgical data can save significant expense and time in
the later stages of the project 10.2.2.
EXISTING OPERATIONS
At existing operations, the metallurgical characteristics of the ore usually are better
understood as a result of the operating experience gained. However, this understanding
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effectively is limited to ore already processed and the geologists expectations about the
metallurgical characteristics of the ore remaining to be mined.
Short-term changes in metallurgical recoveries that occur during the course of normal
operations should be investigated in order to determine if the fluctuation can be explained
geologically. Although such fluctuations are often ignored once recoveries return to normal,
sometimes it is the result of a different ore type that has gone through the plant unexpectedly.
The metallurgists and mine geologist should discuss any fluctuations in plant recovery and
pay close attention to ore feed both during and after they occur. Likewise, as new drilling
provides additional data that may affect recoveries, whether negatively or positively, the
geologist should update interpretations for remaining ore and communicate those changes to
the metallurgist as soon as possible.
METALLURGICAL SAMPLING
Although it is important that drill hole samples or channel samples taken to determine the
grade of the deposit are representative of the in situ material, metallurgical sampling,
similarly, must adequately represent the material that will eventually be mined and processed.
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diameter core holes are often drilled specifically to provide material for the second round of
metallurgical testwork.
Depending on the metallurgical character and complexity of a given deposit and the results of
the first two rounds of testwork, metallurgical sampling is often then stepped up to provide
multi-ton (tonne) bulk samples for larger-scale metallurgical testwork. Typically the collection
of these larger samples focuses on providing material that closely approximates the grade
and character of the expected average mill feed. These bulk samples sometimes can be
collected from shallow surface pits, provided that the near-surface material in the deposit is
representative of the ore at depth. However, due to deposit complexity and/or near-surface
oxidation, underground workings are often driven specifically for the purpose of collecting bulk
samples for metallurgical testwork. These workings also provide valuable rock mechanical
and other data needed for mine engineering decisions (see Section 11, MINING DATA
COLLECTION AND SELECTION OF MINING METHOD, of this reference volume).
Finally, if uncertainties relative to metallurgical recoveries, reagent consumption, or
processing costs remain after bulk testwork, or if a novel flowsheet is required to treat the ore,
a pilot plant test may be warranted (see Section 10.1.1). Because pilot plant tests strive to
match actual production conditions as closely as possible, selection of the source(s) of
material for this type of test is critical. Determination of the source(s) should be a joint effort
between project geologists and metallurgists, aided by project mining engineers where
necessary.
rates, recovery and operating costs, along with the material characteristics of the
products and tailing. The objective is to ensure that the entire resource, including all
lithologies and alteration types, has been tested and that material representing the
range of grades in the deposit also has been tested. During the test program, samples
must include material that represents the dilution that will be introduced during mining
in an amount considered typical for the mining method proposed. Geotechnical issues
with respect to the stability of the hanging and footwall must be considered at this
stage also.
A typical example of this procedure for a gold ore is described in the following section.
10.3.1.
Once the core has been logged by the geologist and sample assay data received from the
laboratory, the information is presented to the metallurgist. In addition to the assay data, the
geologist will provide information such as:
The association of the valuable mineral with any of the other mineral species,
particularly sulphides, sulphates, and silicates.
Typically, gold ores are classified as free milling, refractory, or double refractory. A free milling
ore is one that responds to normal processing methods such as gravity, flotation or cyanide
leaching. A refractory ore does not respond to normal treatment methods because the gold is
either locked in sulphides or there is carbonaceous material present that acts as a preg
robber (i.e. material that competes with the activated carbon for the gold in the gold-bearing,
or pregnant solution). This type of ore requires a more complex treatment process,
including pretreatment or oxidation in order to liberate the gold or to destroy the preg robber.
The oxidation treatment can be pressure leach, bio leach or roasting.
The metallurgist will then conduct a series of scoping or feeler tests (see Section 10.1.1) to
determine whether the gold is amenable to the normal extraction methods (gravity, flotation,
or cyanide leach). A common method is to perform a diagnostic leach. The sample will be
leached with cyanide and various acids in order to determine the refractory gold content. In
addition to refractory issues, the search for other problematic constituents should be well
funded and thorough. Early detection of processing problems is critical.
10.3.2.
Given the results of Step 1 and input from the geologist, the metallurgist can then compare
this information to other operations that treat, or have treated, similar material in order to
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identify individual process stages that may be required for each of the process options under
consideration. At this point, it is important to know whether the ore source will be mined by
open pit, underground, or a combination of both, since the mining method will affect the
particle size of the process feed.
10.3.3.
Based on work completed in Steps 1 and 2, the primary extraction method is identified. For
example, crushing, grinding and cyanide leaching may be identified as the primary extraction
processes.
10.3.4.
In Step 4, the decision is made about how to link each of the selected processes together.
These links are very much dependent on the characteristics of the material at each stage.
10.3.5.
This step focuses on defining the key processing characteristics in greater detail. Typically,
this involves development of the grade-recovery curve, determination of the sensitivity of
recovery to grind, determination of the crushing, grinding and abrasion indices, establishment
of the reagent addition rates, and the definition of process operating conditions.
10.3.6.
In Stage 6 the selected key processes are optimized. Based on the previous tests, the
optimum conditions are established by repeating the tests under slightly different sets of
conditions. Several iterations of testing may be required. If a particularly difficult ore is
encountered, then intensive mineralogical work also is required. Samples of residues are
examined in order to determine the deportment of the gold-bearing minerals and to establish
the treatment required to unlock the gold.
Typical tests performed for leaching include bottle rolls and agitation leach tests. Samples of
ore are crushed or ground to a particular size and leached in cyanide, usually in the presence
of activated carbon, to extract gold and silver. Solution samples are taken at set time
intervals during the leach tests, without carbon, and assayed for gold content in order to
establish the kinetics or rates of reaction. Final metal recovery rates are based on the assay
of the head or feed material and the residue after leaching. See the illustration below.
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Other tests are run to determine the crushing, rod mill and ball mill work indices and the
abrasion index in order to determine the mill size and power required for crushing and
grinding. Other specific tests are conducted to establish breakage functions, if SAG or AG
milling is being considered.
Flotation bench-scale tests are run if the ore is primarily sulphide in nature. Flotation can be
used as a pre-concentration process where the sulphides collected are then subject to other
treatment, such as oxidation or additional grinding and leaching, or as a final concentrating
process where the concentrates are sold to a smelter and a credit is received for the precious
metal content. Typically, flotation tests are bench-scale at the scoping level and locked cycle
when establishing final concentrate grades and operating conditions. Gravity separation tests
are also run, particularly if the ores contain visible gold.
When the ores are low grade, the process selection tends toward low cost processing
technology such as heap leaching. Scoping tests are completed using bottle rolls at both
coarse and fine size fractions, small-diameter column tests, and large-diameter columns in
order to establish grade, recovery and crush size relationships. To gain confidence in the
data, crib tests or pilot heap tests also are performed.
Pilot tests are also run to confirm flowsheets developed from laboratory bench-scale work,
particularly when the metallurgy is complex and there are internal recirculating streams in the
process. Pilot tests are necessary because bench-scale tests cannot replicate the interactive
reactions of the recirculating streams.
For ore that is more refractory, specialized testing is required. For example, bioleaching,
pressure oxidation, roasting, and ultra-fine grinding (UFG) may be investigated. This work
can be performed on whole ores or on concentrates. Pressure oxidation can either be
performed in acid or alkaline environments, while roasting can be run in oxidizing or reducing
atmospheres.
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10.4.1
HEAP LEACHING
Heap leaching is a low cost treatment method that is usually applied to low grade ores. With
this process, an area (referred to as the leach pad) is prepared for treatment of the ore. A
pad is constructed by first creating an impervious soil layer then overlaying this soil with one
or two layers of plastic liner. The ore then is placed in lifts over the liner using trucks or
conveyor systems, and cyanide solution is applied to the ore mass, using either a spray or
drip system, for a predetermined period of time. The solution permeates through the mass
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and the pregnant (gold-bearing) solution is collected in a pond or within the pad itself. The
pregnant solution is transferred to a gold recovery plant where it is subject to carbon or Merrill
Crowe treatment to recover the precious metals. Cyanide and lime are then added to the
barren solution and it is returned to the leach pad.
There are several design variations within heap leaching operations. The two basic types are
valley fills and stacks. The valley fill leach pad is usually constructed where the natural
topography is used to define the base area of the pad. Ore is placed on the pad in layers,
and the pad gradually fills up the valley. With stacks, pads can either be on-off, where the
ore is placed on a pad, leached for its time cycle, rinsed and removed for final storage in a
waste area, or permanent, where ore is stacked permanently on a pad that increases in size
over time.
10.4.2
CYANIDE MILLING
The cyanide milling process was developed in the late 1800s when it was found that gold
would go into solution when exposed to cyanide in the presence of oxygen. The early leach
technology utilized agitated tanks and airlifts to aerate the slurry. The pregnant solution was
then separated from the slurry by thickeners and filters, clarified and de-aerated. Zinc was
added to the clean de-aerated solution to precipitate the gold, silver and other metals. The
precipitate was collected in filter presses, then dried, retorted to remove mercury and, finally,
mixed with fluxes and smelted to produce dor. In this process, the barren solution is reused.
However, over time the barren solution becomes stale and a portion must be bled to tailings.
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Carbon-in-leach tanks
More recently, modifications to this method include exposing the cyanide leach solution to
activated carbon. Gold and other metals adsorb on the carbon, which is then separated from
the slurry by screening. The loaded carbon is stripped by a caustic cyanide solution and the
gold is recovered by electrowinning or zinc precipitation. Another variation is the carbon-inleach (CIL) process, where the gold is exposed to carbon at the same time that it is being
leached. This mitigates the effect of preg robbers in the solution, since the gold preferentially
adsorbs on the higher activity carbon. The loaded carbon is then stripped and the gold
recovered by electrowinning. The carbon is reactivated and recirculated to the adsorption
circuit.
10.4.3
GRAVITY CIRCUITS
Gravity separation was one of the first methods applied by man to recover gold. Gold has an
extremely high specific gravity (21) and, thus, can be separated easily from some of the
minerals that host gold (such as silica) by using gravity. Panning gravels from riverbeds to
recover alluvial gold was an early method of gold recovery using gravity. Sluice boxes and
blanket tables were also common. Over time, the technology improved and machines such
as jigs and centrifugal concentrators were developed to recover the metal. These methods
result in a concentrate from which the gold is extracted by tabling (see illustration below) or
via more stages of centrifugal concentration to produce a concentrate that can be direct
smelted.
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In some cases, the gravity concentrate was amalgamated (that is, mixed with mercury to
produce a gold-silver amalgam), which could be retorted to remove the mercury and leave a
gold sponge for smelting into dor. Amalgamation processes were replaced in most
commercial plants by more sophisticated gravity separators and tables due to the
environmental hazards associated with mercury. However, artisanal miners in less developed
countries still commonly practice amalgamation. In these places, controls or restrictions on
mercury usage may be non-existent, or are simply ignored.
10.4.4
FLOTATION
Flotation is a process that is commonly used to treat gold ores containing sulphide minerals
(gold often is associated with pyrite, chalcopyrite and galena). The flotation process is used
to pre-concentrate the gold ore either for subsequent treatment or for sale to a smelter where
the concentrate is treated and the gold is paid for as a by-product credit.
With flotation, the ore first is ground then mixed with a reagent known as a collector. Air and
a frothing agent are introduced into the flotation cell. The collector wets the surface of the
sulphide mineral particles to make them preferentially adhere to the surface of an air bubble.
The air is dispersed to create fine bubbles to which the mineral particles attach themselves
and rise to the surface of the cell. As the bubbles rise, the gangue minerals and slimes drop
back into the cell and exit as tailing. The mineral-bearing froth is collected as concentrate.
Additional stages of flotation are added to scavenge more sulphide minerals from the tailing
stream and to increase the grade of the concentrate via cleaning stages.
10.4.5
PRE-OXIDATION
Refractory ores require pretreatment to liberate gold that may be locked in sulphide or
associated with preg robbers. Common pretreatment processes utilized are roasting,
pressure leaching, and bacterial leaching.
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Roasting is a pyrometallurgical process where the ore is heated in the presence of air or
oxygen which oxidizes the sulphur and produces sulphur dioxide (SO2) gas and a calcine,
which can then be treated conventionally. Roasters are also used to treat preg-robbing ores.
Here the carbonaceous material is converted to carbon dioxide (CO2) gas and carbonates.
There are several types of roasters used, including fluid bed, recirculating bed, rabble
roasters and Dwight-Lloyd horizontal bed roasters. Reducing roasters are utilized where the
ore contains enargite which decomposes under reducing conditions to yield arsenic, sulphur
compounds and iron oxides. These products are then oxidized to complete the treatment
process.
In addition to the SO2, any arsenic or mercury present in the ore reports to the gas stream.
Early roasters discharged all gases into the atmosphere. Modern practice requires the gases
to be treated to meet stringent emissions standards and, as a result, arsenic and mercury
now are recovered as by-products. The SO2 is recovered as sulphuric acid or fixed as a
calcium sulphate (gypsum) and discharged to tailing.
Pressure leaching is a hydrometallurgical process where the raw ore or a concentrate is
heated and agitated in a pressure vessel called an autoclave at elevated temperature and
pressure to convert the sulphide minerals present to sulphates and to liberate the gold. In the
presence of iron, any arsenic present in the ore or concentrate is precipitated as a stable
compound, usually scorodite. The autoclave discharge is neutralized with lime and then
leached to recover the gold.
In bio-oxidation, bacteria are used to oxidize sulphide ores. The common bacteria,
Thiobacillus Ferro-oxidans will oxidize sulphides under controlled conditions to liberate the
recoverable metals. This essentially is a slow version of the hydrometallurgical, heap leach
process. The sulphates are neutralized and the oxidized ore is treated conventionally to
recover the gold. Bio-reactions can take place in stirred tanks, leach pads and also naturally
in tailing ponds or waste dumps where a by-product of the process may be acid drainage.
Concentrate roaster
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The waste product of milling operations is commonly referred to as tailing. The tailing consists
primarily of the ground gangue minerals from the ore, any diluting waste rock that was mined
with the ore and any chemical residues carried over from processing. In most gold mills, the
mass of tailing generated is approximately equal to the tonnes fed to the mill. Only in cases
where a concentrate is recovered and shipped to a separate location for treatment is there
any measurable reduction in the mass of tailing produced.
Tailings disposal is an integral part of any milling operation. Historically, tailings were
sometimes discharged indiscriminately into rivers, lakes and wetlands without concern over
the potential environmental impacts. Today, the importance of tailings management is
recognized in order to mitigate potential risks during operation and after closure.
Nowadays, all tailings system designs are subject to intense environmental reviews and, at a
minimum, must take into account the following parameters:
Limits for metals and toxins in effluents from the tailings impoundments under
operating and closure conditions, with appropriate treatment to achieve discharge
limits.
Storm events and possible diversions to reduce the amount of water entering the
tailing area.
Seismic risk.
Tailings systems are designed to minimize environmental impacts during operation and after
closure. It is imperative that the tailing area functions as designed during mine operation and,
also, that it can be closed and remediated economically in order to minimize long term
environmental impacts and costs after mine operations cease.
The design and
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implementation of closure and remediation efforts are very dependent on the tailings contents
and the project location. For example, a potentially acid generating tailing system must be
closed in a manner that prevents the chemical reactions that generate acid. If acid generation
prevention is not possible, then perpetual monitoring and treatment of the effluent from the
tailing will be required.
Tailing disposal methods vary by location. Generally, most tailings are discharged as slurry
into a prepared containment area. Typically the containment consists of earth or rock wall
dams constructed to contain the tailing slurry within a designated area. Where possible, the
tailings dams are located in depressions or valleys to minimize the amount of dam
construction. Tailing containments are constructed with an impermeable liner made from
either compacted clays or plastic (PVC or HDPE) to limit the migration of solutions into the
ground water and/or through the dam walls. The dam walls are monitored for build up of
hydrostatic head, and have chimney and finger drains to prevent the buildup of hydraulic
pressure in the dams.
The tailings discharge is often detoxified prior to discharge into the tailings pond. The slurry
may be discharged either from the end of a pipe or spigotted along the dam walls. In either
case, the coarser particles settle first and beach near the discharge point, while the fines
typically settle in the centre of the pond. Excess water collects against the dam and, in most
cases, is reclaimed for process use.
10.5.2.
To reduce the size of tailing containment areas and provide backfill material for underground
mines (if needed), mill tailings are cycloned to scalp the coarse fractions of the solids from the
tailing pulp. When used for underground backfill, the coarse fractions are either returned
hydraulically to the mine as-is, or mixed with a binder such as Portland cement and/or fly ash
and delivered hydraulically to mined out workings in order to provide strength and ground
stability in the mine. In this case, the tailings remain as a pulp and the pulp has a critical line
velocity, which must be achieved to prevent segregation in the pipeline. The proportion of the
tailings that can be utilized as fill is dependent on the size distribution of the tailing pulp.
10.5.2.1
Increasing the pulp density of the tailing slurry results in a thickened or high-density tailing.
Filters and specially designed thickeners are used to achieve the high densities. Critical line
velocities still must be maintained in transport, but the percent solids are now sufficiently high
that settling will be hindered if the flow is slowed or stopped. Solid/liquid separation occurs but
the solids do not segregate into sand and silt. Upon discharge, the solids separate quickly
and the supernatant (liquid portion) flows quickly off the stack. The settled solids do not
significantly segregate by size.
Typical applications of this approach are in place in the aluminum industry and at the
Falconbridge Kidd Creek metallurgical complex.
10.5.2.2
Paste Tailings
Increasing the pulp density further results in the formation of a paste. Paste has no free water
and exhibits no size segregation during pumping and discharge. Paste is pumped to its
destination as a slug via positive displacement pumps. As a result, the paste can be
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deposited in a relatively simple containment area, as the dam does not have to withstand
hydraulic forces. The deposited paste gains strength through desiccation and evaporation,
eventually resting in place as a stable, impervious mass. Because there is little or no
migration of pore water, the risk of acid generation and transport of metals is minimal. Also,
since there is no ponded water, the tailing area can be progressively reclaimed as soon as
the design height of deposition is reached. The paste tailing can also be mixed with a binder,
such as cement, and pumped underground for backfill.
Paste tailings offer many advantages over slurry deposition:
Bulyanhulu is a classic example of true paste surface deposition of tailings. La Coipa also
practices paste deposition, but utilizes a belt conveyor rather than positive displacement
pumps to transport the paste to the storage area. It is generally believed in industry that
paste may be the preferred route for tailing deposition in the future.
10.5.3.
Mining activities almost always require that some sterile or non-mineral-bearing material must
be mined in order to access the ore. It is also a common occurrence that mineralized material
in which the metal content is too low to process economically must be mined in conjunction
with ore. These materials are usually mined and stored on surface. Generally, the
mineralized material is segregated from the sterile material to create waste dumps and lowgrade stockpiles. While there may be opportunities to use some waste rock as backfill in
underground mines to avoid the cost of bringing it to surface, or it may be possible to use
mined-out parts of an open pit as dump areas, the majority of waste generated by a mine
ultimately will be stored on the surface in waste dumps.
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While historical waste sites nearly always were selected for their proximity to the mine in
order to reduce haulage costs, today waste dumps consist of specially prepared areas that
are built to contain the waste generated over the life of a mine.
For current mines, operating and closure plans are required for the dumps as part of the
environmental approval process, prior to receiving a permit to operate (see Section 13,
OPERATING/ENVIRONMENTAL PERMIT REQUIREMENTS, of this reference volume). Lift
height and compaction must be engineered in order to prevent catastrophic failure of the
dumps. To mitigate acid rock discharge (ARD), it is necessary to design and operate the
dump to limit the ingress of air and water to the rock mass. By managing the dump design
and operation, it is possible to reduce, and in some cases avoid, the need for perpetual
treatment of effluent.
Mine wastes are characterized prior to commencement of mining in order to determine the
long-term stability of the waste material. The key factors that must be established are the
acid generating potential of the waste and the availability of buffering material, such as
limestone or other carbonate rocks. If the wastes do not generate acids, then the dump
design is primarily driven by geotechnical constraints. The dump must be stable during mine
operation and a plan put in place to contour and revegetate the dump at closure. If the waste
material is acidic, then the design not only must meet geotechnical constraints but also must
mitigate the effects of acid generation. Under these circumstances, the dump would be likely
be situated in a catchment area where all runoff from the dump can be collected and treated
to meet local discharge standards.
The base of the dump must be prepared to minimize infiltration of runoff to groundwater.
Downstream monitoring wells are also required to test groundwater for indications of
infiltration. Depending on dump height, piezometers may be required to monitor stability of the
rock mass. Where possible, storm water would be diverted around the dump area to reduce
the amount of water subject to treatment. During operation, if particularly acid generating
material is identified, the waste may be encapsulated in clay within the dump to reduce the
quantity of acid generated. A buffering material may also be mixed with waste to limit acid
production.
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For budget and reporting purposes, these elements are estimated by process area. Typically
the process includes crushing, grinding, gravity separation, oxidation, leaching, dewatering,
gold extraction (carbon or MerrillCrowe), refining on-site, transportation and sales, cyanide
destruction, tailing disposal, backfill, administration/supervision (including staff salaries,
training and professional development and any overheads), assay laboratory, technical
services (metallurgy, environmental and any external process support) and other services
(compressed air and water).
Major operating cost components include: labour, electric power, grinding media, mill liners,
reagents such as cyanide and lime, flotation reagents, flocculants, and other components
appropriate for a particular operation or project site. Maintenance costs are subdivided
between mechanical, electrical, and instrumentation, and include breakdowns for lubricants,
filters, V-belts, sheaves, motors, and maintenance service contracts. The distinction between
an operating material and a maintenance material is in the application of the material. For
example, if a component comes in direct contact with the ore then it is classified as an
operating supply, but if not, it is considered a maintenance cost. For example, a pump casing
is classified as an operating supply, while the motor and sheave and the barrel are
maintenance items. Although the definition varies between operations, what is important is
that all elements are defined and accounted for, and that the rules and definitions are
established up front and are known to everyone responsible for preparing and managing
budgets.
10.7. REFERENCES
Hayes, P. C., Process Selection in Extractive Metallurgy, Hayes Publishing Co., 1985.
G. Barbery, A.W. Fletcher, L. Sirios, Exploitation of Complex Sulphide Deposits-a review of
processing options from ore to metal., Symposium on Complex Sulphide Ores, IMM, Rome
1980
Mineral Processing Plant Design, Ed. A.L. Mular and R.B. Bhappu, SME-AIME, 2nd ed.
1980.
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Section 11
APPENDIX
Appendix 11-1
Section 11 Mining Data Collection, Selection of Mining Method & Mine Planning
Ver. 1 November, 2002
11.1. INTRODUCTION
This section of this reference volume is designed to give those Barrick personnel responsible
for stating mineral resources and reserves an overview of the mine planning process and the
resultant implications on resource estimation and management.
Mine planning and design tasks form a circle, as shown below, with each area relying on the
other for information. Using an open pit operating scenario as an example, pit limit analysis
represents the first of these tasks and identifies the potential pit and mineable resource limits
under a defined and simplified set of financial assumptions. To start the process, an initial set of
assumptions has to be made.
Initial mine, process and general parameters are assumed for purposes of open pit limit
analysis (or in the case of underground mines, stope limit analysis). Subsequently, these may
be refined as the circle is completed. This iterative process may be repeated several times and
be part of project development, from conceptual iterations to feasibility-level engineering.
Major emphasis is placed on the collection of geologic data during all stages of a project,
particularly in the early phases of exploration. However, collection of data that are useful for
early stages of conceptual mine layout and planning is often neglected until later in the project.
This can result in misconceptions about what mining method is most appropriate for the deposit
and which then can lead to crash programs to collect the data needed by mine development
engineers in order to make informed choices. Often these programs include additional drilling
at substantial cost, and result in project delays.
A significant portion of the data needed by mine development engineers can be collected as
part of a comprehensive and well designed geologic mapping, sampling and drill core logging
program. It is important for exploration geologists and mine development engineers to
communicate as early as possible in the life of a project, so that the geologists understand the
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Section 11 Mining Data Collection, Selection of Mining Method & Mine Planning
Ver. 1 November, 2002
types of data most useful to the engineers and steps can be taken for the timely collection of
these data.
Lastly, but far from least in importance, the Barrick person responsible for the reporting of
mineral resources and reserves for an undeveloped project or an existing operation must
understand what constitutes ore, which is defined as that portion of the resource base that can
meet break-even costs or be mined at a profit. This includes an understanding of the bases for
the capture and buildup of mine operating costs, and also the associated constraints (mining
losses and dilution).
To determine order of magnitude project size and mining and processing methods.
To attract a buyer to the project, to attract a joint venture partner, or as a basis for a
major underwriting to raise the required risk capital. A pre-feasibility study may also be
prepared in full or in part by potential purchasers as part of the due diligence process.
To provide justification for a timely Board-level decision for approval of the risk capital
required for certain tasks (such as to overcome seasonal restrictions to road
construction in remote areas) that must be completed before proceeding to a final
feasibility study.
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Ver. 1 November, 2002
As stated previously, mining data for development projects should be collected throughout the
exploration stage. These data, which are required for mine engineering and planning, can be
divided into technical data and supplementary data categories.
11.2.1.1.
Technical Data
As noted above, collection of the technical data needed for engineering and mine planning of
an undeveloped deposit must begin in the early stages of exploration drilling. All too frequently,
early misconceptions about a deposit are carried forward into the development phase of a
project, resulting in additional and sometimes substantial expenditures for collection of data in
subsequent stages of the project.
The first drill holes that intersect potentially mineable mineralization can provide important early
indications of the geometry and distribution of grades in the deposit to the mine development
engineers who will eventually be assigned to the project. For example, if the first round of
exploration holes reveals consistent low gold grades in the range of 0.05oz/t to 0.10oz/t over
significant hole distances (+100ft or 30m), then open pit mining would appear to be a likely
option since such grades are unlikely to support an underground operation. If the same
exploration holes show abundant fractured ground associated with the mineralization or the
presence of groundwater, this indicates that the collection of geotechnical and hydrogeological
data will be extremely important throughout the course of the drilling and evaluation programs.
Similarly, if the mineralization is confined to very narrow but high grade structures, then
preliminary thinking may tend towards one of the selective open pit or underground mining
methods. Poor rock quality in drill core will again serve as a warning that geotechnical data
collection must be carefully planned and implemented.
As with the collection of metallurgical data (see Section 10, METALLURGICAL DATA
COLLECTION AND METALLURGICAL TESTWORK, of this reference volume), the importance
of early and frequent communication between the exploration geologists, development team
geologists, project engineers and mine planners cannot be overemphasized. In every project
there are decision points in the early stages when it must be determined if additional exploration
expenditures or further development work are warranted. The early analysis of deposit
geometry and potential mining conditions allows for the most efficient planning of development
drilling, geotechnical testing programs and other basic engineering studies required for
completion of initial scoping and pre-feasibility level studies.
For example, consider the case of a deposit where it appears that some form of underground
blast hole stoping could be the mining method of choice, based on the results of the first phase
of exploration drilling. At this point, engineers should begin to focus not only on potential
ground conditions in ore, but also on the quality of the host rock adjacent to the potential ore, in
order to assess dilution scenarios, maximum sizes of underground openings, potential mining
methods, productivities and mine operating costs. In addition, the geology and geotechnical
characteristics of the country rocks that both host and surround the deposit must be understood
as soon as possible. Early conceptual designs for shaft or decline placement, primary
development access and mine services (ore passes, vent raises) can be significantly enhanced
by having an understanding of the local host rock geology. Potential problem areas such as
major fault zones or formational units that would require major ground support can be identified
and avoided where possible.
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The types of mining data that should begin to be collected as early as possible during a project
consist principally of measurements of rock quality and stability. These are required in order to
deal with important issues affecting mine development and production, including:
External dilution of open pit ore and associated preferred bench height selection.
Size limitations for underground openings (shafts and shaft stations, ramps,
development crosscuts and laterals, stopes, shops, et cetera).
Generally, the data required for mine engineering and development work are assembled and
recorded during the course of standard geologic logging. More detailed information about each
data type can be found in Section 5, GEOTECHNICAL AND GEOLOGICAL DATA
COLLECTION, of this reference volume. Care should be taken to ensure that proper recording
of these data takes place before the core is disturbed by sampling. It is not unusual for the
opportunity to collect these data to be lost because of technical manpower shortages during
exploration or, simply in the rush to get samples submitted for assay. When this happens,
additional costs (sometimes very substantial) and delays during subsequent scoping and prefeasibility level evaluations often are incurred.
Each Barrick operation or project site should have a site-specific list of the types of mine
engineering data required. If no site-specific guidelines are in place, it is recommended that the
following data are recorded. Similar descriptions of these data types are provided in Section
5.2.1.1. The data types are summarized below, along with comments on how these data
pertain to mine engineering issues.
Core and/or RC sample recovery - Poor core or RC cuttings recovery is generally a good
indication of potential ground problems in underground workings and possible high rates of ore
dilution with waste material. For RC holes, a qualitative determination of the amount of sample
returned to the cyclone (generally based on the weight of the sample collected at the rig),
compared to the amount of sample expected based on the diameter of the hole and the hole
interval drilled, can provide an estimate of sample recovery. Poor RC sample recovery
generally indicates the presence of voids, a cause for potential concern in both open pits and
underground mines. Excessive RC sample return usually indicates the presence of badly
fractured ground.
Structure orientation - When logging structural discontinuities present in oriented drill core, it
is possible to determine the true dip and dip direction of discontinuities from alpha () and beta
() angles (see Section 5, GEOTECHNICAL AND GEOLOGICAL DATA COLLECTION, of this
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Section 11 Mining Data Collection, Selection of Mining Method & Mine Planning
Ver. 1 November, 2002
reference volume). These data can be very helpful in determining maximum opening sizes in
underground mines and potential wedge failures in open pits.
Seepage - Evidence of water flow from structures, based on drilling shift reports. Reported
water flow can sometimes be correlated to individual structures based on the presence of vugs,
voids or other signs of dissolution. Seepage can be an important indicator to assist in early
estimation of de-watering requirements. Where applicable, data should be collected relative to
aquifer drawdown and recharge for determining potential impact of groundwater on mine
design.
Rock type - The early understanding of variations in rock types across a deposit are very
important for preliminary slope stability evaluations and bench configurations. For geotechnical
and development engineering purposes, it is often necessary for the geologists to combine rock
types into more general zones for the engineers.
Rock strength - A general description of rock strength is included in Section 5,
GEOTECHNICAL AND GEOLOGICAL DATA COLLECTION, of this reference volume. Rock
strength data are used to help determine open pit slope angles, the maximum allowable
opening size in underground stopes, penetration rates for production drills, and excavation
characteristics of the rock. The data are also used to determine production powder factors.
A powder factor is the amount of explosive agent required to break a particular rock type into a
desired fragment size range.
RC and/or diamond drill penetration rates - The penetration rates experienced by RC and
diamond drill rigs can give project engineers a general feel for drilling efficiencies that might be
expected in either open pit or underground operations. For open pits, these data are used to
establish productivity estimates for blast hole rigs in various ore and waste types, and which in
turn, provide meaningful estimates of direct drilling costs. For underground operations, drill
penetration rates provide the basis for productivity estimates for drift advance in ore and waste,
production drill productivity estimates in various ore types, and resulting estimates of direct
mining costs for development drifting in ore and waste and stope production drilling.
Ore and waste density - Early collection of samples for density determinations of mineralized
and unmineralized material is important. For more information on recommended sample
collection and density measurement methods, see Section 8, DENSITY DETERMINATION, of
this reference volume.
Other geotechnical data - The following geotechnical data types also are required for
determining maximum opening sizes in underground mines and potential wedge failures in
open pits. Because these data are routinely collected as part of geotechnical logging and
mapping, the basic definitions for these are included in Section 5, GEOTECHNICAL AND
GEOLOGICAL DATA COLLECTION.
Structure frequency.
RQD.
Structural block size.
Number of structural sets.
Structure spacing.
Filling.
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11.2.1.2.
Supplementary Data
Site ownership (mining rights, surface rights, access rights, water rights, agricultural
rights, national reserves, First Nation or other native or indigenous peoples rights).
The particular seismic zone where the mine is located and general information on past
seismic activity.
A general description of local climatic conditions (i.e. tropical, temperate, arid, highAndes, sub-arctic), when climatic extremes occur, and any other applicable climate data
that could affect mine design and equipment selection, such as temperature ranges and
the length and intensity of the rainy season.
Altitude data, which is necessary for determining whether engine de-rating is required
(for example, at altitudes in excess of 3,000m, engine de-rating may be appropriate).
Section 11 Mining Data Collection, Selection of Mining Method & Mine Planning
Ver. 1 November, 2002
unexpected high dilution, poor extraction, or other production issues. As with open pit
operations, the timely entry of new data from stope definition drilling and underground sublevel
and stope geologic mapping provides a valuable tool for addressing production problems.
Once production begins, the use of cavity monitor surveys (CMS) greatly enhances the mine
engineers ability to measure mining recovery and external dilution in stopes. These surveys
also help engineers and geologists to make meaningful reconciliations between resource model
predictions, mine production and mill production (see Section 15, PRODUCTION
RECONCILIATIONS, of this reference volume).
Where CMS data are not available,
conventional transit surveys must be used to the extent practicable.
Typical mine production data that should be collected in support of the ore reserve estimates at
existing operations includes:
Mine and plant production capacities for the previous year, the year following the
Statement of Ore Reserves, and the maximum capacities projected for the duration of
the life of mine planning period.
Production reconciliation data for at least the previous year (see Section 15,
PRODUCTION RECONCILIATIONS, of this reference volume).
A short description of historical and future mining methods (if changes to current
methods are anticipated).
Operating costs for the mine, processing and administrative departments, with specific
attention paid to consistency of reference units (for example, whether mining costs are
expressed consistently, per ton (tonne) or per metre (foot) of advance).
A statement of any stockpiled material remaining at the time of the Statement of Ore
Reserves, including the following information for each pile:
Type (i.e. low-grade, refractory, autoclave, et cetera) and cutoff grades applied at
time of deposition on the stockpile.
Volumes (if surveyed), tonnage and associated grades, with descriptions of the
bases for estimates.
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Selection of an appropriate mining method for a deposit often relies most heavily on the grade
and geometry of the mineralization. Large, shallow, low grade deposits are particularly
amenable to open pit mining, while extraction of deeper, higher grade mineralization typically
requires an underground method. However, for deposits where the choice of mining method is
not clear based on grade and geometry alone, other considerations come into play. These
include geotechnical issues (such as rock strength and RQD), environmental concerns
(underground operations may be more environmentally acceptable, depending on the deposit
location), manpower availability (skilled underground miners may not be readily available in
some remote locations), as well as issues that are purely economic, such as high import tariffs
on large equipment, royalties or government fees based on ore tons (tonnes) produced, or very
substantial employee wage burdens (which can approach 300% of base hourly or salary pay in
some countries).
It is not unusual for a gold deposit to be amendable to both open pit and underground mining
approaches. The bulk-tonnage, lower grade shallow portions of some deposits that are
attractive for open pit mining are often connected to a system of narrow, higher grade
mineralization feeder structures that can best be developed using one of several underground
methods. In these cases, it is important to ensure that the proper trade-off studies are
completed in order to determine the point at which mining should be transferred from an open
pit to an underground operation.
Similarly, the mining method(s) used at an existing operation must be appropriate to the
geometry, character, forecast throughput rate and grade, and geotechnical aspects of the
remaining reserves. Often, changes in the geometry and character of mineralization
encountered during the course of mining a deposit require a change in mining method. Such
changes can be made successfully only if the necessary geological and mining data are
available.
11.3.1.1.
Dilution
Mining dilution is that portion of mined material that is extracted in addition to the planned ore
grade material. Dilution can be further defined as:
Internal - Below cutoff grade material that must be taken internal to (within) the limits of
a stope block due to mining method constraints and geological conditions.
External - Material that is intentionally taken in order to allow for required minimum
mining widths (based on the selected mining unit, or SMU), and material unintentionally
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mined, such as backfill from adjacent cuts, and material that is external to the limits of
the stope block that must be taken without choice due to blasting overbreak.
Dilution is normally applied to the in situ resource as a width, thickness or volume, and is
typically expressed as a percentage. In lieu of a percentage, dilution tonnage and grade can
also be estimated using three dimensional grade models. Also, for undeveloped projects, any
available geotechnical data and planned opening sizes should be taken into account when
making preliminary dilution estimates. Underground resources and mineable reserves are
stated with the planned internal and external dilution included. Open pit reserves usually
incorporate internal dilution during the resource modeling phase as a function of the selection of
an appropriate SMU or block size. In cases where one or more narrow ore zones are
separated by waste blocks that are wider than the SMU, external dilution to allow for overdigging along the margins of the zones is sometimes included in reserve statements. All other
diluting material that is mined in excess of the plan is referred to as unplanned dilution.
Underground dilution varies as a function of mining method, orebody width and dip, and ground
conditions. For projects where no underground experience factors are available, preliminary
dilution estimates can be made using the following formulae, based on OHara:
Block Caving:
Cut and Fill:
Room and Pillar:
Shrinkage:
Long-hole with sublevels:
The mining methods that are most amenable to controlling dilution are cut and fill stoping and
shrinkage stoping. When the more productive longhole stoping and sublevel caving methods
are used, control of dilution often is more difficult.
11.3.1.2.
Mining Recovery
Also referred to as mining extraction, mining recovery is based on the undiluted portion of the
reserve that is mined out of the total volume of ore grade material contained in the resource
base. Mining recovery is normally stated as a percentage, and is a function of ore body
geometry, ground conditions and mining method. Ore grade material that is not recovered
during mining is termed ore loss, of which there are two types:
The in situ ore material that is not mined due to smoothing of mining shapes (i.e. it is not
possible for stope shapes or dig boundaries to exactly match actual ore outlines).
The material that is left in place before abandonment of a mining area. This includes
broken ore unintentionally left in underground stopes due to frozen blasts or misfired
holes, and ore intentionally left for geotechnical reasons (bench step-outs in open pits or
underground pillars) or because of management decisions related to backfill scheduling.
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Mining recovery is not generally stated in the case of an open pit, since it is assumed that all
resource blocks contained within an optimized pit will be mined at the scale of the selective
mining unit.
Metal prices - The Barrick corporate office will provide commodity prices for optimum
pit analyses. Care should be taken to ensure that the same metal prices are used in pit
limit design, cut-off calculation, royalty and NSR calculations.
Preliminary operating costs - For purposes of pit limit design, an initial set of cost
assumptions is required. These assumptions should be as close as possible to projected
actual costs (or within sensitivity limits) and should include:
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As a general rule, where not constrained by local ore geometry, the maximum bench
height applicable to the selected loading equipment should be used. However,
depending on the deposit, in selected areas a trade-off analysis of ore losses and/or
dilution realized with higher bench heights against higher mining costs (primarily drilling
and blasting) associated with lower bench heights, may be required. This analysis may
indicate that mining of flitches (split benches) less than a normal bench height may be
required in certain areas. If necessary, the quantity of material affected by this should
be identified in the resource model and appropriate (higher) mining costs assigned.
Pit slope angles - Prior to pit optimization simulations, preliminary pit slope angles must
be determined. Normally, these angles are established for the different sectors of a pit,
which allows flexibility for any different rock types and/or structural regimes present in
the deposit. Pit slope angles usually are determined by a third party geotechnical firm
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F
C1
C2
Haul road design - This is a function of expected truck haulage capacities, dimensions
and traffic densities. Typically the design will also include a provision for a crest safety
berm, drainage ditch and area for wall slough. If tapering of berms is applied at ramp
intersections, the percentage of taper is important on the overall slope design. Gradients
of ramps (vertical to horizontal ratio, expressed as a percent) are typically 8-10%.
In addition to these parameters, if the deposit extends to depth where underground mining may
also be an option, a trade-off study between underground and open pit mining methods may be
required, depending on the value and configuration of in-situ resources (see Section 11.3.4
which follows). If underground mining is viable, its timing may impact the optimum final depth of
the open pit.
In order to examine the robustness of the mineable resource defined by the optimum pit, a
number of sensitivity analyses should be performed, including:
Section 11 Mining Data Collection, Selection of Mining Method & Mine Planning
Ver. 1 November, 2002
Exclusion of and inclusion of inferred resources (i.e. separate analyses using only
measured and indicated resources, and measured, indicated and inferred resources).
Section 11 Mining Data Collection, Selection of Mining Method & Mine Planning
Ver. 1 November, 2002
production blasting. The downside to these methods is the lower mining recoveries that result
due to the pillars left for support.
Block Caving - Block caving is the single most productive underground mining method. Truly
a bulk method, block caving is designed to exploit large deposits that have broad lateral and
vertical extents that exceed 100m (300ft) in all dimensions. Although the least expensive in
terms of direct mining costs, block caving also requires extensive pre-production development,
including the installation of drawpoints on a regular and predetermined pattern and spacing,
and the development of a broad undercut level (required to induce caving) in ore at the bottom
of the ore block just above the draw level. Once caving begins, the method is completely nonselective. Dilution that occurs during caving is highly dependent on the geometry of the cave
block, ground conditions adjacent to the cave block and the management of the drawdown of
the cave.
In addition to the five most commonly used underground methods described above, a less
common method is sometimes used to mine wide, steeply dipping deposits. Sublevel caving
requires extensive development on sublevels in a systematic layout across the ore zone.
Generally, sublevels are driven at regular, pre-determined vertical spacings from footwall to
hangingwall in wider deposits. The pattern of sublevel development is mirrored between
sublevels, such that drifts on one sublevel are positioned directly over and under drifts on the
adjacent sublevels. Longhole rigs drill large diameter fan patterns (rings) of holes into the
defined ore block above each drift. Blasting begins on the uppermost sublevel at the hanging
wall and retreats toward the footwall along a straight front. The sublevel cave becomes filled
with broken muck and waste that has fallen from the walls. One ring is blasted at a time and is
mucked with an LHD according to an engineered bucket count, often 110% of the tonnes
blasted in the ring. Ore recovery and dilution are dependant on the many factors that influence
the gravity flow within the cave. However, recovery on the order of 80% and dilution around
30% is typical.
For underground mine planning, stope optimization (Floating Stope) programs are being
developed to determine underground resource limits in ways similar to open pit optimization
methods. An example is Datamines OreFinder which can best be described as a three
dimensional block compositor that analyzes the distribution of grades in a block model and
builds optimal envelopes of mineable reserves that are based on user-supplied criteria and
objectives such as:
The program generates the optimal stoping envelope for each set of criteria and reports the
mineable reserves.
As with open pit optimizers, stope optimization programs do not generate mineable resources,
and actual stope limits must be determined by detailed mine design and scheduling. The stope
optimizers are not yet widely used or proven in the underground mining industry and great care
must be taken with the results generated by these programs. However, it seems certain that
this technology will develop further and become a standard practice.
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3) Production is roughly equivalent to one-half ton (tonne) per day for every ton (tonne) of
reserves per vertical foot. For example, if the general spatial distribution of ore reserves
averages 2,000 tons (tonnes) per vertical foot, the mine should be able to produce 1,000
tons (tonnes) per day.
It should be noted that the last rule, as well as Taylors Law, are both somewhat outdated, since
the rates at which underground mines are deepened are typically less than 150 vertical feet per
year. However, these are preliminary guidelines rather than rigorous technical limits, as
demonstrated at Bulyanhulu, where sinking rates for all general workings (not just shaft sinking
or ramp access advance) exceed 300 vertical feet per year.
Generally, mine sizing is performed at the conceptual and pre-feasibility study stages of a
project, where a number of alternate mine and plant sizes and strategies can be rapidly
evaluated and an optimum can be selected based on multiple criteria. However, these
analyses sometimes suffer because of a lack of data pertaining to the deeper, narrower
portions of the deposit. As stated previously, care should be taken to ensure that the lower
portions of the deposit are adequately defined by drilling prior to completing mine sizing and
open pit/underground trade-off studies.
Section 11 Mining Data Collection, Selection of Mining Method & Mine Planning
Ver. 1 November, 2002
capture all costs relative to a specific activity, such as waste stripping, haul road maintenance,
equipment maintenance, or mine dewatering. These allocations should not be of concern to the
Barrick person responsible for reporting ore reserves, except to cross-check with mine
engineers that all labour and burden costs have been considered.
For new projects with no operating history, operating costs typically are built up around a similar
cost centre system, based on first principles. Where possible, it is also helpful to benchmark
preliminary operating cost estimates against existing operations that have similar operating
conditions.
The following sections summarize typical mine operating cost centres for open pit and
underground operations.
11.4.1
Labour (salary and hourly) - Mine hourly labour costs are straightforward and typically include
maintenance labor for mine equipment. For mine salaried labour, care must be taken that
technical and environmental services and administrative management costs applicable to the
mine are accounted for, either in mine operating costs, technical services operating costs, or
administrative costs. Mine labour is often allocated to other cost centres, such as maintenance
and/or dewatering.
Labour burden - Labour burden includes country-mandated and managed retirement benefits
such as FICA (US Social Security), Medicare (or similar country-mandated medical plan),
Federal and State or Province unemployment taxes, benefits such as medical and dental
insurance, pension plan contributions, company-paid education, and other benefits unique to
the mine or project location, such as hazard or high-altitude pay, foreign service allowances,
etc. In the United States, Canada, and Australia, labour burden typically ranges from 25% to
60% of base salary. For projects located in countries other than the United States, Canada,
and Australia, care must be taken to include all applicable labour burden items, and there can
be many. In certain countries, labor burden costs can approach 300% of base salary or hourly
pay.
Contract labour - Where applicable, contract labour directly attributable to mine operations
should be included in mine operating costs.
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Explosives - Because explosives costs are high relative to other consumable materials, these
costs, typically, are segregated in a unique cost centre. Costs for Anfo, slurries, gels, primers,
boosters and other blasting agents are included. Where blasting is handled by an outside
contractor, care should be taken to segregate material costs from contract labour costs in order
to ensure that these are not double-counted.
Drill bits and steel As for explosives, the costs for drill bits and steel are high relative to other
consumable materials, so these costs are usually captured in a separate cost centre. Where
blast hole drilling is performed by an outside contractor, care should be taken to segregate
material costs from contract labour costs in order to ensure that these are not double-counted.
Mining supplies and materials (consumables) - This category includes costs for all other
supplies/materials required for mine operations.
Mine maintenance supplies - Mine maintenance supplies include replacement parts
(exclusive of major rebuild components), hand tools, lubricants, haul road dust control materials
and nuts and bolts items.
Mine dewatering - If major amounts of groundwater must be pumped to allow mining and/or if
drain holes are required to maintain stable pit slopes, the costs for mine dewatering are often
captured in a separate cost centre, with allocated labour and burden costs.
Fuel - Includes diesel for major equipment units and gasoline for fleet vehicles.
Power - Includes all costs for providing electricity to run mine equipment. Where separate
meters are not available to segregate mine power usage from the plant and other facilities,
power costs for mine operations are either allocated to mining costs based on usage estimates
or carried in a cost centre separate from mine operating costs.
11.4.2
Typical underground mine operating cost centers are set up in the same manner as open pit
cost centers, but usually with more detailed divisions of labor and burden that avoid allocations:
Development labour (salary and hourly) and burden (medical insurance, FICA, et
cetera).
Mine service (maintenance, dewatering, ventilation) labour (salary and hourly) and
burden.
Mine management and technical support labour (salary and hourly) and burden.
Explosives.
Section 11 Mining Data Collection, Selection of Mining Method & Mine Planning
Ver. 1 November, 2002
Maintenance supplies.
Mine dewatering.
Fuel.
Power.
Development labour (salary and hourly) and burden - Includes hourly and salary (if
applicable) labour costs for mine development headings (ramps, access crosscuts, sublevel
drifts), shop construction, cutouts, and haulage of waste from development workings. Labour
burden includes country-mandated and managed retirement benefits such as FICA (US Social
Security), Medicare (or similar country-mandated medical plan), Federal and State or Province
unemployment taxes, benefits such as medical and dental insurance, pension plan
contributions, company-paid education, and other benefits unique to the mine or project location
such as hazard or high-altitude pay, foreign service allowances, et cetera. In the United States,
Canada and Australia, labour burden ranges from 25% to 60% of base hourly pay or salary.
For projects located in countries other than the United States, Canada and Australia, care must
be taken to include all applicable labour burden items, and there can be many. In certain
countries, labour burden costs can approach 300% of base salary or hourly pay. Salary labour
and burden for mine supervisors (shift bosses and foremen) are sometimes captured separately
and allocated to mine development costs.
Production labour (salary and hourly) and burden - Includes hourly and salary (if applicable)
labour and burden costs for stoping and ore haulage. Burden costs are the same as described
above. Salaried labour and burden for mine supervisors (shift bosses and foremen) are
sometimes captured separately and allocated to mine production costs.
Mine service labor (salary and hourly) and burden - Includes hourly and salary (if
applicable) labour and burden costs for mine services such as maintenance, ventilation,
dewatering, certain types of ground support and, sometimes, hoisting. Burden costs are the
same as described above. Salary labour and burden for mine supervisors (shift bosses and
foremen) are sometimes captured separately and allocated to mine service costs.
Mine management and technical support labor (salary and hourly) and burden - Includes
salary labour and burden costs for mine management (mine manager, mine superintendent,
chief engineer and chief geologist) and staff mining engineers, geologists, surveyors, and
environmental engineers, where applicable. Labour and burden may also include costs
allocated from the laboratory for sample preparation and assaying, and other applicable hourly
labour and burden costs. Burden costs are the same as described above.
Contract Labour - Contract labour costs are those costs incurred by an outside contractor
hired to provide a specific service. Where applicable, contract labour should be included in the
appropriate mine operating costs centre (i.e. development, production, mine services, or mine
technical support). Contract labour costs should not be confused with incentive bonus
payments (sometimes called miners contract) made to development or production miners
employed by Barrick, which are typically included in development and/or production labour cost
centers.
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Ver. 1 November, 2002
Explosives - Costs for ANFO, gels, traditional dynamite, primers, boosters, and any other
blasting agents used are included.
Drill bits and steel As for explosives, the costs for drill bits and steel are high relative to other
consumable materials, so these costs are usually captured in a separate cost centre. Where
underground mining is performed by an outside contractor, care should be taken to segregate
material costs from contract labour costs in order to ensure that these are not double counted.
Mining supplies and materials (consumables) - This category includes costs for all other
supplies/materials required for underground mine operations.
Mine maintenance supplies - Mine maintenance supplies include replacement parts
(exclusive of major rebuild components), hand tools, lubricants and nuts and bolts items.
Mine dewatering - If major amounts of groundwater must be pumped from either surface
dewatering wells or major underground pumping stations to allow underground development
and mining, the costs for mine dewatering are sometimes captured in a separate cost centre,
with allocated labour and burden costs.
Fuel - Includes all diesel used for underground equipment units and surface equipment units at
operations where surface haulage to the mill crusher is captured as part of mine operating
costs. Also includes gasoline for surface fleet vehicles, where applicable.
Power - Includes all costs for providing electricity to run mine equipment. Where separate
meters are not available to segregate mine power usage from the plant and other facilities,
power costs for mine operations are either allocated to mining costs based on usage estimates,
or carried in a cost centre separate from mine operating costs.
11.5. REFERENCES
LANE, K. 1988. Economic Definition of Ore. ISMN: 0900117516
OHARA, T.A. 1980. Quick guides to the evaluation of orebodies. CIM Bulletin, Feb. 1980.
HARTMAN, H.L. (Ed.). 1992, SME Mining Engineering Handbook.
Metallurgy, and Exploration, Inc.
Society of Mining,
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Ver. 1 November, 2002
APPENDIX
APPENDIX 11-1
DATA INTERPRETATION, ROCK MASS CLASSIFICATION AND
DESIGN
The first step towards data interpretation involves final compilation of the field record. An
analysis of structural orientation data is a useful starting point. Stereographic plotting of
various orientation or dip and dip direction data points will allow rapid interpretation of the
number of joint sets and their relationships with one another. The frequency or density of
discontinuities within a particular set, and an average description of the physical nature of
these discontinuities can also provide fast and reliable information about the potential
influence of each set within the overall geomechanical environment. Both tasks are readily
undertaken from the field record without the need for extensive geotechnical experience.
STEREOGRAPHIC ANALYSIS
The program DIPS developed by the Rock Engineering Group at the University of Toronto,
Canada is perhaps the most effective and user-friendly tool for manipulating orientation data.
The input file allows direct input of and angles from oriented drill core, as well as dip and
dip direction from line mapping. A typical data file is shown on the following page. Detailed
stereographic analysis is possible using a menu driven format, however, reference to a
detailed description of the principles behind the analysis such as Priest (1985) may be
beneficial.
A second program, GEOTECH, distributed by Widenbar and Associates Pty Ltd of Perth
Western Australia, also allows plotting of stereographic projections, but without the advanced
analysis capability of DIPS. GEOTECH does have the advantage of allowing data to be
projected onto a plane such as a drill hole trace or a wall section in a real space relationship.
This ability may be useful in block size estimation. As with the DIPS program, either direct dip
and dip direction or and angles can be interpreted from the input file.
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An example of a DIPS data input file. Text included in data input lines, which is not read by
DIPS, is presented in italics. Comment lines are indicated with the symbol, *. The input text
that you will have to input for each problem is shown in bold type.
*Filename:
example.dip
* Project titles:
PROJECT IDENTIFICATION
DATA COLLECTOR, DATE
* Traverse identifiers:
* To turn off the traverse option, enter 0,
* or where traverse data have been identified,
* Enter a positive integer.
1 traverse (s)
* Traverse information:
1;LINEAR;120;30;LEVEL 3,Stope 3A sublevel 310
* Global data orientation type flag:
STRIKE/DIPR
* Magnetic declination is given next:
-5.5 degrees (east)
* In the next line, the number of extra data
* columns are indicated. If there are no extra data
* Columns, enter NO QUANTITY
QUANTITY
* If there are extra data columns, enter the number
* Next:
3 extra data columns
* The next line is the header for the data
* Columns, which follow:
Number
Strike
1
2
3
4
5
6
7
8
9
10
Dip(rt)
53
57
51
50
48
231
47
244
83
64
Quantity
86
83
84
82
83
86
82
87
84
86
By convention will
always be 180 if
recording and
Travers
1
1
1
1
1
2
2
1
1
1
Spacing
1
1
1
1
1
1
1
1
1
1
Type
2
1
1.5
2
3
0.5
1
0.3
0.75
1.5
Joint
Joint
Joint
Joint
Joint
Joint
Shear
Joint
Joint
Joint
Surface
Smooth
Smooth
Smooth
Sl.rough
Rough
Rough
Slickens
V.rough
Rough
Smooth
The two most commonly used rock mass classification schemes are the Geomechanics
Classification or Rock Mass Rating (RMR) System devised by Bieniawski (1973) and the QSystem of Barton, Lein and Lunde (1974). Both these are described in appendix 2 which is
taken directly from Stillborg (1986). The Q-System is preferred for underground mining
situations, as the design output is more realistic in that environment. The RMR System was
designed specifically for civil engineering applications, and as such is somewhat
conservative. Subsequent modifications to the RMR System proposed by Laubscher and
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Taylor (1976) go some way towards addressing this deficiency. Both systems carry right
through to the design and ground support and reinforcement requirements of underground
excavations in the rock mass, based entirely on information that can either be measured or
directly induced from drill core logging or line mapping. At this stage though, experience on
the part of the geotechnical engineer is an essential component.
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Section 12
CUTOFF GRADE
DETERMINATION
12.4.
12.1. INTRODUCTION
Cutoff grades, which have been the subject of extensive debate over many years, can be
calculated to address many different operating scenarios. In an effort to provide consistency
between operations, Barrick has developed definitions for four distinct types of cutoff grades:
Break-even.
Incremental.
Mill.
Next Best Ore.
In practice, operations can have more than one break-even cutoff grade in order to take into
account different underground mining methods, different ore types, significant differences in
haulage distances and other factors. Different cutoff grades can be applied to differentiate
between break-even and incremental ores in order to facilitate blending for a constant mill
feed grade, or to segregate high grade material for separate processing through a gravity
circuit.
12.2. DEFINITIONS
In general terms, four different types of cutoff grade calculations or concepts are currently
implemented to varying degrees at all Barrick operations. The cutoff grades and concepts
described below apply across the full spectrum of reserve accounting, from summarizing
global resources for an exploration project to making daily production calls in an operating
mine.
The following definitions attempt to unify and clarify industry standard nomenclature within the
context of Barricks worldwide operations and development projects.
12.2.1.
Also referred to as a fully-costed or site cutoff, this calculation is used exclusive of other
cutoffs when there is no excess mining or milling capacity. For an underground operation, a
break-even cutoff must cover all fixed and variable costs (including mining, milling, general
and administration (G&A), gross royalties, transport and shipping costs, smelting and refining
costs, limits to payable metals and refining penalties for deleterious metals). However, in the
case of an open pit, all mining costs are accounted for during the optimization phase of open
pit mine planning. Once the optimum pit is defined, the mining cost should not be included in
the break-even cutoff calculation, since the operational decisions in routing ore versus waste
are made at the pit crest, after the mining cost has been incurred. In a practical sense,
therefore, the break-even cutoff grade in an open pit is equivalent to the incremental cutoff
grade (see Section 12.2.2, below).
A break-even cutoff calculation should not include sustaining capital (other than as noted
below), capital development, NSR or net profits royalties, or taxes, but it must cover total site
costs. Capital items or expenses deemed to be directly proportional to ore tonnage (tailings
dam or leach pad expansions, for example) should be fully accounted for in the calculation of
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cutoff grade. The break-even cutoff grade may vary across a given site, depending on mining
method, metallurgy or royalties. If the mine capacity exceeds the mill capacity and the mine
has the ability to stockpile, then material at the break-even cutoff grade can be set aside for
later processing, provided that it can bear the additional cost of rehandling. In practice, all
operations utilize a break-even cutoff approach, although some also are able to take
advantage of incremental and/or mill cutoff grades, depending on any constraints to
throughput in either the mine or the mill.
If the mill consistently runs at capacity while processing underground ore which has grades at
or above the break-even cutoff, and the mine frequently encounters material between the
incremental cutoff grade and the break-even cutoff grade that must be left unmined, a
potential opportunity may be lost. When this occurs, the feasibility of increasing mine
production and expanding the mill should be considered.
12.2.2.
An incremental cutoff grade can be applied if the mine or mill is not operating at capacity, or if
the concept of next best ore applies (see Section 12.2.4). At an underground operation,
incremental material must carry the direct underground mining costs, additional secondary
development costs (if more development is required in order to mine the incremental
material), incremental capital costs (tailings dam and/or leach pad expansions), and only the
variable portion of mine support costs, process operating costs, G&A costs and gross
royalties. If the mill is operating at capacity and the mine has the ability to provide material for
placement in stockpiles, then incremental grade material can be set aside for later
processing, provided it can additionally bear the fixed portion of processing and G&A costs,
as well as the costs associated with rehandling. When mining underground, material at the
incremental cutoff grade should never displace break-even cutoff grade material in mill feed.
In the case of an open pit, incremental grade ore must carry any incremental haulage costs
(i.e. any haulage costs over and above the cost required to haul the material to the
appropriate waste dump), incremental capital costs (tailings dam and/or leach pad
expansions), gross royalties, and only the variable portions of process operating costs and
G&A costs.
If the pit is capable of producing more incremental grade material than the mill can process
(which is common), then the incremental grade material can be placed in stockpiles, provided
that it can bear its portion of the cost of stockpile construction, maintenance and future
rehandling.
12.2.3.
As with an incremental cutoff grade, a mill cutoff grade is applied if the mine or mill are not at
capacity or if the concept of next best ore applies (see Section 12.2.4). A mill cutoff
considers low grade material, such as underground development muck, that must be broken
and removed from the mine. Such material must carry the portion of the variable costs
incurred above the shaft or decline collar, or beyond the crest of the pit. If the mill is operating
at capacity and the mine has the ability to provide material to stockpile, then incremental
grade material can be set aside for later processing, provided it can bear the additional cost of
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rehandling. Mill cutoff grade material should never displace break-even cutoff grade material
as mill feed.
12.2.4.
In daily practice, incremental cutoff and mill cutoff grade material compete directly with any
available material coming from either the open pit or from surface stockpiles. The material
having the highest net revenue of these three types should take precedence as mill feed.
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The units used for the variables in the cutoff grade calculation must match those used
by the operation, whether Imperial or metric (i.e., troy ounces per ton, grams per
tonne).
Units of tonnage and volume used in the calculation for mining, milling, and G&A costs
must be the same as the tonnage units used at the operation, whether Imperial or
metric.
The currency portion of the mining, milling and G&A costs must be consistent with the
currency used to capture the costs for accounting purposes at the operation. This can
be an issue at remote project sites, where certain local costs (particularly labour and
some supplies) may be expressed in the currency of the country where the project is
located.
Refining and transportation costs are usually accounted for on a per-troy ounce basis
if the mine produces a dor product. These costs should be captured as a deduction
from the metal revenue portion of the cutoff formulae, in order to avoid confusion with
costs expressed on a per-tonne basis.
Gold and silver prices are typically expressed in United States dollars per troy ounce
(US$/oz). If the mine expresses grades on a gram per tonne basis, however, the
price(s) used in the calculation of cutoff grades must also be expressed in United
States dollars per gram US$/g. If costs are expressed in local currency, the metal
prices must be converted from dollars to local currency, at the exchange rates
provided by Barrick corporate management.
Cutoff grade equations can be kept simple, as shown in the following examples, where
several individual cost centres are combined to comprise total mining or milling costs.
Alternatively, the equations can be made quite complex, with individual variables included for
the different cost centres. Although more complex, such equations do have the advantage
that mistakes are easier to identify than when numerous cost centres are consolidated into
one composite unit cost variable.
12.5.1.
A break-even cutoff grade is the grade at which the revenue equals operating costs for all
ore mining and ore processing. It is important to stress that calculations of break-even cutoff
grades contain no profit assumptions (hence the break-even designation). Because breakeven cutoff grades are the basis for the estimation of mineral reserves, it is technically
possible (although highly unlikely) to have an ore reserve that generates no profit to the
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company, but still qualifies as an ore reserve by the definitions discussed in Section 1,
REPORTING CODES, of this reference volume.
The following is a simple example of the method used to calculate a break-even cutoff at an
underground mine expressed in troy ounces per short ton, assuming costs in United States
dollars per short ton (US$/st):
BREAK-EVEN CUTOFF GRADE (BCG) x REVENUE = OPERATING COSTS
or
BCG = OPERATING COSTS/REVENUE
Thus,
BCG =
Where:
Mining Costs
Process Costs
G&A Costs
Refining Costs
Gross Royalties
Recovery
Price
For open pit operations, the break-even cutoff grade equation is equivalent to the incremental
cutoff calculation for the reasons discussed in Section 12.2.1.
12.5.2.
For an underground operation, incremental ore must carry the direct mining costs, additional
secondary development costs (if additional development is required to mine the incremental
ore), any incremental process capital costs required to process the incremental ore (such as
tailings dam and/or leach pad expansions), non-NSR (gross) royalties, and only the variable
portion of mine support costs, process costs and (G&A) costs. The same holds true for
calculation of an open pit incremental cutoff grade, except that mining costs are not included,
as all material must be hauled to the crest of the pit regardless of whether it is ore or waste. If
flagged as incremental ore, the material incurs all downstream direct costs beyond the crest
of the pit, including incremental haulage costs if the distance to the crusher is greater than the
distance to the waste dump. From a practical standpoint, an open pit incremental cutoff
grade is equivalent to the break-even cutoff grade, as stated previously.
The following is an example of a simple underground incremental cutoff grade (ICG)
calculation expressed in troy ounces per short ton, assuming costs in dollars per short ton:
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12.5.3.
This cutoff grade is applied to material that must be broken and removed from the mine but
which does not meet either break-even or incremental cutoff grade criteria. In an
underground mine, it usually is comprised of material from development headings. In order to
qualify for milling, such material must be able to carry the portion of the variable costs
incurred beyond the shaft or decline collar or the crest of the pit. This material can be placed
in a surface stockpile if the mill is operating at capacity with material above the break-even
cutoff grade, provided that the material can bear the additional costs of rehandling.
The following is an example of a simple underground mill cutoff grade (MCG) calculation
expressed in troy ounces per short ton:
MCG = Variable Process Costs + Variable G&A Costs
Recovery x (Price - Refining - Gross Royalties)
Where:
Variable Process Costs
Variable G&A Costs
Refining Costs
Gross Royalties
Recovery
Price
For an open pit operation, incremental ore cutoff and mill cutoff grades are the same.
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Section 13
OPERATING/ENVIRONMENTAL
PERMIT REQUIREMENTS
Section 14
Section 15
PRODUCTION RECONCILIATIONS
15.2
15.1 INTRODUCTION
Within the mining industry, the general term production reconciliation is applied in
different ways to describe comparisons made at operating mines between something that
is predicted and something that is produced. In practice, the variables being compared
vary from place to place.
For example, one operation may define production
reconciliation as the comparison between what the mine forecasts in the mine plan and
schedule and what the mill states that the mine delivered to the plant. Another may
consider production reconciliation to be what the mineral resource model predicted for
one or more areas of the mine and what the mine produced in terms of tons (or tonnes)
and grade from those areas, as estimated by the mine grade control department. Others
consider production reconciliation to be the comparison between the resource model
predictions (in terms of tons or tonnes and grade) and the tonnage and metal produced by
the mill.
Most production reconciliations, regardless of type, are not straightforward, and the
confidence of the tonnage and grade estimates of the various reconciliation components
varies widely. For example, resource model predictions of tonnage and grade are based
on various methods of interpolating assay data between sample points and applying those
grade interpolations to volumes defined by individual blocks in the resource model (see
Section 9, RESOURCE MODELING, of this reference volume). Expected waste dilution is
considered, and usually is based on mining experience or estimates derived from
operations using similar mining methods after making allowances for local ground
conditions. The resulting resource model is the basis for all mine plans, schedules and
production forecasts. The tonnage and grade of the local portions of the model that are
used for production reconciliations, generally, are based on a significantly smaller set of
samples than the mine and mill production estimates. Thus, from a purely statistical
standpoint, the confidence in the resource model tonnage and grade estimates is lower
than the mine and mill production estimates.
On the mining side, estimates of the tonnage of ore produced must rely on surveyed
volume calculations, truck counts, skip counts, belt weightometer data, or a combination of
two or more of these data types. Estimates of the grade of mined ore are based on
assays, whether from open pit blastholes, underground channel and/or grab sampling, belt
sampling, or some combination of these. These data typically are adjusted for external
waste dilution, which is based on estimates that are derived from surveyed volumes and
visual determinations. These methods provide ample opportunities for the introduction of
sampling error, lowering the level of quality of the production grade estimate.
Most mills are capable of providing measured (weighed) dry tonnage throughput totals for
a given period of time, usually based on a conveyer belt weigh-scale with adjustments for
moisture content. However, the grade of mill throughput may not be based on empirical
data from mill head sampling but, instead, may be back-calculated from the total metal
produced (refined) and other down-stream measurements, and from sampling the tails.
Metallurgical recoveries are estimated using the same procedure. Regardless of the
errors induced this way, the tonnage or grade estimates that define mill throughput or
actual metal produced for a given period become the standard against which mine
production and resource estimates are judged.
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In summary, production reconciliations are inexact comparisons using data that are often
suspect, sometimes incomplete, and typically carry different levels of confidence.
Nevertheless, these comparisons are key to the evaluation of the performance of major
components of the operation, and of the quality of the resource and ore reserve estimation
at Barricks operating mines.
The following sections provide descriptions and guidelines for setting up and performing
meaningful production reconciliations.
15.2 DEFINITIONS
The following definitions are appropriate to the subsequent discussion of production
reconciliations.
Sampled Mill Head Grade A sampled mill head grade is the grade of the mill
throughput that is based on physical samples taken from the mill feed stream. It is
superior to a back-calculated mill head grade provided that the samples are taken
correctly, sample sizes address the ore fragment size distribution at the point of sampling,
and the point of sampling is representative of the mill feed. The use of SAG mills and of
complex crushing circuits where portions of the ore stream are recirculated, both have
contributed to the general demise of the sampled mill head.
Back-Calculated Mill Head This is a common alternative to a sampled mill head. Daily
head grades are back-calculated, based on samples from the tailings stream, samples
from various points in the circuit (cyclone overflows et cetera), and calculated recoveries.
Belt Weightometer A device commonly used to weigh the material fed to a mill.
Normally positioned beneath the primary feed conveyor, the weightometer determines the
weight of the material on the conveyor belt as it passes over a series of sensors. Because
belt weightometers record wet tons (tonnes), allowances must be made for the moisture
content of the material weighed in order to determine the dry tonnage fed to the mill.
Dry Tons (Tonnes) There is no moisture component in volumes reported in dry tons
(tonnes). The tonnages estimated during resource modeling are in situ dry tons, based on
in situ density factors (see Section 8, DENSITY DETERMINATION, of this reference
volume). All measurements of tonnage made during production activities are made on a
wet basis and a factor for moisture must be applied to the measurement in order to
convert it to dry tons (tonnes).
Truck Factor For trucks that do not have load cells installed to allow tabulation of wet
tonnage hauled on a load-by-load basis, a calculated truck factor that represents the
average load (tonnage) carried by a surface or underground haul truck is used. The ore
tonnage shipped to the mill is determined by tallying the total number of trucks sent to the
crusher or to stockpiles and multiplying the total(s) by the calculated truck factor. Care
should be taken when using mine tonnage estimates that are based on truck factors for
production reconciliations, since there are several sources of potential error: For example:
If more than one size of surface or underground trucks is used, the truck factors
should be check in order to ensure that they have been applied correctly to the
count for trucks of each size.
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The truck factors may include moisture or be based on dry weight. Either is
acceptable, but care must be taken that moisture factors are not improperly applied
later.
Truck factors are based on the assumption that, although some loads will be
heavier or lighter than normal, the variances will even out over a reasonable period
of time. In general, this assumption holds true, but truck factors can be skewed
when a new or replacement loader/shovel operator loads the trucks differently than
the other operators.
Skip Factor A calculated factor that represents the average load (tonnage) capacity of a
skip in a shaft. The tonnage hoisted is determined by tallying the total number of skips
hoisted and multiplying that total by the skip factor.
As Mined The total mine production (tonnage and grade) as determined by mine grade
control procedures or other methods used by mine departments.
Declared Ore Mined This term is used at some Barrick operations to refer to the
tonnage and grade shipped to the mill by the mine, as determined by the mill. As such, it
is the production figure against which the as mined production (as estimated by mine
grade control procedures) is compared.
Mine Call Factor (MCF) A factor applied to mine production data in order to achieve
acceptable reconciliations between mine and mill production. In practice, an MCF is
applied to as mined production estimates either as a tonnage factor, a grade factor, or
both. MCFs are more common in certain areas of the world (such as South Africa) than
others and are used as a result of the inability of an operation to determine the reasons for
mine to mill tonnage and/or grade discrepancies.
Reconciliations should be completed in the order above. Because the mill production
numbers are considered the true tonnage and grade milled for the period in question, the
mine production should first be reconciled to the mill, then the resource model to the mine.
Several key criteria must be considered when performing open pit and underground
production reconciliations:
Reconcile tons (tonnes) before grade. If significant disparities exist between the
tonnage of ore reported as received by the mill and the tonnage that the mine
believes was sent, a meaningful reconciliation of grade is hardly possible.
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The longer the time period of the reconciliation, the less susceptible the
reconciliation is to short-term variability due to local production issues, grade
shortfalls or windfalls, or variations in the mine plan and schedule. Although
operation reporting requirements demand monthly reconciliations in almost all
Barrick operations, quarterly and annual reconciliations allow more meaningful
assessment of the performance of an operation.
The flow of material through stockpiles creates a major issue for reconciliations,
due to the difficulties in tracking the tonnage and grade into and out of the stockpile
during the period covered by the reconciliation. While the tonnage and grade of
the material entering the stockpile sometimes can be tracked reasonably well (as
in the case of open pit operations, where truck dispatch and grade control data can
be used to account for trucks dumping into the stockpile), material flowing out of
the pile is usually tracked only by truck or loading unit bucket count. The material
leaving the stockpile is seldom sampled. As a result, the grade of a dynamic pile is
carried as an average for the total pile, and this average is adjusted as new
material of known grade enters the pile. Material exiting the stockpile is assigned
the average grade of the pile at that point in time. Although this approach
generally will not badly skew longer-term reconciliations, it can introduce significant
errors into shorter-term comparisons.
Unless different companies are involved, mills that receive ore from more than one
operating mine often have no provision for properly tracking the specific tonnage
and grade from each operation. When this occurs (and several Barrick operations
have this issue), tonnage and grade are usually allocated back to the individual
operations using formulae based on whatever data are available. These situations
can make production reconciliations at the individual mines somewhat
meaningless, particularly when one of the operations mines significantly higher
average grades compared to the others.
The use of mine call factors (adjustment factors applied to mine or mill tonnage
and grade totals in order match mine and mill production) should be avoided if at
all possible (see Section 15.4). The continued use of a call factor at an operation
is proof that one ore more chronic measurement errors are present in the tracking
of tonnage and grade. The cause of such errors should be pursued diligently, as
these errors adversely affect the ability of the mine to apply cutoffs correctly in
order to make necessary ore-waste decisions.
15.3.1
Because open pit operations generally have better control and knowledge of the flow of
ore from the mine, open pit reconciliations generally are more straightforward than
reconciliations involving underground operations. Actual haul truck destinations can be
tracked visually or with GPS-based dispatch systems, and except for material that flows
through stockpiles, open pit ore almost always proceeds directly from the bench face to
the mill crusher. Tonnage mined and hauled from the bench face is based on data
generated by load cells on each truck or on truck factors that are periodically adjusted
based on surveyed volumes mined. The grade assigned to the ore shipped to the mill
during a given shift is normally based on pit grade control department estimates that are
derived from blasthole sampling.
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15.3.1.1
The following points should be kept in mind when making open pit mine versus mill
reconciliations:
Mill operations management usually reports mill ore production as dry tons
(tonnes). Care must be taken to ensure that mine production tonnages also are
compiled as dry tons. Unless ore moisture is highly variable, moisture can be
accounted for using a factor. The same moisture factor should be used by the
mine and mill for reporting tonnages;
For monthly reconciliations, surge piles at the crusher pad can be ignored, unless
for some reason an unusually large amount of material is in the pile at the end of a
given month;
At operations where open pit ore and underground ore both feed a common mill,
reconciliations can be difficult due to the wide disparity between the grades fed to
the mill from the individual mines. This is particularly true if the mill is not set up to
sample the mill feed streams individually. Reconciliation difficulties at these
operations often are compounded because of low grade material from the open pit
that flows through stockpiles (see Section 12, CUTOFF GRADE
DETERMINATION, for a discussion of incremental ore cutoffs and mill ore cutoffs).
15.3.1.2
The reconciliations between the resource model and the mine are not as straightforward
as mine versus mill comparisons, due to the fact that mining does not always occur
exactly in the places predicted by the resource model. Ore expected on a certain bench
may not be encountered until the bench below, or it may be more erratically distributed
than forecast, which often results in more tons (tonnes) mined than forecast, but usually at
a lower grade. Or the presence of old underground workings on a bench can contribute to
variances in both positive and negative ways. Any of these occurrences can radically
skew monthly reconciliations. For example, at KCMGs Fimiston operation in Australia,
reconciliations over twelve-month and nine-month periods can be reasonably close, but
bench-by-bench comparisons can show variances that exceed 200 percent.
When performing model versus mine reconciliations, care must be taken to try and match
the areas where ore is produced on a bench with the position of the ore on the bench as
predicted by the model. Keeping track of model performance in this manner can provide
early warning for potential problems that could persist for several benches and thus
adversely affect the ore schedule beyond the current month.
15.3.2
UNDERGROUND RECONCILIATIONS
almost all ore usually reaches the mill shortly after it is drilled, sampled, and blasted. In
contrast, underground ore generally takes a much more indirect path from the point of
drilling, sampling and blasting to the mill. It is not unusual for underground ore to be
handled several times, and depending on the mining method and the layout of the mine,
the length of time required for ore to reach the mill can range from hours to weeks, or
where very large blasthole stopes are in place, even months.
Comparisons between resource model estimates and actual mining are also more
complex. In an open pit, the ore may not be found exactly where the resource model
predicted it would be on a given bench. However, because all of the material on the
bench is eventually drilled, sampled, blasted, and hauled, all material is subject to
ore/waste classification. Ore may be found in lesser or greater quantities on the bench, or
at a different grade than predicted, but it nevertheless will be mined and shipped to the
mill. But in underground operations, access restrictions sometimes severely limit the
mines ability to easily or routinely locate ore that is not found where predicted.
The following sections provide a summary of the procedures required for effective
production reconciliations at underground mines.
15.3.2.1
As discussed above, the delay in ore reaching the mill once it has been drilled, sampled,
and broken makes the reconciliation of production between the mine and mill less than
straightforward. This delay is due mainly to ore residence times in stopes, ore cycling
through ore passes or transfer raises, muck bays, and underground and surface
stockpiles. Because of these delays, it is often difficult to determine the origin of the ore
actually passing through the mill during a given period of time. The lack of a tie back to in
situ production sampling sometimes makes grade estimation of the mill throughput
problematic.
Reconciliation of mine production with the mill should follow these steps:
1) Reconcile the estimate of tons (tonnes) produced from the mine with the
tonnage reported through the mill for the period in question.
Ore tonnage mined underground should be determined using CMS data, where
access to stopes is available. Where CMS data are not available due to survey
crew backlog (which generally occurs at the end of the last month in a quarter) or
other reasons, truck/LHD count data can be used. In all cases, individual stope
and development heading tonnages should be tracked, preferably on a daily basis.
Stope tonnages should then subsequently be determined by CMS, which allows for
calibration of truck/LHD factors.
2) Reconcile the grade produced from the mine with the grade reported through
the mill for the period in question.
Grades are reconciled by compiling the sample data routinely collected by the
geologists or sampling technicians as part of ongoing grade control/grade
monitoring procedures. Such sample data can consist of assays from chip or
channel sampling of the face and back, muck pile grab sampling, truck or loader
bucket grab sampling, belt sampling, or other valid sampling of the ore produced.
These data should then be weighted by the CMS tonnes, and the weighted
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average grade compared to the grade reported produced by the mill for the
quarter. Where CMS is not used to estimate in situ tonnage mined, other data that
are systematically collected will suffice (such as tonnage computed from
conventional transit surveying of mined volumes).
15.3.2.2
When reconciling resource model predictions with open pit mine production, local (bench
by bench) comparisons are fairly straightforward due to the fact that all material on each
bench is mined and classified. If the actual position of the ore is different than predicted, it
still can be found and recovered, as long as the shift in position does not result in the ore
falling outside of the limits of the optimum pit.
In contrast, underground reconciliations are made difficult when ore is not found in the
location or shape that was predicted by the resource model. Because an underground
operation does not have the luxury of sorting through all of the material in the spatial
vicinity of the stope(s), it is often difficult to determine the reason for an apparent ore
shortfall when not all predicted ore is found. Similarly, it is sometimes difficult to determine
if any ore found over and above predictions is due to a local overestimation in the model
or if it represents new ore that was not modeled because it was not defined by drilling. It
should be noted that this also happens in open pits, but rarely is any effort made to
distinguish unmodeled ore from predicted ore, unless an apparent ore windfall persists for
more than one or two benches.
Reconciliations between the resource model and actual mine production must follow the
same two basic steps that are done for mine versus mill reconciliations:
1) Reconcile the estimate of tons (tonnes) produced from the mine with the
tonnage predicted by the resource model for the period in question.
Ore tonnage mined underground should be determined using CMS data, where
access to stopes is available. Where access is not available for collection of CMS
survey data, or where CMS data are not available due to survey crew backlog
(which generally occurs at the end of the last month in a quarter) or for other
reasons, truck count or loading unit (LHD bucket count) data can be used. Where
possible, individual stope tonnages should be tracked, along with development
heading tonnages.
Comparisons of tonnage mined with tonnage predicted by the model are often
skewed by mine operations departing from the production mine plan and schedule.
These departures are sometimes beyond the control of the mine operators bad
ground in a particular area, or failure of a stope to meet forecast predictions can
cause necessary shifts in the production plan and schedule. In other cases, the
departure from the plan is sometimes due to the mine operators shifting production
to higher-grade stopes in an effort to meet production forecast goals. Whatever
the reasons, departures from the mine plan and schedule can make direct
comparisons between tonnage predicted by the resource model and the tonnage
mined for a given period impossible, without first determining where production
occurred in the mine on a stope-by-stope basis. Stope-by-stope comparisons of
diluted tonnages are essential for determining how the resource model is
performing in local areas.
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2) Reconcile the grade produced from the mine with the grade predicted by the
resource model for the period in question.
As described in Section 15.3.2.1, as mined grades are determined by compiling
the sample data routinely collected by the geologists or sampling technicians as
part of ongoing grade control/grade monitoring procedures. These data should
then be compared to the grades predicted by the resource model for the mined
volumes. The mined volumes are best determined by using CMS data to construct
three-dimensional shapes that represent individual workings (stopes, sublevels,
raises) where mining has taken place. The collection of CMS data is essential for
the reconciliation mine production against the tonnage predicted by the fully diluted
reserve model. If CMS methods are not in use, conventional underground transit
survey data must be used to the extent practicable.
In order to compare the as-mined grades with the grades predicted by the resource
model, it is essential to first determine where mining took place on a stope-bystope basis during the period covered by the reconciliation. If the as-mined
position and shapes of stopes compare closely to the geometry of the preproduction ore shapes predicted by the resource model, then the CMS outlines can
be used to cut the resource model and the modeled grades contained within the
CMS outlines then can be compared directly to the sampled grades. It is important
to note that if the CMS outlines do not compare well with the ore outlines predicted
by the resource model, then a simple comparison of modeled grades and sampled
grades within the CMS outlines can result in badly skewed reconciliations.
When the CMS outlines and the modeled ore outlines do not compare well
spatially, judgment is required on the part of the geologists to determine what
blocks in the model should be used as a basis for the predicted grade mined.
Often, this process consists of nothing more than determining that the same
relative tonnage of ore predicted by the resource model was indeed mined, only it
was found in a different position than projected by the model. However, when the
differences are more complex than a simple shift between the predicted position of
ore and the actual location where it was found, determining what portion of the
resource model was mined can be very difficult.
Unfortunately, when this problem occurs, the common solution is to simply
compare the tonnage and grade reported as mined during the reconciliation period
with the tonnage and grade predicted by the resource model-based mine plan and
schedule for the same period. While this gross approach to reconciliation
sometimes gives acceptable results (that is, the overall forecast tonnage and grade
compares reasonably well with the as mined tonnage and grade), it can ignore the
mining of ore not predicted by the model, hide external dilution and mining
recovery problems, and mask serious issues relative to the resource model, which
include:
The inability of the model to predict the position and geometry of ore sufficiently
for adequate mine planning and scheduling.
Apparent remnant ore that can inflate reserve totals if not critically evaluated
and purged from the reserves where appropriate.
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Any remnant blocks that are above cutoff but are situated reasonably close outside
of the CMS shape must be deleted from future resource/reserve statements,
unless it is clear that these remnants are truly present in sufficient quantity and
grade to pay for their separate extraction (including any development required to
access these remnants).
15.5.1
MILL
While resource model estimates and mine production data are reasonable sources of
reconciliation errors, there are many points downstream of the model and mine where
biased data may be generated that could significantly impact production reconciliations.
These include:
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15.5.2
MINE
The items in the mine that require attention in response to poor mine/mill or resource
model/mine reconciliations include:
Measurement of Tonnage Mined Tonnage produced from either open pit or
underground operations is usually based on surveyed volumes and/or truck counts. Both
require the application of material density factors to the surveyed volumes or truck counts
to arrive at tons (tonnes) produced from the mine. Where tonnage discrepancies between
the mine and mill vary consistently in the same direction, the focus in the mine should be
on confirming the validity of the density factor(s). Where tonnage differences are sporadic
but chronic, truck count accuracy and survey accuracy should be examined.
Misdirection of Trucks In open pits (and to a lesser extent in underground mines),
misdirection of trucks can result in sporadic variations in tonnage reconciliations. Truck
misdirection occurs as a result of poor dispatch procedures or operator error (both
intentional and unintentional). Dispatch systems that use GPS technology help eliminate
this potential source of error.
Measurement of Ore Grade In open pits, the determination of the grade of ore mined is
based primarily on blasthole sampling or trench sampling of bench floors. At underground
operations, as-mined grade estimates are derived from development and production face
sampling, truck grab sampling, loader bucket grab sampling, muck pile grab sampling, or
some combination of these methods. Where grade discrepancies exist between mine and
mill, each sampling method should be thoroughly reviewed to determine if one or more of
the methods (especially the various types of grab sampling) have introduced a bias into
the mines grade estimate. Where as-mined grades are based on face sampling, the
dilution assumptions must be carefully reviewed.
Theft of Gold - Theft of gold within a mine is difficult to prevent, even with elaborate
security measures in place. However, it is generally not a serious problem because the
vast majority of gold in most ores occurs in grains that are too small to visually distinguish.
Unless theft of high grade material is rampant, the gold lost as a result of theft by mine
workers will not significantly affect mine/mill reconciliations.
15.5.3
RESOURCE MODEL
The resource model is always the first suspect when model/mine reconciliations go awry.
This section does not delve into the specific aspects of resource modeling in detail (see
Section 9, RESOURCE MODELING, for additional information). What follows are brief
descriptions of the model parameters or components that should be reviewed when poor
reconciliations occur.
The tonnage and grade predicted by the resource model should be checked against the
as mined volumes (tonnages) and grades as described in Sections 15.3.1.2 and 15.3.2.2.
When discrepancies occur, the following items checked relative to the model:
Spatial Distribution of Ore Tonnage Simply stated, the model should accurately
estimate ore tonnage as defined by the underground as mined boundaries or the open pit
dig lines.
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Material Density The material densities used in the resource model should be checked
against the densities used by the mine operations staff to determine as mined tonnages.
It is not unusual for the densities used for resource modeling to be more detailed than the
densities used every day by the mine department.
Grade Estimation The local grades in the model should be compared with
corresponding as-mined grades from pit grade control sampling or underground stope or
development heading sampling. It is not uncommon for the global estimation of metal in a
deposit to compare closely with the total metal mined and recovered, while at the same
time the models local grade estimates vary widely compared to as mined grades. Poor
local grade estimates in the model often play havoc with short-term reconciliations.
Mining Recovery For areas where mining is finished, the mining recovery assumptions
made during resource modeling should be checked against actual ore recovery. For
underground mines, care must be taken to ensure that the volume mined corresponds
reasonably well to the planned ore outlines (see Section 15.3.2.2).
Dilution Check to ensure that the dilution assumptions made during resource modeling
are valid.
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